CN1087245A - Additive for filter tip of cigarette and preparation thereof and adding method - Google Patents
Additive for filter tip of cigarette and preparation thereof and adding method Download PDFInfo
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- CN1087245A CN1087245A CN 92113748 CN92113748A CN1087245A CN 1087245 A CN1087245 A CN 1087245A CN 92113748 CN92113748 CN 92113748 CN 92113748 A CN92113748 A CN 92113748A CN 1087245 A CN1087245 A CN 1087245A
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- additive
- adsorbent
- binding agent
- filter tip
- cigarette
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Abstract
Additive for filter tip of cigarette and preparation thereof and adding method is characterized in that said additive is made up of the homogeneous mixture of adsorbent and binding agent, and adsorbent content is 1-20%, and surplus is a binding agent.Said adsorbent is Al
2O
3, that selects in the nontoxic inorganic porous material powder such as zeolite is at least a, and binding agent is triacetyl glycerine or carboxymethyl cellulose aqueous solution.Adsorbent mixes with binding agent after the activation of heating again, is sprayed onto equably on Filter tip shaping machine after stirring in the mouth rod matrix again.During additive of the present invention is specially adapted to, rudimentary quality cigarette, can obviously reduce the tar content in its flue gas, improve the smoking mouthfeel.
Description
The present invention relates to cigarette, particularly in, use and the preparation and the adding method of the filter tip material of rudimentary quality cigarette.
Contain multiple harmful composition in the cigarette, particularly in, content of harmful such as the tar in the rudimentary quality cigarette, carbon monoxide, aldehydes is higher, and is bigger to smoker's health hazard.In order to reduce the harm of these harmful components to health, people have taked some measures.For example now being commonly the tobacco smoke filter element that various countries production of cigarettes person adopted chews.It is by acetate fiber, or polypropylene fibre, perhaps nonwoven polypropylene fabric, and perhaps composite is that matrix is made.Filter tip is connected on the cigarette, and the smoker can reduce the tar content of suction to a certain extent by filter tip smoking.But because cigarette burning is insufficient, the carbon monoxide soakage increases on the contrary to some extent.For this reason, the production of cigarettes person who has adds some additives again in filter tip, in the hope of reducing the harmful components in the cigarette smoke effectively.Mild Seven (Mild Seven) cigarette that Japan produces just is added with active carbon in its filter tip.It utilizes the suction-operated of active carbon, the harmful components in the absorption flue gas.China's big slab bridge in Kunming is chewed the filter tip that excellent factory (Britain's import complete set of equipments) produces, and wherein also is the active carbon that adds.But, since used active carbon be black and particle bigger, it conflicts mutually with the white of chewing excellent matrix, consumer psychology be difficult to acceptance.For this reason, add the filter tip of active carbon, generally by two sections compositions, one section that joins with cigarette for having added the rod of chewing of active carbon, with the contacted one section common rod of chewing that does not add any additives for white in smoking people oral cavity.So just increased production process, made complicated operationization, production cost also increases to some extent.In addition, the two-period form filter tip that is added with active carbon that the big slab bridge in Kunming is chewed the production of excellent factory is used on certain cigarette of Kunming factory production, though reduced the tar content in the flue gas, the taste of cigarette is also thin out, and the consumer also is difficult to accept.
The objective of the invention is to overcome the deficiency of above-mentioned prior art, a kind of new have optionally filter tip additive and preparation and adding method are provided.Additive of the present invention both can reduce the tar content in the cigarette smoke effectively, and in keeping normal smoke again and suitably improving, the mouthfeel of rudimentary quality cigarette, and the preparation method is simple and easy, and production cost is low.
Technical solution of the present invention is: with nontoxic white or subalbous inorganic porous material powder as adsorbent, with organic compound as binding agent, the homogeneous mixture of the two is as additive with filter tip, add among the filter tip matrix material, suction-operated by porous mass further reduces tar and other aldehydes content in the cigarette smoke, when reducing harmful components, and in improving, the mouthfeel of rudimentary quality cigarette.
Feature of the present invention is: said additive is made up of the homogeneous mixture of adsorbent and binding agent, and the content of said adsorbent in said mixture is 1-20(weight) %, surplus is a binding agent; The content of the preferential adsorbent of recommending is 3-15(weight) %, surplus is a binding agent.Said adsorbent is select from inorganic porous material powders such as white or subalbous alundum (Al, zeolite, kaolin, diatomite, magnesia, calcium oxide, silica, titanium dioxide, alkali carbonate at least a, said binding agent is select from triacetyl glycerine, carboxymethyl cellulose (CMC) aqueous solution a kind of, the granularity of said absorbent powder is≤150 orders, and preferential powder size of recommending is between the 200-300 order.
In additive, add adsorbent, its effect mainly is the suction-operated that utilizes its highly active numerous micropores, optionally filter tar and aldehyde material in the flue gas, not only reduce tar content but also keep cigarette active ingredient thereby reach, and play the effect that improves mouthfeel.Therefore, if the content of adsorbent＜1% then a little less than the suction-operated of additive, can not effectively reduce the content of harmful components; And content＞20% o'clock, then will be when reducing tar content, make that nicotine also obviously reduces in the cigarette, thereby make smoke thin out, the consumer can not welcome yet.Simultaneously, the difference of adsorbent composition also will produce significant impact to this.The effect of binding agent, the one, adsorbent is attached among the filter tip matrix material very securely, the 2nd, matrix material is welded together to a certain extent, increase the rigidity and the intensity of chewing rod.
The preparation method of additive of the present invention is as follows:
1, said adsorbent material is pulverized, ground, and sieve, take minus sieve powder with 150 mesh sieve; The most handy 200 orders and 300 mesh sieve sieve for twice, take the powder between the 200-300 order;
2, powder activation: the qualified powder after the above-mentioned screening is heated to 300-500 ℃ in electric furnace, is incubated 4-10 hour, it is fully activated, cool off with stove then;
3, the powder after will activating joins in triacetyl glycerine or the carboxymethyl cellulose aqueous solution, fully stirs, and forms highly homodisperse suspension mixture, and in this mixture, said absorbent powder content is 1-20(weight) %.
The adding method of said additive is:
1, with filter rod matrix material (acetate fiber, polypropylene fibre or composite etc.) complete loose opening on the filter stick make-up machine;
2, according to the weight ratio matrix material: additive=1: the 0.08-0.2 ratio is spread across additive agent mixture in the matrix material equably and goes;
3, spill matrix material machine-shaping on the filter rod make-up machine of additive, air dry 6-15 hour, promptly became the filter rod finished product.
Two kinds of components of said additive also can be sprayed onto respectively in the matrix, promptly spray binding agent earlier, spray adsorbent subsequently again.
Compare with existing filter tip additive, the present invention has following advantage:
1, make filter tip with additive of the present invention, only need make the uniform filter tip of one-part form, need not make two-period form, its color and luster is with filter tip matrix material unanimity, thereby simplified production technology, reduced production cost;
2, can reduce tar and aldehyde matter content in the flue gas effectively, thereby alleviate in the cigarette harmful components the harm of human body.Paperback " Kun Hu " the board cigarette that side such as Kun Ming volume Factory branch are produced, not additivated cigarette in the filter tip, its tar content are 20.22 milligrams/, and have added 8% A
12O
3Filter tip, tar content in its flue gas has dropped to 17.32 milligrams/, and mouthfeel is obviously improved, reduced the acid in the flue gas, smoke panel test through expert and many people, its mouthfeel is obviously improved, and many people think and are equivalent to " camellia " or Yuxi Yan Chang " red plum " the board cigarette that Kunming Cigarette Factory is produced, and are equivalent to make " Kun Hu " cigarette to improve 1-2 class.
Embodiment 1-15
Press listed each additive component of table 1, adsorbent is pulverized, grinds, sieved, wherein embodiment 1-5 crosses 200 mesh sieves, embodiment 6-7 crosses 150 mesh sieves, embodiment 8-15 crosses 200 orders, twice screening of 300 orders, the powder activation after the screening, activation condition: 400 ℃ of insulations of embodiment 1-5 6 hours, 350 ℃ of insulations of embodiment 6-7 10 hours, 500 ℃ of insulations of embodiment 8-15 7 hours.Absorbent powder after the activation adds in the triacetyl glycerine or carboxymethyl cellulose (CMC) aqueous solution by the listed data of table 1, stirs.Data by table 1 evenly are sprayed onto additive in the filter tip matrix material (acetate fiber) on the filter rod make-up machine then, machine-shaping, air dry 6-15 hour.The finished product filter tip is contained on paperback " Kun Hu " the board cigarette of Kun Ming volume Factory branch production, extract flue gas (at every turn testing 4 cigarettes) with the self-control smoke extractor, filter out the tar in the flue gas, take by weighing tar weight with precision balance, calculate the average tar content in every cigarette, and and the not tar content of additivated cigarette (20.24 millimeters /) contrast, its result is as shown in table 1.From table 1 result as seen, add the filter tip of additive of the present invention, the tar content in the cigarette has obviously been reduced, and reduced the strange taste of cigarette, improved the mouthfeel of smoking.
Claims (8)
1, a kind of tobacco smoke filter element is chewed additive, said additive adds among the filter tip matrix material in producing the filter tip process, it is characterized in that: said additive is made up of the homogeneous mixture of adsorbent and binding agent, the content of said adsorbent in said mixture is 1-20 (weight) %, surplus is said binding agent, said adsorbent is from nontoxic white or subalbous alundum (Al, zeolite, kaolin, diatomite, magnesia, calcium oxide, silica, titanium dioxide, that selects in the inorganic porous material powder such as alkali carbonate is at least a, and said binding agent is from triacetyl glycerine, that selects in carboxymethyl cellulose (CMC) aqueous solution is a kind of.
2, additive as claimed in claim 1 is characterized in that the content of said adsorbent in said additive is 3-15(weight) %, surplus is said binding agent.
3,, it is characterized in that said absorbent powder granularity≤150 orders as the additive of claim 1 and 2.
4,, it is characterized in that said absorbent powder granularity is between the 200-300 order as the additive of claim 1 and 2.
5, additive as claimed in claim 3, the granularity that it is characterized in that said absorbent powder is between the 200-300 order.
6, a kind of tobacco smoke filter element is chewed the preparation method of additive, it is characterized in that the operation of said method is:
6.1 said adsorbent material is pulverized, is ground, sieves (150 orders, best 200 and 300 orders sieve for twice);
6.2 powder activation: the qualified powder of 6.1 operations screening gained is heated to 300-500 ℃ in electric furnace, is incubated 4-10 hour, it is fully activated, be cooled to suitable temperature with stove subsequently;
6.3 the powder after the 6.2 operations activation is joined among the triacetyl glycerine, perhaps among the carboxymethyl cellulose aqueous solution, fully stir, form highly homodisperse suspension mixture, in this mixture, the content of said absorbent powder is 1-20(weight) %;
7, a kind of tobacco smoke filter element is chewed the adding method of additive, it is characterized in that:
7.1 with filter rod matrix material (acetate fiber, polypropylene fibre, composite etc.) complete loose opening on the filter rod make-up machine;
7.2 according to the weight ratio matrix material: the ratio of additive=1: 0.08-0.2 is spread across additive agent mixture in the matrix material equably and goes;
7.3 spilt matrix material machine-shaping on the filter rod make-up machine of additive, air dry 6-15 hour, promptly became the filter rod finished product.
8, additive adding method as claimed in claim 7 is characterized in that adsorbent in the said additive agent mixture and binding agent can be taken up in order of priority to be sprayed onto in the filter tip matrix material, promptly sprays binding agent earlier, then sprays adsorbent again.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92113748 CN1087245A (en) | 1992-11-27 | 1992-11-27 | Additive for filter tip of cigarette and preparation thereof and adding method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92113748 CN1087245A (en) | 1992-11-27 | 1992-11-27 | Additive for filter tip of cigarette and preparation thereof and adding method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1087245A true CN1087245A (en) | 1994-06-01 |
Family
ID=4946585
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 92113748 Pending CN1087245A (en) | 1992-11-27 | 1992-11-27 | Additive for filter tip of cigarette and preparation thereof and adding method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1087245A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101862037A (en) * | 2010-05-28 | 2010-10-20 | 华南理工大学 | Preparation method and application of hexagonal mesoporous monox coated nano-TiO2 composite material |
| CN101438851B (en) * | 2008-12-29 | 2011-08-31 | 浙江中烟工业有限责任公司 | Method for reducing dry sensation of cigarette smoke |
| CN102499474A (en) * | 2011-10-31 | 2012-06-20 | 益阳科嘉轻工机械制造有限公司 | Cigarette filter tip firming method |
| CN101262785B (en) * | 2005-09-14 | 2012-10-03 | R.J.雷诺兹烟草公司 | Filtered smoking article |
| CN103393218A (en) * | 2013-08-06 | 2013-11-20 | 上海华宝生物科技有限公司 | Solid-type filter stick formed by granular assembling and preparation method thereof |
| CN105967645A (en) * | 2016-05-09 | 2016-09-28 | 黄贵鑫 | Nanometer compound ceramic material with high adsorptivity as well as preparation method and application thereof |
| CN112678833A (en) * | 2020-11-17 | 2021-04-20 | 广西中烟工业有限责任公司 | Nano-silica modified squalene organic silicon particles and preparation and use methods thereof |
-
1992
- 1992-11-27 CN CN 92113748 patent/CN1087245A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101262785B (en) * | 2005-09-14 | 2012-10-03 | R.J.雷诺兹烟草公司 | Filtered smoking article |
| CN101438851B (en) * | 2008-12-29 | 2011-08-31 | 浙江中烟工业有限责任公司 | Method for reducing dry sensation of cigarette smoke |
| CN101862037A (en) * | 2010-05-28 | 2010-10-20 | 华南理工大学 | Preparation method and application of hexagonal mesoporous monox coated nano-TiO2 composite material |
| CN101862037B (en) * | 2010-05-28 | 2012-05-09 | 华南理工大学 | Preparation method and application of hexagonal mesoporous silica coated nano titanium oxide composite material |
| CN102499474A (en) * | 2011-10-31 | 2012-06-20 | 益阳科嘉轻工机械制造有限公司 | Cigarette filter tip firming method |
| CN103393218A (en) * | 2013-08-06 | 2013-11-20 | 上海华宝生物科技有限公司 | Solid-type filter stick formed by granular assembling and preparation method thereof |
| CN105967645A (en) * | 2016-05-09 | 2016-09-28 | 黄贵鑫 | Nanometer compound ceramic material with high adsorptivity as well as preparation method and application thereof |
| CN105967645B (en) * | 2016-05-09 | 2019-04-19 | 黄贵鑫 | A kind of Nano compound ceramic material of high adsorption and preparation method thereof, application |
| CN112678833A (en) * | 2020-11-17 | 2021-04-20 | 广西中烟工业有限责任公司 | Nano-silica modified squalene organic silicon particles and preparation and use methods thereof |
| CN112678833B (en) * | 2020-11-17 | 2023-08-04 | 广西中烟工业有限责任公司 | Nano silicon dioxide modified squalene organic silicon particles and preparation and use methods thereof |
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