CN109119254A - 一种橘络状明胶改性壳聚糖基活性炭材料的制备方法 - Google Patents
一种橘络状明胶改性壳聚糖基活性炭材料的制备方法 Download PDFInfo
- Publication number
- CN109119254A CN109119254A CN201811300329.4A CN201811300329A CN109119254A CN 109119254 A CN109119254 A CN 109119254A CN 201811300329 A CN201811300329 A CN 201811300329A CN 109119254 A CN109119254 A CN 109119254A
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- Prior art keywords
- activated carbon
- carbon material
- preparation
- modified chitosan
- gelatin
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 56
- 229920001661 Chitosan Polymers 0.000 title claims abstract description 50
- 108010010803 Gelatin Proteins 0.000 title claims abstract description 41
- 229920000159 gelatin Polymers 0.000 title claims abstract description 41
- 239000008273 gelatin Substances 0.000 title claims abstract description 41
- 235000019322 gelatine Nutrition 0.000 title claims abstract description 41
- 235000011852 gelatine desserts Nutrition 0.000 title claims abstract description 41
- 239000000463 material Substances 0.000 title claims abstract description 31
- 241000675108 Citrus tangerina Species 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 40
- 229960000583 acetic acid Drugs 0.000 claims abstract description 20
- 239000012362 glacial acetic acid Substances 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000000243 solution Substances 0.000 claims abstract description 18
- 239000000843 powder Substances 0.000 claims abstract description 16
- 239000008367 deionised water Substances 0.000 claims abstract description 13
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 13
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims abstract description 12
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 10
- 239000007864 aqueous solution Substances 0.000 claims abstract description 9
- 229910052786 argon Inorganic materials 0.000 claims abstract description 6
- 239000007789 gas Substances 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 7
- 230000004913 activation Effects 0.000 claims description 5
- 238000013019 agitation Methods 0.000 claims description 5
- 239000012300 argon atmosphere Substances 0.000 claims description 5
- 238000002791 soaking Methods 0.000 claims description 4
- 239000002250 absorbent Substances 0.000 claims description 2
- 230000002745 absorbent Effects 0.000 claims description 2
- 239000003610 charcoal Substances 0.000 claims description 2
- 238000004090 dissolution Methods 0.000 claims description 2
- 238000004821 distillation Methods 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- 239000007772 electrode material Substances 0.000 abstract description 11
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 9
- 239000003990 capacitor Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000003575 carbonaceous material Substances 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 239000003792 electrolyte Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000010025 steaming Methods 0.000 description 3
- 238000003763 carbonization Methods 0.000 description 2
- 150000004676 glycans Chemical class 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229920002101 Chitin Polymers 0.000 description 1
- SXRSQZLOMIGNAQ-UHFFFAOYSA-N Glutaraldehyde Chemical compound O=CCCCC=O SXRSQZLOMIGNAQ-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000006196 deacetylation Effects 0.000 description 1
- 238000003381 deacetylation reaction Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000012776 electronic material Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 125000003147 glycosyl group Chemical group 0.000 description 1
- 125000005842 heteroatom Chemical group 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 238000000967 suction filtration Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/32—Carbon-based
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/24—Electrodes characterised by structural features of the materials making up or comprised in the electrodes, e.g. form, surface area or porosity; characterised by the structural features of powders or particles used therefor
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/84—Processes for the manufacture of hybrid or EDL capacitors, or components thereof
- H01G11/86—Processes for the manufacture of hybrid or EDL capacitors, or components thereof specially adapted for electrodes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
Landscapes
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
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CN201811300329.4A CN109119254B (zh) | 2018-11-02 | 2018-11-02 | 一种橘络状明胶改性壳聚糖基活性炭材料的制备方法 |
Applications Claiming Priority (1)
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CN201811300329.4A CN109119254B (zh) | 2018-11-02 | 2018-11-02 | 一种橘络状明胶改性壳聚糖基活性炭材料的制备方法 |
Publications (2)
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CN109119254A true CN109119254A (zh) | 2019-01-01 |
CN109119254B CN109119254B (zh) | 2020-08-18 |
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CN201811300329.4A Active CN109119254B (zh) | 2018-11-02 | 2018-11-02 | 一种橘络状明胶改性壳聚糖基活性炭材料的制备方法 |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109686583A (zh) * | 2019-01-22 | 2019-04-26 | 齐鲁工业大学 | 一种多孔海绵状壳聚糖基活性炭复合材料的制备方法 |
CN110182803A (zh) * | 2019-06-11 | 2019-08-30 | 武汉科技大学 | 一种活性炭材料及其制备方法 |
CN112194132A (zh) * | 2020-09-30 | 2021-01-08 | 浙江大学 | 一种基于毛竹水热炭化的铁修饰炭微球/炭纳米片复合多孔炭的制备方法及其应用 |
CN113611543A (zh) * | 2021-08-13 | 2021-11-05 | 南开大学 | 一种碳纳米管掺杂的壳聚糖基活性炭材料、电容去离子电极及制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102951636A (zh) * | 2012-11-19 | 2013-03-06 | 大连理工大学 | 氮掺杂壳聚糖基活性炭及其制备方法 |
CN103303912A (zh) * | 2013-07-05 | 2013-09-18 | 黑龙江大学 | 一种高比表面积多孔氮掺杂石墨化纳米碳材料的制备方法 |
CN104085877A (zh) * | 2014-06-30 | 2014-10-08 | 湖北工程学院 | 一种基于壳聚糖及其衍生物多孔碳电极材料及其制备方法和用途 |
-
2018
- 2018-11-02 CN CN201811300329.4A patent/CN109119254B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102951636A (zh) * | 2012-11-19 | 2013-03-06 | 大连理工大学 | 氮掺杂壳聚糖基活性炭及其制备方法 |
CN103303912A (zh) * | 2013-07-05 | 2013-09-18 | 黑龙江大学 | 一种高比表面积多孔氮掺杂石墨化纳米碳材料的制备方法 |
CN104085877A (zh) * | 2014-06-30 | 2014-10-08 | 湖北工程学院 | 一种基于壳聚糖及其衍生物多孔碳电极材料及其制备方法和用途 |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109686583A (zh) * | 2019-01-22 | 2019-04-26 | 齐鲁工业大学 | 一种多孔海绵状壳聚糖基活性炭复合材料的制备方法 |
CN110182803A (zh) * | 2019-06-11 | 2019-08-30 | 武汉科技大学 | 一种活性炭材料及其制备方法 |
CN112194132A (zh) * | 2020-09-30 | 2021-01-08 | 浙江大学 | 一种基于毛竹水热炭化的铁修饰炭微球/炭纳米片复合多孔炭的制备方法及其应用 |
CN113611543A (zh) * | 2021-08-13 | 2021-11-05 | 南开大学 | 一种碳纳米管掺杂的壳聚糖基活性炭材料、电容去离子电极及制备方法 |
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Effective date of registration: 20211119 Address after: No. 18, Fangshui Road, Jiangbei new district, Nanjing, Jiangsu 210000 Patentee after: MULINSEN ACTIVATED CARBON JIANGSU Co.,Ltd. Address before: No.13, 3rd floor, building 1, No.1, Tidu street, Qingyang District, Chengdu, Sichuan 610031 Patentee before: Chengdu yishenrui Technology Co.,Ltd. Effective date of registration: 20211119 Address after: No.13, 3rd floor, building 1, No.1, Tidu street, Qingyang District, Chengdu, Sichuan 610031 Patentee after: Chengdu yishenrui Technology Co.,Ltd. Address before: 250353 Qilu Industrial University, 3501 University Road, Changqing District, Ji'nan, Shandong Patentee before: Qilu University of Technology |
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