CN108619036A

CN108619036A - A kind of preparation method of Post-basking repairing mask

Info

Publication number: CN108619036A
Application number: CN201810831208.6A
Authority: CN
Inventors: 卜俊超
Original assignee: Individual
Current assignee: Individual
Priority date: 2018-07-26
Filing date: 2018-07-26
Publication date: 2018-10-09

Abstract

A kind of preparation method of Post-basking repairing mask belongs to facial mask preparing technical field, including：Aloe polysaccharide is prepared, prepared by water phase liquid, emulsification, cool down and etc..Radix Glycyrrhizae and chamomile have clearing heat and detoxicating, antibacterial anti-inflammatory, the effect for pacifying calmness, and various skin, particularly suitable sensibility skin is suitble to can be used for the impaired skin of after-sun.For aloe polysaccharide other than with immunological regulation, sterilization, promoting cell reactivation, also having significantly makes skin contraction, anti-inflammatory, moisturizing and other effects, can be used for the impaired skin of after-sun.The present invention uses nanometer supercritical bee-glue, it is easy to which infiltration and absorption successfully solve the compatibility issues with other ingredients, and nanometer supercritical bee-glue has the function of that strength is anti-oxidant, inhibits tyrosinase activity, whitening spot-removing significant effect.

Description

A kind of preparation method of Post-basking repairing mask

Technical field

The present invention relates to facial mask preparing technical field, more particularly to a kind of preparation method of Post-basking repairing mask.

Background technology

Facial mask is the important step of skin care, and the active ingredients such as moisturizing, whitening and anti-aging in facial mask can be preferably by flesh Skin absorbs.And now many facial masks occurred in the market, all contain a large amount of synthetics, long-time service will produce one to skin Fixed side effect so that the nutritional ingredient in facial mask is not easy to be absorbed, or even can cause the adverse reactions such as scytitis, if choosing Take it is improper will result in immeasurable loss, when making, the selection of chemical substance and dosage exist many facial masks on the market Prodigious problem, natural component is less, and skin effect is bad, is further improved, and functional result have it is to be hoisted.

Invention content

It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of preparation method of Post-basking repairing mask, tools Have good penetrability, easily absorb, after-sun, releive skin the effect of.

The present invention uses following technical scheme：

A kind of preparation method of Post-basking repairing mask, includes the following steps：

Step 1：Aloe Barbadensis Miller fresh leaf is cleaned, 7 times of bodies are added at mucus shape in tissue mashing machine's homogenate in homogenate Long-pending distilled water stirring extraction 2h, filtering, filter residue repeat extraction 2 times, and merging filtrate, 40 DEG C are concentrated under reduced pressure into original volume 25%, the ethyl alcohol of 3 times of volume mass a concentration of 95% is added in concentrate, mixes well, is filtered after precipitation to be precipitated, collects Precipitation, by sediment with after hot water dissolving plus activated carbon decolorizing 20min, 40 DEG C be concentrated under reduced pressure into original volume 25%, concentrating The ethyl alcohol of 3 times of volume mass a concentration of 95% is added in liquid, mixes well, centrifuges, go under the rotating speed of 1000r/min Clear liquid collects precipitation to get aloe polysaccharide；

Step 2：Raw material is matched by weight：2-4 aloe polysaccharides, 2-4 part propolis extract, 0.5-1 parts of albumen Enzyme, 0.5-1 part aminopeptidase, 1-2 parts of camomile extracts, 1-2 parts of licorices, 1-3 parts of yeast polypeptides, 2-4 parts of tip edges Bladder-wrack extract, 1-3 part oligopeptides -20,0.5-1 parts of carbomers, 0.6-2 parts of aminomethyl propanols, 3-6 parts of propylene glycol, 3-6 parts 1, 3- butanediols, 0.5-1 part Cremophor RH40,0.5-1 parts of blumea oils, 0.5-1 parts of glycerol caprylates, 0.1-0.2 parts Methyl hydroxybenzoate, 0.1-0.2 part allantoin, 0.02-0.1 parts of EDETATE SODIUMs, 0.03-0.1 parts of Sodium Hyaluronates, 70-100 parts go from Sub- water；

Step 3：It weighs in deionized water to water phase pot, sequentially adds the measured EDETATE SODIUM of accurate scale, hyaluronic acid Sodium, carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3- Butanediol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；

Step 4：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, under stirring successively Aloe polysaccharide, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast polypeptides, tip edge is added Bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；

Step 5：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, octanoic acid is added Glyceride, and stir；

Step 6：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, then cold But to room temperature to get Essence；

Step 7：After mask substrate sterilization irradiation, after examining qualification to cut folding according to version type, it is packed into aluminium foil bag conveying To packaging production line, after bottle placer injects Essence, sealing machine sealing.

Preferably, the propolis extract is nanometer supercritical bee-glue.

It is further preferred that the nanometer supercritical bee-glue is the nanometer being process by Phospholipids nano-encapsulated technology Supercritical bee-glue.

Preferably, the licorice is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtains powder The NaOH aqueous solutions of a concentration of 0.2mol/L are added in body, are 1 by solid-to-liquid ratio:10 ratios mix, the hot dipping extraction 2h at 80 DEG C, It is repeated 2 times, filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifuged under the rotating speed of 4000r/min Separation, goes supernatant to obtain sediment, as licorice.

Preferably, the camomile extract is prepared using following methods：5g chamomiles are crushed, sieving, obtains powder The NaOH aqueous solutions of a concentration of 0.2mol/L are added in body, are 1 by solid-to-liquid ratio:10 ratios mix, the hot dipping extraction 2h at 80 DEG C, It is repeated 2 times, filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifuged under the rotating speed of 4000r/min Separation, goes supernatant to obtain sediment, as camomile extract.

Preferably, the tip edge bladder-wrack extract is prepared using following methods：Tip edge bladder-wrack is washed, is put It sets and is air-dried at aeration-drying, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, moderate heat dries 4min, after drying Tip edge bladder-wrack be put into pulverizer and crush, the tip edge bladder-wrack after crushing is crossed into 60 mesh sieve, tip edge bladder-wrack powder is obtained, weighs Tip edge bladder-wrack powder 10g, deionized water 100g, are added to the container, and extraction 100min are decocted at 90 DEG C, by the substance in container It all takes out, is cooled to room temperature, filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, in collection Clear liquid obtains tip edge bladder-wrack extract after filtering.

It is further preferred that described is filtered into three layers of filtered through gauze.

It is further preferred that being filtered using the membrane filter in 0.2 μm of aperture after three layers of filtered through gauze.

Preferably, the grinding and sieving was 40 mesh sieve.

The beneficial effects of the present invention are：

1) Radix Glycyrrhizae and chamomile have clearing heat and detoxicating, and antibacterial anti-inflammatory pacifies calm effect, are suitble to various skin, especially It is suitble to sensibility skin, can be used for the impaired skin of after-sun.

2) for aloe polysaccharide other than with immunological regulation, sterilization, promoting cell reactivation, also having significantly makes skin Convergence, anti-inflammatory, moisturizing and other effects can be used for the impaired skin of after-sun.

3) present invention uses nanometer supercritical bee-glue, it is easy to which infiltration and absorption successfully solve and other ingredients Compatibility issues, nanometer supercritical bee-glue have the function of that strength is anti-oxidant, inhibit tyrosinase activity, and whitening spot-removing effect is aobvious It writes.

4) tip edge bladder-wrack can provide the natural nutrient needed for skin rapid regeneration and cell normal growth, extra-nutrition It is lost in, promotes skin metabolism, increase the ATP synthesis of skin energy element；It protects skin cell mitochondria and maintains mitochondria work( Energy；Promote skin revitalization, skin is helped to reply health and vigor.

Specific implementation mode

With reference to embodiments, the technical solution in the present invention is clearly and completely described.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.

The propolis extract is nanometer supercritical bee-glue.The nanometer supercritical bee-glue is wrapped by Phospholipids nanometer The nanometer supercritical bee-glue that the technology of wrapping up in is process.

The licorice is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtain powder, is added The NaOH aqueous solutions of a concentration of 0.2mol/L are 1 by solid-to-liquid ratio:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times at 80 DEG C, Filtering, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, centrifuges, goes under the rotating speed of 4000r/min Supernatant obtains sediment, as licorice.

The grinding and sieving was 40 mesh sieve.

The camomile extract is prepared using following methods：5g chamomiles are crushed, sieving, obtain powder, is added The NaOH aqueous solutions of a concentration of 0.2mol/L are 1 by solid-to-liquid ratio:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times at 80 DEG C, Filtering, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, centrifuges, goes under the rotating speed of 4000r/min Supernatant obtains sediment, as camomile extract.

The grinding and sieving was 40 mesh sieve.

The tip edge bladder-wrack extract is prepared using following methods：Tip edge bladder-wrack is washed, is placed on logical It air-dries dry place to be air-dried, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, moderate heat dries 4min, by the tip edge after drying Bladder-wrack is put into pulverizer and crushes, and the tip edge bladder-wrack after crushing is crossed 60 mesh sieve, obtains tip edge bladder-wrack powder, weighs tip edge ink Angle algae powder 10g, deionized water 100g, are added to the container, and extraction 100min is decocted at 90 DEG C, the substance in container is all taken Go out, be cooled to room temperature, filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, collects supernatant, mistake After filter tip edge bladder-wrack extract, it is described to be filtered into three layers of filtered through gauze, using 0.2 after described three layers of filtered through gauze The membrane filter filtering in μm aperture.

The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above, As long as using the improvement of the various unsubstantialities of inventive concept and technical scheme of the present invention progress, or not improved this is sent out Bright design and technical solution directly applies to other occasions, within protection scope of the present invention.The protection of the present invention Range should be determined by the scope of protection defined in the claims.

Claims

1. a kind of preparation method of Post-basking repairing mask, which is characterized in that include the following steps：

Step 1：Aloe Barbadensis Miller fresh leaf is cleaned, 7 times of volumes are added at mucus shape, in homogenate for tissue mashing machine's homogenate Distilled water stirring extraction 2h, filtering, filter residue repeat extraction 2 times, merging filtrate, 40 DEG C be concentrated under reduced pressure into original volume 25%, The ethyl alcohol of 3 times of volume mass a concentration of 95% is added in concentrate, mixes well, is filtered after precipitation to be precipitated, collects precipitation, By sediment with after hot water dissolving plus activated carbon decolorizing 20min, 40 DEG C be concentrated under reduced pressure into original volume 25%, in concentrate plus The ethyl alcohol for entering 3 times of volume mass a concentration of 95%, mixes well, and is centrifuged under the rotating speed of 1000r/min, supernatant is gone to receive Collection precipitation is to get aloe polysaccharide；

Step 2：Raw material is matched by weight：2-4 aloe polysaccharides, 2-4 part propolis extract, 0.5-1 parts of protease, 0.5-1 parts of aminopeptidases, 1-2 parts of camomile extracts, 1-2 parts of licorices, 1-3 parts of yeast polypeptides, 2-4 parts of tip edge ink angles Algae extract, 1-3 part oligopeptides -20,0.5-1 parts of carbomers, 0.6-2 parts of aminomethyl propanols, 3-6 parts of propylene glycol, 3-6 parts of 1,3- fourths Glycol, 0.5-1 part Cremophor RH40,0.5-1 parts of blumea oils, 0.5-1 parts of glycerol caprylates, 0.1-0.2 parts of oxybenzenes Methyl esters, 0.1-0.2 part allantoin, 0.02-0.1 parts of EDETATE SODIUMs, 0.03-0.1 parts of Sodium Hyaluronates, 70-100 parts of deionizations Water；

Step 3：Weigh in deionized water to water phase pot, sequentially add the measured EDETATE SODIUM of accurate scale, Sodium Hyaluronate, Carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3- fourths Glycol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；

Step 4：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, is sequentially added under stirring Aloe polysaccharide, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast polypeptides, tip edge ink angle Algae extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；

Step 5：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, sad glycerine is added Ester, and stir；

Step 6：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, is cooled to Room temperature is to get Essence；

Step 7：After mask substrate sterilization irradiation, after examining qualification to cut folding according to version type, it is packed into aluminium foil bag and is transported to packet Assembling production lines, after bottle placer injects Essence, sealing machine sealing.

2. a kind of preparation method of Post-basking repairing mask according to claim 1, it is characterised in that：The propolis extraction Object is nanometer supercritical bee-glue.

3. a kind of preparation method of Post-basking repairing mask according to claim 2, it is characterised in that：The nanometer is super to face Boundary's propolis is the nanometer supercritical bee-glue being process by Phospholipids nano-encapsulated technology.

4. a kind of preparation method of Post-basking repairing mask according to claim 1, which is characterized in that the Radix Glycyrrhizae extraction Object is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtains powder, the NaOH water of a concentration of 0.2mol/L is added Solution is 1 by solid-to-liquid ratio:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times at 80 DEG C, filters, and it is dense that quality is added in filtrate It spends for 3% hydrochloric acid tune pH value to 1-2.5, is centrifuged under the rotating speed of 4000r/min, supernatant is gone to obtain sediment, it is as sweet Careless extract.

5. a kind of preparation method of Post-basking repairing mask according to claim 1, which is characterized in that the chamomile carries Object is taken to be prepared using following methods：5g chamomiles are crushed, sieving, obtains powder, the NaOH water of a concentration of 0.2mol/L is added Solution is 1 by solid-to-liquid ratio:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times at 80 DEG C, filters, and it is dense that quality is added in filtrate It spends for 3% hydrochloric acid tune pH value to 1-2.5, is centrifuged under the rotating speed of 4000r/min, supernatant is gone to obtain sediment, it is as foreign Flos Chrysanthemi extract.

6. a kind of preparation method of Post-basking repairing mask according to claim 1, which is characterized in that the tip edge ink angle Algae extract is prepared using following methods：Tip edge bladder-wrack is washed, is placed at aeration-drying and is air-dried, will be air-dried Tip edge bladder-wrack afterwards is placed in micro-wave oven, and moderate heat dries 4min, and the tip edge bladder-wrack after drying is put into pulverizer and is crushed, Tip edge bladder-wrack after crushing is crossed into 60 mesh sieve, tip edge bladder-wrack powder is obtained, weighs tip edge bladder-wrack powder 10g, deionized water 100g, It is added to the container, extraction 100min is decocted at 90 DEG C, the substance in container is all taken out, room temperature is cooled to, uses low temperature cold Freeze centrifuge filtering, rotating speed 3000r/min, centrifugation time 5min collect supernatant, and the extraction of tip edge bladder-wrack is obtained after filtering Object.

7. a kind of preparation method of Post-basking repairing mask according to claim 6, it is characterised in that：Described is filtered into three Layer filtered through gauze.

8. a kind of preparation method of Post-basking repairing mask according to claim 7, it is characterised in that：Three layers of gauze It is filtered using the membrane filter in 0.2 μm of aperture after filtering.

9. a kind of preparation method of Post-basking repairing mask according to claim 4 or 5, it is characterised in that：The crushing Sieving was 40 mesh sieve afterwards.