CN108938528A - A kind of fresh tea leaves essential oil toner and preparation method thereof - Google Patents
A kind of fresh tea leaves essential oil toner and preparation method thereof Download PDFInfo
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- CN108938528A CN108938528A CN201811168180.9A CN201811168180A CN108938528A CN 108938528 A CN108938528 A CN 108938528A CN 201811168180 A CN201811168180 A CN 201811168180A CN 108938528 A CN108938528 A CN 108938528A
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- essential oil
- tea leaves
- fresh tea
- dendrobium candidum
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention discloses a kind of fresh tea leaves essential oil toners and preparation method thereof, the toner is mainly made of the raw material of following mass fraction: 5-8 parts of fresh tea leaves essential oil, 10-15 parts of dendrobium candidum leaf extract, 4-8 parts of butanediol, 0.8-1.6 parts of pure plant emulsifier, 0.5-1.0 parts of Sodium Hyaluronate, 70-80 parts of deionized water.The present invention is using natural plants fresh tea leaves and dendrobium candidum leaf as raw material, rich in nutritional ingredients such as esters, alcohols, terpenes, polysaccharide, vitamin C, protein, there is pleasant fragrance, cooperate between various composition, by optimizing constituent content, make end formulation green natural, safety is mild, nontoxic, it is nonirritant, with anti-oxidant, anti-aging, antibacterial anti-inflammatory, promote re-epithelilization, repairs the effect of damage skin.Meanwhile preparation method process flow of the present invention is simple, and it is easy to operate, it is suitable for large-scale production.
Description
Technical field
The present invention relates to household chemicals technical field is belonged to, it is related to a kind of fresh tea leaves essential oil toner and its preparation side
Method.
Background technique
As the improvement of people's living standards, people focus more on the external of oneself.Especially face of the women to oneself
It even more extraordinarily takees good care of in portion.Currently, cosmetics are many kinds of on the market, toner is a kind of common cosmetics.It belongs to aqua
Type skin care item, suitable for moisture and nutrition needed for supplementing skin.In toner than water, general also moisturizer, pigment,
Fragrance, preservative, emulsifier etc..Chemically synthesized substance is excessive in existing toner, although can play in a short time certain
Effect, but these the toner rich in synthetic chemical is used for a long time, there is certain damaging action to application on human skin, it is this
It damages even irreversible.The health of these synthetics confrontation people also has a great impact simultaneously.Therefore, day is developed
So, green, moist functional cosmetic water have broad prospects.
Functional component rich in tealeaves, drinks in general, people are processed into tealeaves only with the tender leaf in tea tree spring.
The tealeaves in old leaf and other seasons generally discards, and causes the very big wasting of resources.In order to improve the added value of tealeaves, we are from tea
Fresh leaf propose essential oil, the essential oil have strong tea perfume, smell is naturally pleasant, and have certain anti-inflammatory, sterilization, anti-aging,
Anti-oxidant curative effect analyzes its main chemical compositions with GC-MS, it is found that the BHT that it is rich in is extraordinary antioxidant, anti-aging
Agent；Its wintergreen being rich in has good desinsection, bactericidal effect.The ingredients such as its ethyl propionate contained, benzyl carbinol, carvene
With natural aromatic smell, therefore it has very high application value in food, drug, cosmetic field.
Dendrobium candidum enjoys the good reputation of " civil mesona ", and the research of modern science also demonstrates the stone inside dendrobium candidum
The plurality of active ingredients such as dry measure used in former times polysaccharide can increase the vigor of internal T cell and B cell, to improve body immunity.Meanwhile iron
Skin dendrobium nobile is to stabilizing blood sugar, reducing blood lipid, relieving insomnia and gastrointestinal health, relief of constipation, improving eyesight is promoted to have good effect.Especially
It is that young female friend often eats dendrobium candidum, can effectively improve term symptom, and to beautifying face and moistering lotion, delaying senescence has obviously
Effect.In general, people eat the stem of dendrobium nobile, and leaf is discarded.But dendrobium candidum leaf is a part of dendrobium candidum,
There is very high medical value as dendrobium candidum.It is detected according to GC-MS, the functional components such as polysaccharide, dendrobine in dendrobium nobile
In stem of Dendrobium at most, followed by leaf and root, dendrobium candidum leaf have been also enriched in dendrobium polysaccharide, dendrobine etc. to content, same to have
There is health care anti-aging function.
The Chinese patent of publication No. CN104095793A discloses a kind of dendrobium candidum toner and preparation method thereof, includes
Weight fraction is water: 65.6-70.6 parts, 8-13 parts of dendrobium candidum extract liquor, and 5-7 parts of butanediol, hamamelis extract 5-7
Part, 2-4 parts of niacinamide, 4-6 parts of glycine betaine, 0.15-0.35 parts of dipotassium glycyrrhizinate, 0.1-0.3 parts of allantoin, Sodium Hyaluronate
0.2-0.4 parts, 0.25-0.45 parts of iodopropynyl formic acid esters and dihydroxymethyl hydantoins mixture.This formula chemistry
The moisturizer of synthesis, preservative add more, shared large percentage, and dendrobium nobile higher cost.Butanediol is colourless
Viscous oil-like liquid can be such that the quality of toner relatively sticks greasy, skin sense is bad as moisturizer with 5-7 parts.
The Chinese patent of publication No. CN106309187A discloses a kind of toner containing Rosemary Oil, main component group
Become: 10-15 parts of Rosemary Oil, 1-2 parts of lemon, 100-120 parts of distilled water, 15-20 parts of apple vinegar.The toner at
Divide simply, there is certain inoxidizability, cost is not also high, but the emulsifier that two kinds of essential oils do not have, stability and dispersion
Property will not be fine.
The Chinese patent of publication No. CN107714574A discloses a kind of jasmine essential oil toner, jasmine essential oil
0.01%-2%, lemonade 1%-5%, Gynostemma pentaphylla extract 1%-5%, safflower seed oil 0.001%-1%, Rosa Damascana 0.1-
1%, surplus is bamboo juice.Emulsifier is not used in the invention, content of functional component is relatively low, and the ability of skin care is slightly weak, beauty
Skin effect is impacted.
Summary of the invention
Goal of the invention: in order to overcome the shortage of prior art, the present invention is using natural green as objective, with from being ignored by people
The fresh tea leaves essential oil extracted in fresh leaves of tea plant is primary raw material, and the abstraction function ingredient from the dendrobium candidum leaf discarded by people becomes
Waste be changed into values, and addition pure plant surfactant is used as emulsifier, for people provide it is a kind of it is safe, can deeply nourish and moisturize skin,
Anti-aging, antibacterial anti-inflammatory repair toner of skin and preparation method thereof.
Technical solution: in order to achieve the above-mentioned object of the invention, the present invention adopts the following technical scheme:
A kind of fresh tea leaves essential oil toner, it is by including that the raw material of following mass fraction is made:
5~8 parts of fresh tea leaves essential oil, 10~15 parts of dendrobium candidum leaf extract, 2~5 parts of butanediol, pure plant emulsifier
0.8-1.6 parts, 0.5~1.0 part of Sodium Hyaluronate, 70~80 parts of deionized water.
It is preferred that the fresh tea leaves essential oil toner is made of the raw material including following mass fraction, pure fresh tea leaves essential oil 8
Part, 12 parts of dendrobium candidum leaf extract, 3 parts of butanediol, 1.0 parts of pure plant emulsifier, 0.5 part of Sodium Hyaluronate, deionized water
75.5 parts.
Wherein, the fresh tea leaves essential oil is as nutritional agents, antioxidant, antibacterial agent, fragrance
Wherein, the dendrobium candidum leaf extract is as nutritional agents, moisturizer, antioxidant
Wherein, the butanediol is as moisturizer,
Wherein, pure plant emulsifier is as emulsifier,
Wherein, Sodium Hyaluronate is as moisturizer.
Heretofore described fresh tea leaves refer to the tealeaves of fresh picking.
The present invention also provides a kind of fresh tea leaves essential oil toners, comprising the following steps:
(1) fresh tea leaf is picked, cleans and drains, is crushed, is distilled using 0.075~0.095MPa reduced steam, distillation
Shi Wendu is 65~80 °, obtains fresh tea leaves hydrosol, is extracted with anhydrous ether, the volume ratio of ether and fresh tea leaves hydrosol be 1:5~
1:10, adds solid sodium chloride, and the ratio of sodium chloride and liquid is to take 1g:20ml~1g:30ml, obtains fresh tea leaves essential oil；
(2) it takes fresh dendrobium candidum leaf to clean to drain, ultraviolet disinfection, low temperature is added by solid-liquid ratio 1:5-1:10 (g/mL) and goes
Ionized water crushes, is filtered under diminished pressure, obtains dendrobium candidum leaf extract；
(3) formula ratio deionized water, butanediol, pure plant emulsifier, Sodium Hyaluronate, fresh leaves of tea plant essential oil are poured into and is matched
Expect stir about 30 minutes, to be emulsified in pot；
(4) dendrobium candidum leaf extract is poured into above-mentioned ingredients pot and continues stir about 30 minutes to uniform, obtain the fresh of tea
Leaf essential oil toner；
(5) gained toner carries out independent packaging with 1.5mL brown bottle.
Fresh tea leaves essential oil is fresh tea leaves piece by vacuum distillation, product extracted, and the temperature of vacuum distillation is controlled 80
Degree hereinafter, can to greatest extent in retention of oil effective component.It is tested and analyzed through GC-MS, main component propionic acid in the essential oil
Ethyl ester (30.39%), butyl acetate (12.03%) have fruit aroma, are the addition fragrance allowed in food.Main component second
Sour agalloch eaglewood ester has the quiet and tastefully laid out fragrance of the lily of the valley, is the advanced indispensable fragrance of essence of system, and property is stablized；Main component 14-
Methylpentadecanoic methyl esters is a kind of fine perfumery, is also commonly used for emulsifier, moisturizer, bleeding agent；Main component leaf-alcohol, has
Intense green tender leaf fragrance, is one of rare spice of world pop；Main component styracitol has cape jasmine floral scent；Mainly
Ingredient benzyl carbinol has hyacinthine fragrance, and main component benzylalcohol is very useful fixastive, preservative；Main component geraniol tool
There is rose fragrance, be important blending raw material, while there is the ability of antibacterial；Main component wintergreen has peppermint fragrance, commonly uses
In blending, while the effect to promote blood circulation with anti-inflammatory having；Main component BHT, is widely used in food industry and cosmetics
Industrially, free radical can be removed, is the antioxidant having many uses.
Dendrobium candidum, which arranges the main component dendrobium polysaccharide first of nine big mesonas, in dendrobium candidum leaf extract, to be had centainly
Physiological activity can effectively remove the accumulation of skin free radical, repair damaged cell, while having effects that antibacterial anti-inflammatory.
Important ingredient dendrobine therein belongs to alkaloid, has physiological activity, plays the role of adjusting immunity of organisms,
And fungi and bacterium can be inhibited.
Wherein contain 18 kinds of amino acid, mainly has aspartic acid, glutamic acid, valine, leucine, these amino acid energy
The immune function of skin is improved, skin-nourishing is supplied, prevents wrinkle from generating.
Its vitamin A being rich in, vitamin C, vitamin E, all have it is anti-oxidant, promote blood circulation, delay cell old
The effect of change.While skin nutrition, there is good skin sense.
The pure plant emulsifier is by 8-15 parts of tri- glyceryl isostearate of PEG-20, PEG-15 glycerol isostearic acid
1-4 parts and 1-4 parts of PEG-7 olive grease of ester are made, in terms of mass fraction.PEG-20 glyceryl triisostearate HLB value be 8,
PEG-7 olive grease HLB value is that 11, PEG-15 iso stearic acid of glycerine ester HLB value is 12, and the mixture of three has excellent
HLB value, emulsifying effectiveness are better than single emulsifier.And it is safe and non-stimulating, and can moisturize the skin.
Above-mentioned fresh leaves of tea plant essential oil and dendrobium candidum leaf extract ingredient, full of nutrition, functional component is complementary to one another, and is had
Good synergistic function.
The utility model has the advantages that
(1) present invention is main component using fresh tea leaves essential oil and dendrobium candidum leaf extract, this two kinds of ingredients respectively have spy
Color mutually acts synergistically between ingredient, so that the toner of preparation is salubrious, faint scent, non-greasy, moistens moisturizing after smearing, antibacterial disappears
Scorching, reparation damage skin, preferably safeguards the elasticity and glossiness of skin.
(2) the fresh tea leaves essential oil that the present invention uses assigns toner pleasant tea perfume smell, does not have to another plus chemical fragrance.
(3) the fresh tea leaves essential oil and dendrobium candidum leaf extract that the present invention uses inherently contain there are many antioxidant and prevent
Rotten agent, pure natural, safety are without side-effects.Without separately adding antioxidant and preservative.In addition packed using independent brown vial,
Make the shelf life of toner up to 2 years or more.
As a whole, various composition cooperates supplements technical solution of the present invention, by optimizing constituent content, makes
End formulation reached it is safe it is mild, nourishes rough skin, salubrious non-greasy can be goed deep into, antibacterial anti-inflammatory repairs the effect of skin.This hair
Bright toner smell, color, centrifugal stability, cold-resistant stability and heat-resistant stability are very excellent.And preparation method letter
Single, equipment requirement is low, easy to industrialized production.
Detailed description of the invention
The detection of Fig. 1 fresh tea leaves essential oil gas chromatography mass spectrometry is schemed, and 1 is ethyl propionate in Fig. 1；2 be butyl acetate；3 be 3- hexene -1-
Alcohol, (suitable)-；4 be 2- hexen-1-ol, (anti-)-；7 be 1,6- linalool -3- alcohol, 3,7- dimethyl-acetic acid esters；11 be benzene second
Ketone；15 be 2- pentadecanone；6,10,14- trimethyl；17 be pentadecanoic acid, 14- methyl-, methyl ester.
Specific embodiment
According to following embodiments, the present invention may be better understood.However, as it will be easily appreciated by one skilled in the art that real
It applies content described in example and is merely to illustrate the present invention, without sheet described in detail in claims should will not be limited
Invention.
Embodiment 1: the preparation method of fresh tea leaf essential oil.
Fresh tea leaf is picked, cleans and drains, is crushed, is distilled using 0.075~0.095MPa reduced steam, temperature when distillation
Degree is 65~80 °, obtains fresh tea leaves hydrosol, is extracted with anhydrous ether, and the volume ratio of ether and fresh tea leaves hydrosol is 1:5~1:
10, add solid sodium chloride, the ratio of sodium chloride and liquid is to take 1g:20ml~1g:30ml, obtains fresh tea leaves essential oil.It obtains
Fresh tea leaf essential oil utilizes Gc-mss.It is as shown in Figure 1 to analyze result.Gas chromatography mass spectrometry testing result is as shown in table 1.
1 fresh tea leaves essential oil gas chromatography mass spectrometry testing result of table
Embodiment 2:
A kind of fresh tea leaves essential oil toner formula, calculates, the raw material including following number according to mass fraction:
5 parts of fresh tea leaves essential oil, 15 parts of dendrobium candidum leaf extract, 2 parts of butanediol, 1.0 parts of pure plant emulsifier, hyalomitome
1 part of sour sodium, 76 parts of deionized water.
Implement 3:
A kind of fresh tea leaves essential oil toner formula, calculates, the raw material including following number according to mass fraction:
6 parts of fresh tea leaves essential oil, 14 parts of dendrobium candidum leaf extract, 1 part of butanediol, 1.5 parts of pure plant emulsifier, hyalomitome
0.5 part of sour sodium, 77 parts of deionized water.
Embodiment 4:
A kind of fresh tea leaves essential oil toner formula, calculates, the raw material including following number according to mass fraction:
It is 7 parts of fresh tea leaves essential oil, 15 parts of dendrobium candidum leaf extract, 1.0 parts of butanediol, 1.0 parts of pure plant emulsifier, transparent
0.5 part of matter acid sodium, 75.5 parts of deionized water.
Embodiment 5:
A kind of tealeaves essential oil toner formula, calculates, the raw material including following number according to mass fraction:
8 parts of fresh tea leaves essential oil, 12 parts of dendrobium candidum leaf extract, 2 parts of butanediol, 1.0 parts of pure plant emulsifier, hyalomitome
1.0 parts of sour sodium, 76 parts of deionized water.
Embodiment 6:
A kind of tealeaves essential oil toner formula, calculates, the raw material including following number according to mass fraction:
It is 10 parts of fresh tea leaves essential oil, 12 parts of dendrobium candidum leaf extract, 2 parts of butanediol, 0.7 part of pure plant emulsifier, transparent
1 part of matter acid sodium, 74.3 parts of deionized water.
Toner using effect of the present invention:
1, general information
Panellist: at least makeup 4 times 18-45 years old volunteers weekly, totally 40.
Control group: the volunteer of use control toner (commercially available toner), totally 30.
2. service life and application method
Service life: surrounding is a period.
Application method: it after face cleaning, takes suitable toner in the palm of the hand, is extremely absorbed with neck on the face patting.
3. effect criterion
Effect is divided into 3 grades
1 grade: it is soft moist using rear skin sense, it easily absorbs, moistening effect is good.
2 grades: being lubricated using rear skin sense, be easier to absorb, moistening effect is preferable.
3 grades: after use, skin sense is general, absorbs generally, moistening effect is general.
4. using effect is shown in Table 2.
The test of 2 toner using effect of table
| Group/effect | Number of cases | 1 grade | 2 grades | 3 grades |
| Toner of the present invention | 40 | 33 | 5 | 2 |
| Compare toner | 30 | 14 | 11 | 5 |
It can be obtained by 2 result of table, compare toner, there is the number of cases of 1 grade of effect, only 46.7% after use, and use this hair
After bright toner, there is the number of cases of 1 grade of effect to can achieve 82.5%, much higher than control toner.
Claims (5)
1. a kind of fresh tea leaves essential oil toner, which is characterized in that it is by including that the raw material of following mass fraction is made:
5~8 parts of fresh tea leaves essential oil, 10~15 parts of dendrobium candidum leaf extract, 4~8 parts of butanediol, pure plant emulsifier 0.8~
1.6 parts, 0.5~1.0 part of Sodium Hyaluronate, 70~80 parts of deionized water.
2. fresh tea leaves essential oil toner according to claim 1, which is characterized in that it is by the original including following mass fraction
Material is made:
8 parts of fresh tea leaves essential oil, 12 parts of dendrobium candidum leaf extract, 3 parts of butanediol, 1.0 parts of pure plant emulsifier, Sodium Hyaluronate
0.5 part, 75.5 parts of deionized water.
3. fresh tea leaves essential oil toner according to claim 1, which is characterized in that the preparation side of the fresh tea leaves essential oil
Method is as follows:
Take fresh tea leaves, clean and drain, crush, distilled using 0.075~0.095MPa reduced steam, when distillation temperature be 65~
80 °, fresh tea leaves hydrosol is obtained, is extracted with anhydrous ether, the volume ratio of ether and fresh tea leaves hydrosol is 1:5~1:10, chlorination
The ratio of sodium solid, sodium chloride and liquid is to take 1g:20ml~1g:30ml, obtains fresh tea leaves essential oil.
4. requiring the fresh leaves of tea plant essential oil toner according to right 1, which is characterized in that the dendrobium candidum leaf extract
The preparation method is as follows:
The dendrobium candidum blade of picking is cleaned and is drained, ultraviolet disinfection, and deionization is added by solid-liquid ratio 1g:8mL~1g:10mL
Water crushes, by being filtered under diminished pressure, obtains dendrobium candidum leaf extract.
5. the preparation method of any fresh tea leaves essential oil toner of Claims 1 to 4, which is characterized in that by deionized water, fourth
Glycol, pure plant emulsifier, Sodium Hyaluronate, fresh tea leaves essential oil pour into ingredients pot in proportion, stir 10~30 minutes, then press
Dendrobium candidum leaf extract is added in ratio, continues to mix for stirring 30 minutes, obtains fresh leaves of tea plant essential oil toner.
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| CN112641685A (en) * | 2019-10-10 | 2021-04-13 | 广州樱奈儿化妆品有限公司 | Moisturizing and circulation promoting essence and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110537612A (en) * | 2019-09-10 | 2019-12-06 | 方红霞 | preparation method for simultaneously obtaining tea hydrolat and primary tea |
| CN112641685A (en) * | 2019-10-10 | 2021-04-13 | 广州樱奈儿化妆品有限公司 | Moisturizing and circulation promoting essence and preparation method thereof |
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