CN108815083B - Nourishing and moisturizing facial cleanser and preparation method thereof - Google Patents
Nourishing and moisturizing facial cleanser and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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Abstract
The invention discloses a nourishing and moisturizing facial cleanser and a preparation method thereof, and the nourishing and moisturizing facial cleanser comprises the following components in percentage by mass: performing enzymolysis and ultrafiltration on rice washing water: 35% -45%; amino acid surfactant: 15% -25%; polyol: 35% -45%; thickening agent: 1% -3%; triethanolamine: 0.5 to 2 percent; plant essential oil: 0.5 to 5 percent; disodium EDTA: 0.1 to 0.2 percent. The preparation method comprises the following steps: uniformly mixing polyol, a thickening agent and enzymolysis ultrafiltration rice washing water, adding EDTA disodium, uniformly mixing, adding triethanolamine, adjusting the pH value of a formula system to 5.5-6.5, finally adding uniformly premixed plant essential oil and amino acid surfactant, uniformly mixing, standing and defoaming. The nourishing and moisturizing facial cleanser disclosed by the invention has a good degreasing and dirt removing effect, contains rich water-soluble vitamins, micromolecular polypeptides, amino acids and micromolecular polysaccharides which are easy to be absorbed by skin, and can play the effects of moisturizing, increasing the skin elasticity and preventing the skin from being dry, tight and skinned.
Description
Technical Field
The invention relates to nourishing and moisturizing facial cleanser and a preparation method thereof.
Background
A face cleaning cream, also called facial cleanser, is a face washing agent capable of cleaning dirt on the face and removing makeup, and generally comprises oil phase substances, water phase substances, surfactants, moisturizing agents, nutritional agents and the like. At present, the cleaning and oil removing effects of commercially available facial cleansers are good, but most of the facial cleansers are added with fatty acid metal salts, so that the skin is easy to dry, tighten and peel after the facial cleansers are used, and the skin aging is accelerated to a certain extent after the facial cleansers are used for a long time, so that irreversible damage is caused to the skin. The fatty acid metal salt is obtained by saponifying oil and alkaline substances, and has strong alkalinity, excessively strong degreasing force and large irritation. Therefore, it is important to develop a facial cleanser which can mildly clean the skin and protect and nourish the skin.
The rice washing water is water after rice washing, and is acidic, and the pH value is 5.5-6. In the process of washing rice, vitamin B1The loss rate can reach 25 to 50 percent, and the vitamin B2And vitamin B3The loss rate can reach 20-25%, and in addition, protein, fat, sugar and the like can also be lost to different degrees. Therefore, the rice washing water contains rich cereal substances, is just the nutrient components required by the skin, can make the skin smooth and elastic after long-term insisting of washing the face and hands with the rice washing water, and can also lighten melanin.
Disclosure of Invention
The invention aims to provide nourishing and moisturizing facial cleanser and a preparation method thereof.
The technical scheme adopted by the invention is as follows:
the nourishing and moisturizing facial cleanser comprises the following components in percentage by mass:
performing enzymolysis and ultrafiltration on rice washing water: 35% -45%;
amino acid surfactant: 15% -25%;
polyol: 35% -45%;
thickening agent: 1% -3%;
triethanolamine: 0.5 to 2 percent;
plant essential oil: 0.5 to 5 percent;
disodium EDTA: 0.1 to 0.2 percent.
The relative molecular weight of water-soluble vitamins, polypeptides, amino acids and polysaccharides in the rice washing water obtained by enzymolysis and ultrafiltration is less than or equal to 1000 Da.
The amino acid surfactant is at least one of sodium lauroyl oat amino acid, sodium cocoyl malic amino acid, sodium lauroyl glutamate, sodium lauroyl sarcosinate, sodium lauroyl amphoacetate, disodium lauryl sulfosuccinate and potassium cocoyl glycinate.
The polyalcohol is at least one of glycerol, propylene glycol, butanediol, dehydrated xylitol, glycerol polyether-26, hydroxyethyl urea, trehalose, beta-dextran, and 1, 2-hexanediol.
The thickening agent is acrylic acid (ester)/C10～30At least one of an alkanol acrylate crosspolymer, an acrylic acid (ester) copolymer, and an acrylic acid (ester)/vinyl isodecanoate crosspolymer.
The plant essential oil is at least one of rose essential oil and jasmine essential oil.
The preparation method of the nourishing and moisturizing facial cleanser comprises the following steps: uniformly mixing polyol, a thickening agent and enzymolysis ultrafiltration rice washing water, adding EDTA disodium, uniformly mixing, adding triethanolamine, adjusting the pH value of a formula system to 5.5-6.5, finally adding uniformly premixed plant essential oil and amino acid surfactant, uniformly mixing, standing and defoaming.
The invention has the beneficial effects that: the nourishing and moisturizing facial cleanser disclosed by the invention has a good degreasing and dirt removing effect, contains rich water-soluble vitamins, micromolecular polypeptides, amino acids and micromolecular polysaccharides which are easy to be absorbed by skin, and can play the effects of moisturizing, increasing the skin elasticity and preventing the skin from being dry, tight and skinned.
1) The nourishing and moisturizing cleansing milk disclosed by the invention is added with enzymolysis and ultrafiltration rice washing water obtained through enzymolysis and ultrafiltration separation, the enzymolysis can decompose macromolecular proteins in the rice washing water into micromolecular polypeptides and amino acids, so that the stimulation of the macromolecular proteins serving as foreign matters to skin is avoided, the skin can absorb the micromolecular polypeptides and amino acids, the skin is healthier and more elastic, and components with the relative molecular weight of more than 1000Da can be intercepted through ultrafiltration separation. The rice washing water subjected to enzymolysis and ultrafiltration separation treatment contains rich water-soluble vitamins, micromolecular polypeptides, amino acids and micromolecular polysaccharides, and is easier to be absorbed by skin compared with untreated rice washing water, so that the moisture retention of the epidermis can be improved, the elasticity of the skin is increased, and the skin is prevented from being dried and stretched due to over-cleaning;
2) the nourishing and moisturizing facial cleanser disclosed by the invention is not added with essence, pigment and preservative, so that the irritation to eyes and facial skin during facial cleansing is greatly reduced, and environmental pollutants such as chlorine, phosphorus and the like are not contained;
3) the nourishing and moisturizing facial cleanser disclosed by the invention is simple in production process, suitable for large-scale production and wide in market prospect.
Detailed Description
The nourishing and moisturizing facial cleanser comprises the following components in percentage by mass:
performing enzymolysis and ultrafiltration on rice washing water: 35% -45%;
amino acid surfactant: 15% -25%;
polyol: 35% -45%;
thickening agent: 1% -3%;
triethanolamine: 0.5 to 2 percent;
plant essential oil: 0.5 to 5 percent;
disodium EDTA: 0.1 to 0.2 percent.
Preferably, the relative molecular weight of the water-soluble vitamins, polypeptides, amino acids and polysaccharides in the rice washing water obtained by enzymolysis and ultrafiltration is less than or equal to 1000 Da.
Preferably, the enzymatic ultrafiltration rice washing water is prepared by the following method: adding neutral protein complex enzyme into rice washing water, performing enzymolysis, filtering the enzymolysis solution with hollow fiber ultrafiltration membrane, and intercepting components with relative molecular weight more than 1000 Da.
Preferably, the neutral protein complex enzyme also contains cellulase, hemicellulase and amylase, and is purchased from Ningxia Shenshenghuo industry group GmbH.
Preferably, the rice is at least one of yellow rice, millet, rice, black rice, purple rice and glutinous rice.
Preferably, the amino acid surfactant is at least one of sodium lauroyl oat amino acid, sodium cocoyl malic amino acid, sodium lauroyl glutamate, sodium lauroyl sarcosinate, sodium lauroyl amphoacetate, disodium lauryl sulfosuccinate and potassium cocoyl glycinate.
Preferably, the polyhydric alcohol is at least one of glycerol, propylene glycol, butanediol, dehydrated xylitol, glycerol polyether-26, hydroxyethyl urea, trehalose, beta-glucan, and 1, 2-hexanediol.
Preferably, the thickener is acrylic acid (ester)/C10～30At least one of an alkanol acrylate crosspolymer, an acrylic acid (ester) copolymer, and an acrylic acid (ester)/vinyl isodecanoate crosspolymer.
Preferably, the acrylic acid (ester)/C10～30The alkanol acrylate cross-linked polymer was Carbopol Ultrez 20 available from Luobo Runz advanced materials, Inc.
Preferably, the acrylic copolymer is Carbopol Aqua SF-1 available from Luoborun advanced materials, Inc.
Preferably, the acrylic/vinyl isodecanoate crosspolymer is Stabylen 30, available from 3V international group ltd.
Preferably, the plant essential oil is at least one of rose essential oil and jasmine essential oil.
The preparation method of the nourishing and moisturizing facial cleanser comprises the following steps: uniformly mixing polyol, a thickening agent and enzymolysis ultrafiltration rice washing water, adding EDTA disodium, uniformly mixing, adding triethanolamine, adjusting the pH value of a formula system to 5.5-6.5, finally adding uniformly premixed plant essential oil and amino acid surfactant, uniformly mixing, standing and defoaming.
The invention will be further explained and illustrated with reference to specific examples.
Example 1:
the nourishing and moisturizing facial cleanser comprises the following raw materials in percentage by weight:
table 1A composition table of nourishing and moisturizing facial cleanser
Example 2:
the nourishing and moisturizing facial cleanser comprises the following raw materials in percentage by weight:
table 2A composition table of nourishing and moisturizing facial cleanser
Example 3:
the nourishing and moisturizing facial cleanser comprises the following raw materials in percentage by weight:
table 3A composition table of nourishing and moisturizing facial cleanser
| Raw materials | Mass percent (%) |
| Enzymolysis ultrafiltration rice washing water | 40 |
| Sodium cocoyl malate | 15 |
| Glycerol | 25 |
| Butanediol | 13 |
| 1, 2-hexanediol | 2 |
| Acrylic acid (ester) copolymer | 2 |
| Triethanolamine | 1.5 |
| Rose essential oil | 1.3 |
| EDTA disodium salt | 0.2 |
Example 4:
the nourishing and moisturizing facial cleanser comprises the following raw materials in percentage by weight:
table 4A composition table of nourishing and moisturizing facial cleanser
Example 5:
the nourishing and moisturizing facial cleanser comprises the following raw materials in percentage by weight:
table 5A composition table of nourishing and moisturizing facial cleanser
| Raw materials | Mass percent (%) |
| Enzymolysis ultrafiltration rice washing water | 42 |
| Lauroamphoacetate sodium salt | 16 |
| Glycerol | 18 |
| Hydroxyethyl urea | 6 |
| Trehalose | 1.2 |
| Butanediol | 8 |
| 1, 2-hexanediol | 2.5 |
| Acrylic acid (ester) copolymer | 2.5 |
| Triethanolamine | 1.8 |
| Rose essential oil | 1.8 |
| EDTA disodium salt | 0.2 |
Example 6:
the nourishing and moisturizing facial cleanser comprises the following raw materials in percentage by weight:
table 6A composition of nourishing and moisturizing facial cleanser
| Raw materials | Mass percent (%) |
| Enzymolysis ultrafiltration rice washing water | 35 |
| Disodium lauryl sulfosuccinate | 20 |
| Glycerol | 21 |
| Butanediol | 15 |
| Beta-glucan | 1.5 |
| 1, 2-hexanediol | 2.5 |
| Acrylic acid (ester) copolymer | 1.9 |
| Triethanolamine | 1.4 |
| Jasmine essential oil | 1.6 |
| EDTA disodium salt | 0.1 |
Comparative example 1:
the rice washing water facial cleanser comprises the following raw materials in percentage by weight:
TABLE 7 composition table of raw materials of rice washing face cleaning milk
Comparative example 2:
the rice washing water facial cleanser comprises the following raw materials in percentage by weight:
table 8 raw material composition table of rice washing water face cleaning cream
Comparative example 3:
the rice washing water facial cleanser comprises the following raw materials in percentage by weight:
TABLE 9 composition table of raw materials of rice washing face cleaning milk
| Raw materials | Mass percent (%) |
| Rice washing water | 40 |
| Sodium cocoyl malate | 15 |
| Glycerol | 25 |
| Butanediol | 13 |
| 1, 2-hexanediol | 2 |
| Acrylic acid (ester) copolymer | 2 |
| Triethanolamine | 1.5 |
| Rose essential oil | 1.3 |
| EDTA disodium salt | 0.2 |
Test example:
1. skin moisture content comparative test:
test objects: 30 volunteers (male and female ratio 1:1), aged 20-45 years, and healthy. The 30 volunteers were randomly divided into groups A, B and C.
And (3) testing conditions are as follows: 1) an indoor environment; 2) no strong sunlight or direct light; 3) the environmental temperature is 25 +/-2 ℃, and the environmental humidity is 40-60%.
The test method comprises the following steps: selecting commercially available facial cleanser (Jiaozi Tao Rice washing goat milk handmade soap) and the rice washing facial cleanser of comparative example 1 as controls, wherein the nourishing and moisturizing facial cleanser of example 1 is used in group A, the rice washing facial cleanser of comparative example 1 is used in group B, and the commercially available facial cleanser (Jiaozi Tao Rice washing goat milk handmade soap) is used in group C; selecting a rectangular area of 2CM multiplied by 3CM at the same part of the forehead of a volunteer as a test area, after the volunteer sits still and has a rest for 1 hour under the test condition, cleaning the face with clear water, testing by using a skin moisture tester MDD4-Corneometer CM825 half an hour later, and taking the average number of the areas as the skin moisture content before use; the volunteers moistened the face with warm water, followed by cleansing the face with the corresponding face cleanser (1 g in amount), and the skin moisture content was measured after 0.5 hour and 24 hours using a skin moisture tester MDD4-Corneometer CM825, respectively, and the average thereof was taken as the skin moisture content after 0.5 hour of use and the skin moisture content after 24 hours of use.
And (3) testing results:
TABLE 10 comparative skin moisture content test results
As can be seen from table 10: the skin moisture content of the volunteers increased significantly after using the nourishing and moisturizing facial cleanser of example 1 for 24 hours, the skin moisture content increased slightly after using the rice washing facial cleanser of comparative example 1 for 24 hours, and the skin moisture content decreased significantly after using the commercially available facial cleanser for 24 hours, which resulted in dry and peeling skin after long-term use.
2. Skin elasticity comparative test:
test objects: 30 volunteers (male and female ratio 1:1), aged 20-45 years, and healthy. The 30 volunteers were randomly divided into groups A, B and C.
And (3) testing conditions are as follows: 1) an indoor environment; 2) no strong sunlight or direct light; 3) the environmental temperature is 25 +/-2 ℃, and the environmental humidity is 40-60%.
The test method comprises the following steps: selecting commercially available facial cleanser (Jiaozi Tao Rice washing goat milk handmade soap) and the rice washing facial cleanser of comparative example 2 as controls, wherein the nourishing and moisturizing facial cleanser of example 2 is used in group A, the rice washing facial cleanser of comparative example 2 is used in group B, and the commercially available facial cleanser (Jiaozi Tao Rice washing goat milk handmade soap) is used in group C; selecting a rectangular area of 2cm multiplied by 3cm at the same part of the forehead of a volunteer as a test area, measuring the test area by using a revisometer RV600 (elastic fiber tissue test probe) of a skin elasticity tester MPA580 of CK company Germany before using the facial cleanser, and recording the skin elasticity index R of the test area2、R5、R7Values were averaged as initial data for volunteers (constant negative pressure of 450mbar during the test). The volunteers were then asked to use the corresponding facial cleanser (1 gram per dose) once a day, morning and evening, for a month (during which no other skin care product was used). Measuring the test area again to record the skin elasticity index R of the test area2、R5、R7The average of the values was taken as the final data of the volunteers (the negative pressure during the test was constant at 450 mbar).
And (3) testing results:
table 11 skin elasticity comparative test results
Note:
elastic finger for skinNumber R2、R5、R7The closer to 1, the better the elasticity of the skin.
R2＝Ua/Uf；R5＝Ur/Ue；R7＝Ur/Uf；
Uf-maximum amount of skin stretching;
Ue-the amount of stretching of the skin at 0.1 second after a constant negative pressure has been applied to the skin, to locate the amount of stretching of the elastic portion;
Urafter the negative pressure is removed, the skin is quickly restored to its original state, which is also divided into a value of elastic fraction UrNamely, the recovery value and the viscoelastic part value, or the plastic part value, of the skin after the negative pressure is removed for 0.1 second;
Ua-the recovery value of the skin from the removal of the negative pressure to the next successive testing of the skin surface plus the negative pressure.
As can be seen from Table 11: the skin elasticity index of the volunteers was greatly increased after one month using the nourishing and moisturizing facial cleanser of example 2, slightly increased after one month using the rice washing water facial cleanser of comparative example 2, and significantly decreased after one month using the commercially available facial cleanser. Therefore, the nourishing and moisturizing facial cleanser disclosed by the invention has a good effect of improving the skin elasticity.
3. Skin feel evaluation comparative test:
test objects: 45 volunteers (male and female ratio 1:2), aged 20-45 years, and healthy. These 45 volunteers were randomly divided into groups A, B and C.
And (3) testing conditions are as follows: 1) an indoor environment; 2) no strong sunlight or direct light; 3) the environmental temperature is 25 +/-2 ℃, and the environmental humidity is 40-60%.
The test method comprises the following steps: selecting commercially available facial cleanser (Jiaozi Tao Rice washing goat milk handmade soap) and rice washing facial cleanser of comparative example 3 as control, wherein group A uses the nourishing and moisturizing facial cleanser of example 3, group B uses the rice washing facial cleanser of comparative example 3, and group C uses commercially available facial cleanser (Jiaozi Tao Rice washing goat milk handmade soap); volunteers first wet their faces with warm water, then cleanse their faces with the corresponding facial cleanser (1 g), and evaluate their skin feel after resting for 0.5 hours.
And (3) testing results:
table 12 skin feel evaluation comparative test results
As can be seen from table 12: the satisfaction of the skin tightness and irritation after rinsing using the nourishing and moisturizing cleanser of example 3 was significantly higher in the volunteers than the rice-washed water cleanser and the commercial cleanser of comparative example 3.
4. Microbial challenge experiments:
the test method comprises the following steps: european pharmacopoeia EP4(5.1.3 microbial preservative efficacy test).
The microbial species used for the tests were:
bacteria: pseudomonas aeruginosa (Pseudomonas aeruginosa) ATCC 9027; escherichia coli (Escherichia coli) ATCC 8739; staphylococcus aureus (Staphylococcus aureus) ATCC 6538;
and (3) mould: aspergillus niger (Aspergillus niger) ATCC 16404; candida albicans (Candida albicans) ATCC 10231.
The test samples were: the nourishing and moisturizing facial cleanser of examples 1-6.
And (3) testing results:
TABLE 13 microbial challenge test results
Note:
evaluation criteria for microbial challenge experiments: the total number of bacterial colonies is reduced by 3 logs at the 7 th day, no growth occurs at the 28 th day, the total number of mould is reduced by 2 logs at the 14 th day, no growth occurs at the 28 th day, and the preservative effect is judged to be good.
As can be seen from table 13: the nourishing and moisturizing facial cleanser disclosed by the invention has a good preservative effect.
In conclusion: the nourishing and moisturizing facial cleanser disclosed by the invention can improve the moisture retention of the epidermis, increase the skin elasticity and prevent the skin from being dried and stretched due to over-cleaning. Meanwhile, the facial cleanser disclosed by the invention is not added with any preservative harmful to a human body, does not contain toxic substances such as heavy metals and the like, and is safe and non-irritant to the human body.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (6)
1. The nourishing and moisturizing facial cleanser is characterized in that: the composite material comprises the following components in percentage by mass:
performing enzymolysis and ultrafiltration on rice washing water: 35% -45%;
amino acid surfactant: 15% -25%;
polyol: 35% -45%;
thickening agent: 1% -3%;
triethanolamine: 0.5 to 2 percent;
plant essential oil: 0.5 to 5 percent;
disodium EDTA: 0.1 to 0.2 percent;
the relative molecular weight of water-soluble vitamins, polypeptides, amino acids and polysaccharides in the rice washing water obtained by enzymolysis and ultrafiltration is less than or equal to 1000 Da.
2. The nourishing and moisturizing cleanser according to claim 1, characterized in that: the amino acid surfactant is at least one of sodium lauroyl oat amino acid, sodium cocoyl malic amino acid, sodium lauroyl glutamate, sodium lauroyl sarcosinate, sodium lauroyl amphoacetate, disodium lauryl sulfosuccinate and potassium cocoyl glycinate.
3. The nourishing and moisturizing cleanser according to claim 1, characterized in that: the polyalcohol is at least one of glycerol, propylene glycol, butanediol, dehydrated xylitol, glycerol polyether-26, hydroxyethyl urea, trehalose, beta-dextran, and 1, 2-hexanediol.
4. The nourishing and moisturizing cleanser according to claim 1, characterized in that: the thickening agent is acrylic acid (ester)/C10～30At least one of an alkanol acrylate crosspolymer, an acrylic acid (ester) copolymer, and an acrylic acid (ester)/vinyl isodecanoate crosspolymer.
5. The nourishing and moisturizing cleanser according to claim 1, characterized in that: the plant essential oil is at least one of rose essential oil and jasmine essential oil.
6. The method for preparing the nourishing and moisturizing facial cleanser according to any one of claims 1 to 5, comprising the steps of: the method comprises the following steps: uniformly mixing polyol, a thickening agent and enzymolysis ultrafiltration rice washing water, adding EDTA disodium, uniformly mixing, adding triethanolamine, adjusting the pH value of a formula system to 5.5-6.5, finally adding uniformly premixed plant essential oil and amino acid surfactant, uniformly mixing, standing and defoaming.
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| CN112842924B (en) * | 2020-12-22 | 2022-10-18 | 青岛黛优佳生物科技有限公司 | High-viscosity moisturizing amino acid facial cleanser embedded with squalane as well as preparation method and application of facial cleanser |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105496899A (en) * | 2016-01-08 | 2016-04-20 | 佛山市恒南医药科技有限公司 | Washing liquor for skin whitening |
| CN105769744A (en) * | 2016-05-21 | 2016-07-20 | 李明 | Facial cleanser capable of eliminating senile plaques and preparation method of facial cleanser |
| CN106176452A (en) * | 2016-08-27 | 2016-12-07 | 朱耀灯 | A kind of deep water supplement moisturizing facial milk cleanser |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105496899A (en) * | 2016-01-08 | 2016-04-20 | 佛山市恒南医药科技有限公司 | Washing liquor for skin whitening |
| CN105769744A (en) * | 2016-05-21 | 2016-07-20 | 李明 | Facial cleanser capable of eliminating senile plaques and preparation method of facial cleanser |
| CN106176452A (en) * | 2016-08-27 | 2016-12-07 | 朱耀灯 | A kind of deep water supplement moisturizing facial milk cleanser |
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Denomination of invention: A nourishing and moisturizing cleanser and its preparation method Effective date of registration: 20230222 Granted publication date: 20210316 Pledgee: China Co. truction Bank Corp Guangzhou green finance reform and innovation pilot area Huadu Branch Pledgor: GUANGZHOU MEICHI COSMETICS Co.,Ltd. Registration number: Y2023980033167 |