CN108743515A - A kind of preparation method of after-sun Essence - Google Patents

A kind of preparation method of after-sun Essence Download PDF

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Publication number
CN108743515A
CN108743515A CN201810710180.0A CN201810710180A CN108743515A CN 108743515 A CN108743515 A CN 108743515A CN 201810710180 A CN201810710180 A CN 201810710180A CN 108743515 A CN108743515 A CN 108743515A
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added
preparation
tip edge
sun
wrack
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张春松
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Wuhu Yangzhan New Material Technology Service Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/66Enzymes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9711Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/004Aftersun preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74Biological properties of particular ingredients
    • A61K2800/78Enzyme modulators, e.g. Enzyme agonists
    • A61K2800/782Enzyme inhibitors; Enzyme antagonists

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Zoology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

A kind of preparation method of after-sun Essence, belongs to Essence preparing technical field, including:Aloe polysaccharide is prepared, prepared by water phase liquid, emulsification, cool down and etc..Radix Glycyrrhizae and chamomile have clearing heat and detoxicating, antibacterial anti-inflammatory, the effect for pacifying calmness, and various skin, particularly suitable sensibility skin is suitble to can be used for the impaired skin of after-sun.For aloe polysaccharide other than with immunological regulation, sterilization, promoting cell reactivation, also having significantly makes skin contraction, anti-inflammatory, moisturizing and other effects, can be used for the impaired skin of after-sun.The present invention uses nanometer supercritical bee-glue, it is easy to which infiltration and absorption successfully solve the compatibility issues with other ingredients, and nanometer supercritical bee-glue has the function of that strength is anti-oxidant, inhibits tyrosinase activity, whitening spot-removing significant effect.

Description

A kind of preparation method of after-sun Essence
Technical field
The present invention relates to Essence preparing technical field, more particularly to a kind of preparation method of after-sun Essence.
Background technology
Essence is the superfine product in skin care item, and ingredient is exquisite, effect is powerful, significant effect, remains what it possessed It is noble and mysterious, it is suitable for any skin or inclined oily skin, preferably puts in the vial, take at any time.Essence is used for toner Later, before face cream.Commonly there is the problems such as poor permeability, be not easy to absorb, single effect in current Essence.
Invention content
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of preparation method of after-sun Essence, With good penetrability, easily absorb, after-sun, releive skin the effect of.
The present invention uses following technical scheme:
A kind of preparation method of after-sun Essence, includes the following steps:
Step 1:Aloe Barbadensis Miller fresh leaf is cleaned, 7 times of bodies are added at mucus shape in tissue mashing machine's homogenate in homogenate Long-pending distilled water stirring extraction 2h, filtering, filter residue repeat extraction 2 times, and merging filtrate, 40 DEG C are concentrated under reduced pressure into original volume 25%, the ethyl alcohol of 3 times of volume mass a concentration of 95% is added in concentrate, mixes well, is filtered after precipitation to be precipitated, collects Precipitation, by sediment with after hot water dissolving plus activated carbon decolorizing 20min, 40 DEG C be concentrated under reduced pressure into original volume 25%, concentrating The ethyl alcohol of 3 times of volume mass a concentration of 95% is added in liquid, mixes well, centrifuges, go under the rotating speed of 1000r/min Clear liquid collects precipitation to get aloe polysaccharide;
Step 2:It weighs in deionized water to water phase pot, sequentially adds the measured EDETATE SODIUM of accurate scale, hyaluronic acid Sodium, carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3- Butanediol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes;
Step 3:In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, under stirring successively Aloe polysaccharide, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast polypeptides, tip edge is added Bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly;
Step 4:It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, octanoic acid is added Glyceride, and stir;
Step 5:Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, then cold But to room temperature to get Essence.
Preferably, the propolis extract is nanometer supercritical bee-glue.
It is further preferred that the nanometer supercritical bee-glue is the nanometer being process by Phospholipids nano-encapsulated technology Supercritical bee-glue.
Preferably, the licorice is prepared using following methods:5g licorice medicinal materials are crushed, sieving, obtains powder The NaOH aqueous solutions of a concentration of 0.2mol/L are added in body, are 1 by solid-to-liquid ratio:10 ratios mix, the hot dipping extraction 2h at 80 DEG C, It is repeated 2 times, filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifuged under the rotating speed of 4000r/min Separation, goes supernatant to obtain sediment, as licorice.
Preferably, the camomile extract is prepared using following methods:5g chamomiles are crushed, sieving, obtains powder The NaOH aqueous solutions of a concentration of 0.2mol/L are added in body, are 1 by solid-to-liquid ratio:10 ratios mix, the hot dipping extraction 2h at 80 DEG C, It is repeated 2 times, filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifuged under the rotating speed of 4000r/min Separation, goes supernatant to obtain sediment, as camomile extract.
Preferably, the tip edge bladder-wrack extract is prepared using following methods:Tip edge bladder-wrack is washed, is put It sets and is air-dried at aeration-drying, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, moderate heat dries 4min, after drying Tip edge bladder-wrack be put into pulverizer and crush, the tip edge bladder-wrack after crushing is crossed into 60 mesh sieve, tip edge bladder-wrack powder is obtained, weighs Tip edge bladder-wrack powder 10g, deionized water 100g, are added to the container, and extraction 100min are decocted at 90 DEG C, by the substance in container It all takes out, is cooled to room temperature, filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, in collection Clear liquid obtains tip edge bladder-wrack extract after filtering.
It is further preferred that described is filtered into three layers of filtered through gauze.
It is further preferred that being filtered using the membrane filter in 0.2 μm of aperture after three layers of filtered through gauze.
Preferably, the grinding and sieving was 40 mesh sieve.
The beneficial effects of the present invention are:
1) Radix Glycyrrhizae and chamomile have clearing heat and detoxicating, and antibacterial anti-inflammatory pacifies calm effect, are suitble to various skin, especially It is suitble to sensibility skin, can be used for the impaired skin of after-sun.
2) aloe polysaccharide it in addition to immunological regulation, sterilization, promote cell reactivation other than, also have significantly make skin Skin convergence, anti-inflammatory, moisturizing and other effects can be used for the impaired skin of after-sun.
3) present invention uses nanometer supercritical bee-glue, it is easy to which infiltration and absorption successfully solve and other ingredients Compatibility issues, nanometer supercritical bee-glue have the function of that strength is anti-oxidant, inhibit tyrosinase activity, and whitening spot-removing effect is aobvious It writes.
4) tip edge bladder-wrack can provide the required natural nutrient needed for skin rapid regeneration and cell normal growth, Replacement Battalion Foster loss promotes skin metabolism, increases the ATP synthesis of skin energy element;It protects skin cell mitochondria and maintains line grain Body function;Promote skin revitalization, skin is helped to reply health and vigor.
Specific implementation mode
With reference to embodiments, the technical solution in the present invention is clearly and completely described.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.
A kind of after-sun Essence, includes the raw material of following parts by weight:2-4 parts of aloe polysaccharides, 2-4 parts of propolis extractions Object, 0.5-1 part protease, 0.5-1 parts of aminopeptidases, 1-2 parts of camomile extracts, 1-2 parts of licorices, 1-3 parts of yeast Polypeptide, 2-4 parts of tip edge bladder-wrack extracts, 1-3 parts of oligopeptides -20,0.5-1 parts of carbomers, 0.6-2 parts of aminomethyl propanols, 3-6 parts Propylene glycol, 3-6 part 1,3 butylene glycol, 0.5-1 parts of Cremophor RH40s, 0.5-1 parts of blumea oils, 0.5-1 parts of octanoic acids are sweet Grease, 0.1-0.2 part methyl hydroxybenzoate, 0.1-0.2 parts of allantoins, 0.02-0.1 parts of EDETATE SODIUMs, 0.03-0.1 parts of hyaluronic acids Sodium, 70-100 part deionized water.
A kind of preparation method of after-sun Essence, includes the following steps:
Step 1:Aloe Barbadensis Miller fresh leaf is cleaned, 7 times of bodies are added at mucus shape in tissue mashing machine's homogenate in homogenate Long-pending distilled water stirring extraction 2h, filtering, filter residue repeat extraction 2 times, and merging filtrate, 40 DEG C are concentrated under reduced pressure into original volume 25%, the ethyl alcohol of 3 times of volume mass a concentration of 95% is added in concentrate, mixes well, is filtered after precipitation to be precipitated, collects Precipitation, by sediment with after hot water dissolving plus activated carbon decolorizing 20min, 40 DEG C be concentrated under reduced pressure into original volume 25%, concentrating The ethyl alcohol of 3 times of volume mass a concentration of 95% is added in liquid, mixes well, centrifuges, go under the rotating speed of 1000r/min Clear liquid collects precipitation to get aloe polysaccharide;
Step 2:It weighs in deionized water to water phase pot, sequentially adds the measured EDETATE SODIUM of accurate scale, hyaluronic acid Sodium, carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3- Butanediol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes;
Step 3:In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, under stirring successively Aloe polysaccharide, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast polypeptides, tip edge is added Bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly;
Step 4:It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, octanoic acid is added Glyceride, and stir;
Step 5:Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, then cold But to room temperature to get Essence.
The propolis extract is nanometer supercritical bee-glue.The nanometer supercritical bee-glue is wrapped by Phospholipids nanometer The nanometer supercritical bee-glue that the technology of wrapping up in is process.
The licorice is prepared using following methods:5g licorice medicinal materials are crushed, sieving, obtain powder, is added The NaOH aqueous solutions of a concentration of 0.2mol/L are 1 by solid-to-liquid ratio:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times at 80 DEG C, Filtering, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, centrifuges, goes under the rotating speed of 4000r/min Supernatant obtains sediment, as licorice.
The grinding and sieving was 40 mesh sieve.
The camomile extract is prepared using following methods:5g chamomiles are crushed, sieving, obtain powder, is added The NaOH aqueous solutions of a concentration of 0.2mol/L are 1 by solid-to-liquid ratio:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times at 80 DEG C, Filtering, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, centrifuges, goes under the rotating speed of 4000r/min Supernatant obtains sediment, as camomile extract.
The grinding and sieving was 40 mesh sieve.
The tip edge bladder-wrack extract is prepared using following methods:Tip edge bladder-wrack is washed, is placed on logical It air-dries dry place to be air-dried, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, moderate heat dries 4min, by the tip edge after drying Bladder-wrack is put into pulverizer and crushes, and the tip edge bladder-wrack after crushing is crossed 60 mesh sieve, obtains tip edge bladder-wrack powder, weighs tip edge ink Angle algae powder 10g, deionized water 100g, are added to the container, and extraction 100min is decocted at 90 DEG C, the substance in container is all taken Go out, be cooled to room temperature, filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, collects supernatant, mistake After filter tip edge bladder-wrack extract, it is described to be filtered into three layers of filtered through gauze, using 0.2 after described three layers of filtered through gauze The membrane filter filtering in μm aperture.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above, As long as using the improvement of the various unsubstantialities of inventive concept and technical scheme of the present invention progress, or not improved this is sent out Bright design and technical solution directly applies to other occasions, within protection scope of the present invention.The protection of the present invention Range should be determined by the scope of protection defined in the claims.

Claims (9)

1. a kind of preparation method of after-sun Essence, which is characterized in that include the following steps:
Step 1:Aloe Barbadensis Miller fresh leaf is cleaned, 7 times of volumes are added at mucus shape, in homogenate for tissue mashing machine's homogenate Distilled water stirring extraction 2h, filtering, filter residue repeat extraction 2 times, merging filtrate, 40 DEG C be concentrated under reduced pressure into original volume 25%, The ethyl alcohol of 3 times of volume mass a concentration of 95% is added in concentrate, mixes well, is filtered after precipitation to be precipitated, collects precipitation, By sediment with after hot water dissolving plus activated carbon decolorizing 20min, 40 DEG C be concentrated under reduced pressure into original volume 25%, in concentrate plus The ethyl alcohol for entering 3 times of volume mass a concentration of 95%, mixes well, and is centrifuged under the rotating speed of 1000r/min, supernatant is gone to receive Collection precipitation is to get aloe polysaccharide;
Step 2:Weigh in deionized water to water phase pot, sequentially add the measured EDETATE SODIUM of accurate scale, Sodium Hyaluronate, Carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3- fourths Glycol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes;
Step 3:In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, is sequentially added under stirring Aloe polysaccharide, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast polypeptides, tip edge ink angle Algae extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly;
Step 4:It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, sad glycerine is added Ester, and stir;
Step 5:Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, is cooled to Room temperature is to get Essence.
2. a kind of preparation method of after-sun Essence according to claim 1, it is characterised in that:The propolis carries It is nanometer supercritical bee-glue to take object.
3. a kind of preparation method of after-sun Essence according to claim 2, it is characterised in that:The nanometer is super Critical propolis is the nanometer supercritical bee-glue being process by Phospholipids nano-encapsulated technology.
4. a kind of preparation method of after-sun Essence according to claim 1, which is characterized in that the Radix Glycyrrhizae carries Object is taken to be prepared using following methods:5g licorice medicinal materials are crushed, sieving, obtains powder, the NaOH of a concentration of 0.2mol/L is added Aqueous solution is 1 by solid-to-liquid ratio:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times at 80 DEG C, filters, and quality is added in filtrate A concentration of 3% hydrochloric acid tune pH value is centrifuged to 1-2.5 under the rotating speed of 4000r/min, goes supernatant to obtain sediment, as Licorice.
5. a kind of preparation method of after-sun Essence according to claim 1, which is characterized in that the chamomile Extract is prepared using following methods:5g chamomiles are crushed, sieving, obtains powder, the NaOH of a concentration of 0.2mol/L is added Aqueous solution is 1 by solid-to-liquid ratio:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times at 80 DEG C, filters, and quality is added in filtrate A concentration of 3% hydrochloric acid tune pH value is centrifuged to 1-2.5 under the rotating speed of 4000r/min, goes supernatant to obtain sediment, as Camomile extract.
6. a kind of preparation method of after-sun Essence according to claim 1, which is characterized in that the tip edge ink Angle algae extract is prepared using following methods:Tip edge bladder-wrack is washed, is placed at aeration-drying and is air-dried, by wind Tip edge bladder-wrack after dry is placed in micro-wave oven, and moderate heat dries 4min, and the tip edge bladder-wrack after drying is put into powder in pulverizer It is broken, the tip edge bladder-wrack after crushing is crossed into 60 mesh sieve, tip edge bladder-wrack powder is obtained, weighs tip edge bladder-wrack powder 10g, deionized water 100g is added to the container, and extraction 100min is decocted at 90 DEG C, and the substance in container is all taken out, is cooled to room temperature, use is low Warm refrigerated centrifuge filtering, rotating speed 3000r/min, centrifugation time 5min collect supernatant, and tip edge bladder-wrack is obtained after filtering and is carried Take object.
7. a kind of preparation method of after-sun Essence according to claim 6, it is characterised in that:Described is filtered into Three layers of filtered through gauze.
8. a kind of preparation method of after-sun Essence according to claim 7, it is characterised in that:Three layers of yarn It is filtered using the membrane filter in 0.2 μm of aperture after cloth filtering.
9. a kind of preparation method of after-sun Essence according to claim 4 or 5, it is characterised in that:The powder Sieving was 40 mesh sieve after broken.
CN201810710180.0A 2018-07-02 2018-07-02 A kind of preparation method of after-sun Essence Withdrawn CN108743515A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101543468A (en) * 2009-05-05 2009-09-30 天津大学 Liquorice whitening moisturizing lotion and preparation method thereof
CN102920646A (en) * 2012-10-29 2013-02-13 皖南医学院 Nourishing moisture-retention emulsion and preparation method thereof
CN103976907A (en) * 2014-05-29 2014-08-13 暨南大学 Cosmetic comprising composition with slow anti-allergic action as well as preparation method and application thereof
CN107281020A (en) * 2017-06-06 2017-10-24 安徽吉乃尔电器科技有限公司 A kind of preparation method of maca whitening and skin-protecting emulsion

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101543468A (en) * 2009-05-05 2009-09-30 天津大学 Liquorice whitening moisturizing lotion and preparation method thereof
CN102920646A (en) * 2012-10-29 2013-02-13 皖南医学院 Nourishing moisture-retention emulsion and preparation method thereof
CN103976907A (en) * 2014-05-29 2014-08-13 暨南大学 Cosmetic comprising composition with slow anti-allergic action as well as preparation method and application thereof
CN107281020A (en) * 2017-06-06 2017-10-24 安徽吉乃尔电器科技有限公司 A kind of preparation method of maca whitening and skin-protecting emulsion

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
杨跃飞: "一种含纳米超临界蜂胶美白淡斑精华素及其制备方法", 《中国蜂业》 *
董志超 等: "库拉索芦荟粗多糖提取工艺优化", 《制剂技术》 *

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