CN109010884A - Excitated type deodorant and preparation method thereof - Google Patents

Excitated type deodorant and preparation method thereof Download PDF

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Publication number
CN109010884A
CN109010884A CN201811043209.0A CN201811043209A CN109010884A CN 109010884 A CN109010884 A CN 109010884A CN 201811043209 A CN201811043209 A CN 201811043209A CN 109010884 A CN109010884 A CN 109010884A
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parts
maintained
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sawdust
type deodorant
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张雅萍
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Zhejiang Nine Tian Environmental Protection Technology Co Ltd
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Zhejiang Nine Tian Environmental Protection Technology Co Ltd
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Priority to CN201811043209.0A priority Critical patent/CN109010884A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/014Deodorant compositions containing sorbent material, e.g. activated carbon
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12NMICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N1/00Microorganisms, e.g. protozoa; Compositions thereof; Processes of propagating, maintaining or preserving microorganisms or compositions thereof; Processes of preparing or isolating a composition containing a microorganism; Culture media therefor
    • C12N1/20Bacteria; Culture media therefor
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20Method-related aspects
    • A61L2209/21Use of chemical compounds for treating air or the like
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2209/00Aspects relating to disinfection, sterilisation or deodorisation of air
    • A61L2209/20Method-related aspects
    • A61L2209/22Treatment by sorption, e.g. absorption, adsorption, chemisorption, scrubbing, wet cleaning

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • Genetics & Genomics (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Biotechnology (AREA)
  • Veterinary Medicine (AREA)
  • Organic Chemistry (AREA)
  • Epidemiology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Wood Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Microbiology (AREA)
  • Biomedical Technology (AREA)
  • Virology (AREA)
  • Biochemistry (AREA)
  • General Engineering & Computer Science (AREA)
  • Tropical Medicine & Parasitology (AREA)
  • Materials Engineering (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The present invention relates to the technical field of deodorization, especially a kind of excitated type deodorant and preparation method thereof, excitated type deodorant, including following parts by weight component: 52 parts~64 parts of probiotics;25 parts~37 parts of acetic acid;13 parts~28 parts of citric acid;19 parts~30 parts of activated carbon powder;32 parts~49 parts of catalyst;72 parts~86 parts of culture medium.The step of manufacturing method, is successively: step 1: mixed culture, step 2: high pressure steam sterilization, step 3: centrifugal treating, step 4: freezing processing, step 5: cooling treatment and step 6: gasification process.The long shelf-life of excitated type deodorant, longer using the time, deodorizing effect is better;Preparation method advantages of simple, process, operational safety is high, and products obtained therefrom quality is guaranteed.

Description

Excitated type deodorant and preparation method thereof
Technical field
The present invention relates to the technical field of deodorization, especially a kind of excitated type deodorant and preparation method thereof.
Background technique
Foul gas not only causes to seriously affect to ecological environment, but also has greatly harm to human health, can make Nervous centralis generates obstacle, lesion, causes chronic disease, acute disease.Foreign countries have just started effluvium early in late 1950s The research that body pollution is administered, and have accumulated theoretical knowledge abundant and practical experience.Just carry out stench the 1980s in China Research in terms of the investigation of gaseous contamination, test and standard, and to the research of deodorization technique just opened from the 1990s Begin to carry out.
The purpose of various foul gas processing methods is the effect by physics, chemistry, biology, makes the object of foul gas Matter structure changes, and eliminates stench.The conventional common processing method of foul gas has combustion method, oxidizing process, absorption process, absorption Method, neutralisation and bioanalysis etc..Biological deodorizing is using bioanalysis by specially cultivating in biofilter on biologic packing material Microbial film carries out the biological exhaust gas treatment technology of deodorization to waste odour-gas molecule.However, existing most biological on the market The shelf-life of deodorant is shorter, and in long-time use process, deodorizing effect can be worse and worse.
Summary of the invention
The technical problem to be solved by the present invention is being provided a kind of sharp to solve the problems, such as above-mentioned background technique Hair style deodorant and preparation method thereof, the long shelf-life of excitated type deodorant is longer using the time, and deodorizing effect is better;It is made Preparation Method advantages of simple, process, operational safety is high, and products obtained therefrom quality is guaranteed.
The technical solution adopted by the present invention to solve the technical problems is: a kind of excitated type deodorant, including following weight Part component:
52 parts~64 parts of probiotics;25 parts~37 parts of acetic acid;13 parts~28 parts of citric acid;19 parts~30 parts of activated carbon powder;Catalysis 32 parts~49 parts of agent;72 parts~86 parts of culture medium.
Further specifically, the culture medium is by venison cream, peptone and sodium chloride structure in above-mentioned technical proposal At, wherein 48 parts~52 parts of venison cream, 12 parts~17 parts of peptone, 12 parts~17 parts of sodium chloride.
Further specifically, in above-mentioned technical proposal, the probiotics is lactobacillus acidophilus, Lactobacillus casei, Zhan One of family name's lactobacillus, Raman lactobacillus, bifidobacterium longum, bifidobacterium breve, oval Bifidobacterium and bifidobacterium thermophilum Or two or more combination.
Further specifically, in above-mentioned technical proposal, the catalyst be titanium dioxide, zinc oxide, tin oxide and The combination of one or more of cadmium sulfide.
Further specifically, in above-mentioned technical proposal, the activated carbon powder is pine sawdust, oak sawdust, English walnut Sawdust, cypress sawdust, boxwood sawdust, rosewood sawdust, linden sawdust, elm sawdust, toothed oak wood sawdust, birch sawdust, peach Wood sawdust, apple pericarp, Banana peel, dragon fruit pericarp, mangosteen peel, pineapple peel, durian pericarp, Hami melon and fruit fickle in love The combination of one or more of skin, orange pericarp, grape pomace and mango pericarp.
A kind of manufacturing method for manufacturing excitated type deodorant, comprising the following steps:
Step 1: probiotics, acetic acid, citric acid and activated carbon powder being uniformly mixed, and is inoculated on culture medium and is cultivated, is trained Feeding temperature is maintained within the scope of 28 degrees Celsius~33 degrees Celsius, and incubation time is maintained at 96 hours~120 hours ranges Within;
Step 2: after the completion of culture, liquid medium being utilized into high pressure steam sterilization, the high pressure steam sterilization time is maintained at 30 points Within the scope of clock~40 minute, steam sterilizing temperatures are maintained within the scope of 130 degrees Celsius~150 degrees Celsius, high Pressure steam sterilizing pressure is maintained within the scope of 100 kPas~120 kPas;
Step 3: after the completion of high pressure steam sterilization, liquid medium being made into centrifugal treating using centrifugation apparatus, by liquid medium In extra impurity removal, retain simple liquid medium;
Step 4: after the completion of centrifugation, simple liquid medium being made into freezing processing using refrigerator, cryogenic temperature is maintained at -50 and takes the photograph Within the scope of family name degree~-20 degree Celsius, cooling time is maintained within the scope of 100 hours~120 hours;
Step 5: after the completion of freezing, the culture solution of freezing being made into cooling treatment using vacuum tank, it is Celsius that cooling temperature is maintained at 25 Within the scope of~34 degrees Celsius of degree, it is maintained at cooling time within the scope of 130 hours~160 hours;
Step 6: after the completion of cooling, cooling culture solution is uniformly mixed with catalyst, and make gasification process using equipment for gasification, Gasification temperature is maintained within the scope of 160 degrees Celsius~200 degrees Celsius, and vaporization time is maintained at 90 minutes~120 minutes Within the scope of.
Further specifically, in above-mentioned technical proposal, the nitrogen in the outside air is to the resulting gas that gasifies Play excitation.
Further specifically, in above-mentioned technical proposal, the oxygen in the outside air is to the resulting gas that gasifies Play excitation.
Further specifically, in above-mentioned technical proposal, the carbon dioxide gas in the outside air is to gasification institute The gas obtained plays excitation.
The beneficial effects of the present invention are: excitated type deodorant and preparation method thereof of the invention, the guarantor of excitated type deodorant The matter phase is long, longer using the time, and deodorizing effect is better;Preparation method advantages of simple, process, operational safety is high, institute It is guaranteed to obtain product quality.
Specific embodiment
In order to which the technical problems, technical solutions and beneficial effects solved by the present invention is more clearly understood, below in conjunction with Embodiment, the present invention will be described in further detail.It should be appreciated that specific embodiment described herein is only used to explain The present invention is not intended to limit the present invention.
Embodiment 1
A kind of excitated type deodorant, including following parts by weight component:
52 parts of probiotics;25 parts of acetic acid;13 parts of citric acid;19 parts of activated carbon powder;32 parts of catalyst;72 parts of culture medium.Culture medium It is made of venison cream, peptone and sodium chloride, wherein 48 parts of venison cream, 12 parts of peptone, 12 parts of sodium chloride.
Probiotics is the combination of lactobacillus acidophilus, Lactobacillus casei and Lactobacillus Jensenii.
Catalyst is the combination of titanium dioxide and zinc oxide.
Activated carbon powder is pine sawdust, oak sawdust, walnut sawdust, cypress sawdust, apple pericarp, Banana peel and fire The combination of imperial fruit pericarp.
For manufacturing the manufacturing method of excitated type deodorant, comprising the following steps:
Step 1: probiotics, acetic acid, citric acid and activated carbon powder being uniformly mixed, and is inoculated on culture medium and is cultivated, is trained Feeding temperature is maintained within the scope of 28 degrees Celsius, and incubation time was maintained within the scope of 96 hours;
Step 2: after the completion of culture, liquid medium being utilized into high pressure steam sterilization, the high pressure steam sterilization time is maintained at 30 points Within the scope of clock, steam sterilizing temperatures are maintained within the scope of 130 degrees Celsius, and high pressure steam sterilization pressure is maintained at Within the scope of 100 kPas;
Step 3: after the completion of high pressure steam sterilization, liquid medium being made into centrifugal treating using centrifugation apparatus, by liquid medium In extra impurity removal, retain simple liquid medium;
Step 4: after the completion of centrifugation, simple liquid medium being made into freezing processing using refrigerator, cryogenic temperature is maintained at -50 and takes the photograph Within the scope of family name's degree, cooling time was maintained within the scope of 100 hours;
Step 5: after the completion of freezing, the culture solution of freezing being made into cooling treatment using vacuum tank, it is Celsius that cooling temperature is maintained at 25 Within the scope of degree, it is maintained at cooling time within the scope of 130 hours;
Step 6: after the completion of cooling, cooling culture solution is uniformly mixed with catalyst, and make gasification process using equipment for gasification, Gasification temperature is maintained within the scope of 160 degrees Celsius, and vaporization time was maintained within the scope of 90 minutes.In outside air Nitrogen, oxygen and carbon dioxide gas play excitation to the resulting gas that gasifies.
The long shelf-life of the excitated type deodorant, longer using the time, deodorizing effect is better;Preparation method simply closes Reason, process, operational safety is high, and products obtained therefrom quality is guaranteed.
Embodiment 2
A kind of excitated type deodorant, including following parts by weight component:
58 parts of probiotics;30 parts of acetic acid;20 parts of citric acid;25 parts of activated carbon powder;40 parts of catalyst;79 parts of culture medium.Culture medium It is made of venison cream, peptone and sodium chloride, wherein 50 parts of venison cream, 12 parts of peptone, 17 parts of sodium chloride.
Probiotics is the combination of Raman lactobacillus, bifidobacterium longum and bifidobacterium breve.
Catalyst is the combination of zinc oxide and tin oxide.
Activated carbon powder be boxwood sawdust, rosewood sawdust, linden sawdust, elm sawdust, mangosteen peel, pineapple peel, The combination of durian pericarp and Hami melon and fruit peel.
For manufacturing the manufacturing method of excitated type deodorant, comprising the following steps:
Step 1: probiotics, acetic acid, citric acid and activated carbon powder being uniformly mixed, and is inoculated on culture medium and is cultivated, is trained Feeding temperature is maintained within the scope of 30 degrees Celsius, and incubation time was maintained within the scope of 106 hours;
Step 2: after the completion of culture, liquid medium being utilized into high pressure steam sterilization, the high pressure steam sterilization time is maintained at 35 points Within the scope of clock, steam sterilizing temperatures are maintained within the scope of 140 degrees Celsius, and high pressure steam sterilization pressure is maintained at Within the scope of 110 kPas;
Step 3: after the completion of high pressure steam sterilization, liquid medium being made into centrifugal treating using centrifugation apparatus, by liquid medium In extra impurity removal, retain simple liquid medium;
Step 4: after the completion of centrifugation, simple liquid medium being made into freezing processing using refrigerator, cryogenic temperature is maintained at -35 and takes the photograph Within the scope of family name's degree, cooling time was maintained within the scope of 110 hours;
Step 5: after the completion of freezing, the culture solution of freezing being made into cooling treatment using vacuum tank, it is Celsius that cooling temperature is maintained at 30 Within the scope of degree, it is maintained at cooling time within the scope of 145 hours;
Step 6: after the completion of cooling, cooling culture solution is uniformly mixed with catalyst, and make gasification process using equipment for gasification, Gasification temperature is maintained within the scope of 180 degrees Celsius, and vaporization time was maintained within the scope of 105 minutes.In outside air Nitrogen, oxygen and carbon dioxide gas excitation is played to the resulting gas of gasifying.
The long shelf-life of the excitated type deodorant, longer using the time, deodorizing effect is better;Preparation method simply closes Reason, process, operational safety is high, and products obtained therefrom quality is guaranteed.
Embodiment 3
A kind of excitated type deodorant, including following parts by weight component:
64 parts of probiotics;37 parts of acetic acid;28 parts of citric acid;30 parts of activated carbon powder;49 parts of catalyst;86 parts of culture medium.Culture medium It is made of venison cream, peptone and sodium chloride, wherein 52 parts of venison cream, 17 parts of peptone, 17 parts of sodium chloride.
Probiotics is the combination of bifidobacterium breve, oval Bifidobacterium and bifidobacterium thermophilum.
Catalyst is the combination of tin oxide and cadmium sulfide.
Activated carbon powder is elm sawdust, toothed oak wood sawdust, birch sawdust, mahogany sawdust, Hami melon and fruit peel, orange fruit The combination of skin, grape pomace and mango pericarp.
For manufacturing the manufacturing method of excitated type deodorant, comprising the following steps:
Step 1: probiotics, acetic acid, citric acid and activated carbon powder being uniformly mixed, and is inoculated on culture medium and is cultivated, is trained Feeding temperature is maintained within the scope of 33 degrees Celsius, and incubation time was maintained within the scope of 120 hours;
Step 2: after the completion of culture, liquid medium being utilized into high pressure steam sterilization, the high pressure steam sterilization time is maintained at 40 points Within the scope of clock, steam sterilizing temperatures are maintained within the scope of 150 degrees Celsius, and high pressure steam sterilization pressure is maintained at Within the scope of 120 kPas;
Step 3: after the completion of high pressure steam sterilization, liquid medium being made into centrifugal treating using centrifugation apparatus, by liquid medium In extra impurity removal, retain simple liquid medium;
Step 4: after the completion of centrifugation, simple liquid medium being made into freezing processing using refrigerator, cryogenic temperature is maintained at -20 and takes the photograph Within the scope of family name's degree, cooling time was maintained within the scope of 120 hours;
Step 5: after the completion of freezing, the culture solution of freezing being made into cooling treatment using vacuum tank, it is Celsius that cooling temperature is maintained at 34 Within the scope of degree, it is maintained at cooling time within the scope of 160 hours;
Step 6: after the completion of cooling, cooling culture solution is uniformly mixed with catalyst, and make gasification process using equipment for gasification, Gasification temperature is maintained within the scope of 200 degrees Celsius, and vaporization time was maintained within the scope of 120 minutes.In outside air Nitrogen, oxygen and carbon dioxide gas excitation is played to the resulting gas of gasifying.
The long shelf-life of the excitated type deodorant, longer using the time, deodorizing effect is better;Preparation method simply closes Reason, process, operational safety is high, and products obtained therefrom quality is guaranteed.
It is above-described, it is merely preferred embodiments of the present invention, but protection scope of the present invention is not limited to This, anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention And its inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (9)

1. a kind of excitated type deodorant, it is characterised in that: including following parts by weight component:
52 parts~64 parts of probiotics;25 parts~37 parts of acetic acid;13 parts~28 parts of citric acid;19 parts~30 parts of activated carbon powder;Catalysis 32 parts~49 parts of agent;72 parts~86 parts of culture medium.
2. excitated type deodorant according to claim 1, it is characterised in that: the culture medium is by venison cream, peptone It is constituted with sodium chloride, wherein 48 parts~52 parts of venison cream, 12 parts~17 parts of peptone, 12 parts~17 parts of sodium chloride.
3. excitated type deodorant according to claim 1, it is characterised in that: the probiotics is lactobacillus acidophilus, does Lactobacillus paracasei, Lactobacillus Jensenii, Raman lactobacillus, bifidobacterium longum, bifidobacterium breve, oval Bifidobacterium and thermophilic bifid bar The combination of one or more of bacterium.
4. excitated type deodorant according to claim 1, it is characterised in that: the catalyst is titanium dioxide, oxidation The combination of one or more of zinc, tin oxide and cadmium sulfide.
5. excitated type deodorant according to claim 1, it is characterised in that: the activated carbon powder is pine sawdust, rubber Sawdust, walnut sawdust, cypress sawdust, boxwood sawdust, rosewood sawdust, linden sawdust, elm sawdust, toothed oak wood sawdust, Birch sawdust, mahogany sawdust, apple pericarp, Banana peel, dragon fruit pericarp, mangosteen peel, pineapple peel, durian The combination of one or more of skin, Hami melon and fruit peel, orange pericarp, grape pomace and mango pericarp.
6. a kind of manufacturing method for manufacturing excitated type deodorant as described in claim 1, it is characterised in that: including following Step:
Step 1: probiotics, acetic acid, citric acid and activated carbon powder being uniformly mixed, and is inoculated on culture medium and is cultivated, is trained Feeding temperature is maintained within the scope of 28 degrees Celsius~33 degrees Celsius, and incubation time is maintained at 96 hours~120 hours ranges Within;
Step 2: after the completion of culture, liquid medium being utilized into high pressure steam sterilization, the high pressure steam sterilization time is maintained at 30 points Within the scope of clock~40 minute, steam sterilizing temperatures are maintained within the scope of 130 degrees Celsius~150 degrees Celsius, high Pressure steam sterilizing pressure is maintained within the scope of 100 kPas~120 kPas;
Step 3: after the completion of high pressure steam sterilization, liquid medium being made into centrifugal treating using centrifugation apparatus, by liquid medium In extra impurity removal, retain simple liquid medium;
Step 4: after the completion of centrifugation, simple liquid medium being made into freezing processing using refrigerator, cryogenic temperature is maintained at -50 and takes the photograph Within the scope of family name degree~-20 degree Celsius, cooling time is maintained within the scope of 100 hours~120 hours;
Step 5: after the completion of freezing, the culture solution of freezing being made into cooling treatment using vacuum tank, it is Celsius that cooling temperature is maintained at 25 Within the scope of~34 degrees Celsius of degree, it is maintained at cooling time within the scope of 130 hours~160 hours;
Step 6: after the completion of cooling, cooling culture solution is uniformly mixed with catalyst, and make gasification process using equipment for gasification, Gasification temperature is maintained within the scope of 160 degrees Celsius~200 degrees Celsius, and vaporization time is maintained at 90 minutes~120 minutes Within the scope of;
Step 7: after the completion of gasification, the resulting gas that gasifies plays bigger deodorizing effect under the excitation of outside air.
7. manufacturing method according to claim 6, it is characterised in that: the nitrogen in the outside air is to gasification gained Gas play excitation.
8. manufacturing method according to claim 6, it is characterised in that: the oxygen in the outside air is to gasification gained Gas play excitation.
9. manufacturing method according to claim 6, it is characterised in that: the carbon dioxide gas pair in the outside air The resulting gas that gasifies plays excitation.
CN201811043209.0A 2018-09-07 2018-09-07 Excitated type deodorant and preparation method thereof Pending CN109010884A (en)

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