CN108815093A - A kind of pore shrinks Essence and preparation method thereof - Google Patents
A kind of pore shrinks Essence and preparation method thereof Download PDFInfo
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
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Abstract
A kind of pore shrinks Essence and preparation method thereof, belongs to Essence preparation technical field, the raw material including following parts by weight：2-4 parts of tea polyphenol extract objects, 2-4 parts of propolis extracts, 1-3 parts of double sweet ammonia skins, 0.5-1 parts of protease, 0.5-1 parts of aminopeptidases, 1-2 parts of camomile extracts, 1-2 parts of licorices, 1-3 parts of yeast polypeptides, 2-4 parts of tip edge bladder-wrack extracts, 1-3 parts of oligopeptides -20, 0.5-1 parts of carbomers, 0.6-2 parts of aminomethyl propanols, 3-6 parts of propylene glycol, 3-6 part 1, 3- butanediol, 0.5-1 parts of Cremophor RH40s, 0.5-1 parts of blumea oils, 0.5-1 parts of glycerol caprylates, 0.1-0.2 parts of methyl hydroxybenzoates, 0.1-0.2 parts of allantoins, 0.02-0.1 parts of EDETATE SODIUMs, 0.03-0.1 parts of Sodium Hyaluronates, 70-100 parts of deionized waters.Double sweet ammonia skins, which contain, inhibits the dysgenic ingredient of unsaturated fatty acid, can not only reduce the structure that pore expands outwardly, while can also improve the skin condition around pore.The effect of tea polyphenols are water-soluble substances, have and remove the greasy of face, convergence pore, anti-acne, antiphlogistic and bactericidal.
Description
Technical field
The present invention relates to Essence preparation technical field, in particular to a kind of pore shrinks Essence and preparation method thereof.
Background technique
Essence is the superfine product in skin care item, and ingredient is exquisite, effect is powerful, significant effect, remains what it possessed
It is noble and mysterious, it is suitable for any skin or inclined oily skin, preferably puts in the vial, take at any time.Essence is used for toner
Later, before face cream.Commonly there is poor permeability, be not easy the problems such as absorbing, single effect in current Essence.
Summary of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of pores to shrink Essence and its preparation side
The effect of method has good penetrability, easily absorbs, pore refining.
The present invention uses following technical scheme：
A kind of pore contraction Essence, the raw material including following parts by weight：2-4 parts of tea polyphenol extract objects, 2-4 parts of propolis
Extract, 1-3 parts of double sweet ammonia skins, 0.5-1 parts of protease, 0.5-1 parts of aminopeptidases, 1-2 parts of camomile extracts, 1-2 parts it is sweet
Careless extract, 1-3 part yeast polypeptides, 2-4 parts of tip edge bladder-wrack extracts, 1-3 parts of oligopeptides -20,0.5-1 parts of carbomers, 0.6-2
Part aminomethyl propanol, 3-6 parts of propylene glycol, 3-6 parts of 1,3 butylene glycols, 0.5-1 parts of Cremophor RH40s, 0.5-1 parts of Ai Na
Sesame oil, 0.5-1 part glycerol caprylate, 0.1-0.2 parts of methyl hydroxybenzoates, 0.1-0.2 parts of allantoins, 0.02-0.1 parts of EDETATE SODIUMs,
0.03-0.1 parts of Sodium Hyaluronates, 70-100 parts of deionized waters.
A kind of pore shrinks the preparation method of Essence, includes the following steps：
Step 1：It takes tealeaves to crush, crosses 80 meshes, obtain tea powder, accurately weighed tea powder 4g, with 120mL volumetric concentration 25%
Ethanol solution wetting, is added by cellulase and pectase in mass ratio 1:The complex enzyme 6mg of 1 composition, is placed in 50 DEG C of thermostatted waters
Completely cut off air stirring 30min in bath, extracted under conditions of 50 DEG C, microwave power 400W, gained extract liquor is diluted 5 times and quiet
10min is set, supernatant liquor is drawn, both obtains tea polyphenol extract object；
Step 2：It weighs in deionized water to water phase pot, sequentially adds the measured EDETATE SODIUM of accurate scale, hyaluronic acid
Sodium, carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3-
Butanediol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；
Step 3：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, under stirring successively
Be added tea polyphenol extract object, propolis extract, protease, aminopeptidase, camomile extract, licorice, double sweet ammonia skins,
Yeast polypeptides, tip edge bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；
Step 4：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, octanoic acid is added
Glyceride, and stir；
Step 5：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, then cold
But to room temperature to get Essence.
Preferably, the propolis extract is nanometer supercritical bee-glue.
It is further preferred that the nanometer supercritical bee-glue is the nanometer being process by Phospholipids nano-encapsulated technology
Supercritical bee-glue.
Preferably, the licorice is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtains powder
The NaOH aqueous solution that concentration is 0.2mol/L is added in body, is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C,
It is repeated 2 times, filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifuged under the revolving speed of 4000r/min
Separation, goes supernatant to obtain sediment, as licorice.
Preferably, the camomile extract is prepared using following methods：5g chamomile is crushed, sieving, obtains powder
The NaOH aqueous solution that concentration is 0.2mol/L is added in body, is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C,
It is repeated 2 times, filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifuged under the revolving speed of 4000r/min
Separation, goes supernatant to obtain sediment, as camomile extract.
Preferably, the tip edge bladder-wrack extract is prepared using following methods：Tip edge bladder-wrack is washed, is put
It sets and is carried out at aeration-drying air-dried, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, the dry 4min of moderate heat, after drying
Tip edge bladder-wrack be put into pulverizer and crush, smashed tip edge bladder-wrack is crossed into 60 meshes, tip edge bladder-wrack powder is obtained, weighs
Tip edge bladder-wrack powder 10g, deionized water 100g, are added to the container, and decoct at 90 DEG C and extract 100min, by the substance in container
It all takes out, is cooled to room temperature, filtered with cryogenic freezing centrifuge, revolving speed 3000r/min, centrifugation time 5min, in collection
Clear liquid obtains tip edge bladder-wrack extract after filtering.
It is further preferred that described is filtered into three layers of filtered through gauze.
It is further preferred that being filtered after three layers of filtered through gauze using the membrane filter in 0.2 μm of aperture.
Preferably, the grinding and sieving was 40 meshes.
The beneficial effects of the present invention are：
1) double sweet ammonia skins, which contain, inhibits the dysgenic ingredient of unsaturated fatty acid, can not only reduce what pore expanded outwardly
Structure, while the skin condition around pore can also be improved.
2) the effect of tea polyphenols are water-soluble substances, have and remove the greasy of face, convergence pore, anti-acne, antiphlogistic and bactericidal,
It can also stop ultraviolet light and remove the free radical of ultraviolet induction, to protect the normal function of melanocyte, inhibit black
The formation of pigment, while inhibition is generated to lipid oxidation, mitigate pigmentation.
3) the effect of Radix Glycyrrhizae has clearing heat and detoxicating, antibacterial anti-inflammatory.It is especially suitable for the skin for having small pox, frequent inflammation, has
Calmness is pacified, facial acne is eliminated, and effectively prevents the generation of small pox acne, is suitble to various skin, is particularly suitable for sensibility flesh
Skin.
4) chamomile have disinfecting, antimicrobial, releive sensitive skin the effect of.
5) present invention uses nanometer supercritical bee-glue, it is easy to which infiltration and absorption successfully solve and other ingredients
Compatibility issues, nanometer supercritical bee-glue have the function of that strength is anti-oxidant, inhibit tyrosinase activity, and whitening spot-removing effect is aobvious
It writes.
6) required natural nutrient needed for tip edge bladder-wrack can provide skin rapid regeneration and cell normal growth, Replacement Battalion
Feeding loss promotes skin metabolism, increases skin energy element ATP synthesis；It protects skin cell mitochondria and maintains line grain
Body function；Promote skin revitalization, skin is helped to reply health and vigor.
Specific embodiment
With reference to embodiments, the technical solution in the present invention is clearly and completely described.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
A kind of pore contraction Essence, the raw material including following parts by weight：2-4 parts of tea polyphenol extract objects, 2-4 parts of propolis
Extract, 1-3 parts of double sweet ammonia skins, 0.5-1 parts of protease, 0.5-1 parts of aminopeptidases, 1-2 parts of camomile extracts, 1-2 parts it is sweet
Careless extract, 1-3 part yeast polypeptides, 2-4 parts of tip edge bladder-wrack extracts, 1-3 parts of oligopeptides -20,0.5-1 parts of carbomers, 0.6-2
Part aminomethyl propanol, 3-6 parts of propylene glycol, 3-6 parts of 1,3 butylene glycols, 0.5-1 parts of Cremophor RH40s, 0.5-1 parts of Ai Na
Sesame oil, 0.5-1 part glycerol caprylate, 0.1-0.2 parts of methyl hydroxybenzoates, 0.1-0.2 parts of allantoins, 0.02-0.1 parts of EDETATE SODIUMs,
0.03-0.1 parts of Sodium Hyaluronates, 70-100 parts of deionized waters.
A kind of pore shrinks the preparation method of Essence, includes the following steps：
Step 1：It takes tealeaves to crush, crosses 80 meshes, obtain tea powder, accurately weighed tea powder 4g, with 120mL volumetric concentration 25%
Ethanol solution wetting, is added by cellulase and pectase in mass ratio 1:The complex enzyme 6mg of 1 composition, is placed in 50 DEG C of thermostatted waters
Completely cut off air stirring 30min in bath, extracted under conditions of 50 DEG C, microwave power 400W, gained extract liquor is diluted 5 times and quiet
10min is set, supernatant liquor is drawn, both obtains tea polyphenol extract object；
Step 2：It weighs in deionized water to water phase pot, sequentially adds the measured EDETATE SODIUM of accurate scale, hyaluronic acid
Sodium, carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3-
Butanediol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；
Step 3：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, under stirring successively
Be added tea polyphenol extract object, propolis extract, protease, aminopeptidase, camomile extract, licorice, double sweet ammonia skins,
Yeast polypeptides, tip edge bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；
Step 4：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, octanoic acid is added
Glyceride, and stir；
Step 5：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, then cold
But to room temperature to get Essence.
The propolis extract is nanometer supercritical bee-glue.The nanometer supercritical bee-glue is wrapped by Phospholipids nanometer
The nanometer supercritical bee-glue that the technology of wrapping up in is process.
The licorice is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtain powder, is added
Concentration is the NaOH aqueous solution of 0.2mol/L, is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times,
It filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifugated, goes under the revolving speed of 4000r/min
Supernatant obtains sediment, as licorice.
The grinding and sieving was 40 meshes.
The camomile extract is prepared using following methods：5g chamomile is crushed, sieving, obtain powder, is added
Concentration is the NaOH aqueous solution of 0.2mol/L, is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times,
It filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifugated, goes under the revolving speed of 4000r/min
Supernatant obtains sediment, as camomile extract.
The grinding and sieving was 40 meshes.
The tip edge bladder-wrack extract is prepared using following methods：Tip edge bladder-wrack is washed, is placed on logical
It air-dries dry place and carries out air-dried, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, the dry 4min of moderate heat, by the tip edge after drying
Bladder-wrack is put into pulverizer and crushes, and smashed tip edge bladder-wrack is crossed 60 meshes, obtains tip edge bladder-wrack powder, weighs tip edge ink
Angle algae powder 10g, deionized water 100g, are added to the container, and decoct at 90 DEG C and extract 100min, the substance in container is all taken
Out, it is cooled to room temperature, is filtered with cryogenic freezing centrifuge, revolving speed 3000r/min, centrifugation time 5min, supernatant, mistake are collected
After filter tip edge bladder-wrack extract, it is described to be filtered into three layers of filtered through gauze, using 0.2 after three layers of filtered through gauze
The membrane filter filtering in μm aperture.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above,
As long as using the improvement for the various unsubstantialities that the inventive concept and technical scheme of the present invention carry out, or not improved this is sent out
Bright conception and technical scheme directly apply to other occasions, within the scope of the present invention.Protection of the invention
Range should be determined by the scope of protection defined in the claims.
Claims (10)
1. a kind of pore shrinks Essence, which is characterized in that the raw material including following parts by weight：2-4 parts of tea polyphenol extract objects,
2-4 parts of propolis extracts, 1-3 parts of double sweet ammonia skins, 0.5-1 parts of protease, 0.5-1 parts of aminopeptidases, 1-2 parts of chamomiles are extracted
Object, 1-2 part licorice, 1-3 parts of yeast polypeptides, 2-4 parts of tip edge bladder-wrack extracts, 1-3 parts of oligopeptides -20,0.5-1 parts of cards
Wave nurse, 0.6-2 part aminomethyl propanol, 3-6 parts of propylene glycol, 3-6 parts of 1,3 butylene glycols, 0.5-1 parts of Cremophor RH40s,
0.5-1 parts of blumea oils, 0.5-1 parts of glycerol caprylates, 0.1-0.2 parts of methyl hydroxybenzoates, 0.1-0.2 parts of allantoins, 0.02-0.1
Part EDETATE SODIUM, 0.03-0.1 parts of Sodium Hyaluronates, 70-100 parts of deionized waters.
2. the preparation method that a kind of pore as described in claim 1 shrinks Essence, which is characterized in that include the following steps：
Step 1：It takes tealeaves to crush, crosses 80 meshes, obtain tea powder, accurately weighed tea powder 4g, with 25% ethyl alcohol of 120mL volumetric concentration
Solution-wet is added by cellulase and pectase in mass ratio 1:The complex enzyme 6mg of 1 composition, is placed in 50 DEG C of waters bath with thermostatic control
Completely cut off air stirring 30min, extracted under conditions of 50 DEG C, microwave power 400W, gained extract liquor is diluted 5 times and stands
10min draws supernatant liquor, both obtains tea polyphenol extract object；
Step 2：Weigh in deionized water to water phase pot, sequentially add the measured EDETATE SODIUM of accurate scale, Sodium Hyaluronate,
Carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3- fourth
Glycol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；
Step 3：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, is sequentially added under stirring
Tea polyphenol extract object, propolis extract, protease, aminopeptidase, camomile extract, licorice, double sweet ammonia skins, yeast
Polypeptide, tip edge bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；
Step 4：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, sad glycerol is added
Ester, and stir；
Step 5：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, is cooled to
Room temperature is to get Essence.
3. the preparation method that a kind of pore according to claim 2 shrinks Essence, it is characterised in that：The propolis mentions
Taking object is nanometer supercritical bee-glue.
4. the preparation method that a kind of pore according to claim 3 shrinks Essence, it is characterised in that：The nanometer is super
Critical propolis is the nanometer supercritical bee-glue being process by Phospholipids nano-encapsulated technology.
5. the preparation method that a kind of pore according to claim 2 shrinks Essence, which is characterized in that the Radix Glycyrrhizae mentions
Object is taken to prepare using following methods：5g licorice medicinal materials are crushed, sieving, obtain powder, the NaOH that concentration is 0.2mol/L is added
Aqueous solution is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, and quality is added in filtrate
Concentration is 3% hydrochloric acid tune pH value to 1-2.5, is centrifugated under the revolving speed of 4000r/min, goes supernatant to obtain sediment, as
Licorice.
6. the preparation method that a kind of pore according to claim 2 shrinks Essence, which is characterized in that the chamomile
Extract is prepared using following methods：5g chamomile is crushed, sieving, obtain powder, the NaOH that concentration is 0.2mol/L is added
Aqueous solution is 1 by solid-to-liquid ratio:The mixing of 10 ratios, 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, and quality is added in filtrate
Concentration is 3% hydrochloric acid tune pH value to 1-2.5, is centrifugated under the revolving speed of 4000r/min, goes supernatant to obtain sediment, as
Camomile extract.
7. the preparation method that a kind of pore according to claim 2 shrinks Essence, which is characterized in that the tip edge ink
Angle algae extract is prepared using following methods：Tip edge bladder-wrack is washed, be placed at aeration-drying carry out it is air-dried, by wind
Tip edge bladder-wrack after dry is placed in micro-wave oven, and the tip edge bladder-wrack after drying is put into powder in pulverizer by the dry 4min of moderate heat
It is broken, smashed tip edge bladder-wrack is crossed into 60 meshes, obtains tip edge bladder-wrack powder, weighs tip edge bladder-wrack powder 10g, deionized water
100g is added to the container, and is decocted at 90 DEG C and is extracted 100min, and the substance in container is all taken out, is cooled to room temperature, use is low
Warm refrigerated centrifuge filtering, revolving speed 3000r/min, centrifugation time 5min collect supernatant, and tip edge bladder-wrack is obtained after filtering and is mentioned
Take object.
8. the preparation method that a kind of pore according to claim 7 shrinks Essence, it is characterised in that：Described is filtered into
Three layers of filtered through gauze.
9. the preparation method that a kind of pore according to claim 8 shrinks Essence, it is characterised in that：Three layers of yarn
It is filtered after cloth filtering using the membrane filter in 0.2 μm of aperture.
10. the preparation method that a kind of pore according to claim 5 or 6 shrinks Essence, it is characterised in that：The powder
Sieving was 40 meshes after broken.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810710183.4A CN108815093A (en) | 2018-07-02 | 2018-07-02 | A kind of pore shrinks Essence and preparation method thereof |
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| CN201810710183.4A CN108815093A (en) | 2018-07-02 | 2018-07-02 | A kind of pore shrinks Essence and preparation method thereof |
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| CN201810710183.4A Withdrawn CN108815093A (en) | 2018-07-02 | 2018-07-02 | A kind of pore shrinks Essence and preparation method thereof |
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| CN113712871A (en) * | 2021-09-26 | 2021-11-30 | 湖北省麦诗特生物科技有限公司 | Essence emulsion composition containing liposome with comedones removing effect and preparation method thereof |
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| CN112121000A (en) * | 2020-10-12 | 2020-12-25 | 北京蜜慕科技有限公司 | Propolis acne-removing balancing base solution and preparation method thereof |
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Application publication date: 20181116 |