CN108815092A - A kind of preparation method of the anti-acne maintenance Essence containing tea polyphenols - Google Patents
A kind of preparation method of the anti-acne maintenance Essence containing tea polyphenols Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Abstract
A kind of preparation method of the anti-acne maintenance Essence containing tea polyphenols, belongs to Essence preparation technical field, including：Tea polyphenol extract object, the preparation of water phase liquid are prepared, is emulsified, cool down and etc..Tea polyphenols are water-soluble substances; with the greasy of removing face; restrain pore; the effect of anti-acne, antiphlogistic and bactericidal, additionally it is possible to stop ultraviolet light and remove the free radical of ultraviolet induction; to protect the normal function of melanocyte; inhibit the formation of melanin, while inhibition is generated to lipid oxidation, mitigates pigmentation.Radix Glycyrrhizae has the effect of clearing heat and detoxicating, antibacterial anti-inflammatory.It is especially suitable for the skin for having small pox, frequent inflammation, has and pacify calmness, eliminate facial acne, and effectively prevents the generation of small pox acne.Chamomile has disinfecting, antimicrobial, sensitive skin of releiving, lasting the effect of protecting skin not interfered by whelk acne.
Description
Technical field
The present invention relates to Essence preparation technical field, in particular to a kind of anti-acne maintenance Essence containing tea polyphenols
Preparation method.
Background technique
Essence is the superfine product in skin care item, and ingredient is exquisite, effect is powerful, significant effect, remains what it possessed
It is noble and mysterious, it is suitable for any skin or inclined oily skin, preferably puts in the vial, take at any time.Essence is used for toner
Later, before face cream.Commonly there is poor permeability, be not easy the problems such as absorbing, single effect in current Essence.
Summary of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of anti-acne maintenance Essence containing tea polyphenols
Preparation method, there is good penetrability, easily absorb, the effect of anti-acne.
The present invention uses following technical scheme：
A kind of preparation method of the anti-acne maintenance Essence containing tea polyphenols, includes the following steps：
Step 1：It takes tealeaves to crush, crosses 80 meshes, obtain tea powder, accurately weighed tea powder 4g, with 120mL volumetric concentration 25%
Ethanol solution wetting, is added by cellulase and pectase in mass ratio 1:The complex enzyme 6mg of 1 composition, is placed in 50 DEG C of thermostatted waters
Completely cut off air stirring 30min in bath, extracted under conditions of 50 DEG C, microwave power 400W, gained extract liquor is diluted 5 times and quiet
10min is set, supernatant liquor is drawn, both obtains tea polyphenol extract object；
Step 2：It weighs in deionized water to water phase pot, sequentially adds the measured EDETATE SODIUM of accurate scale, hyaluronic acid
Sodium, carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3-
Butanediol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；
Step 3：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, under stirring successively
Be added tea polyphenol extract object, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast polypeptides,
Tip edge bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；
Step 4：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, octanoic acid is added
Glyceride, and stir；
Step 5：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, then cold
But to room temperature to get Essence.
Preferably, the propolis extract is nanometer supercritical bee-glue.
It is further preferred that the nanometer supercritical bee-glue is the nanometer being process by Phospholipids nano-encapsulated technology
Supercritical bee-glue.
Preferably, the licorice is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtains powder
The NaOH aqueous solution that concentration is 0.2mol/L is added in body, is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C,
It is repeated 2 times, filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifuged under the revolving speed of 4000r/min
Separation, goes supernatant to obtain sediment, as licorice.
Preferably, the camomile extract is prepared using following methods：5g chamomile is crushed, sieving, obtains powder
The NaOH aqueous solution that concentration is 0.2mol/L is added in body, is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C,
It is repeated 2 times, filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifuged under the revolving speed of 4000r/min
Separation, goes supernatant to obtain sediment, as camomile extract.
Preferably, the tip edge bladder-wrack extract is prepared using following methods：Tip edge bladder-wrack is washed, is put
It sets and is carried out at aeration-drying air-dried, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, the dry 4min of moderate heat, after drying
Tip edge bladder-wrack be put into pulverizer and crush, smashed tip edge bladder-wrack is crossed into 60 meshes, tip edge bladder-wrack powder is obtained, weighs
Tip edge bladder-wrack powder 10g, deionized water 100g, are added to the container, and decoct at 90 DEG C and extract 100min, by the substance in container
It all takes out, is cooled to room temperature, filtered with cryogenic freezing centrifuge, revolving speed 3000r/min, centrifugation time 5min, in collection
Clear liquid obtains tip edge bladder-wrack extract after filtering.
It is further preferred that described is filtered into three layers of filtered through gauze.
It is further preferred that being filtered after three layers of filtered through gauze using the membrane filter in 0.2 μm of aperture.
Preferably, the grinding and sieving was 40 meshes.
The beneficial effects of the present invention are：
1) the effect of tea polyphenols are water-soluble substances, have and remove the greasy of face, convergence pore, anti-acne, antiphlogistic and bactericidal,
It can also stop ultraviolet light and remove the free radical of ultraviolet induction, to protect the normal function of melanocyte, inhibit black
The formation of pigment, while inhibition is generated to lipid oxidation, mitigate pigmentation.
2) the effect of Radix Glycyrrhizae has clearing heat and detoxicating, antibacterial anti-inflammatory.It is especially suitable for the skin for having small pox, frequent inflammation, has
Calmness is pacified, facial acne is eliminated, and effectively prevents the generation of small pox acne.It is suitble to various skin, is particularly suitable for sensibility flesh
Skin.
3) chamomile has disinfecting, antimicrobial, sensitive skin of releiving, the function for persistently protecting skin not interfered by whelk acne
Effect.
4) present invention uses nanometer supercritical bee-glue, it is easy to which infiltration and absorption successfully solve and other ingredients
Compatibility issues, nanometer supercritical bee-glue have the function of that strength is anti-oxidant, inhibit tyrosinase activity, and whitening spot-removing effect is aobvious
It writes.
5) required natural nutrient needed for tip edge bladder-wrack can provide skin rapid regeneration and cell normal growth, Replacement Battalion
Feeding loss promotes skin metabolism, increases skin energy element ATP synthesis；It protects skin cell mitochondria and maintains line grain
Body function；Promote skin revitalization, skin is helped to reply health and vigor.
Specific embodiment
With reference to embodiments, the technical solution in the present invention is clearly and completely described.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
A kind of anti-acne maintenance Essence containing tea polyphenols, the raw material including following parts by weight：2-4 parts of tea polyphenol extracts
Object, 2-4 part propolis extract, 0.5-1 parts of protease, 0.5-1 parts of aminopeptidases, 1-2 parts of camomile extracts, 1-2 portions of Radix Glycyrrhizaes
Extract, 1-3 part yeast polypeptides, 2-4 parts of tip edge bladder-wrack extracts, 1-3 parts of oligopeptides -20,0.5-1 parts of carbomers, 0.6-2 parts
Aminomethyl propanol, 3-6 part propylene glycol, 3-6 parts of 1,3 butylene glycols, 0.5-1 parts of Cremophor RH40s, 0.5-1 parts of Blumea balsamiferas
Oil, 0.5-1 parts of glycerol caprylates, 0.1-0.2 parts of methyl hydroxybenzoates, 0.1-0.2 parts of allantoins, 0.02-0.1 parts of EDETATE SODIUMs,
0.03-0.1 parts of Sodium Hyaluronates, 70-100 parts of deionized waters.
A kind of preparation method of the anti-acne maintenance Essence containing tea polyphenols, includes the following steps：
Step 1：It takes tealeaves to crush, crosses 80 meshes, obtain tea powder, accurately weighed tea powder 4g, with 120mL volumetric concentration 25%
Ethanol solution wetting, is added by cellulase and pectase in mass ratio 1:The complex enzyme 6mg of 1 composition, is placed in 50 DEG C of thermostatted waters
Completely cut off air stirring 30min in bath, extracted under conditions of 50 DEG C, microwave power 400W, gained extract liquor is diluted 5 times and quiet
10min is set, supernatant liquor is drawn, both obtains tea polyphenol extract object；
Step 2：It weighs in deionized water to water phase pot, sequentially adds the measured EDETATE SODIUM of accurate scale, hyaluronic acid
Sodium, carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3-
Butanediol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；
Step 3：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, under stirring successively
Be added tea polyphenol extract object, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast polypeptides,
Tip edge bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；
Step 4：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, octanoic acid is added
Glyceride, and stir；
Step 5：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, then cold
But to room temperature to get Essence.
The propolis extract is nanometer supercritical bee-glue.The nanometer supercritical bee-glue is wrapped by Phospholipids nanometer
The nanometer supercritical bee-glue that the technology of wrapping up in is process.
The licorice is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtain powder, is added
Concentration is the NaOH aqueous solution of 0.2mol/L, is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times,
It filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifugated, goes under the revolving speed of 4000r/min
Supernatant obtains sediment, as licorice.
The grinding and sieving was 40 meshes.
The camomile extract is prepared using following methods：5g chamomile is crushed, sieving, obtain powder, is added
Concentration is the NaOH aqueous solution of 0.2mol/L, is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times,
It filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifugated, goes under the revolving speed of 4000r/min
Supernatant obtains sediment, as camomile extract.
The grinding and sieving was 40 meshes.
The tip edge bladder-wrack extract is prepared using following methods：Tip edge bladder-wrack is washed, is placed on logical
It air-dries dry place and carries out air-dried, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, the dry 4min of moderate heat, by the tip edge after drying
Bladder-wrack is put into pulverizer and crushes, and smashed tip edge bladder-wrack is crossed 60 meshes, obtains tip edge bladder-wrack powder, weighs tip edge ink
Angle algae powder 10g, deionized water 100g, are added to the container, and decoct at 90 DEG C and extract 100min, the substance in container is all taken
Out, it is cooled to room temperature, is filtered with cryogenic freezing centrifuge, revolving speed 3000r/min, centrifugation time 5min, supernatant, mistake are collected
After filter tip edge bladder-wrack extract, it is described to be filtered into three layers of filtered through gauze, using 0.2 after three layers of filtered through gauze
The membrane filter filtering in μm aperture.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above,
As long as using the improvement for the various unsubstantialities that the inventive concept and technical scheme of the present invention carry out, or not improved this is sent out
Bright conception and technical scheme directly apply to other occasions, within the scope of the present invention.Protection of the invention
Range should be determined by the scope of protection defined in the claims.
Claims (9)
1. a kind of preparation method of the anti-acne maintenance Essence containing tea polyphenols, which is characterized in that include the following steps：
Step 1：It takes tealeaves to crush, crosses 80 meshes, obtain tea powder, accurately weighed tea powder 4g, with 25% ethyl alcohol of 120mL volumetric concentration
Solution-wet is added by cellulase and pectase in mass ratio 1:The complex enzyme 6mg of 1 composition, is placed in 50 DEG C of waters bath with thermostatic control
Completely cut off air stirring 30min, extracted under conditions of 50 DEG C, microwave power 400W, gained extract liquor is diluted 5 times and stands
10min draws supernatant liquor, both obtains tea polyphenol extract object；
Step 2：Weigh in deionized water to water phase pot, sequentially add the measured EDETATE SODIUM of accurate scale, Sodium Hyaluronate,
Carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3- fourth
Glycol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；
Step 3：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, is sequentially added under stirring
Tea polyphenol extract object, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast polypeptides, tip edge
Bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；
Step 4：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, sad glycerol is added
Ester, and stir；
Step 5：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, is cooled to
Room temperature is to get Essence.
2. a kind of preparation method of anti-acne maintenance Essence containing tea polyphenols according to claim 1, it is characterised in that：
The propolis extract is nanometer supercritical bee-glue.
3. a kind of preparation method of anti-acne maintenance Essence containing tea polyphenols according to claim 2, it is characterised in that：
The nanometer supercritical bee-glue is the nanometer supercritical bee-glue being process by Phospholipids nano-encapsulated technology.
4. a kind of preparation method of anti-acne maintenance Essence containing tea polyphenols according to claim 1, which is characterized in that
The licorice is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtain powder, concentration, which is added, is
The NaOH aqueous solution of 0.2mol/L is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered,
It is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, removes supernatant
Obtain sediment, as licorice.
5. a kind of preparation method of anti-acne maintenance Essence containing tea polyphenols according to claim 1, which is characterized in that
The camomile extract is prepared using following methods：5g chamomile is crushed, sieving, obtain powder, concentration, which is added, is
The NaOH aqueous solution of 0.2mol/L is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered,
It is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, removes supernatant
Obtain sediment, as camomile extract.
6. a kind of preparation method of anti-acne maintenance Essence containing tea polyphenols according to claim 1, which is characterized in that
The tip edge bladder-wrack extract is prepared using following methods：Tip edge bladder-wrack is washed, is placed at aeration-drying
Carry out air-dried, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, and the dry 4min of moderate heat puts the tip edge bladder-wrack after drying
Enter in pulverizer and crush, smashed tip edge bladder-wrack is crossed into 60 meshes, obtains tip edge bladder-wrack powder, weighs tip edge bladder-wrack powder
10g, deionized water 100g, are added to the container, and decoct at 90 DEG C and extract 100min, the substance in container are all taken out, drop
It warms to room temperature, is filtered with cryogenic freezing centrifuge, revolving speed 3000r/min, centrifugation time 5min, supernatant is collected, after filtering
Obtain tip edge bladder-wrack extract.
7. a kind of preparation method of anti-acne maintenance Essence containing tea polyphenols according to claim 6, it is characterised in that：
Described is filtered into three layers of filtered through gauze.
8. a kind of preparation method of anti-acne maintenance Essence containing tea polyphenols according to claim 7, it is characterised in that：
It is filtered after three layers of filtered through gauze using the membrane filter in 0.2 μm of aperture.
9. a kind of preparation method of anti-acne maintenance Essence containing tea polyphenols according to claim 4 or 5, feature exist
In：The grinding and sieving was 40 meshes.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113712873A (en) * | 2021-09-26 | 2021-11-30 | 湖北省麦诗特生物科技有限公司 | Essence emulsion composition with acne-removing and anti-inflammatory effects and preparation method thereof |
| CN114903947A (en) * | 2022-05-14 | 2022-08-16 | 广州南雪药业有限公司 | Composition with acne removing effect and application thereof in preparation of medicines or skin care products |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1699586A (en) * | 2005-04-29 | 2005-11-23 | 西北大学 | Process for extracting tea polyphenol, caffeine as a byproduct thereof and tea polysaccharide from tea |
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| CN113712873A (en) * | 2021-09-26 | 2021-11-30 | 湖北省麦诗特生物科技有限公司 | Essence emulsion composition with acne-removing and anti-inflammatory effects and preparation method thereof |
| CN114903947A (en) * | 2022-05-14 | 2022-08-16 | 广州南雪药业有限公司 | Composition with acne removing effect and application thereof in preparation of medicines or skin care products |
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Application publication date: 20181116 |