CN108922876A - A kind of billon bonding wire and its manufacturing method - Google Patents

A kind of billon bonding wire and its manufacturing method Download PDF

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Publication number
CN108922876A
CN108922876A CN201810678000.5A CN201810678000A CN108922876A CN 108922876 A CN108922876 A CN 108922876A CN 201810678000 A CN201810678000 A CN 201810678000A CN 108922876 A CN108922876 A CN 108922876A
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China
Prior art keywords
annealing
bonding wire
billon
wire
billon bonding
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CN201810678000.5A
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Chinese (zh)
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CN108922876B (en
Inventor
周振基
周博轩
于锋波
彭政展
麦宏全
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Shantou Junma Kaisa Coltd
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Shantou Junma Kaisa Coltd
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    • HELECTRICITY
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    • H01L24/45Structure, shape, material or disposition of the wire connectors prior to the connecting process of an individual wire connector
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21CMANUFACTURE OF METAL SHEETS, WIRE, RODS, TUBES OR PROFILES, OTHERWISE THAN BY ROLLING; AUXILIARY OPERATIONS USED IN CONNECTION WITH METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL
    • B21C37/00Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape
    • B21C37/04Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of bars or wire
    • B21C37/047Manufacture of metal sheets, bars, wire, tubes or like semi-manufactured products, not otherwise provided for; Manufacture of tubes of special shape of bars or wire of fine wires
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    • C22CALLOYS
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    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/02Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working in inert or controlled atmosphere or vacuum
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    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
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  • Engineering & Computer Science (AREA)
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  • Wire Bonding (AREA)

Abstract

The present invention provides a kind of billon bonding wire, it is characterised in that contains Pd 0.5-2% by weight, Ag 15-30%, Cu 0.5-3%, Pt 0.1-2%, trace additives 2-200 ppm, surplus is gold;The trace additives are one of Ca, In, Co, Be, Ga, Mg, Ce and Ni or in which two or more combinations.The present invention provides a kind of manufacturing method of also above-mentioned billon bonding wire.Billon bonding wire of the invention has excellent high reliability and sulfuration resistant performance, and tensile strength is high, and solder joint zygosity is good, and can reduce cost.

Description

A kind of billon bonding wire and its manufacturing method
Technical field
The present invention relates to the bonding wires of IC, LED encapsulation, and in particular to a kind of billon bonding wire and its manufacturing method.
Background technique
Bonding wire(Bonding wire, also known as bonding line)It is connection chip and outer enclosure substrate(substrate)With/ Or multilayer circuit board(PCB)Main connection type.The development trend of bonding wire, from the line of production, mainly line footpath is subtle Change, the high workshop service life(floor life)And high spool length;Chemically on ingredient, mainly there is copper wire(Including bare copper wire, plating Palladium copper wire dodges gold plating palladium copper wire)Significantly replace gold thread in semiconductor field, and silver wire and silver alloy wire are in LED and part IC package applies upper substitution gold thread.Another important directions is the development of alloy gold wire, to further reduce the cost and protect Hold or improve the performance requirements of bonding process.
Due to the demand for development of miniaturization of electronic products and thin thinning, (Wafer is thinned by chip thickness in semicon industry Thinning), encapsulation uses chip stack (Die stacking), flip-chip (flip chip), wafer-level packaging(wafer level packaging), the methods of 2.5D and 3D encapsulation cope with, however traditional bonding packaging(wire bonding)Still It is so mainstream packing forms.
Traditional gold bonding silk made of proof gold material has excellent chemical stability and electrical and thermal conductivity performance, Thus it is widely used as IC lead.But with rising steadily for international price of gold, the also rising all the way of the price of gold bonding silk is led It causes the cost of end product excessively high, is unfavorable for enterprise and improves competitiveness.In addition to this, the tensile strength of gold bonding silk is lower(Example Such as 20 microns of diameter of gold bonding silk, after welding, maximum pulling strength is less than 5 gram forces), elongation percentage is not easily controlled.With Upper two aspects factor, which becomes, hinders gold bonding silk using the bottleneck with development.
To reduce cost, various bonding wires are continued to bring out out, such as Silver alloy wire, golden alloy wire and plating electrum bonding Silk etc., price is relatively low, is also able to satisfy the different demands of different clients;But the engagement for high-end LED, to product Property and reliability it is more demanding, the oxidation of conventional silver alloy and plating gold-silver alloy wire because of silver, it may appear that bonding oxidation, silver from The defects of sub- current potential migrates, solder joint eutectic is bad, is also not achieved the requirement of client in terms of reliability.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of billon bonding wire and this billon bonding wires Manufacturing method, this billon bonding wire have excellent high reliability and sulfuration resistant performance, and tensile strength is high, solder joint engagement Property is good, and can reduce cost.The technical solutions adopted are as follows:
A kind of billon bonding wire, it is characterised in that contain Pd 0.5-2%, Ag 15-30%, Cu 0.5-3%, Pt by weight 0.1-2%, trace additives 2-200 ppm, surplus are gold;The trace additives are Ca, In, Co, Be, Ga, Mg, Ce With one of Ni or in which two or more combinations.
The present invention promotes the tensile strength of wire rod, and can improve asking for billon solder joint associativity by the design of alloy Topic, also promotes the sulfuration resistant ability of wire rod, closes to obtain the gold that solder joint zygosity is good, sulfuration resistant ability is strong, tensile strength is high Gold bonding silk.For proof gold bonding wire, billon bonding wire of the invention for IC, LED encapsulation in, can reduce at Sheet and the problem for improving gold line tensile strength deficiency, and other performances can reach the performance requirement of proof gold bonding wire.
In billon bonding wire of the invention, except for gold, there are also the silver containing 15-30%, silver and gold can sufficiently be consolidated It is molten, play the role of solution strengthening, improve the tensile strength of wire rod, but since silver itself is easy vulcanization, will lead to wire rod and making All Shortcomings, therefore the copper of addition content 0.5-3% on this basis in terms of industry aspect and reliability(Cu), can be effectively Improve the sulfuration resistant performance of wire rod, and improves reliability of the encapsulating products in thermal shock test;The platinum of 0.1-2% is added(Pt) Etc. the recrystallization temperature that can improve billon wire rod, wire rod fatigue durability in a high temperauture environment is promoted, it is disconnected that neck is effectively reduced The probability of line;The palladium of content 0.5-2% is added(Pd), the anti-oxidant and sulfuration resistant performance of wire rod can be effectively improved, and improve envelope Fill reliability of the product in thermal shock test.Mechanical performance of suitable trace additives to improve wire rod, wherein Ca, In, Ga, Mg, Ce, Ni can effectively promote the bonding wire workability of billon, can enhance the adhesion property of wire rod and chip and substrate, It is promoted and trusts performance;Co, Be etc. can improve the recrystallization temperature of billon wire rod, promote wire rod endurance in a high temperauture environment Property, the probability of neck broken string is effectively reduced.
In a kind of preferred embodiment, above-mentioned trace additives contain the Mg's and 2-50ppm of Ca, 2-50ppm of 10-100ppm Ce.In another preferred embodiment, above-mentioned trace additives contain the In's and 2-50ppm of Ca, 2-50ppm of 10-80ppm Be.In another preferred embodiment, above-mentioned trace additives contain the Ca of the Ce and 10-50ppm of 2-100ppm.It is another preferred In scheme, above-mentioned trace additives contain the Co of the Ca and 2-20ppm of Ni, 10-100ppm of 2-80ppm.It is another preferred In scheme, above-mentioned trace additives contain the Ca of the Be and 2-80ppm of Ga, 2-60ppm of 2-50ppm.Using above various The combination of trace additives can effectively promote the recrystallization temperature of wire rod, improve the institutional framework of wire rod, promote wire rod in height Fatigue durability under warm environment, is effectively reduced the probability of neck broken string, and can enhance the adhesiveness of wire rod and chip and substrate Can, it is promoted and trusts performance.
The present invention also provides a kind of manufacturing methods of above-mentioned billon bonding wire, it is characterised in that includes the following steps:
(1)Founding:Pd, Ag, Cu, Pt and trace additives are added in golden raw material in proportion, by vacuum melting and determined To casting process is continuously drawn, the wire rod that diameter is 6-8 millimeters is obtained;
(2)Wire drawing:To step(1)Obtained wire rod carries out wire drawing, and acquisition diameter is 0.08-0.5mm(Millimeter)Bonding wire half Finished product;
(3)To step(2)It obtains bonding wire semi-finished product and continues wire drawing, acquisition diameter is 15-50 um(Micron)Billon Bonding wire;
Para-linkage silk semi-finished product carry out intermediate annealing several times in drawing process, and N is used in annealing process2As annealing gas Atmosphere, annealing furnace effective length are 600-2000mm, and annealing temperature is 500-800 DEG C, annealing rate 30-100m/min;
(4)Finally anneal:Step(3)After the completion of wire drawing, is finally annealed to billon bonding wire, used in annealing process N2Come as annealing atmosphere, annealing furnace effective length is 600-1000mm, and annealing temperature is 300-800 DEG C, annealing rate 60- 120m/min;
(5)It is cooling:After finally annealing, billon bonding wire is cooled to 20-30 DEG C, obtains required billon bonding Silk.
To step(5)Obtained billon bonding wire is wound, and can be coiled into the finished product of 500 meters/volume or 1000 meters/volume.
Step(3)Intermediate annealing is carried out by para-linkage silk semi-finished product, processing hardening can be eliminated, make bonding wire semi-finished product With certain elongation percentage.
Billon bonding wire of the invention compared with prior art, has the advantages that:
(1)The billon design combined by special elements, the billon bonding wire of formation have excellent high reliability and Sulfuration resistant performance, tensile strength is high, and solder joint zygosity is good, high reliablity;
(2)The billon bonding wire that the present invention obtains has the HAZ of 45-55 um range, significantly reduces the camber of routing;
(3)It is moderate to obtain number after FAB burns ball for the billon bonding wire that the present invention obtains(The long axialite number in terms of FAB section Between 6-10)Symmetrical column crystal, it is ensured that the out of roundness of shape-changeable ball;
(4)Cost is relatively low.
Specific embodiment
Embodiment 1
The billon bonding wire of the present embodiment contains Pd 1.0%, Ag 30%, Cu 0.5%, Pt 1%, Ce 80ppm by weight, Ca 20ppm, surplus are gold.
In the present embodiment, the manufacturing method of billon bonding wire includes the following steps:
(1)Founding:Pd, Ag, Cu, Pt, Ce and Ca are added in golden raw material in proportion, continuously drawn by vacuum melting and orientation Casting process obtains the wire rod that diameter is 8 millimeters;
(2)Wire drawing:To step(1)Obtained wire rod carries out wire drawing, obtains the bonding wire semi-finished product that diameter is 0.5mm;
(3)To step(2)It obtains bonding wire semi-finished product and continues wire drawing, acquisition diameter is 15-50 um(Such as 20 um)Gold Alloy bonding silk;
Para-linkage silk semi-finished product carry out intermediate annealing several times in drawing process, and N is used in annealing process2As annealing gas Atmosphere, annealing furnace effective length are 1000mm, and annealing temperature is 600 DEG C, annealing rate 50m/min;
(4)Finally anneal:Step(3)After the completion of wire drawing, is finally annealed to billon bonding wire, used in annealing process N2Come as annealing atmosphere, annealing furnace effective length is 800mm, and annealing temperature is 500 DEG C, annealing rate 80m/min;
(5)It is cooling:After finally annealing, billon bonding wire is cooled to 25 DEG C, obtains required billon bonding wire.
To step(5)Obtained billon bonding wire is wound, and can be coiled into the finished product of 500 meters/volume or 1000 meters/volume.
Embodiment 2
The billon bonding wire of the present embodiment contains Pd 1.5%, Ag 20%, Cu 0.6%, Pt 2%, Ca 80ppm by weight, Surplus is gold.
In the present embodiment, the manufacturing method of billon bonding wire includes the following steps:
(1)Founding:Pd, Ag, Cu, Pt and Ca are added in golden raw material in proportion, continuously draw casting by vacuum melting and orientation Technique obtains the wire rod that diameter is 8 millimeters;
(2)Wire drawing:To step(1)Obtained wire rod carries out wire drawing, obtains the bonding wire semi-finished product that diameter is 0.2mm;
(3)To step(2)It obtains bonding wire semi-finished product and continues wire drawing, acquisition diameter is 15-50 um(Such as 20 um)Gold Alloy bonding silk;
Para-linkage silk semi-finished product carry out intermediate annealing several times in drawing process, and N is used in annealing process2As annealing gas Atmosphere, annealing furnace effective length are 2000mm, and annealing temperature is 500 DEG C, annealing rate 100m/min;
(4)Finally anneal:Step(3)After the completion of wire drawing, is finally annealed to billon bonding wire, used in annealing process N2Come as annealing atmosphere, annealing furnace effective length is 600mm, and annealing temperature is 800 DEG C, annealing rate 60m/min;
(5)It is cooling:After finally annealing, billon bonding wire is cooled to 20 DEG C, obtains required billon bonding wire.
To step(5)Obtained billon bonding wire is wound, and can be coiled into the finished product of 500 meters/volume or 1000 meters/volume.
Embodiment 3
The billon bonding wire of the present embodiment contains Pd 2% by weight, Ag 15%, Cu 1%, Pt 0.2%, Ni 100ppm, remaining Amount is gold.
In the present embodiment, the manufacturing method of billon bonding wire includes the following steps:
(1)Founding:Pd, Ag, Cu, Pt and Ni are added in golden raw material in proportion, continuously draw casting by vacuum melting and orientation Technique obtains the wire rod that diameter is 6 millimeters;
(2)Wire drawing:To step(1)Obtained wire rod carries out wire drawing, obtains the bonding wire semi-finished product that diameter is 0.08mm;
(3)To step(2)It obtains bonding wire semi-finished product and continues wire drawing, acquisition diameter is 15-50 um(Such as 20 um)Gold Alloy bonding silk;
Para-linkage silk semi-finished product carry out intermediate annealing several times in drawing process, and N is used in annealing process2As annealing gas Atmosphere, annealing furnace effective length are 600mm, and annealing temperature is 800 DEG C, annealing rate 30m/min;
(4)Finally anneal:Step(3)After the completion of wire drawing, is finally annealed to billon bonding wire, used in annealing process N2Come as annealing atmosphere, annealing furnace effective length is 1000mm, and annealing temperature is 300 DEG C, annealing rate 80m/min;
(5)It is cooling:After finally annealing, billon bonding wire is cooled to 30 DEG C, obtains required billon bonding wire.
To step(5)Obtained billon bonding wire is wound, and can be coiled into the finished product of 500 meters/volume or 1000 meters/volume.
Embodiment 4
The billon bonding wire of the present embodiment contains Pd 0.5%, Ag 25%, Cu 3%, Pt 0.1%, Ca by weight 100ppm, Mg 50ppm, Ce 50ppm, surplus are gold.
In the present embodiment, the manufacturing method of billon bonding wire includes the following steps:
(1)Founding:Pd, Ag, Cu, Pt, Ca, Mg and Ce are added in golden raw material in proportion, connected by vacuum melting and orientation It is continuous to draw casting process, obtain the wire rod that diameter is 6 millimeters;
(2)Wire drawing:To step(1)Obtained wire rod carries out wire drawing, obtains the bonding wire semi-finished product that diameter is 0.4mm;
(3)To step(2)It obtains bonding wire semi-finished product and continues wire drawing, acquisition diameter is 15-50 um(Such as 20 um)Gold Alloy bonding silk;
Para-linkage silk semi-finished product carry out intermediate annealing several times in drawing process, and N is used in annealing process2As annealing gas Atmosphere, annealing furnace effective length are 1500mm, and annealing temperature is 700 DEG C, annealing rate 50m/min;
(4)Finally anneal:Step(3)After the completion of wire drawing, is finally annealed to billon bonding wire, used in annealing process N2Come as annealing atmosphere, annealing furnace effective length is 900mm, and annealing temperature is 400 DEG C, annealing rate 90m/min;
(5)It is cooling:After finally annealing, billon bonding wire is cooled to 30 DEG C, obtains required billon bonding wire.
To step(5)Obtained billon bonding wire is wound, and can be coiled into the finished product of 500 meters/volume or 1000 meters/volume.
Embodiment 5
The billon bonding wire of the present embodiment contains Pd 0.8%, Ag 18%, Cu 1.5%, Pt 1.2%, Ca by weight 50ppm, In 40ppm, Be 50ppm, surplus are gold.
In the present embodiment, the manufacturing method of billon bonding wire includes the following steps:
(1)Founding:Pd, Ag, Cu, Pt, Ca, In and Be are added in golden raw material in proportion, connected by vacuum melting and orientation It is continuous to draw casting process, obtain the wire rod that diameter is 8 millimeters;
(2)Wire drawing:To step(1)Obtained wire rod carries out wire drawing, obtains the bonding wire semi-finished product that diameter is 0.3mm;
(3)To step(2)It obtains bonding wire semi-finished product and continues wire drawing, acquisition diameter is 15-50 um(Such as 20 um)Gold Alloy bonding silk;
Para-linkage silk semi-finished product carry out intermediate annealing several times in drawing process, and N is used in annealing process2As annealing gas Atmosphere, annealing furnace effective length are 1200mm, and annealing temperature is 600 DEG C, annealing rate 60m/min;
(4)Finally anneal:Step(3)After the completion of wire drawing, is finally annealed to billon bonding wire, used in annealing process N2Come as annealing atmosphere, annealing furnace effective length is 600mm, and annealing temperature is 800 DEG C, annealing rate 100m/min;
(5)It is cooling:After finally annealing, billon bonding wire is cooled to 25 DEG C, obtains required billon bonding wire.
To step(5)Obtained billon bonding wire is wound, and can be coiled into the finished product of 500 meters/volume or 1000 meters/volume.
Embodiment 6
The billon bonding wire of the present embodiment contains Pd 1.5%, Ag 20%, Cu 2.5%, Pt 0.6%, Ni by weight 80ppm, Ca 80ppm, Co 20ppm, surplus are gold.
In the present embodiment, the manufacturing method of billon bonding wire includes the following steps:
(1)Founding:Pd, Ag, Cu, Pt, Ni, Ca and Co are added in golden raw material in proportion, connected by vacuum melting and orientation It is continuous to draw casting process, obtain the wire rod that diameter is 6 millimeters;
(2)Wire drawing:To step(1)Obtained wire rod carries out wire drawing, obtains the bonding wire semi-finished product that diameter is 0.4mm;
(3)To step(2)It obtains bonding wire semi-finished product and continues wire drawing, acquisition diameter is 15-50 um(Such as 20 um)Gold Alloy bonding silk;
Para-linkage silk semi-finished product carry out intermediate annealing several times in drawing process, and N is used in annealing process2As annealing gas Atmosphere, annealing furnace effective length are 1000mm, and annealing temperature is 600 DEG C, annealing rate 100m/min;
(4)Finally anneal:Step(3)After the completion of wire drawing, is finally annealed to billon bonding wire, used in annealing process N2Come as annealing atmosphere, annealing furnace effective length is 1000mm, and annealing temperature is 600 DEG C, annealing rate 100m/min;
(5)It is cooling:After finally annealing, billon bonding wire is cooled to 30 DEG C, obtains required billon bonding wire.
To step(5)Obtained billon bonding wire is wound, and can be coiled into the finished product of 500 meters/volume or 1000 meters/volume.
The above embodiments 1-6 billon bonding wire obtained is tested for the property(Comparative example is using the routine bought in the market Gold content is the alloy gold wire of 80%wt).
1, the test method of HAZ length
Embodiment 1-6 and the wire rod of comparative example are subjected to the cutting of FIB (Focused Ion beam) focused ion beam, utilize SEM (scanning electron microscopy) scanning electron microscope is observed, by comparing the crystal size of different wire positions Variation, the length information of available HAZ.
2, ageing testing method
Wire rod obtained by embodiment 1-6 and comparative example reliability difference mainly in thermal shock part.Specific degradation item Part such as table 1.Test packing forms be LED encapsulation in SMD2835, BSOB routing, packaging silicon rubber use DOW CORNING OE6650, For packaged sample after each thermal shock for completing 50 circulations, seeing whether can also be electric bright, records the number for the dead lamp that fails.
Table 1
3, vulcanize test method
The good sample lamp bead of encapsulating is placed in closed container(Distil certain sulphur concentration), 85 DEG C of constant temperature;One timing of vulcanization Between after take out test light decay.
The performance test results are as shown in table 2.
Table 2
Note:Shape-changeable ball out of roundness number of non-compliances is the summation of the undesirable alternating compression ball of out of roundness and eccentric sphere.
Above-mentioned the performance test results show:
1, wire rod of the HAZ that the billon bonding wire of 1-6 of the embodiment of the present invention obtains well below comparative example.
2, the routing performance of the billon bonding wire of 1-6 of the embodiment of the present invention(Shape-changeable ball out of roundness)It is substantially better than comparison Example.
The excellent routing performance of wire rod of the present invention, which is primarily due to the wire rod, to ensure stable burning ball performance(Including The property placed in the middle of FAB is to prevent the symmetrical and suitable column crystal of number generated in eccentric sphere and FAB).
3, relative to comparative example, reliability is greatly improved the billon bonding wire of 1-6 of the embodiment of the present invention.
After the thermal shock that the billon bonding wire of 1-6 of the embodiment of the present invention is recycled by 550, still without the dead lamp feelings that fail Condition(After the thermal shock that wherein embodiment 4,6 is recycled by 600, still without the dead lamp situation that fails);And comparative example has then gone out Now fail dead lamp(Comparative example can only be subjected to the thermal shock of 400 circulations).This illustrates that the reliability of the technology of the present invention wire rod is higher.
4, vulcanize
The billon bonding wire of 1-6 of the embodiment of the present invention is tested through over cure, and light decay is below 18%;And comparative example light decay exists 25%.This illustrates that the sulfuration resistant ability of the technology of the present invention wire rod is stronger.

Claims (7)

1. a kind of billon bonding wire, it is characterised in that contain Pd 0.5-2%, Ag 15-30%, Cu 0.5-3%, Pt by weight 0.1-2%, trace additives 2-200 ppm, surplus are gold;The trace additives are Ca, In, Co, Be, Ga, Mg, Ce With one of Ni or in which two or more combinations.
2. billon bonding wire according to claim 1, it is characterized in that:The trace additives contain 10-100ppm Ca, 2-50ppm Mg and 2-50ppm Ce.
3. billon bonding wire according to claim 1, it is characterized in that:The trace additives contain 10-80ppm's The Be of the In and 2-50ppm of Ca, 2-50ppm.
4. billon bonding wire according to claim 1, it is characterized in that:The trace additives contain 2-100ppm's The Ca of Ce and 10-50ppm.
5. billon bonding wire according to claim 1, it is characterized in that:The trace additives contain 2-80ppm's The Co of the Ca and 2-20ppm of Ni, 10-100ppm.
6. billon bonding wire according to claim 1, it is characterized in that:The trace additives contain 2-50ppm's The Ca of the Be and 2-80ppm of Ga, 2-60ppm.
7. the manufacturing method of billon bonding wire described in any one of claims 1-6, it is characterised in that include the following steps:
(1)Founding:Pd, Ag, Cu, Pt and trace additives are added in golden raw material in proportion, by vacuum melting and determined To casting process is continuously drawn, the wire rod that diameter is 6-8 millimeters is obtained;
(2)Wire drawing:To step(1)Obtained wire rod carries out wire drawing, obtains the bonding wire semi-finished product that diameter is 0.08-0.5mm;
(3)To step(2)It obtains bonding wire semi-finished product and continues wire drawing, obtain the billon that diameter is 15-50 um and be bonded Silk;
Para-linkage silk semi-finished product carry out intermediate annealing several times in drawing process, and N is used in annealing process2As annealing gas Atmosphere, annealing furnace effective length are 600-2000mm, and annealing temperature is 500-800 DEG C, annealing rate 30-100m/min;
(4)Finally anneal:Step(3)After the completion of wire drawing, is finally annealed to billon bonding wire, used in annealing process N2Come as annealing atmosphere, annealing furnace effective length is 600-1000mm, and annealing temperature is 300-800 DEG C, annealing rate 60- 120m/min;
(5)It is cooling:After finally annealing, billon bonding wire is cooled to 20-30 DEG C, obtains required billon bonding Silk.
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