CN109090163B - Bacteriostatic agent with pure plant formula and preparation method thereof - Google Patents
Bacteriostatic agent with pure plant formula and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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Abstract
The invention discloses a bacteriostatic agent with a pure plant formula, which comprises the following raw materials in parts by weight: 35 parts of Chinese ilex leaf, 28 parts of Chinese chive, 22 parts of mint leaf, 13 parts of pithecellobium clypearia, 11 parts of radix sophorae flavescentis and 3 parts of solubilizer. The bacteriostatic agent is compounded by a plurality of plant formulas, is safe and reliable to use, can effectively overcome the defect of weak broad-spectrum bacteriostatic effect of the existing bacteriostatic agent under the synergistic action of all components, and has a wider action range and a better effect.
Description
Technical Field
The invention relates to a bacteriostatic agent, in particular to a bacteriostatic agent with a pure plant formula and a preparation method thereof.
Background
Surrounding germs invade our bodies all the time, and most of the time, the immune systems in our bodies can deal with the invasion of the germs. However, if the germs suddenly multiply in large quantities and exceed the range which can be met by a defense system, the germs will be ill. Therefore, it is important to suppress the growth of bacteria from the viewpoint of preventive medicine.
The bacteriostatic agent for the daily necessities has very important functions in the process of prolonging the storage life of the daily necessities and ensuring the quality of the daily necessities. The main component of the traditional daily use product bacteriostatic agent is a chemical synthetic product, the synthetic bacteriostatic agent has the problem of toxicity and is gradually limited to be used in many countries, so that the daily use product additive has developed an international trend towards non-toxicity, safety and natural development.
The existing plant bacteriostatic agent mostly takes single plant as raw material, and although the bacteriostatic effect on harmful bacteria of certain daily necessities is better, the broad-spectrum bacteriostatic effect is weaker, and the overall performance is not ideal.
Disclosure of Invention
The invention aims to provide a bacteriostatic agent with a pure plant formula so as to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a bacteriostatic agent with a pure plant formula comprises the following raw materials in parts by weight: 35-46 parts of Chinese ilex leaf, 28-36 parts of Chinese chive, 22-31 parts of mint leaf, 13-21 parts of pithecellobium clypearia, 11-19 parts of radix sophorae flavescentis and 3-7 parts of solubilizer.
As a further scheme of the invention: the feed comprises the following raw materials in parts by weight: 38-43 parts of Chinese ilex leaf, 30-34 parts of Chinese chive, 24-29 parts of mint leaf, 15-19 parts of pithecellobium clypearia, 13-17 parts of radix sophorae flavescentis and 4-6 parts of solubilizer.
As a still further scheme of the invention: the feed comprises the following raw materials in parts by weight: 41 parts of Chinese ilex leaf, 32 parts of Chinese chive, 26 parts of mint leaf, 17 parts of pithecellobium clypearia, 15 parts of radix sophorae flavescentis and 5 parts of solubilizer.
As a still further scheme of the invention: the solubilizer is formed by combining one or two of polyethylene glycol 400 and polyethylene glycol 600.
As a still further scheme of the invention: the solubilizer is formed by mixing polyethylene glycol 400 and polyethylene glycol 600 according to the weight ratio of 1: 2.
The preparation method of the bacteriostatic agent with the pure plant formula comprises the following steps:
1) crushing the Chinese ilex leaf and the mint leaf, adding absolute ethyl alcohol which is 8-11 times of the mass of the Chinese ilex leaf and the mint leaf, leaching twice, wherein the leaching temperature is 65-78 ℃ each time, the leaching time is 1.3-1.5h, combining the two extracting solutions, and concentrating to 15-20% of the original volume to obtain a first extracting solution;
2) dehydrating and drying the Chinese chives, crushing, sieving by a 100-mesh sieve, adding distilled water 7-9 times of the mass of the Chinese chives, and leaching for three times, wherein the leaching temperature is 60-72 ℃ each time. Leaching for 2.2-2.6h, mixing the three extractive solutions, and concentrating to 20-25% of the original volume to obtain folium Allii tuberosi extractive solution;
3) drying Pithecellobium clypearia, mixing with radix Sophorae Flavescentis, pulverizing, and sieving with 150 mesh sieve to obtain mixed powder;
4) mixing the first extractive solution and folium Allii tuberosi extractive solution, adding the mixed powder, stirring, placing in an ultrasonic processor, performing ultrasonic treatment at 62-70 deg.C for 1-1.2h, adding solubilizer, and reacting to obtain mixed solution;
5) and carrying out vacuum filtration on the mixed solution, and concentrating the filtrate to 40-55% of the original volume to obtain the bacteriostatic agent.
As a still further scheme of the invention: the power of the ultrasonic wave in the step 4) is 1000W.
Compared with the prior art, the invention has the beneficial effects that:
the bacteriostatic agent is compounded by a plurality of plant formulas, is safe and reliable to use, can effectively overcome the defect of weak broad-spectrum bacteriostatic effect of the existing bacteriostatic agent under the synergistic action of all components, and has a wider action range and a better effect.
Detailed Description
The technical solution of the present patent will be described in further detail with reference to the following embodiments.
Example 1
A bacteriostatic agent with a pure plant formula comprises the following raw materials in parts by weight: 35 parts of Chinese ilex leaf, 28 parts of Chinese chive, 22 parts of mint leaf, 13 parts of pithecellobium clypearia, 11 parts of radix sophorae flavescentis and 3 parts of solubilizer;
wherein the solubilizer is polyethylene glycol 400.
The preparation method of the bacteriostatic agent with the pure plant formula in the embodiment comprises the following steps:
1) crushing the Chinese ilex leaf and the mint leaf, adding absolute ethyl alcohol which is 8 times of the mass of the Chinese ilex leaf and the mint leaf, leaching twice, wherein the leaching temperature is 65 ℃ and the leaching time is 1.3h, combining the two extracting solutions, and concentrating to 15% of the original volume to obtain a first extracting solution;
2) dehydrating and drying the Chinese chives, crushing the Chinese chives, sieving the Chinese chives by a 100-mesh sieve, adding distilled water 7 times of the mass of the Chinese chives, and leaching the Chinese chives for three times, wherein the leaching temperature is 60 ℃ each time. Leaching for 2.2h, mixing the three extractive solutions, and concentrating to 20% of the original volume to obtain folium Allii tuberosi extractive solution;
3) drying Pithecellobium clypearia, mixing with radix Sophorae Flavescentis, pulverizing, and sieving with 150 mesh sieve to obtain mixed powder;
4) mixing the first extract and the leek extract, adding the mixed powder, fully stirring and mixing, then placing in an ultrasonic processor, carrying out ultrasonic treatment for 1h at 62 ℃, adding a solubilizer into the mixture during the ultrasonic treatment, and obtaining a mixed solution after the reaction is finished;
5) and carrying out vacuum filtration on the mixed solution, and concentrating the filtrate to 40% of the original volume to obtain the bacteriostatic agent.
The power of the ultrasonic wave in the step 4) is 1000W.
Example 2
A bacteriostatic agent with a pure plant formula comprises the following raw materials in parts by weight: 38 parts of Chinese ilex leaf, 30 parts of Chinese chive, 24 parts of mint leaf, 15 parts of pithecellobium clypearia, 13 parts of radix sophorae flavescentis and 4 parts of solubilizer;
wherein the solubilizer is polyethylene glycol 600.
The preparation method of the bacteriostatic agent with the pure plant formula in the embodiment comprises the following steps:
1) crushing the Chinese ilex leaf and the mint leaf, adding absolute ethyl alcohol with the mass being 9 times of that of the Chinese ilex leaf and the mint leaf, leaching twice, wherein the leaching temperature is 70 ℃ and the leaching time is 1.4h each time, combining the two extracting solutions, and concentrating to 20% of the original volume to obtain a first extracting solution;
2) dehydrating and drying the Chinese chives, crushing the Chinese chives, sieving the Chinese chives by a 100-mesh sieve, adding distilled water with the mass being 8 times of that of the Chinese chives, and leaching the Chinese chives for three times, wherein the leaching temperature is 62 ℃ each time. Leaching for 2.4h, mixing the three extractive solutions, and concentrating to 20% of the original volume to obtain folium Allii tuberosi extractive solution;
3) drying Pithecellobium clypearia, mixing with radix Sophorae Flavescentis, pulverizing, and sieving with 150 mesh sieve to obtain mixed powder;
4) mixing the first extract and the leek extract, adding the mixed powder, fully stirring and mixing, then placing in an ultrasonic processor, carrying out ultrasonic treatment for 1h at 66 ℃, adding a solubilizer into the mixture during the ultrasonic treatment, and obtaining a mixed solution after the reaction is finished;
5) and carrying out vacuum filtration on the mixed solution, and concentrating the filtrate to 45% of the original volume to obtain the bacteriostatic agent.
The power of the ultrasonic wave in the step 4) is 1000W.
Example 3
A bacteriostatic agent with a pure plant formula comprises the following raw materials in parts by weight: 41 parts of Chinese ilex leaf, 32 parts of Chinese chive, 26 parts of mint leaf, 17 parts of pithecellobium clypearia, 15 parts of radix sophorae flavescentis and 5 parts of solubilizer;
wherein the solubilizer is formed by mixing polyethylene glycol 400 and polyethylene glycol 600 according to the weight ratio of 1: 2.
The preparation method of the bacteriostatic agent with the pure plant formula in the embodiment comprises the following steps:
1) crushing the Chinese ilex leaf and the mint leaf, adding absolute ethyl alcohol which is 10 times of the mass of the Chinese ilex leaf and the mint leaf, leaching twice, wherein the leaching temperature is 70 ℃ and the leaching time is 1.5h each time, combining the two extracting solutions, and concentrating to 15% of the original volume to obtain a first extracting solution;
2) dehydrating and drying the Chinese chives, crushing the Chinese chives, sieving the Chinese chives by a 100-mesh sieve, adding distilled water with the mass being 8 times of that of the Chinese chives, and leaching the Chinese chives for three times, wherein the leaching temperature is 65 ℃ each time. Leaching for 2.4h, mixing the three extractive solutions, and concentrating to 20% of the original volume to obtain folium Allii tuberosi extractive solution;
3) drying Pithecellobium clypearia, mixing with radix Sophorae Flavescentis, pulverizing, and sieving with 150 mesh sieve to obtain mixed powder;
4) mixing the first extract and the leek extract, adding the mixed powder, fully stirring and mixing, then placing in an ultrasonic processor, carrying out ultrasonic treatment for 1h at 65 ℃, adding a solubilizer into the mixture during the ultrasonic treatment, and obtaining a mixed solution after the reaction is finished;
5) and carrying out vacuum filtration on the mixed solution, and concentrating the filtrate to 50% of the original volume to obtain the bacteriostatic agent.
The power of the ultrasonic wave in the step 4) is 1000W.
Example 4
A bacteriostatic agent with a pure plant formula comprises the following raw materials in parts by weight: 39 parts of Chinese ilex leaf, 31 parts of Chinese chive, 25 parts of mint leaf, 18 parts of pithecellobium clypearia, 15 parts of radix sophorae flavescentis and 6 parts of solubilizer;
wherein the solubilizer is polyethylene glycol 600.
The preparation method of the bacteriostatic agent with the pure plant formula in the embodiment comprises the following steps:
1) crushing the Chinese ilex leaf and the mint leaf, adding absolute ethyl alcohol with the mass being 9 times of that of the Chinese ilex leaf and the mint leaf, leaching twice, wherein the leaching temperature is 68 ℃ each time, the leaching time is 1.4h, combining the two extracting solutions, and concentrating to 15% of the original volume to obtain a first extracting solution;
2) dehydrating and drying the Chinese chives, crushing the Chinese chives, sieving the Chinese chives by a 100-mesh sieve, adding distilled water with the mass being 8 times of that of the Chinese chives, and leaching the Chinese chives for three times, wherein the leaching temperature is 65 ℃ each time. Leaching for 2.3h, mixing the three extractive solutions, and concentrating to 20% of the original volume to obtain folium Allii tuberosi extractive solution;
3) drying Pithecellobium clypearia, mixing with radix Sophorae Flavescentis, pulverizing, and sieving with 150 mesh sieve to obtain mixed powder;
4) mixing the first extractive solution and folium Allii tuberosi extractive solution, adding the mixed powder, stirring, placing in an ultrasonic processor, performing ultrasonic treatment at 62 deg.C for 1.1h, adding solubilizer therein, and reacting to obtain mixed solution;
5) and carrying out vacuum filtration on the mixed solution, and concentrating the filtrate to 45% of the original volume to obtain the bacteriostatic agent.
The power of the ultrasonic wave in the step 4) is 1000W.
Example 5
A bacteriostatic agent with a pure plant formula comprises the following raw materials in parts by weight: 43 parts of Chinese ilex leaf, 34 parts of Chinese chive, 29 parts of mint leaf, 19 parts of pithecellobium clypearia, 17 parts of radix sophorae flavescentis and 6 parts of solubilizer;
wherein the solubilizer is polyethylene glycol 400.
The preparation method of the bacteriostatic agent with the pure plant formula in the embodiment comprises the following steps:
1) crushing the Chinese ilex leaf and the mint leaf, adding absolute ethyl alcohol which is 11 times of the mass of the Chinese ilex leaf and the mint leaf, leaching twice, wherein the leaching temperature is 70 ℃ and the leaching time is 1.4h, combining the two extracting solutions, and concentrating to 15% of the original volume to obtain a first extracting solution;
2) dehydrating and drying the Chinese chives, crushing the Chinese chives, sieving the Chinese chives by a 100-mesh sieve, adding distilled water 7 times of the mass of the Chinese chives, and leaching the Chinese chives for three times, wherein the leaching temperature is 65 ℃ each time. Leaching for 2.5h, mixing the three extractive solutions, and concentrating to 20% of the original volume to obtain folium Allii tuberosi extractive solution;
3) drying Pithecellobium clypearia, mixing with radix Sophorae Flavescentis, pulverizing, and sieving with 150 mesh sieve to obtain mixed powder;
4) mixing the first extract and the leek extract, adding the mixed powder, fully stirring and mixing, then placing in an ultrasonic processor, carrying out ultrasonic treatment for 1h at 65 ℃, adding a solubilizer into the mixture during the ultrasonic treatment, and obtaining a mixed solution after the reaction is finished;
5) and carrying out vacuum filtration on the mixed solution, and concentrating the filtrate to 45% of the original volume to obtain the bacteriostatic agent.
The power of the ultrasonic wave in the step 4) is 1000W.
Example 6
A bacteriostatic agent with a pure plant formula comprises the following raw materials in parts by weight: 46 parts of Chinese ilex leaf, 36 parts of Chinese chive, 31 parts of mint leaf, 21 parts of pithecellobium clypearia, 19 parts of radix sophorae flavescentis and 7 parts of solubilizer;
wherein the solubilizer is polyethylene glycol 400.
The preparation method of the bacteriostatic agent with the pure plant formula in the embodiment comprises the following steps:
1) crushing the Chinese ilex leaf and the mint leaf, adding absolute ethyl alcohol which is 11 times of the mass of the Chinese ilex leaf and the mint leaf, leaching twice, wherein the leaching temperature is 78 ℃ and the leaching time is 1.5h, combining the two extracting solutions, and concentrating to 20% of the original volume to obtain a first extracting solution;
2) dehydrating and drying the Chinese chives, crushing the Chinese chives, sieving the Chinese chives by a 100-mesh sieve, adding distilled water 9 times of the mass of the Chinese chives, and leaching the Chinese chives for three times, wherein the leaching temperature is 72 ℃ each time. Leaching for 2.6h, mixing the three extractive solutions, and concentrating to 25% of the original volume to obtain folium Allii tuberosi extractive solution;
3) drying Pithecellobium clypearia, mixing with radix Sophorae Flavescentis, pulverizing, and sieving with 150 mesh sieve to obtain mixed powder;
4) mixing the first extractive solution and folium Allii tuberosi extractive solution, adding the mixed powder, stirring, placing in an ultrasonic processor, performing ultrasonic treatment at 70 deg.C for 1.2h, adding solubilizer therein, and reacting to obtain mixed solution;
5) and carrying out vacuum filtration on the mixed solution, and concentrating the filtrate to 55% of the original volume to obtain the bacteriostatic agent.
The power of the ultrasonic wave in the step 4) is 1000W.
Comparative example 1: the formulation and preparation were identical to example 3, except that it contained no ilex purpurea.
Comparative example 2: the formulation and preparation were identical to those of example 3, except that no pithecellobium clypearia was included.
Comparative example 3: only the leaves of Chinese ilex and the pithecellobium clypearia were included, and the preparation process was the same as in example 3.
Performance testing
Bacteriostatic comparison tests are carried out on the bacteriostatic agents corresponding to the embodiment 3 and the comparative examples 1-3 under the same conditions, test tube method is adopted for test, Minimum Inhibitory Concentration (MIC) is carried out, and the following table is obtained after data are recorded
As can be seen from the data corresponding to the example 3 and the comparative examples 1 to 3 in the table above, the bacteriostatic agent has a larger bacteriostatic spectrum under the synergistic action of the components, effectively overcomes the defect of weak broad-spectrum bacteriostatic effect of the existing bacteriostatic agent, and has a wider action range and a better effect.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (7)
1. The bacteriostatic agent with a pure plant formula is characterized by comprising the following raw materials in parts by weight: 35-46 parts of Chinese ilex leaf, 28-36 parts of Chinese chive, 22-31 parts of mint leaf, 13-21 parts of pithecellobium clypearia, 11-19 parts of radix sophorae flavescentis and 3-7 parts of solubilizer.
2. The bacteriostatic agent with pure plant formula according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 38-43 parts of Chinese ilex leaf, 30-34 parts of Chinese chive, 24-29 parts of mint leaf, 15-19 parts of pithecellobium clypearia, 13-17 parts of radix sophorae flavescentis and 4-6 parts of solubilizer.
3. The bacteriostatic agent with pure plant formula according to claim 2, which is characterized by comprising the following raw materials in parts by weight: 41 parts of Chinese ilex leaf, 32 parts of Chinese chive, 26 parts of mint leaf, 17 parts of pithecellobium clypearia, 15 parts of radix sophorae flavescentis and 5 parts of solubilizer.
4. The bacteriostatic agent according to claim 3, wherein the solubilizer is selected from one or two of polyethylene glycol 400 and polyethylene glycol 600.
5. The bacteriostatic agent according to claim 3, wherein the solubilizer is prepared by mixing polyethylene glycol 400 and polyethylene glycol 600 in a weight ratio of 1: 2.
6. A method of preparing a bacteriostatic agent according to any one of claims 1 to 5 in a pure plant formulation, comprising the steps of:
1) crushing the Chinese ilex leaf and the mint leaf, adding absolute ethyl alcohol which is 8-11 times of the mass of the Chinese ilex leaf and the mint leaf, leaching twice, wherein the leaching temperature is 65-78 ℃ each time, the leaching time is 1.3-1.5h, combining the two extracting solutions, and concentrating to 15-20% of the original volume to obtain a first extracting solution;
2) dehydrating and drying Chinese chives, crushing, sieving with a 100-mesh sieve, adding distilled water 7-9 times the mass of the Chinese chives, leaching for three times, wherein the leaching temperature is 60-72 ℃ each time, the leaching time is 2.2-2.6h, combining the three extracting solutions, and concentrating to 20-25% of the original volume to obtain a Chinese chive extracting solution;
3) drying Pithecellobium clypearia, mixing with radix Sophorae Flavescentis, pulverizing, and sieving with 150 mesh sieve to obtain mixed powder;
4) mixing the first extractive solution and folium Allii tuberosi extractive solution, adding the mixed powder, stirring, placing in an ultrasonic processor, performing ultrasonic treatment at 62-70 deg.C for 1-1.2h, adding solubilizer, and reacting to obtain mixed solution;
5) and carrying out vacuum filtration on the mixed solution, and concentrating the filtrate to 40-55% of the original volume to obtain the bacteriostatic agent.
7. The method of claim 6, wherein the ultrasonic power in step 4) is 1000W.
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|---|---|---|---|---|
| CN101637189A (en) * | 2009-08-21 | 2010-02-03 | 安徽神健生物工程有限公司 | Compound traditional Chinese medicine disinfection solution and preparation method thereof |
| CN103349025A (en) * | 2013-07-17 | 2013-10-16 | 黄利辉 | Botanical disinfecting, sterilizing and deodorizing liquid, and preparation method and application thereof |
| CN107788229A (en) * | 2017-07-27 | 2018-03-13 | 浦江县合洪园艺研发有限公司 | A kind of purposes of plant-based bacteriostat |
| CN108159108A (en) * | 2018-02-26 | 2018-06-15 | 辽宁昱众合医药科技有限公司 | The preparation of pithecellobium clypearia total phenolics and its application in antimicrobial antiphlogistic drug |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101637189A (en) * | 2009-08-21 | 2010-02-03 | 安徽神健生物工程有限公司 | Compound traditional Chinese medicine disinfection solution and preparation method thereof |
| CN103349025A (en) * | 2013-07-17 | 2013-10-16 | 黄利辉 | Botanical disinfecting, sterilizing and deodorizing liquid, and preparation method and application thereof |
| CN107788229A (en) * | 2017-07-27 | 2018-03-13 | 浦江县合洪园艺研发有限公司 | A kind of purposes of plant-based bacteriostat |
| CN108159108A (en) * | 2018-02-26 | 2018-06-15 | 辽宁昱众合医药科技有限公司 | The preparation of pithecellobium clypearia total phenolics and its application in antimicrobial antiphlogistic drug |
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