CN108743463A - A kind of preparation method of the after-sun lotion of the red algae extract containing decoloration - Google Patents
A kind of preparation method of the after-sun lotion of the red algae extract containing decoloration Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/9717—Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q19/00—Preparations for care of the skin
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
A kind of preparation method of the after-sun lotion of the red algae extract containing decoloration, belongs to lotion preparing technical field, including：Decoloration red algae extract is prepared, raw material is matched by weight, prepared by water phase liquid, emulsification, cool down and etc..Red algae extract contains a large amount of uvioresistant active material, and anti-uv-ray is good, plays the role of good chemical sunscreen.Radix Glycyrrhizae and chamomile have clearing heat and detoxicating, antibacterial anti-inflammatory, the effect for pacifying calmness, and various skin, particularly suitable sensibility skin is suitble to can be used for the impaired skin of after-sun.The present invention uses nanometer supercritical bee-glue, it is easy to which infiltration and absorption successfully solve the compatibility issues with other ingredients, and nanometer supercritical bee-glue has the function of that strength is anti-oxidant, inhibits tyrosinase activity, whitening spot-removing significant effect.
Description
Technical field
The present invention relates to lotion preparing technical field, more particularly to the after-sun lotion of a kind of red algae extract containing decoloration
Preparation method.
Background technology
Lotion is the most basic step of skin care, and the active ingredients such as moisturizing, whitening and anti-aging in lotion being capable of better quilt
Percutaneous absorption possesses many lotions that one bottle of good lotion is extremely important, and now occurs in the market, all contains a large amount of chemistry and closes
At object, long-time service will produce skin certain side effect so that the nutritional ingredient in lotion is not easy to be absorbed, or even can draw
The adverse reactions such as scytitis are sent out, if selection is improper to will result in immeasurable loss, many lotions are making on the market
When, the selection of chemical substance and dosage are there are prodigious problem, and natural component is less, and skin effect is bad, need further
It improves.
Invention content
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of after-suns of the red algae extract containing decoloration
The preparation method of lotion, have good penetrability, easily absorb, after-sun, releive skin the effect of.
The present invention uses following technical scheme：
A kind of preparation method of the after-sun lotion of the red algae extract containing decoloration, includes the following steps：
Step 1：After Sargassum horneri is cleaned up, drying crushes to obtain algae powder, by algae powder and ethanol solution according to 1：15-20w/
The solid-liquid ratio of v is uniformly mixed, and maintains the temperature at 40-50 DEG C, and extracting solution, extracting solution heating are extracted 4-6 hours to obtain under stirring condition
To 60-70 DEG C, it is ultrasonically treated 10-15min, filtering and impurity removing, filter vacuum is concentrated under reduced pressure into the 10-20% of original volume, and spraying is dry
Red algae extract is obtained after dry, and the red algae extract that mass concentration is 69-72% will be configured to after red algae extract plus deionized water
Solution, is then added decolorising agent into red algae extract solution, and decolorising agent dosage is the 6%- of red algae extract solution weight
8%, it is stirred 2-3 hours, decoloration red algae extract is obtained after flame filter press filtering；The mass concentration of the ethanol solution
For 85%-90%；The speed of the stirring is 80-100r/min；The power of the ultrasound is 300-400w；The decolorising agent by
Activated carbon and diatomite mixing composition, the activated carbon：Diatomaceous weight ratio is 2-4:1；
Step 2：Raw material is matched by weight：2-4 parts of decoloration red algae extracts, 2-4 parts of propolis extracts, 0.5-1
Part protease, 0.5-1 parts of aminopeptidases, 1-2 parts of camomile extracts, 1-2 parts of licorices, 1-3 parts of yeast polypeptides, 2-4
Part tip edge bladder-wrack extract, 1-3 parts of oligopeptides -20,0.5-1 parts of carbomers, 0.6-2 parts of aminomethyl propanols, 3-6 parts of propylene glycol,
3-6 parts of 1,3 butylene glycols, 0.5-1 parts of Cremophor RH40s, 0.5-1 parts of blumea oils, 0.5-1 parts of glycerol caprylates,
0.1-0.2 parts of methyl hydroxybenzoates, 0.1-0.2 parts of allantoins, 0.02-0.1 parts of EDETATE SODIUMs, 0.03-0.1 parts of Sodium Hyaluronates, 70-
100 parts of deionized waters；
Step 3：It weighs in deionized water to water phase pot, sequentially adds the measured EDETATE SODIUM of accurate scale, hyaluronic acid
Sodium, carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3-
Butanediol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；
Step 4：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, under stirring successively
It is more that decoloration red algae extract, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast is added
Peptide, tip edge bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；
Step 5：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, octanoic acid is added
Glyceride, and stir；
Step 6：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, then cold
But to room temperature to get lotion.
Preferably, the propolis extract is nanometer supercritical bee-glue.
It is further preferred that the nanometer supercritical bee-glue is the nanometer being process by Phospholipids nano-encapsulated technology
Supercritical bee-glue.
Preferably, the licorice is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtains powder
The NaOH aqueous solutions of a concentration of 0.2mol/L are added in body, are 1 by solid-to-liquid ratio:10 ratios mix, the hot dipping extraction 2h at 80 DEG C,
It is repeated 2 times, filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifuged under the rotating speed of 4000r/min
Separation, goes supernatant to obtain sediment, as licorice.
Preferably, the camomile extract is prepared using following methods：5g chamomiles are crushed, sieving, obtains powder
The NaOH aqueous solutions of a concentration of 0.2mol/L are added in body, are 1 by solid-to-liquid ratio:10 ratios mix, the hot dipping extraction 2h at 80 DEG C,
It is repeated 2 times, filters, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, is centrifuged under the rotating speed of 4000r/min
Separation, goes supernatant to obtain sediment, as camomile extract.
Preferably, the tip edge bladder-wrack extract is prepared using following methods：Tip edge bladder-wrack is washed, is put
It sets and is air-dried at aeration-drying, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, moderate heat dries 4min, after drying
Tip edge bladder-wrack be put into pulverizer and crush, the tip edge bladder-wrack after crushing is crossed into 60 mesh sieve, tip edge bladder-wrack powder is obtained, weighs
Tip edge bladder-wrack powder 10g, deionized water 100g, are added to the container, and extraction 100min are decocted at 90 DEG C, by the substance in container
It all takes out, is cooled to room temperature, filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, in collection
Clear liquid obtains tip edge bladder-wrack extract after filtering.
It is further preferred that described is filtered into three layers of filtered through gauze.
It is further preferred that being filtered using the membrane filter in 0.2 μm of aperture after three layers of filtered through gauze.
Preferably, the grinding and sieving was 40 mesh sieve.
The beneficial effects of the present invention are：
1) red algae extract contains a large amount of uvioresistant active material, and anti-uv-ray is good, plays good chemistry
Anti-sunlight function.
2) Radix Glycyrrhizae and chamomile have clearing heat and detoxicating, and antibacterial anti-inflammatory pacifies calm effect, are suitble to various skin, especially
It is suitble to sensibility skin, can be used for the impaired skin of after-sun.
3) present invention uses nanometer supercritical bee-glue, it is easy to which infiltration and absorption successfully solve and other ingredients
Compatibility issues, nanometer supercritical bee-glue have the function of that strength is anti-oxidant, inhibit tyrosinase activity, and whitening spot-removing effect is aobvious
It writes.
4) tip edge bladder-wrack can provide the required natural nutrient needed for skin rapid regeneration and cell normal growth, Replacement Battalion
Foster loss promotes skin metabolism, increases the ATP synthesis of skin energy element；It protects skin cell mitochondria and maintains line grain
Body function；Promote skin revitalization, skin is helped to reply health and vigor.
Specific implementation mode
With reference to embodiments, the technical solution in the present invention is clearly and completely described.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
A kind of preparation method of the after-sun lotion of the red algae extract containing decoloration, includes the following steps：
Step 1：After Sargassum horneri is cleaned up, drying crushes to obtain algae powder, by algae powder and ethanol solution according to 1：15-20w/
The solid-liquid ratio of v is uniformly mixed, and maintains the temperature at 40-50 DEG C, and extracting solution, extracting solution heating are extracted 4-6 hours to obtain under stirring condition
To 60-70 DEG C, it is ultrasonically treated 10-15min, filtering and impurity removing, filter vacuum is concentrated under reduced pressure into the 10-20% of original volume, and spraying is dry
Red algae extract is obtained after dry, and the red algae extract that mass concentration is 69-72% will be configured to after red algae extract plus deionized water
Solution, is then added decolorising agent into red algae extract solution, and decolorising agent dosage is the 6%- of red algae extract solution weight
8%, it is stirred 2-3 hours, decoloration red algae extract is obtained after flame filter press filtering；The mass concentration of the ethanol solution
For 85%-90%；The speed of the stirring is 80-100r/min；The power of the ultrasound is 300-400w；The decolorising agent by
Activated carbon and diatomite mixing composition, the activated carbon：Diatomaceous weight ratio is 2-4:1；
Step 2：Raw material is matched by weight：2-4 parts of decoloration red algae extracts, 2-4 parts of propolis extracts, 0.5-1
Part protease, 0.5-1 parts of aminopeptidases, 1-2 parts of camomile extracts, 1-2 parts of licorices, 1-3 parts of yeast polypeptides, 2-4
Part tip edge bladder-wrack extract, 1-3 parts of oligopeptides -20,0.5-1 parts of carbomers, 0.6-2 parts of aminomethyl propanols, 3-6 parts of propylene glycol,
3-6 parts of 1,3 butylene glycols, 0.5-1 parts of Cremophor RH40s, 0.5-1 parts of blumea oils, 0.5-1 parts of glycerol caprylates,
0.1-0.2 parts of methyl hydroxybenzoates, 0.1-0.2 parts of allantoins, 0.02-0.1 parts of EDETATE SODIUMs, 0.03-0.1 parts of Sodium Hyaluronates, 70-
100 parts of deionized waters；
Step 3：It weighs in deionized water to water phase pot, sequentially adds the measured EDETATE SODIUM of accurate scale, hyaluronic acid
Sodium, carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3-
Butanediol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；
Step 4：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, under stirring successively
It is more that decoloration red algae extract, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast is added
Peptide, tip edge bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；
Step 5：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, octanoic acid is added
Glyceride, and stir；
Step 6：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, then cold
But to room temperature to get lotion.
The propolis extract is nanometer supercritical bee-glue.The nanometer supercritical bee-glue is wrapped by Phospholipids nanometer
The nanometer supercritical bee-glue that the technology of wrapping up in is process.
The licorice is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtain powder, is added
The NaOH aqueous solutions of a concentration of 0.2mol/L are 1 by solid-to-liquid ratio:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times at 80 DEG C,
Filtering, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, centrifuges, goes under the rotating speed of 4000r/min
Supernatant obtains sediment, as licorice.
The grinding and sieving was 40 mesh sieve.
The camomile extract is prepared using following methods：5g chamomiles are crushed, sieving, obtain powder, is added
The NaOH aqueous solutions of a concentration of 0.2mol/L are 1 by solid-to-liquid ratio:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times at 80 DEG C,
Filtering, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, centrifuges, goes under the rotating speed of 4000r/min
Supernatant obtains sediment, as camomile extract.
The grinding and sieving was 40 mesh sieve.
The tip edge bladder-wrack extract is prepared using following methods：Tip edge bladder-wrack is washed, is placed on logical
It air-dries dry place to be air-dried, the tip edge bladder-wrack after air-drying is placed in micro-wave oven, moderate heat dries 4min, by the tip edge after drying
Bladder-wrack is put into pulverizer and crushes, and the tip edge bladder-wrack after crushing is crossed 60 mesh sieve, obtains tip edge bladder-wrack powder, weighs tip edge ink
Angle algae powder 10g, deionized water 100g, are added to the container, and extraction 100min is decocted at 90 DEG C, the substance in container is all taken
Go out, be cooled to room temperature, filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, collects supernatant, mistake
After filter tip edge bladder-wrack extract, it is described to be filtered into three layers of filtered through gauze, using 0.2 after described three layers of filtered through gauze
The membrane filter filtering in μm aperture.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above,
As long as using the improvement of the various unsubstantialities of inventive concept and technical scheme of the present invention progress, or not improved this is sent out
Bright design and technical solution directly applies to other occasions, within protection scope of the present invention.The protection of the present invention
Range should be determined by the scope of protection defined in the claims.
Claims (9)
1. a kind of preparation method of the after-sun lotion of the red algae extract containing decoloration, which is characterized in that include the following steps：
Step 1：After Sargassum horneri is cleaned up, drying crushes to obtain algae powder, by algae powder and ethanol solution according to 1：15-20w/v's
Solid-liquid ratio is uniformly mixed, and maintains the temperature at 40-50 DEG C, and extracting solution is extracted 4-6 hours to obtain under stirring condition, and extracting solution is warming up to
60-70 DEG C, it is ultrasonically treated 10-15min, filtering and impurity removing, filter vacuum is concentrated under reduced pressure into the 10-20% of original volume, is spray-dried
Red algae extract is obtained afterwards, and it is molten that the red algae extract that mass concentration is 69-72% will be configured to after red algae extract plus deionized water
Then decolorising agent is added in liquid into red algae extract solution, decolorising agent dosage is the 6%-8% of red algae extract solution weight,
It is stirred 2-3 hours, decoloration red algae extract is obtained after flame filter press filtering；The mass concentration of the ethanol solution is
85%-90%；The speed of the stirring is 80-100r/min；The power of the ultrasound is 300-400w；The decolorising agent is by living
Property charcoal and diatomite mixing composition, the activated carbon：Diatomaceous weight ratio is 2-4:1；
Step 2：Raw material is matched by weight：2-4 portions of decoloration red algae extracts, 2-4 parts of propolis extracts, 0.5-1 portions of eggs
White enzyme, 0.5-1 parts of aminopeptidases, 1-2 parts of camomile extracts, 1-2 parts of licorices, 1-3 parts of yeast polypeptides, 2-4 parts of teeth
Edge bladder-wrack extract, 1-3 parts of oligopeptides -20,0.5-1 parts of carbomers, 0.6-2 parts of aminomethyl propanols, 3-6 parts of propylene glycol, 3-6 parts
1,3 butylene glycol, 0.5-1 part Cremophor RH40,0.5-1 parts of blumea oils, 0.5-1 parts of glycerol caprylates, 0.1-0.2
Part methyl hydroxybenzoate, 0.1-0.2 parts of allantoins, 0.02-0.1 parts of EDETATE SODIUMs, 0.03-0.1 parts of Sodium Hyaluronates, 70-100 parts go
Ionized water；
Step 3：Weigh in deionized water to water phase pot, sequentially add the measured EDETATE SODIUM of accurate scale, Sodium Hyaluronate,
Carbomer, and heating mixes while stirring, is sufficiently stirred and is uniformly dissolved under temperature 60 C, sequentially adds propylene glycol, 1,3- fourths
Glycol, methyl hydroxybenzoate, allantoin, temperature 60 C keep the temperature 30 minutes；
Step 4：In temperature 60 C, material in water phase pot is pumped into vacuum emulsifying pot, is sequentially added under stirring
Decolourize red algae extract, propolis extract, protease, aminopeptidase, camomile extract, licorice, yeast polypeptides, tooth
Edge bladder-wrack extract, oligopeptides -20 stir 30 minutes, are sufficiently mixed uniformly；
Step 5：It cools, when temperature drops to 45 DEG C, Cremophor RH40, blumea oil, sad glycerine is added
Ester, and stir；
Step 6：Continue to cool down, when temperature drops to 35 DEG C, aminomethyl propanol is added, and stir, is cooled to
Room temperature is to get lotion.
2. a kind of preparation method of the after-sun lotion of red algae extract containing decoloration according to claim 1, feature
It is：The propolis extract is nanometer supercritical bee-glue.
3. a kind of preparation method of the after-sun lotion of red algae extract containing decoloration according to claim 2, feature
It is：The nanometer supercritical bee-glue is the nanometer supercritical bee-glue being process by Phospholipids nano-encapsulated technology.
4. a kind of preparation method of the after-sun lotion of red algae extract containing decoloration according to claim 1, feature
It is, the licorice is prepared using following methods：5g licorice medicinal materials are crushed, sieving, obtain powder, concentration is added
It is 1 by solid-to-liquid ratio for the NaOH aqueous solutions of 0.2mol/L:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times, mistake at 80 DEG C
Filter, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, centrifuges, goes under the rotating speed of 4000r/min
Clear liquid obtains sediment, as licorice.
5. a kind of preparation method of the after-sun lotion of red algae extract containing decoloration according to claim 1, feature
It is, the camomile extract is prepared using following methods：5g chamomiles are crushed, sieving, obtain powder, concentration is added
It is 1 by solid-to-liquid ratio for the NaOH aqueous solutions of 0.2mol/L:10 ratios mix, and hot dipping extraction 2h, is repeated 2 times, mistake at 80 DEG C
Filter, it is 3% hydrochloric acid tune pH value to 1-2.5 that mass concentration is added in filtrate, centrifuges, goes under the rotating speed of 4000r/min
Clear liquid obtains sediment, as camomile extract.
6. a kind of preparation method of the after-sun lotion of red algae extract containing decoloration according to claim 1, feature
It is, the tip edge bladder-wrack extract is prepared using following methods：Tip edge bladder-wrack is washed, it is dry to be placed on ventilation
Dry place is air-dried, and the tip edge bladder-wrack after air-drying is placed in micro-wave oven, and moderate heat dries 4min, by the tip edge ink angle after drying
Algae is put into pulverizer and crushes, and the tip edge bladder-wrack after crushing is crossed 60 mesh sieve, tip edge bladder-wrack powder is obtained, weighs tip edge bladder-wrack
Powder 10g, deionized water 100g, are added to the container, and extraction 100min is decocted at 90 DEG C, and the substance in container is all taken out,
It is cooled to room temperature, is filtered with cryogenic freezing centrifuge, rotating speed 3000r/min, centrifugation time 5min, supernatant, filtering are collected
Tip edge bladder-wrack extract is obtained afterwards.
7. a kind of preparation method of the after-sun lotion of red algae extract containing decoloration according to claim 6, feature
It is：Described is filtered into three layers of filtered through gauze.
8. a kind of preparation method of the after-sun lotion of red algae extract containing decoloration according to claim 7, feature
It is：It is filtered using the membrane filter in 0.2 μm of aperture after three layers of filtered through gauze.
9. a kind of preparation method of the after-sun lotion of red algae extract containing decoloration according to claim 4 or 5, special
Sign is：The grinding and sieving was 40 mesh sieve.
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104224650A (en) * | 2014-06-05 | 2014-12-24 | 温州医科大学 | Large seaweed extract sunscreen skin care emulsion and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104224650A (en) * | 2014-06-05 | 2014-12-24 | 温州医科大学 | Large seaweed extract sunscreen skin care emulsion and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 杨跃飞: "一种含纳米超临界蜂胶美白淡斑精华素及其制备方法", 《中国蜂业》 * |
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Application publication date: 20181106 |