CN108938521B - Anti-hair loss shampoo containing natural plant components and preparation method thereof - Google Patents
Anti-hair loss shampoo containing natural plant components and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/08—Antiseborrheics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/14—Drugs for dermatological disorders for baldness or alopecia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
Abstract
The invention provides an anti-hair loss shampoo containing natural plant components, which belongs to the technical field of washing products and comprises a tremella extract, a zanthoxylum bungeanum fruit extract, a platycladus orientalis extract, a ginger root extract, a mulberry root bark extract, disodium ethylenediaminetetraacetate, citric acid, sodium benzoate, sodium chloride, essence and water. The active ingredients of the anti-hair loss shampoo provided by the invention are natural plant ingredients, so that the anti-hair loss shampoo does not cause toxic or side effect to users, not only has the anti-hair loss effect, but also can promote hair growth after being used by patients.
Description
Technical Field
The invention relates to the technical field of washing and chemical products, and particularly relates to an anti-hair loss shampoo containing natural plant components and a preparation method thereof.
Background
Along with the rapid development of economy and the improvement of the living standard of people, people pay more and more attention to instruments and appearances, not only pay more attention to the skin care, but also pay more and more attention to the hair and scalp care. In recent years, the problem of alopecia has been receiving more and more attention, and according to a year-round follow-up questionnaire data performed on the net friends of male alopecia in the website of the major households such as new waves, etc., 60% of men have alopecia as early as 25 years old, the proportion of alopecia occurring before 30 years old reaches 83.9%, and about 84.8% of net friends with alopecia have been diagnosed as seborrheic alopecia. In the medical field, many anti-alopecia drugs represented by finasteride and minoxidil have certain effects in clinical application, but the drugs bring certain side effects to the body of a patient.
Disclosure of Invention
The active ingredients of the anti-hair loss shampoo provided by the invention are all natural plant ingredients, so that the anti-hair loss shampoo does not cause toxic or side effect to users, not only has the anti-hair loss effect, but also can grow hair after being used.
The invention provides anti-hair loss shampoo containing natural plant components, which comprises the following components in parts by weight:
0.1-0.5 parts of tremella extract;
0.3-0.8 part of a zanthoxylum bungeanum fruit extract;
0.3-0.8 parts of platycladus orientalis extract;
0.05-0.15 parts of ginger root extract;
0.1-0.3 parts of mulberry root bark extract;
0.03-0.08 part of disodium ethylene diamine tetraacetate;
0.3-0.4 part of citric acid;
0.3-0.8 part of sodium benzoate;
0.3-0.8 part of sodium chloride;
0.05-0.15 parts of essence;
90-100 parts of water.
Preferably, the composition comprises the following components in parts by weight:
0.3 part of tremella extract;
0.5 part of zanthoxylum bungeanum maxim fruit extract;
0.5 part of arborvitae extract;
0.1 part of ginger root extract;
0.2 part of mulberry root bark extract;
0.05 part of disodium ethylene diamine tetraacetate;
0.35 part of citric acid;
0.5 part of sodium benzoate;
0.5 part of sodium chloride;
0.1 part of essence;
96.9 parts of water.
Preferably, the preparation method of the tremella extract comprises the following steps:
mixing tremella and water, and then treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
and mixing the first filtrate and the second filtrate, and concentrating and drying the obtained mixed solution to obtain the tremella extract.
Preferably, the preparation method of the extract of the zanthoxylum bungeanum fruit comprises the following steps:
mixing the pepper fruits with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
and mixing the first filtrate and the second filtrate, and concentrating and drying the obtained mixed solution to obtain the zanthoxylum bungeanum fruit extract.
Preferably, the method for preparing the biota orientalis extract comprises the following steps:
mixing the platycladus orientalis with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain the extract of the arborvitae.
Preferably, the preparation method of the ginger root extract comprises the following steps:
mixing ginger root with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain the ginger root extract.
Preferably, the preparation method of the mulberry root bark extract comprises the following steps:
mixing mulberry root bark with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain the mulberry root bark extract.
Preferably, the water is deionized water.
The invention also provides a preparation method of the anti-hair loss shampoo, which comprises the following steps: and mixing the tremella extract, the zanthoxylum bungeanum fruit extract, the platycladus orientalis extract, the ginger root extract, the mulberry root bark extract, disodium edetate, citric acid, sodium benzoate, sodium chloride, essence and water to obtain the anti-hair loss shampoo.
Preferably, the mixing temperature is 60-80 ℃.
The invention provides the hair loss preventing shampoo, the white fungus extract can prevent hair loss, the arborvitae extract has an antibacterial effect, the ginger and the pepper fruit extract can stimulate local skin vasodilatation and hyperemia, enhance local blood supply, improve nutrition of hair follicles and promote hair growth, the mulberry root bark extract has an oil control effect, and under the effects of the white fungus extract, the pepper fruit extract, the arborvitae extract, the ginger root extract and the mulberry root bark extract, the hair loss can be prevented, and the hair growth effect can be realized.
The results of the embodiments of the present invention show that: the active ingredients of the anti-hair loss shampoo provided by the invention are natural plant ingredients, so that the anti-hair loss shampoo does not cause toxic or side effect to users, not only has the anti-hair loss effect, but also can promote hair growth after being used by patients.
Drawings
Fig. 1 is a diagram illustrating hair of a patient in example 4 before using the alopecia prevention shampoo prepared in example 1;
fig. 2 shows the condition of hair of a patient of example 4 after 3 months using the alopecia prevention shampoo prepared in example 1;
fig. 3 is a view showing the condition of hair of a patient in example 5 before using the alopecia prevention shampoo prepared in example 1;
fig. 4 shows the condition of hair of the patient of example 5 after 5 months using the alopecia prevention shampoo prepared in example 1.
Detailed Description
The invention provides anti-hair loss shampoo containing natural plant components, which comprises the following components in parts by weight: 0.1-0.5 parts of tremella extract; 0.3-0.8 part of a zanthoxylum bungeanum fruit extract; 0.3-0.8 parts of platycladus orientalis extract; 0.05-0.15 parts of ginger root extract; 0.1-0.3 parts of mulberry root bark extract; 0.03-0.08 part of disodium ethylene diamine tetraacetate; 0.3-0.4 part of citric acid; 0.3-0.8 part of sodium benzoate; 0.3-0.8 part of sodium chloride; 0.05-0.15 parts of essence; 90-100 parts of water.
The anti-hair loss shampoo provided by the invention comprises 0.1-0.5 part by weight of tremella extract, preferably 0.2-0.4 part by weight, and more preferably 0.3 part by weight.
In the present invention, the preparation method of the tremella extract preferably includes:
mixing tremella and water, and then treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
and mixing the first filtrate and the second filtrate, and concentrating and drying the obtained mixed solution to obtain the tremella extract.
In the invention, the tremella is mixed with water and then is preferably treated at 75-85 ℃ for 2.5-3.5 h, and more preferably at 80 ℃ for 3 h. In the invention, the volume ratio of the mass of the tremella to the water is preferably (0.5-1.5) g, (5-15), more preferably (0.8-1.2) g, (8-12), and most preferably 1: 10. The source of the tremella is not specially limited, and the tremella can be obtained by adopting a commercially available product.
In the invention, the tremella extract has the function of preventing alopecia.
In the present invention, the filtration conditions are not particularly limited, and conventional filtration conditions may be employed.
In the present invention, the concentration of the mixed solution is preferably carried out by a rotary evaporation method, and the conditions of the rotary evaporation method are not particularly limited in the present invention, and may be any conventional conditions.
In the present invention, the drying is preferably performed by a freeze-drying method, and the conditions of the freeze-drying method are not particularly limited in the present invention, and may be any conventional conditions.
The anti-hair loss shampoo provided by the invention comprises 0.3-0.8 part by weight of a zanthoxylum bungeanum fruit extract, preferably 0.4-0.6 part by weight, and more preferably 0.5 part by weight.
In the present invention, the method for preparing the extract of the fruit of zanthoxylum piperitum preferably comprises:
mixing the pepper fruits with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
and mixing the first filtrate and the second filtrate, and concentrating and drying the obtained mixed solution to obtain the zanthoxylum bungeanum fruit extract.
In the invention, the pepper fruits and water are mixed and then are preferably treated at 75-85 ℃ for 2.5-3.5 h, and more preferably at 80 ℃ for 3 h. In the invention, the volume ratio of the mass of the pepper fruits to the water is preferably (0.5-1.5) g, (5-15), more preferably (0.8-1.2) g, (8-12), and most preferably 1: 10. The source of the pepper fruits is not particularly limited, and the pepper fruits can be obtained by adopting a commercial product.
In the invention, the extraction of the zanthoxylum bungeanum maxim fruit can stimulate local skin vasodilatation and hyperemia, enhance local blood supply, improve the nutrition of hair follicles and promote hair growth.
The present invention is not particularly limited to the above filtration conditions, and may be carried out under conventional filtration conditions.
In the present invention, the concentration of the mixed solution is preferably carried out by a rotary evaporation method, and the conditions of the rotary evaporation method are not particularly limited in the present invention, and may be any conventional conditions.
In the present invention, the drying is preferably performed by a freeze-drying method, and the conditions of the freeze-drying method are not particularly limited in the present invention, and may be any conventional conditions.
The anti-hair loss shampoo provided by the invention comprises 0.3-0.8 part by weight of a arborvitae extract, preferably 0.4-0.6 part by weight, and more preferably 0.5 part by weight.
In the present invention, the method for preparing the biota orientalis extract preferably comprises:
mixing the biota orientalis and water, and treating for 2-4 h at 70-90 ℃ to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain the extract of the arborvitae.
In the invention, the biota orientalis is mixed with water and then treated at 75-85 ℃ for 2.5-3.5 h, and more preferably at 80 ℃ for 3 h. In the invention, the volume ratio of the mass of the biota orientalis to the water is preferably (0.5-1.5) g, (5-15), more preferably (0.8-1.2) g, (8-12), and most preferably 1: 10. The source of the biota orientalis is not particularly limited in the present invention, and a commercially available product may be used. In the present invention, the biota orientalis is preferably a branch and/or a leaf of biota orientalis.
In the present invention, the biota orientalis extract has an antibacterial action.
In the present invention, the filtration conditions are not particularly limited, and conventional filtration conditions may be employed.
In the present invention, the concentration of the mixed solution is preferably carried out by a rotary evaporation method, and the conditions of the rotary evaporation method are not particularly limited in the present invention, and may be any conventional conditions.
In the present invention, the drying is preferably performed by a freeze-drying method, and the conditions of the freeze-drying method are not particularly limited in the present invention, and may be any conventional conditions.
The anti-hair loss shampoo provided by the invention comprises 0.05-0.15 part by weight of ginger root extract, preferably 0.08-0.12 part by weight, and more preferably 0.1 part by weight.
In the present invention, the preparation method of the ginger root extract preferably includes:
mixing ginger root with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain the ginger root extract.
In the invention, the ginger root is mixed with water and then treated for 2.5-3.5 h at 75-85 ℃, and more preferably treated for 3h at 80 ℃. In the invention, the volume ratio of the mass of the ginger root to the water is preferably (0.5-1.5) g, (5-15), more preferably (0.8-1.2) g, (8-12), and most preferably 1: 10. The source of the ginger root is not specially limited, and a commercially available product is adopted.
In the present invention, the ginger root extract can stimulate local skin vasodilatation and hyperemia, enhance local blood supply, improve nutrition of hair follicle, and promote hair growth.
In the present invention, the filtration conditions are not particularly limited, and conventional filtration conditions may be employed.
In the present invention, the concentration of the mixed solution is preferably carried out by a rotary evaporation method, and the conditions of the rotary evaporation method are not particularly limited in the present invention, and may be any conventional conditions.
In the present invention, the drying is preferably performed by a freeze-drying method, and the conditions of the freeze-drying method are not particularly limited in the present invention, and may be any conventional conditions.
The anti-hair loss shampoo provided by the invention comprises 0.1-0.3 part by weight of mulberry root bark extract, preferably 0.15-0.25 part by weight, and more preferably 0.2 part by weight.
In the present invention, the preparation method of the sang root bark extract preferably includes:
mixing mulberry root bark with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain the mulberry root bark extract.
In the invention, the mulberry root bark is mixed with water and then treated for 2.5 to 3.5 hours at the temperature of 75 to 85 ℃, and is treated for 3 hours at the temperature of 80 ℃. In the invention, the volume ratio of the mass of the mulberry root bark to the water is preferably (0.5-1.5) g, (5-15), more preferably (0.8-1.2) g, (8-12), and most preferably 1: 10. The source of the mulberry root bark is not particularly limited, and a commercially available product is adopted.
In the present invention, the mulberry root bark extract has an oil control effect.
In the present invention, the filtration conditions are not particularly limited, and conventional filtration conditions may be employed.
In the present invention, the concentration of the mixed solution is preferably carried out by a rotary evaporation method, and the conditions of the rotary evaporation method are not particularly limited in the present invention, and may be any conventional conditions.
In the present invention, the drying is preferably performed by a freeze-drying method, and the conditions of the freeze-drying method are not particularly limited in the present invention, and may be any conventional conditions.
The anti-hair loss shampoo provided by the invention comprises 0.03-0.08 parts by weight of disodium ethylene diamine tetraacetate, preferably 0.04-0.06 parts by weight, and more preferably 0.05 parts by weight.
The anti-hair loss shampoo provided by the invention comprises 0.3-0.4 part by weight of citric acid, and preferably 0.35 part by weight of citric acid.
The anti-hair loss shampoo provided by the invention comprises 0.3-0.8 part by weight of sodium benzoate, preferably 0.4-0.6 part by weight, and more preferably 0.5 part by weight.
The anti-hair loss shampoo provided by the invention comprises 0.3-0.8 part of sodium chloride by weight, preferably 0.4-0.6 part of sodium chloride by weight, and more preferably 0.5 part of sodium chloride by weight.
The anti-hair loss shampoo provided by the invention comprises 0.05-0.15 part by weight of essence, preferably 0.08-0.12 part by weight, and more preferably 0.1 part by weight. The type of the essence is not particularly limited, and the essence used in the shampoo is prepared conventionally. The source of the essence is not particularly limited, and the essence can be prepared from conventional commercial products.
The anti-hair loss shampoo provided by the invention comprises 90-100 parts of water by weight, preferably 63-97 parts of water by weight, and most preferably 96.9 parts of water by weight. In the present invention, the water is preferably deionized water.
The invention also provides a preparation method of the anti-hair loss shampoo, which comprises the following steps: and mixing the tremella extract, the zanthoxylum bungeanum fruit extract, the platycladus orientalis extract, the ginger root extract, the mulberry root bark extract, disodium edetate, citric acid, sodium benzoate, sodium chloride, essence and water to obtain the anti-hair loss shampoo.
In the invention, the mixing temperature is preferably 60-80 ℃, more preferably 65-75 ℃, and most preferably 70 ℃.
In the invention, the dosage of the anti-hair loss shampoo is preferably 2-5 mL/time, and the frequency of use is preferably 1 time per day.
The anti-hair loss shampoo containing natural plant components and the preparation method thereof are further described in detail with reference to specific examples, and the technical scheme of the invention includes but is not limited to the following examples.
Example 1
Mixing 0.3kg of tremella extract, 0.5kg of zanthoxylum piperitum extract, 0.5kg of platycladus orientalis extract, 0.1kg of ginger root extract, 0.2kg of mulberry root bark extract, 0.05kg of disodium edetate, 0.35kg of citric acid, 0.5kg of sodium benzoate, 0.5kg of sodium chloride, 0.1kg of essence and 96.9kg of water at 70 ℃ to obtain the anti-hair loss shampoo containing natural plant components.
The preparation method of the tremella extract comprises the following steps:
mixing Tremella with water, and treating at 80 deg.C for 3h to obtain first treatment solution; filtering the first treatment solution to obtain first filter residue and first filtrate; mixing the first filter residue with water, and treating at 80 ℃ for 2-4 h to obtain a second treatment solution; filtering the second treatment solution to obtain second filter residue and second filtrate; mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain Tremella extract.
The preparation method of the zanthoxylum bungeanum maxim fruit extract comprises the following steps:
mixing the pepper fruits with water, and treating at 80 ℃ for 3h to obtain a first treatment solution; filtering the first treatment solution to obtain first filter residue and first filtrate; mixing the first filter residue with water, and treating at 80 ℃ for 2-4 h to obtain a second treatment solution; filtering the second treatment solution to obtain second filter residue and second filtrate; mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain the extract of fructus Zanthoxyli.
The preparation method of the arborvitae extract comprises:
mixing cacumen biotae with water, and treating at 80 deg.C for 3h to obtain a first treatment solution; filtering the first treatment solution to obtain first filter residue and first filtrate; mixing the first filter residue with water, and treating at 80 ℃ for 2-4 h to obtain a second treatment solution; filtering the second treatment solution to obtain second filter residue and second filtrate; mixing the first filtrate and the second filtrate, concentrating the obtained mixture, and drying to obtain the extract of Chinese arborvitae.
The preparation method of the ginger root extract comprises the following steps:
mixing ginger root with water, and treating at 80 deg.C for 3 hr to obtain a first treating solution; filtering the first treatment solution to obtain first filter residue and first filtrate; mixing the first filter residue with water, and treating at 80 ℃ for 2-4 h to obtain a second treatment solution; filtering the second treatment solution to obtain second filter residue and second filtrate; mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain ginger root extract.
The preparation method of the mulberry root bark extract comprises the following steps:
mixing mulberry root bark with water, and treating at 80 ℃ for 3h to obtain a first treatment solution; filtering the first treatment solution to obtain first filter residue and first filtrate; mixing the first filter residue with water, and treating at 80 ℃ for 2-4 h to obtain a second treatment solution; filtering the second treatment solution to obtain second filter residue and second filtrate; mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain the cortex Mori extract.
Example 2
Mixing 0.1kg of tremella extract, 0.3kg of zanthoxylum piperitum extract, 0.3kg of platycladus orientalis extract, 0.05kg of ginger root extract, 0.1kg of mulberry root bark extract, 0.03kg of disodium edetate, 0.3kg of citric acid, 0.3kg of sodium benzoate, 0.3kg of sodium chloride, 0.05kg of essence and 90kg of water at 70 ℃ to obtain the anti-hair loss shampoo containing natural plant components.
The preparation method of the arborvitae extract comprises:
mixing the cacumen biotae and water, and treating at 80 ℃ for 3h to obtain a first treatment solution; filtering the first treatment solution to obtain first filter residue and first filtrate; mixing the first filter residue with water, and treating at 80 ℃ for 2-4 h to obtain a second treatment solution; filtering the second treatment solution to obtain second filter residue and second filtrate; mixing the first filtrate and the second filtrate, concentrating the obtained mixture, and drying to obtain the extract of Chinese arborvitae.
The preparation method of Tremella extract, fructus Zanthoxyli extract, rhizoma Zingiberis recens extract, and cortex Mori extract is the same as that of the previous one
Example 1.
Example 3
Mixing 0.1kg of tremella extract, 0.3kg of zanthoxylum piperitum extract, 0.3kg of platycladus orientalis extract, 0.05kg of ginger root extract, 0.1kg of mulberry root bark extract, 0.03kg of disodium edetate, 0.3kg of citric acid, 0.3kg of sodium benzoate, 0.3kg of sodium chloride, 0.05kg of essence and 90kg of water at 70 ℃ to obtain the anti-hair loss shampoo containing natural plant components.
The preparation method of the tremella extract, the zanthoxylum bungeanum fruit extract, the platycladus orientalis extract, the ginger root extract and the mulberry root bark extract is the same as that of the example 1.
Example 4
Yellow loyalty, male, age 35, hair condition before use is shown in fig. 1, hair condition after 3 months using the alopecia preventing shampoo prepared in example 1 is shown in fig. 2, and the usage amount of the alopecia preventing shampoo is 5ml once a day.
From fig. 1 and 2, it can be understood that the alopecia phenomenon is controlled to a certain extent after 3 months of using the anti-hair loss shampoo provided by the invention.
Example 5
In the case of hair before use, see fig. 3, and in the case of hair after 5 months using the alopecia preventing shampoo prepared in example 2, see fig. 4. The anti-hair loss shampoo is used once a day, and the using amount is 5 ml.
From fig. 3 and 4, it can be concluded that the hair loss phenomenon is remarkably controlled after 5 months of using the shampoo.
According to the embodiments, the active ingredients of the anti-hair loss shampoo provided by the invention are all natural plant ingredients, so that the anti-hair loss shampoo does not cause toxic or side effect on users, has an anti-hair loss effect, and can also grow hair after being used.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.
Claims (3)
1. An anti-hair loss shampoo containing natural plant components comprises the following components in parts by weight:
0.3 part of tremella extract;
0.5 part of zanthoxylum bungeanum maxim fruit extract;
0.5 part of arborvitae extract;
0.1 part of ginger root extract;
0.2 part of mulberry root bark extract;
0.05 part of disodium ethylene diamine tetraacetate;
0.35 part of citric acid;
0.5 part of sodium benzoate;
0.5 part of sodium chloride;
0.1 part of essence;
96.9 parts of water;
the preparation method of the tremella extract comprises the following steps:
mixing tremella and water, and then treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, and concentrating and drying the obtained mixed solution to obtain a tremella extract;
the preparation method of the zanthoxylum bungeanum fruit extract comprises the following steps:
mixing the pepper fruits with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, and concentrating and drying the obtained mixed solution to obtain a zanthoxylum bungeanum fruit extract;
the preparation method of the arborvitae extract comprises the following steps:
mixing the platycladus orientalis with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, concentrating the obtained mixed solution, and drying to obtain a biota orientalis extract;
the preparation method of the ginger root extract comprises the following steps:
mixing ginger root with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, and concentrating and drying the obtained mixed solution to obtain a ginger root extract;
the preparation method of the mulberry root bark extract comprises the following steps:
mixing mulberry root bark with water, and treating at 70-90 ℃ for 2-4 h to obtain a first treatment solution;
filtering the first treatment solution to obtain first filter residue and first filtrate;
mixing the first filter residue with water, and treating at 70-90 ℃ for 2-4 h to obtain a second treatment solution;
filtering the second treatment solution to obtain second filter residue and second filtrate;
mixing the first filtrate and the second filtrate, and concentrating and drying the obtained mixed solution to obtain a mulberry root bark extract;
the water is deionized water.
2. The method for preparing the hair loss prevention shampoo according to claim 1, comprising the steps of: and mixing the tremella extract, the zanthoxylum bungeanum fruit extract, the platycladus orientalis extract, the ginger root extract, the mulberry root bark extract, disodium edetate, citric acid, sodium benzoate, sodium chloride, essence and water to obtain the anti-hair loss shampoo.
3. The method according to claim 2, wherein the mixing temperature is 60 to 80 ℃.
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| CN106421699A (en) * | 2016-10-20 | 2017-02-22 | 张双奎 | Shampoo capable of preventing hair loss and promoting hair growth and preparation method thereof |
| KR20170141497A (en) * | 2016-06-15 | 2017-12-26 | 박숙우 | Herbal Shampoo Manufacturing Method using Enzyme Extract Fluid of Chinese Medicine and Dendropanax morbifera Lev |
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| KR20170141497A (en) * | 2016-06-15 | 2017-12-26 | 박숙우 | Herbal Shampoo Manufacturing Method using Enzyme Extract Fluid of Chinese Medicine and Dendropanax morbifera Lev |
| CN106421699A (en) * | 2016-10-20 | 2017-02-22 | 张双奎 | Shampoo capable of preventing hair loss and promoting hair growth and preparation method thereof |
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