CN108991599A - A kind of cigarette filter-tip additive agent and preparation method thereof - Google Patents

A kind of cigarette filter-tip additive agent and preparation method thereof Download PDF

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Publication number
CN108991599A
CN108991599A CN201810622587.8A CN201810622587A CN108991599A CN 108991599 A CN108991599 A CN 108991599A CN 201810622587 A CN201810622587 A CN 201810622587A CN 108991599 A CN108991599 A CN 108991599A
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lactate
coconut husk
preparation
cigarette
additive agent
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张莘蔓
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    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06—Use of materials for tobacco smoke filters
    • A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The present invention provides a kind of cigarette filter-tip additive agent and preparation method thereof, the cigarette filter-tip additive agent is to be modified coconut husk charcoal as carrier, be prepared in carrier surface supported sorbents, the adsorbent is by hyperbranched lactate and chinese medicine material according to mass ratio 1:(2 ~ 5) mixing after be prepared；The adsorbent and modified coconut husk charcoal mass ratio are 1:(2 ~ 4)；The cigarette filter-tip additive agent additive amount is 20 ~ 50mg/ branch.Hyperbranched lactate is loaded using plasma modification coconut husk charcoal, the CO and tar in flue gas can be adsorbed, while improving flue gas comfort level.The present invention effectively improves the big problem of cigarette pollutant burst size, improves the fragrance and comfort level of cigarette, has good economic benefit.

Description

A kind of cigarette filter-tip additive agent and preparation method thereof
Technical field
The invention belongs to technical field of tobacco, in particular to a kind of cigarette filter-tip additive agent and preparation method thereof.
Background technique
Smoking is harmful to your health, what this was generally well known, endangers to reduce smoking to mankind's bring, world health group Knit one of the three big main action targets that " back suction cigarette " is classified as to 21 century health field.In this context, international cigarette city Also there is accelerating the trend developed to more low tar, low nicotine and low harmful components cigarette in field, and to harmful ingredients in flue gas into Row analysis and research, reduce harmful components to the greatest extent, produce the cigarette products of low harmful safe healthcare.Therefore, external low-coke tar cigarette The cigarette products in China will be threatened, directly affects the cigarette market in China.In order to preferably protect the health of consumer, China is Including that the fields such as leaf tobacco production, processing and reducing tar and reducing harm technology are increasing research dynamics, develop including modern biotechnology, The reducing tar and reducing harms such as new material technology new technology simultaneously successfully applies in production of cigarettes.
Patent of invention CN200910139721.X, it is a kind of to reduce releasing content of coke tar in cigarette using perilla leaf, folium artemisiae argyi, Du Jingye Method, the water that 5 times of weight are added after herbal raw material perilla leaf, folium artemisiae argyi, leaf of negundo chastetree (weight ratio 1:1:1) are pulverized and mixed decoct 2 Hour, it is repeated twice, is centrifugated out aqueous, merge, 2 times of raw material weight are concentrated into, by 40% ~ 95% ethyl alcohol of water extract After dilution, uniformly it is sprayed on the pipe tobacco that weight is 100 ~ 200 times of extract, routinely cigarette process is made with obvious tar reduction The cigarette of effect.This method raw material is cheap and easy to get, simple process, can reduce releasing content of coke tar in cigarette 10%~20%, has good Good industrial applications prospect.
Patent of invention CN200810140585.1, a kind of pair of low-coke tar cigarette carry out adding containing deoxy fructosazine for compensating aroma Add agent, the additive includes the raw material of following weight ratio: wherein: deoxy fructosazine 0.001~5%, furfural 0~1%, 5- first Base-furfural 0.1~0.5%, 3- ethyl -2- hydroxyl -2- cyclopentene-1-one 0.1~1%, Peru's medicinal extract 0.005~5%, ten Six sour methyl esters 0.1~1%, damascenone 0.1~1%, Megastigmatrienone 0.1~2%, cocoa power tincture 0.1~3%, propionic acid 0~ 1%, aqueous 50% ethyl alcohol is 82~99%；The additive is used for tobacco leaf or dark color with the dosage that weight ratio is 0.1~5% The flavoring of obbbin.The additive can significantly improve the perfume quantity of low-coke tar cigarette, and good with cigarette perfume harmony, reduce stimulation, Improve oral cavity comfort level.
Patent of invention CN201310053860.7, a kind of preparation method of ultra-low tar Virginian-type cigarette, not by sugared content 20 parts of 30 parts of Yunnan tobacco fragment, Zimbabwe's tobacco leaf fragment, Jilin higher than 19% shine 10 parts of tobacco fragment, 40 parts of offal mixings, Be ground into powdery, be made chip base, low tar paper process thin slice is made in coating flavor compensating liquid, by paper process thin slice, import tobacco leaf, After domestic delicate fragrance type tobacco leaf, domestic flat-flavor tobacco leaf, domestic strong-flavor tobacco leaf are sent into loosening and gaining moisture process, reach moisture content 20%；Fragrant liquid will be sprayed after the impurity removing of resurgence, chopping, drying, spray fumet after blowing hot-air and atomized water, then rolled, wrapped Ultra-low tar Virginian-type cigarette is made in dress.The invention is aided with flavouring humectant additive, can be made cigarette mainstream using comprehensive tar reduction method Tarry matters in smoke burst size reaches 3mg, keeps cigarette flavor and sucks satisfaction.After tested, smoke inlet is soft smooth, and fragrance is abundant Gracefulness, cigarette gesture raise up, elegant hair, and Hui Tian and promoting the production of body fluid feels preferably, comfortable taste, and pleasant impression is clean.
Summary of the invention
Aiming at the problem that existing cigarette CO and tar content seriously affect smoker's health more, the present invention provides a kind of reduction Cigarette CO and the cigarette filter of releasing content of coke tar and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of cigarette filter-tip additive agent, the additives of filter tip are loaded in carrier surface and are adsorbed to be modified coconut husk charcoal as carrier Agent is prepared；
The adsorbent is by hyperbranched lactate and chinese medicine material according to mass ratio 1:(2 ~ 5) mixing after be prepared；
The chinese medicine material is one of Kiwi extract, tea polyphenols, Radix Astragali, Radix Isatidis；
The adsorbent and modified coconut husk charcoal mass ratio are 1:(2 ~ 4)；
The cigarette filter-tip additive agent additive amount is 20 ~ 50mg/ branch.
By coconut husk carbon powder in NaNO3After impregnating in solution, coconut husk surface carries alkali metallic sodium ion, passes through plasma After processing, the calcium carbonate in alkali metallic sodium and coconut husk charcoal, at nano-component, improves surface micropore volume by arc through, thus The suction-operated to tar is strengthened, alkali metallic sodium and micropore can improve the calcium carbonate in coconut husk charcoal to CO2The absorption of gas is made With to reduce the release of pernicious gas CO；On the other hand, the NaNO of coconut husk charcoal melt surface3It is Ca with lactate2+Diffusion mentions Ionic liquid channel has been supplied, has distributed filter tip adsorption activity comprehensively, has improved tar adsorption efficiency.
Lactate can remove the acid of result of combustion of tobacco generation, while can improve the humectation of pipe tobacco, so that flue gas lubricates It is tasty and refreshing, improve the comfort of flue gas；By lactate it is hyperbranched after, lactate can be promoted to be scattered in filter tip, so that in lactate Alkali metallic sodium, potassium and lithium energy overall diffusion, thus comprehensively CO absorption, CO2Gas.
Additives of filter tip can improve after a large amount of active function groups that hyperbranched lactate has are in conjunction with chinese medicine material The permeable gas and moisture pick-up properties of cigaratte filter improve organic acid to the improvement result of flue gas suction quality, so that passing through filter tip Flue gas in tar be trapped, become more to lubricate tasty and refreshing after acting on using organic acid, improve flue gas comfort level.
The present invention provides the preparation method of the cigarette filter-tip additive agent simultaneously, comprising the following steps:
A. it is modified the preparation of coconut husk charcoal
(1) by ratio of weight and the number of copies, 10 ~ 15 parts of coconut husk carbon powder and NaNO are weighed3Solution mixes, and 15 ~ 20min is stirred at 80 DEG C, Then the dry 2h at 120 DEG C, obtains compound coconut husk carbon powder；
The NaNO3It is (0.1 ~ 0.2) with coconut husk charcoal powder quality ratio: 1；
(2) compound coconut husk carbon powder is handled into 1h in argon gas discharging plasma system, 6 each 10min, are changed altogether Property coconut husk charcoal；
The argon gas discharging plasma system is to pour argon gas after vacuumizing, and stablizes its pressure in 100 ~ 110Pa, then It is passed through DC power supply, breakdown voltage 900V, burning voltage 600V, electric current are 9 ~ 11mA；
B. the preparation of hyperbranched lactate
By ratio of weight and the number of copies, by 50 ~ 70 parts of lactate, 10 ~ 20 parts of lactic acid, 1 ~ 5 part of glycerine, 3 ~ 5 parts of gluconic acid mixing, side Stirring side is warming up to 120 ~ 165 DEG C, accelerates dehydration, removes after distillating moisture, continues to be decompressed to 1000 ~ 1300Pa, keep 170 ~ 175 DEG C of 10 ~ 12h of isothermal reaction pour out reaction product, are ground into powder after cooling, after acetone solution, are added dropwise to dehydrated alcohol Middle precipitating filters, and washing, 60 DEG C of vacuum drying 12h of filter cake obtain hyperbranched lactate；
The lactate is a kind of in sodium lactate, potassium lactate and lithium lactate；
C. the preparation of adsorbent
The organic acid for taking hyperbranched lactate that its quality 2% ~ 8% is added is mixed, and obtains mixed liquor, mixing liquid is then added The water of 10 ~ 20 times of product stirs 30min at 30 ~ 35 DEG C, and chinese medicine material is added, and after mixing 30 ~ 40min, obtains adsorbent；
The chinese medicine material and hyperbranched lactate mass ratio are (2 ~ 5): 1, it is added while stirring；
The organic acid is one of citric acid, malic acid；
D. the preparation of cigarette filter-tip additive agent
After modified coconut husk charcoal is impregnated 60 ~ 80min in adsorbent, after filtering, distilling water washing, drying, cigarette is obtained Additives of filter tip.
As a further improvement of the present invention, the Kiwi extract the preparation method is as follows:
(1) take Kiwi berry, be put into juice extractor and be beaten broken, the mixing enzyme aqueous solution of equal quality is added, 36 DEG C of temperature ~ 38 DEG C of progress constant temperature digest 2h, are warming up to 80 DEG C and keep 20 ~ 30min inactivation, obtain mixture；
The aqueous solution of the mixed enzyme be pectase, cellulase, carbohydrase, alpha-amylase and acid protease in mass ratio 2:1:1:1:2 is mixed to join in distilled water, and being prepared into mass fraction is 10% mixing enzyme aqueous solution；
(2) pH for adjusting the mixture after enzyme deactivation is 3.5 ~ 4.0, at 25 ~ 30 DEG C, carries out the Maillard reaction of 18h, is obtained anti- Answer mixture；
(3) reaction mixture is distilled, collects fraction, obtain volatile fragrant component, distillation test residue volume The ethanol water that score is 33 ~ 40% extracts, and supernatant is taken to be concentrated, and must dive fragrant component；
(4) head perfume (or spice) component and latent fragrant component are mixed according to 4 ︰ 1 of mass ratio, 2 ~ 4 DEG C carry out refrigeration 8h, take supernatant that can obtain Mi Monkey peach extract.
As a further improvement of the present invention, the Radix Astragali, Radix Isatidis material processing method are as follows:
Radix Astragali or Radix Isatidis are added in 2 ~ 5 times of water, after decoction to moisture content is 0.3 ~ 0.5 times of original volume, material is taken It dries and crushes out, cross 50 ~ 100 meshes, obtain Radix Astragali, Radix Isatidis material.
Beneficial effects of the present invention:
The present invention loads hyperbranched lactate using plasma modification coconut husk charcoal as absorption carrier, can effectively extract tobacco combustion Burn CO, the CO generated2Gas and tar increase additivated diffusion and adsorption efficiency using alkali metal ion diffusion, separately On the one hand the comfortable taste degree that flue gas is improved by hyperbranched lactate, having reached reduces tar and improves the dual of cigarette quality Effect has good economic benefit.
Specific embodiment
Below with reference to embodiment, the present invention is further described.
Embodiment 1
A. it is modified the preparation of coconut husk charcoal
(1) by ratio of weight and the number of copies, 10 parts of coconut husk carbon powder are weighed according to NaNO3With coconut husk charcoal powder quality ratio be 0.1:1 with NaNO3Solution mixes, and stirs 15min at 80 DEG C, and then the dry 2h at 120 DEG C, obtains compound coconut husk carbon powder；
(2) compound coconut husk carbon powder is handled into 1h in argon gas discharging plasma system, 6 each 10min, are changed altogether Property coconut husk charcoal；
The argon gas discharging plasma system is to pour argon gas after vacuumizing, and stablizes its pressure in 100Pa, then passes to DC power supply, breakdown voltage 900V, burning voltage 600V, electric current 9mA；
B. the preparation of hyperbranched lactate
Ratio is counted in parts by weight, and 50 parts of sodium lactate, 10 parts of lactic acid, 1 part of glycerine, 3 parts of gluconic acid mixing rise while stirring Temperature accelerates dehydration, removes after distillating moisture, continue to be decompressed to 1000Pa, keep 170 DEG C of isothermal reaction 10h, pour out to 120 DEG C Reaction product is ground into powder after cooling, after acetone solution, is added dropwise in dehydrated alcohol and precipitates, and filters, washing, filter cake 60 DEG C vacuum drying 12h obtain hyperbranched sodium lactate；
C. the preparation of adsorbent
The citric acid for taking hyperbranched sodium lactate that its quality 2% is added is mixed, and obtains mixed liquor, mixeding liquid volume is then added 10 times of water stirs 30min at 30 DEG C, is (2 ~ 5) according to Kiwi extract and hyperbranched lactate mass ratio: stirring on 1 side Kiwi extract is added, after mixing 30min, obtains adsorbent；
The Kiwi extract the preparation method is as follows:
(1) take Kiwi berry, be put into juice extractor and be beaten broken, the mixing enzyme aqueous solution of equal quality is added, 36 DEG C of temperature ~ 38 DEG C of progress constant temperature digest 2h, are warming up to 80 DEG C and keep 20 ~ 30min inactivation, obtain mixture；
The aqueous solution of the mixed enzyme be pectase, cellulase, carbohydrase, alpha-amylase and acid protease in mass ratio 2:1:1:1:2 is mixed to join in distilled water, and being prepared into mass fraction is 10% mixing enzyme aqueous solution；
(2) pH for adjusting the mixture after enzyme deactivation is 3.5 ~ 4.0, at 25 ~ 30 DEG C, carries out the Maillard reaction of 18h, is obtained anti- Answer mixture；
(3) reaction mixture is distilled, collects fraction, obtain volatile fragrant component, distillation test residue volume The ethanol water that score is 33 ~ 40% extracts, and supernatant is taken to be concentrated, and must dive fragrant component；
(4) head perfume (or spice) component and latent fragrant component are mixed according to 4 ︰ 1 of mass ratio, 2 ~ 4 DEG C carry out refrigeration 8h, take supernatant that can obtain Mi Monkey peach extract；
D. the preparation of cigarette filter-tip additive agent
After modified coconut husk charcoal is impregnated 60 ~ 80min in adsorbent, after filtering, distilling water washing, drying, cigarette is obtained Additives of filter tip.
The cigarette filter-tip additive agent of above-mentioned preparation is added according to 50mg/ branch.
Embodiment 2
A. it is modified the preparation of coconut husk charcoal
(1) by ratio of weight and the number of copies, 15 parts of coconut husk carbon powder are weighed according to NaNO3With coconut husk charcoal powder quality ratio be 0.2:1 with NaNO3Solution mixes, and stirs 20min at 80 DEG C, and then the dry 2h at 120 DEG C, obtains compound coconut husk carbon powder；
(2) compound coconut husk carbon powder is handled into 1h in argon gas discharging plasma system, 6 each 10min, are changed altogether Property coconut husk charcoal；
The argon gas discharging plasma system is to pour argon gas after vacuumizing, and stablizes its pressure in 110Pa, then passes to DC power supply, breakdown voltage 900V, burning voltage 600V, electric current 11mA；
B. the preparation of hyperbranched lactate
By ratio of weight and the number of copies, by 70 parts of potassium lactate, 20 parts of lactic acid, 5 parts of glycerine, 5 parts of gluconic acid mixing, warming while stirring To 165 DEG C, accelerate dehydration, remove after distillating moisture, continue to be decompressed to 1300Pa, keep 175 DEG C of isothermal reaction 12h, pours out anti- Product is answered, powder is ground into after cooling, after acetone solution, is added dropwise in dehydrated alcohol and precipitates, is filtered, washing, 60 DEG C of filter cake Vacuum drying 12h obtains hyperbranched potassium lactate；
C. the preparation of adsorbent
The malic acid for taking hyperbranched potassium lactate that its quality 8% is added is mixed, and obtains mixed liquor, mixeding liquid volume is then added 20 times of water stirs 30min at 35 DEG C, is 5:1 according to Radix Astragali material and hyperbranched lactate mass ratio, is added while stirring Radix Astragali material is added, after mixing 40min, obtains adsorbent；
The chinese medicine material Radix Astragali material processing method is as follows:
Radix Astragali is added in 4 times of water, after decoction to moisture content is 0.5 times of original volume, material taking-up is dried and is crushed, mistake 80 meshes obtain Radix Astragali material；
D. the preparation of cigarette filter-tip additive agent
After modified coconut husk charcoal is impregnated 80min in adsorbent, after filtering, distilling water washing, drying, cigarette filter is obtained Additive.
The cigarette filter-tip additive agent of above-mentioned preparation is added according to 20mg/ branch.
Embodiment 3
A. it is modified the preparation of coconut husk charcoal
(1) by ratio of weight and the number of copies, 12 parts of coconut husk carbon powder are weighed according to NaNO3With coconut husk charcoal powder quality ratio be 0.2:1 with NaNO3Solution mixes, and stirs 20min at 80 DEG C, and then the dry 2h at 120 DEG C, obtains compound coconut husk carbon powder；
(2) compound coconut husk carbon powder is handled into 1h in argon gas discharging plasma system, 6 each 10min, are changed altogether Property coconut husk charcoal；
The argon gas discharging plasma system is to pour argon gas after vacuumizing, and stablizes its pressure in 100Pa, then passes to DC power supply, breakdown voltage 900V, burning voltage 600V, electric current 10mA；
B. the preparation of hyperbranched lactate
By ratio of weight and the number of copies, by 60 parts of lithium lactate, 15 parts of lactic acid, 5 parts of glycerine, 4 parts of gluconic acid mixing, warming while stirring To 150 DEG C, accelerate dehydration, remove after distillating moisture, continue to be decompressed to 1200Pa, keep 172 DEG C of isothermal reaction 11h, pours out anti- Product is answered, powder is ground into after cooling, after acetone solution, is added dropwise in dehydrated alcohol and precipitates, is filtered, washing, 60 DEG C of filter cake Vacuum drying 12h obtains hyperbranched lithium lactate；
C. the preparation of adsorbent
The citric acid for taking hyperbranched lithium lactate that its quality 5% is added is mixed, and obtains mixed liquor, mixeding liquid volume is then added 15 times of water stirs 30min at 32 DEG C, is 4:1 according to Radix Isatidis material and hyperbranched lactate mass ratio, while stirring plus Enter Radix Isatidis material, after mixing 40min, obtains adsorbent；
The Radix Isatidis material processing method is as follows:
Radix Isatidis is added in 4 times of water, after decoction to moisture content is 0.4 times of original volume, material taking-up is dried and is crushed, It sieves with 100 mesh sieve, obtains Radix Isatidis material.
D. the preparation of cigarette filter-tip additive agent
After modified coconut husk charcoal is impregnated 65min in adsorbent, after filtering, distilling water washing, drying, cigarette filter is obtained Additive.
The cigarette filter-tip additive agent of above-mentioned preparation is added according to 35mg/ branch.
Test example
After cigarette filter-tip additive agent prepared by the embodiment of the present invention 1 ~ 3 is prepared cigarette, with conventional cigarette smoke components on the market Compare, the detection method of corresponding ingredient are as follows: " measurement of carbon monoxide is non-scatter in components in cigarette smoke gas phase by GB/T 23356-2009 Infrared method ", in GB/T 19609-2004 " cigarette conventional analysis measures total granules and tar with smoking machine " measurement flue gas Carbon monoxide and tar content, concrete outcome such as table 1.
1 fume component analysis result of table
As shown in Table 1, CO and releasing content of coke tar in the made cigarette smoke of the cigarette filter prepared using the embodiment of the present invention 1 ~ 3 It is below conventional cigarette, CO reduced rate is up to 34.8%, and tar reduced rate is up to 32.1%.
Above embodiments are only exemplary embodiment of the present invention, are not used in the limitation present invention, protection scope of the present invention It is defined by the claims.Those skilled in the art can make various repair to the present invention within the spirit and scope of the present invention Change or equivalent replacement, this modification or equivalent replacement also should be regarded as being within the scope of the present invention.

Claims (4)

1. a kind of cigarette filter-tip additive agent, which is characterized in that the cigarette filter-tip additive agent to be modified coconut husk charcoal as carrier, Carrier surface supported sorbents are prepared；
The adsorbent is by hyperbranched lactate and chinese medicine material according to mass ratio 1:(2 ~ 5) mixing after be prepared；
The chinese medicine material is one of Kiwi extract, tea polyphenols, Radix Astragali, Radix Isatidis；
The adsorbent and modified coconut husk charcoal mass ratio are 1:(2 ~ 4)；
The cigarette filter-tip additive agent additive amount is 20 ~ 50mg/ branch.
2. a kind of preparation method of cigarette filter-tip additive agent as described in claim 1, which comprises the following steps:
A. it is modified the preparation of coconut husk charcoal
(1) by ratio of weight and the number of copies, 10 ~ 15 parts of coconut husk carbon powder and NaNO are weighed3Solution mixes, and 15 ~ 20min is stirred at 80 DEG C, so The dry 2h at 120 DEG C afterwards, obtains compound coconut husk carbon powder；
The NaNO3It is (0.1 ~ 0.2) with coconut husk charcoal powder quality ratio: 1；
(2) compound coconut husk carbon powder is handled into 1h in argon gas discharging plasma system, 6 each 10min, are changed altogether Property coconut husk charcoal；
The argon gas discharging plasma system is to pour argon gas after vacuumizing, and stablizes its pressure in 100 ~ 110Pa, then It is passed through DC power supply, breakdown voltage 900V, burning voltage 600V, electric current are 9 ~ 11mA；
B. the preparation of hyperbranched lactate
By ratio of weight and the number of copies, by 50 ~ 70 parts of lactate, 10 ~ 20 parts of lactic acid, 1 ~ 5 part of glycerine, 3 ~ 5 parts of gluconic acid mixing, side Stirring side is warming up to 120 ~ 165 DEG C, accelerates dehydration, removes after distillating moisture, continues to be decompressed to 1000 ~ 1300Pa, keep 170 ~ 175 DEG C of 10 ~ 12h of isothermal reaction pour out reaction product, are ground into powder after cooling, after acetone solution, are added dropwise to dehydrated alcohol Middle precipitating filters, and washing, 60 DEG C of vacuum drying 12h of filter cake obtain hyperbranched lactate；
The lactate is a kind of in sodium lactate, potassium lactate and lithium lactate；
C. the preparation of adsorbent
The organic acid for taking hyperbranched lactate that its quality 2% ~ 8% is added is mixed, and obtains mixed liquor, mixing liquid is then added The water of 10 ~ 20 times of product stirs 30min at 30 ~ 35 DEG C, and chinese medicine material is added, and after mixing 30 ~ 40min, obtains adsorbent；
The chinese medicine material and hyperbranched lactate mass ratio are (2 ~ 5): 1, it is added while stirring；
The organic acid is one of citric acid, malic acid；
D. the preparation of cigarette filter-tip additive agent
After modified coconut husk charcoal is impregnated 60 ~ 80min in adsorbent, after filtering, distilling water washing, drying, cigarette is obtained Additives of filter tip.
3. the preparation method of cigarette filter-tip additive agent according to claim 2, which is characterized in that the Kiwi berry extracts Object the preparation method is as follows:
(1) take Kiwi berry, be put into juice extractor and be beaten broken, the mixing enzyme aqueous solution of equal quality is added, 36 DEG C of temperature ~ 38 DEG C of progress constant temperature digest 2h, are warming up to 80 DEG C and keep 20 ~ 30min inactivation, obtain mixture；
The aqueous solution of the mixed enzyme be pectase, cellulase, carbohydrase, alpha-amylase and acid protease in mass ratio 2:1:1:1:2 is mixed to join in distilled water, and being prepared into mass fraction is 10% mixing enzyme aqueous solution；
(2) pH for adjusting the mixture after inactivation is 3.5 ~ 4.0, at 25 ~ 30 DEG C, carries out the Maillard reaction of 18h, is obtained anti- Answer mixture；
(3) reaction mixture is distilled, collects fraction, obtain volatile fragrant component, distillation test residue volume The ethanol water that score is 33 ~ 40% extracts, and supernatant is taken to be concentrated, and must dive fragrant component；
(4) head perfume (or spice) component and latent fragrant component are mixed according to 4 ︰ 1 of mass ratio, 2 ~ 4 DEG C carry out refrigeration 8h, take supernatant that can obtain Mi Monkey peach extract.
4. the preparation method of cigarette filter-tip additive agent according to claim 2, which is characterized in that the chinese medicine material is When Radix Astragali or Radix Isatidis material, processing method is as follows:
Radix Astragali or Radix Isatidis are added in 2 ~ 5 times of water, after decoction to moisture content is 0.3 ~ 0.5 times of original volume, material is taken It dries and crushes out, cross 50 ~ 100 meshes, obtain Radix Astragali or Radix Isatidis material.
CN201810622587.8A 2018-06-15 2018-06-15 A kind of cigarette filter-tip additive agent and preparation method thereof Withdrawn CN108991599A (en)

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Application publication date: 20181214