CN108938468A - A kind of Chinese prickly ash hand cleanser and preparation method thereof - Google Patents
A kind of Chinese prickly ash hand cleanser and preparation method thereof Download PDFInfo
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- CN108938468A CN108938468A CN201810993493.1A CN201810993493A CN108938468A CN 108938468 A CN108938468 A CN 108938468A CN 201810993493 A CN201810993493 A CN 201810993493A CN 108938468 A CN108938468 A CN 108938468A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/02—Local antiseptics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention belongs to detergents and cosmetic technical field, a kind of Chinese prickly ash hand cleanser and preparation method thereof is disclosed.The component of the Chinese prickly ash hand cleanser is water, lauryl sodium sulfate, alkyl glycosides citrate salt, pepper extract, ethyl alcohol.Preparation method: each component of above-mentioned parts by weight is weighed, the water of the extra half of weighing is poured into and forms sodium dodecyl sulfate solution in lauryl sodium sulfate, it is stirred 10~20 minutes after sodium dodecyl sulfate solution is heated to 35~60 DEG C, then addition alkyl glycosides citrate salt continues stirring and forms mixed liquor in sodium dodecyl sulfate solution, after adjusting PH to 5~7, pepper extract is added in mixed liquor, ethyl alcohol and remaining water, without the sterilization component being harmful to the human body in the hand cleanser, the hand cleanser dirt-removing power is strong, bactericidal range is wide, it is effective to skin safe.
Description
Technical field
The invention belongs to detergents and cosmetic technical field, in particular to a kind of Chinese prickly ash hand cleanser and preparation method thereof.
Background technique
Chinese prickly ash (Zanthexylum bungeanum maxin) is Rutaceae xanthoxylum, is the important pungent perfume (or spice) in China
Material and medicinal plant.Modern natural product chemistry and pharmaceutical research show that the extract of Chinese prickly ash has antitumor, anti-inflammatory town
Bitterly, a variety of physiological activity such as human Demodex, desinsection and antibacterial anti-corrosion are killed in suppression.
In daily life, hand is the position being in the most contact with the external world, not only easily dirty to go back easy infection germ.If do not paid attention to
Hygiene on hand, is easy for causing that illness finds its way in by the mouth.It sterilizes class hand cleanser and compares general hand cleanser, it is clean in addition to that can will hand-wash
Outside, germ can also effectively be killed.The sterilization component of disinfection hand cleanser is mainly spectrum fungicide at present, and this kind of fungicide is stablized
Property is poor, sterilizing time is short, and is harmful to the human body.This patent utilizes the characteristic of pepper extract, and certain agent is added in hand cleanser
Pepper extract is measured, can effectively kill germ, and effective to skin safe.
Summary of the invention
The object of the present invention is to provide a kind of Chinese prickly ash hand cleanser and preparation method thereof, are free of and are harmful to the human body in the hand cleanser
Sterilization component, the hand cleanser dirt-removing power is strong, and bactericidal range is wide, effective to skin safe.
To achieve the above objectives, the present invention is achieved by the following scheme.
Scheme one:
A kind of Chinese prickly ash hand cleanser, it is characterised in that: the component of the Chinese prickly ash hand cleanser is water, lauryl sodium sulfate, alkane
Base glucosides citrate salt, pepper extract, ethyl alcohol.
The characteristics of above-mentioned technical proposal and further improvement:
Further, the parts by weight of each component are:
Water: 80~100 parts,
Lauryl sodium sulfate: 1~5 part,
Alkyl glycosides citrate salt: 10~20 parts,
0.1~5 part of pepper extract,
1~5 part of ethyl alcohol.
Further, the pepper extract is pepper volatile oil.
Further, the water is deionized water.
Scheme two:
A kind of preparation method of Chinese prickly ash hand cleanser, it is characterised in that: each component for weighing above-mentioned parts by weight, by the more of weighing
The water of remaining half, which pours into, forms sodium dodecyl sulfate solution in lauryl sodium sulfate, sodium dodecyl sulfate solution is heated
Stir 10~20 minutes after to 35~60 DEG C, be then added in sodium dodecyl sulfate solution alkyl glycosides citrate salt after
Continuous stirring forms mixed liquor, and after adjusting PH to 5~7, pepper extract, ethyl alcohol and remaining water, stirring are added in mixed liquor
It is uniformly dispersed to solution.
The characteristics of above-mentioned technical proposal and further improvement:
Further, the pepper extract is pepper volatile oil, is made using steam distillation.
Further, the steam distillation are as follows: Chinese prickly ash is placed in extractor and is distilled, distillation time is 1~3
Hour.
The advantages of Chinese prickly ash hand cleanser of the invention, is: belonging to disinfection hand cleanser, can effectively kill while deep-pollution-removing
Germ, contains handguard ingredient simultaneously, easy cleaning and to be able to maintain hand skin soft;And cost is relatively low, technical process is simple, production
Non-pollutant discharge in the process, environmentally friendly, product foaming abundancy is able to satisfy human lives' needs.
Specific embodiment
The component of Chinese prickly ash hand cleanser of the invention is that water, lauryl sodium sulfate, alkyl glycosides citrate salt, Chinese prickly ash mention
Take object, ethyl alcohol.Pepper extract is pepper volatile oil.Water is deionized water.
The effect of clearly to illustrate this composition, is now described in detail each component:
Alkyl glycosides citrate salt:
Alkyl glycosides, APG for short are synthesized by renewable resource natural fatty alcohol and glucose, be a kind of performance compared with
Comprehensive new non-ionic surfactants have both the characteristic of conventional nonionic and anionic surfactant, have high surface
Active, good ecological security and intermiscibility are internationally recognized preferred " green " functional surfactants.APG is nontoxic,
, safety small to skin irritatin, thickening, thickening, detergency are significant.
Citric acid ester type surfactant is a kind of multifunctional green surfactant, have it is nontoxic, non-stimulated, can drop
Solution, the features such as performance is mild, and emulsifiability and dispersion performance are excellent, be widely used to daily use chemicals, weaving, plastic material and
In the industries such as food.
Above-mentioned active matter is passed through into series reaction, row has both the characteristic of the above active matter at glucosides citrate salt, and
It is more convenient to use.
Lauryl sodium sulfate: white or faint yellow powdery is dissolved in water, insensitive to alkali and hard water.With decontamination, emulsification
With excellent foaming power.It is a kind of nontoxic anionic surfactant.Its biological degradability > 90%.Purposes: it is used as emulsification
Agent, extinguishing chemical, foaming agent and textile auxiliary.Also serve as the foaming agent of toothpaste and paste, powdery, shampoo.
Pepper volatile oil contains the various structures type small-molecule substance such as olefines, alcohols, ketone, esters and epoxies.
Existing research shows that there are notable differences with content for different sources Chinese prickly ash pericarp chemical composition of volatile oil composition.Although different
Relative amount is had nothing in common with each other in 3% or more ingredient in the Chinese prickly ash pericarp of the place of production, but mainly based on Monoterpenes, shared ingredient
There are limonene, laurene, cineole, sabinene, australene, terpinol, linalool and linalool acetate etc..Pepper volatile oil
Content and the composition not only influence vulnerable to external factors such as the home environment factor, extraction processing methods, but also because of kind, extraction unit
Position and harvest time etc. are different to be presented difference.Existing research shows that in pepper volatile oil ingredient, enol and its esters are derivative
Object, terpene compound have stronger bacteriostatic activity.
Modern pharmacology research shows that pepper volatile oil has that antitumor, anti-inflammatory and antalgic, that human Demodex etc. is killed in suppression is a variety of
Physiological activity makees the introduction of more system to its antibacterial anti-corrosion and acaricidal activity below.
The antibacterial spectrum width of pepper volatile oil, activity is significant, and mechanism of action is more clear.It causes numerous food rotten, pathogenic true
Bacterium or bacterium have different degrees of inhibitory effect.Jiang little Long etc. compares Japan pepper essential oil and partial monosomy to seven kinds of grain storage aspergillus
With the fungistatic effect of mould, the pepper volatile oil of 0.5L/cm3 dosage and tested monomer can inhibit mycotic spore sprouting and mould
Bacterium.With the Hancheng Region, Shaanxi Z-bungeanum Maxim volatile oil of SFE preparation to black-koji mould, aspergillus oryzae, Candida albicans and large intestine bar
Bacterium has preferable inhibitory effect.Dry letter etc., which reports pepper volatile oil, can not only inhibit Gram-negative bacteria, can also inhibit to remove from office
Lan Shi positive bacteria, while also having inhibitory activity to mould and fungi, it is especially best to the fungistatic effect of mould and aspergillus niger.Chinese prickly ash
Volatile oil is to bacterium minimal inhibitory concentration > 2%;Minimal inhibitory concentration to brewer's yeast is 2%;To Saccharomyces cerevisiae and mould
Minimal inhibitory concentration >=2%.Tang Yufang etc. studies have shown that pepper volatile oil to the minimum bactericidal concentrations of 6 kinds of bacteriums and 5 kinds of fungies
(MBC or MFC): bacillus subtilis and staphylococcus aureus are 25.00ml/L, Bacillus cercus and proteus vulgaris
For 12.50ml/L, salmonella 6.25ml/L, aspergillus niger, mould, aspergillus flavus, yeast 12.50ml/L, head mold is
25.00ml/L.Researches show that Japan pepper essential oils to bacterium (staphylococcus aureus, bacillus subtilis, wax for newest bacteriostatic activity
Sample bacillus, bacillus laterosporus and the minimum of Escherichia coli inhibit mass concentration and highest sterilization mass concentration to be respectively interposed in
1.25~5.00,2.50~20.00mg/mL has obvious inhibition destruction to for examination bacterial growth and morphosis.
Pepper volatile oil also has bactericidal activity to plant pathogenic fungi.It is to 15 kinds of test plant disease fungus mycelia
Growth has obvious inhibiting effect (IC50 is below 1.0mg/mL), wherein Rhizoctonia solani Kuhn and rhizoctonia cerealis to it most
For sensitivity.Further research announcement pepper volatile oil, which can lead to Rhizoctonia solani Kuhn mycelia branch, to be increased, mycelia branch spacing
Obviously shorten.1.5 μ L/mL its to polygalacturonase, pectin methyl galacturonic acid enzyme and the pectin first in mycelia
The trans- maximum inhibition for eliminating 3 kinds of cell wall degrading enzymes such as enzyme of base respectively reaches 95.12%, 85.94% and 100.00%.With
MAHD, which extracts pepper volatile oil, also has inhibitory effect to the rotten bacterium of cause in cucumber and Kidney bean.
Pepper volatile oil also has good contact efficacy to human body itch mite, and Chinese medicine treatment vermiform mite is more with respect to Western medicine
Have the small advantage of green, safety, toxic side effect, has the agent of pepper volatile oil creams currently on the market.
It is relatively small to the polarity in the mainly volatile oil of fungi its inhibiting effect in pepper volatile oil, to heat, organic
The Monoterpenes of solvent-susceptible, and the polarity mainly in volatile oil that inhibiting effect is risen to bacterium it is relatively large, to heat, have
Solvent has the macromolecular substances of certain tolerance.
Ethyl alcohol adds carrier mainly as pepper volatile oil.Formulation vehicle of the deionized water as hand cleanser effective component.
The parts by weight of each component are: water: 80~100 parts, lauryl sodium sulfate: and 1~5 part, alkyl glycosides citric acid
Ester salt: 10~20 parts, 0.1~5 part of pepper extract, 1~5 part of ethyl alcohol.
The preparation method of Chinese prickly ash hand cleanser of the invention, weighs each component of above-mentioned parts by weight, by the extra half of weighing
Water pour into and form sodium dodecyl sulfate solution in lauryl sodium sulfate, sodium dodecyl sulfate solution is heated to 35~
It is stirred after 60 DEG C 10~20 minutes, alkyl glycosides citrate salt is then added in sodium dodecyl sulfate solution and continues to stir
Mixed liquor is formed, after adjusting PH to 5~7, pepper extract, ethyl alcohol and remaining water, stirring to solution are added in mixed liquor
It is uniformly dispersed.
Pepper extract is pepper volatile oil, is made using steam distillation.Steam distillation are as follows: be placed in Chinese prickly ash
It is distilled in extractor, distillation time is 1~3 hour.In the mentioned volatile oil of steam extraction method, big polarity, high boiling ester
Constituents are more, and non-polar hydrocarbon constituents are less.Steam extraction method is the most universal because of its cheap easy application.
The advantages of Chinese prickly ash hand cleanser of the invention, is: belonging to disinfection hand cleanser, can effectively kill while deep-pollution-removing
Germ, contains handguard ingredient simultaneously, easy cleaning and to be able to maintain hand skin soft;And cost is relatively low, technical process is simple, production
Non-pollutant discharge in the process, environmentally friendly, product foaming abundancy is able to satisfy human lives' needs.
Embodiment one:
1 part and 45 parts of water of lauryl sodium sulfate is stirred 20 minutes at 35 DEG C, alkyl glycosides citrate salt is added
15 parts are continued to stir, and after adjusting PH is 5~7, are added 1.3 parts of pepper extract, 2.7 parts of ethyl alcohol, 35 parts of water.
Embodiment two:
2 parts and 50 parts of water of lauryl sodium sulfate are stirred 10 minutes at 60 DEG C, alkyl glycosides citrate salt is added
15 parts are continued to stir, and after adjusting PH is 5~7, are added 1.5 parts of pepper extract, 1.5 parts of ethyl alcohol, 30 parts of water.
Three-embodiment of embodiment seven is as shown in subscript:
Table one: three-embodiment of embodiment seven of Chinese prickly ash hand cleanser
Below it is the bacteriostatic test of hand cleanser:
Experimental material:
Hand cleanser sample: the foam type hand cleanser prepared by case study on implementation,
Strain: staphylococcus aureus, Escherichia coli, Candida albicans (mark the general limited public affairs of medical sci-tech purchased from Shaanxi
Department),
Culture medium: nutrient agar (bacterium) is improved Martin's culture medium (fungi).
Experimental method foundation:
GB 19877.1-2005 " extraordinary hand cleanser ",
GB 15979-2002 " Disposable Sanitary Accessory sanitary standard ",
QB/T 2738-2012 " evaluation method of daily chemical products antibacterial bacteriostatic effect ",
Experimental method:
Inhibition zone measurement:
The measurement of sample bacteriostasis property is carried out using filter paper enzyme.It is 5.5mm's that filter paper, which is fabricated to diameter, with punch
The roundlet scraps of paper are affixed on the culture medium of even spread bacteria suspension by the roundlet scraps of paper, and separately sampled 50 μ l of product drips to every roundlet
On the scraps of paper, use sterile water as control, in incubator.30 DEG C of bacterium cultures for 24 hours, observe result after 27 DEG C of culture 72h of fungi.
Visual observation simultaneously records.Antibacterial circle diameter is measured, is repeated 3 times.
Determination of tube method fungistatic effect:
Sample is mixed well in test tube with culture medium, does stealthy control with sterile water, final volume 5ml makes respectively
At inclined-plane.Take tested bacterium solution streak inoculation on inclined-plane.30 DEG C of bacterium cultures for 24 hours, observe result after 27 DEG C of culture 72h of fungi.
Visual observation simultaneously records.
Antibacterial circle diameter unit of the 2 two kinds of cases of table to strain: mm
Strain | Case one | Case two | Control |
Escherichia coli | 13.3 | 13.6 | 0 |
Staphylococcus aureus | 12.1 | 12.9 | 0 |
Candida albicans | 8.1 | 9.2 | 0 |
Inhibiting effect of the 3 two kinds of cases of table to strain
Strain | Case one | Case two | Control |
Escherichia coli | — | — | + |
Staphylococcus aureus | — | — | + |
Candida albicans | — | — | + |
In table: "+" indicates thalli growth, and "-" indicates no thalli growth.
Although embodiment of the present invention is described in conjunction with attached drawing above, the invention is not limited to above-mentioned
Specific embodiments and applications field, above-mentioned specific embodiment is only schematical, directiveness, rather than is limited
Property.Those skilled in the art are under the enlightenment of specification, in the range for not departing from the claims in the present invention and being protected
In the case where, a variety of forms can also be made, these belong to the column of protection of the invention.
Claims (7)
1. a kind of Chinese prickly ash hand cleanser, it is characterised in that: the component of the Chinese prickly ash hand cleanser is water, lauryl sodium sulfate, alkyl
Glucosides citrate salt, pepper extract, ethyl alcohol.
2. a kind of Chinese prickly ash hand cleanser as described in claim 1, it is characterised in that: the parts by weight of each component are:
Water: 80~100 parts,
Lauryl sodium sulfate: 1~5 part,
Alkyl glycosides citrate salt: 10~20 parts,
0.1~5 part of pepper extract,
1~5 part of ethyl alcohol.
3. a kind of Chinese prickly ash hand cleanser as claimed in claim 1 or 2, it is characterised in that: the pepper extract is Chinese prickly ash volatilization
Oil.
4. a kind of Chinese prickly ash hand cleanser as claimed in claim 1 or 2, it is characterised in that: the water is deionized water.
5. a kind of preparation method of Chinese prickly ash hand cleanser, it is characterised in that: each component for weighing above-mentioned parts by weight, by the extra of weighing
The water of half, which pours into, forms sodium dodecyl sulfate solution in lauryl sodium sulfate, sodium dodecyl sulfate solution is heated to
It is stirred after 35~60 DEG C 10~20 minutes, alkyl glycosides citrate salt is then added in sodium dodecyl sulfate solution and continues
Stirring forms mixed liquor, after adjusting PH to 5~7, pepper extract, ethyl alcohol and remaining water is added in mixed liquor, stirring is extremely
Solution is uniformly dispersed.
6. a kind of preparation method of Chinese prickly ash hand cleanser as claimed in claim 6, it is characterised in that: the pepper extract is flower
Green pepper volatile oil is made using steam distillation.
7. a kind of preparation method of Chinese prickly ash hand cleanser as claimed in claim 7, it is characterised in that: the steam distillation
Are as follows: Chinese prickly ash is placed in extractor and is distilled, distillation time is 1~3 hour.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110917315A (en) * | 2019-12-30 | 2020-03-27 | 广州元汉药业有限公司 | Formula and preparation method of antibacterial liquid |
CN110946793A (en) * | 2019-12-13 | 2020-04-03 | 汉源县昊业花椒产业研究院 | Antibacterial liquid detergent and preparation method thereof |
CN111713489A (en) * | 2020-07-08 | 2020-09-29 | 郑州师范学院 | Cut flower preservative and application thereof |
CN114288244A (en) * | 2021-12-09 | 2022-04-08 | 扬州大学 | Zanthoxylum oil nano-emulsion and preparation method and application thereof |
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CN102631295A (en) * | 2012-03-30 | 2012-08-15 | 中国日用化学工业研究院 | Multifunctional foam liquid soap containing glucoside and derivatives of glucoside, and preparation method thereof |
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CN1568930A (en) * | 2003-07-12 | 2005-01-26 | 郦安江 | Method for applying active constitutent of Bunge prickly ash to daily used chemical products |
CN102631295A (en) * | 2012-03-30 | 2012-08-15 | 中国日用化学工业研究院 | Multifunctional foam liquid soap containing glucoside and derivatives of glucoside, and preparation method thereof |
CN104031773A (en) * | 2014-06-04 | 2014-09-10 | 韩城市司马迁旅游文化发展有限公司 | Method for preparing pepper volatile oil fragrant skin care soap |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110946793A (en) * | 2019-12-13 | 2020-04-03 | 汉源县昊业花椒产业研究院 | Antibacterial liquid detergent and preparation method thereof |
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CN111713489A (en) * | 2020-07-08 | 2020-09-29 | 郑州师范学院 | Cut flower preservative and application thereof |
CN114288244A (en) * | 2021-12-09 | 2022-04-08 | 扬州大学 | Zanthoxylum oil nano-emulsion and preparation method and application thereof |
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Application publication date: 20181207 |