CN101438851B - Method for reducing dry sensation of cigarette smoke - Google Patents
Method for reducing dry sensation of cigarette smoke Download PDFInfo
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- CN101438851B CN101438851B CN2008102337705A CN200810233770A CN101438851B CN 101438851 B CN101438851 B CN 101438851B CN 2008102337705 A CN2008102337705 A CN 2008102337705A CN 200810233770 A CN200810233770 A CN 200810233770A CN 101438851 B CN101438851 B CN 101438851B
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Abstract
A method for reducing the dry sensation of cigarette smoke relates to a technique for producing cigarettes, in particular to the technique for improving the dry sensation of the cigarette smoke. The method comprises the following steps: mixing adsorbent and feed liquid, or diluting separately with water and adding to tobacco shreds, stems or sheets in the form of the feed liquid on the basis of the feeding process of cigarettes, wherein, the weight percentage is 0.1% to 0.4%. The main ingredients and the composition structure of the absorbent prepared by the technical scheme of the invention are close to the natural tobacco and hardly influence the flavor generated by burning and smoking the cigarettes. The adsorbent can preferentially adsorb and combine small molecules and strong-polarity substances by spatial structure selection and binding group selection, thereby having the function of preferential adsorption on undesirable components in the cigarette smoke, such as formaldehyde, ammonia and the like. Compared with the prior art, the process of the absorption belongs to chemical absorption, and has the characteristics of high selectivity and strong adsorbability, moreover, the method can be directly applied to the tobacco shreds, stems or sheets, thereby ensuring high use value.
Description
Technical field
The present invention relates to a kind of technology of production of cigarettes, particularly a kind of technology of improving dry sensation of cigarette smoke.
Background technology
The part cigarette still has strong dry sensation in place suction with the humid air.Discover, can cause bad impressions such as drying, stimulation when harmful components such as formaldehyde, ammonia reach certain content in the cigarette smoke, reducing these undesirable constituents is the important channels that reduce dry sensation of cigarette smoke, improve comfort level.
The existing technology that reduces dry sensation of cigarette smoke, excitant, the sense of minimizing flue gas drying mainly contains two classes: the first is added activated carbon, attapulgite, nano adsorption material etc. in cigarette filter rod.Utilize the physical absorption function of material, purpose is to adsorb the harmful and excitant composition that reduces in the flue gas, still, because this type of sorbing material is to the suction-operated shortage selectivity of smoke components, cause in the flue gas loss of a large amount of aroma components, cause cigarette smoke jealous thin out, fragrance is not enough; It two is to add plant extracts in pipe tobacco.Extract absorbed air moisture increases the pipe tobacco adsorbed water, reaches the humidification humectation effect to pipe tobacco.This class technology is a purpose to increase the pipe tobacco specific retention, and water soluble ingredients such as flue gas moisture PARA FORMALDEHYDE PRILLS(91,95), ammonia have certain adsorption-buffering effect, but excess water causes cigarette perfume (or spice) thin, and flammability descends, can not fine solution flue gas drying problem.
Chinese patent application number is that 200810073565.7 patent of invention discloses natural tobacco additive of a kind of flavouring and its production and application, this invention relates to a kind of flavouring, mends natural tobacco additive of fragrant and wound perfume and its production and application, its primary raw material is: safflower, its preparation method is to prepare croceous extract earlier, decompression concentrates and makes additive again, with the natural tobacco additive that makes, be used for the production of cigarette in the ratio of 10ppm～0.1% of pipe tobacco weight.Additive of the present invention has the cigarette product of making, particularly low burnt cigarette product flavouring, fragrant, the wound perfume of benefit, promote note, set off nature cigarette perfume (or spice), reduce the flue gas drying sense, improve the cigarette comfort level, alleviate the natural tobacco additive of harmfulness of smoking, main active ingredient is saffron glucoside-1, and its content is: 1.0ng～0.10mg/ props up.But adopt medicinal material as additive, can have influence on the taste of cigarette.
To studies show that of dry sensation of cigarette smoke mechanism, undesirable constituents such as formaldehyde, ammonia are the important sources of causing the flue gas drying sense.Technology is looked into new demonstration, reduces the content of dry sensation of cigarette smoke, raising comfort level by harmful components such as minimizing formaldehyde, ammonias and does not appear in the newspapers.
Summary of the invention
Purpose of the present invention is intended to overcome the defective of prior art, a kind of pointed adsorbent is provided, by strong little minute subconstiuents of polarity such as the formaldehyde in an amount of absorption minimizing flue gas, ammonias, reach the method that reduces the flue gas drying sense, improves the reduction dry sensation of cigarette smoke of cigarette comfort level.The adsorbent constituent does not influence natural cigarette perfume (or spice) near the natural composition of tobacco.
The method of reduction dry sensation of cigarette smoke of the present invention is in cigarette charging technology, adsorbent is mixed with feed liquid or separately behind the dilute with water, adds on pipe tobacco, stem or the thin slice with the feed liquid form, and the percentage by weight of consumption is 0.1-0.4%.
The component of described adsorbent is: soluble sugar 5-15 gram, soluble protein 5-10 gram, water 100 grams, polyphenol 1-5 gram.
A kind of method that reduces dry sensation of cigarette smoke, the preparation of adsorbent method is:
A. take by weighing soluble sugar 5-15 gram, soluble protein 5-10 gram, water 100 gram mixing, regulate PH7-12 with NaOH;
B. heat, stirred 2 hours;
C. the cooling back adds composite organic acid to PH4-7, adds polyphenol 1-5 gram, places 6-10 hour in 30-40 ℃ behind the stirring and evenly mixing;
D. add NaOH and regulate pH value, stir salinization and made the adsorbent aqueous solution in 2 hours.
Described the heating of step b is 90-120 ℃.
The pH value of the described adjusting of steps d is 7-10.
With method for preparing and adsorbent be applied on pipe tobacco, stem or the thin slice, in cigarette charging technology, adsorbent mixed with feed liquid or independent dilute with water after, add on the pipe tobacco consumption 0.1-0.4% to the feed liquid form.
The method of reduction dry sensation of cigarette smoke of the present invention, be to mix with natural soluble sugar, soluble protein, carry out appropriate Maillard reaction, be cross-linked to form the protein-polysaccharide covalent compound, add composite organic acid, polyphenol again,, form polysaccharide, protein, polyphenol, the copolymerized thing of organic acid by intermolecular graft copolymerization, water-soluble with small amount of alkali appropriateness salinization raising again, make selective absorbent.This adsorbent has three-dimensional cross-linked network structure, can only hold little molecule and enter, and strong polar component such as the many carboxyls in the space, polyhydroxy PARA FORMALDEHYDE PRILLS(91,95), ammonia has the function of preferential selection absorption combination.Adsorbent main component that adopts technical scheme preparation of the present invention and get and composition structure are near the tobacco native state, and cigarette is burnt and sucked fragrance does not have influence substantially.Adsorbent by space structure select, conjugated group selects, and preferentially selects absorption in conjunction with little molecule, strong polar substances, and undesirable constituents such as the formaldehyde in the flue gas, ammonia are had the selective absorption function.Compared with the prior art, adsorption process is a chemisorbed, has selectivity height, characteristics that absorption affinity is strong, and can directly add on pipe tobacco, stem, thin slice and use, and practical value is higher.
The demonstration of smokeing panel test: flue gas drying sense, excitant obviously reduce, and cigarette is fragrant natural mellow and full.Add and use comparative sample, detect through environmental monitoring center, Kunming, the result shows: formaldehyde decreased average 42% in the cigarette smoke, ammonia level decreased average 31%.
The specific embodiment
The present invention is described further below in conjunction with embodiment, but be not limited to embodiment.
Embodiment 1
The method of reduction dry sensation of cigarette smoke of the present invention, the component of described adsorbent is: soluble sugar 15 grams, soluble protein 5 grams, water 100 grams, polyphenol 1 gram.Its preparation method is
A. take by weighing soluble sugar 15 grams, soluble protein 5 grams, water 100 gram mixing, regulate PH7 with NaOH;
B. heat to 90 ℃, stirred 2 hours;
C. the cooling back adds composite organic acid to PH7, adds polyphenol 1 gram, places 6 hours 30-40 ℃ of night behind the stirring and evenly mixing;
D. add NaOH and regulate PH10, stir salinization and made the adsorbent aqueous solution in 2 hours.
The method of reduction dry sensation of cigarette smoke of the present invention is applied to adsorbent on the pipe tobacco, in the cigarette technology for making tobacco threds, adsorbent mixed with feed liquid or separately behind the dilute with water, adds on the pipe tobacco consumption 0.1% to the feed liquid form.
Embodiment 2
The method of reduction dry sensation of cigarette smoke of the present invention, the component of described adsorbent is: soluble sugar 5 grams, soluble protein 10 grams, water 100 grams, polyphenol 5 grams.Its preparation method is
A. take by weighing soluble sugar 5 grams, soluble protein 10 grams, water 100 gram mixing, regulate PH12 with NaOH;
B. heat to 20 ℃, stirred 2 hours;
C. the cooling back adds composite organic acid to PH4, adds polyphenol 5 grams, places 8 hours 30-40 ℃ of night behind the stirring and evenly mixing;
D. add NaOH and be adjusted to PH7, stir salinization and made the adsorbent aqueous solution in 2 hours.
The method of reduction dry sensation of cigarette smoke of the present invention is applied to adsorbent on the pipe tobacco, in the cigarette technology for making tobacco threds, adsorbent mixed with feed liquid or separately behind the dilute with water, adds on the pipe tobacco consumption 0.2% to the feed liquid form.
Embodiment 3
The method of reduction dry sensation of cigarette smoke of the present invention, the component of described adsorbent is: soluble sugar 10 grams, soluble protein 7 grams, water 100 grams, polyphenol 3 grams.Its preparation method is
A. take by weighing soluble sugar 10 grams, soluble protein 7 grams, water 100 gram mixing, regulate PH10 with NaOH;
B. heat to 115 ℃, stirred 2 hours;
C. the cooling back adds composite organic acid to PH5, adds polyphenol 3 grams, places 10 hours 30-40 ℃ of night behind the stirring and evenly mixing;
D. add NaOH and be adjusted to PH9, stir salinization and made the adsorbent aqueous solution in 2 hours.
The method of described reduction dry sensation of cigarette smoke, with adsorbent be applied to tobacco stem shred on, in tobacco stem shred charging technology, adsorbent mixed with feed liquid or separately behind the dilute with water, add on the stem consumption 0.3% to the feed liquid form
Embodiment 4
The method of reduction dry sensation of cigarette smoke of the present invention, the component of described adsorbent is: soluble sugar 9 grams, soluble protein 8 grams, water 100 grams, polyphenol 2 grams.Its preparation method is
A. take by weighing soluble sugar 9 grams, soluble protein 8 grams, water 100 gram mixing, regulate PH11 with NaOH;
B. heat to 100 ℃, stirred 2 hours;
C. the cooling back adds composite organic acid to PH6, adds polyphenol 2 grams, places 9 hours 30-40 ℃ of night behind the stirring and evenly mixing;
D. add NaOH and regulate PH8, stir salinization and made the adsorbent aqueous solution in 2 hours.
The method of described reduction dry sensation of cigarette smoke is applied to adsorbent on the reconstituted tobacoo, in the reconstituted tobacoo charging technology, adsorbent mixed with feed liquid or separately behind the dilute with water, adds on the thin slice consumption 0.4% to the feed liquid form.
Claims (4)
1. method that reduces dry sensation of cigarette smoke, it is characterized in that, be in cigarette charging technology, adsorbent mixed with feed liquid or separately behind the dilute with water, add on pipe tobacco, stem or the thin slice with the feed liquid form, the percentage by weight of consumption is 0.1-0.4%, the component of adsorbent is: soluble sugar 5-15 gram, soluble protein 5-10 gram, water 100 grams, polyphenol 1-5 gram.
2. the method for reduction dry sensation of cigarette smoke according to claim 1 is characterized in that, the preparation of adsorbent method is:
A. take by weighing soluble sugar 5-15 gram, soluble protein 5-10 gram, water 100 gram mixing, regulate PH7-12 with NaOH;
B. heat, stirred 2 hours;
C. the cooling back adds composite organic acid to PH4-7, adds polyphenol 1-5 gram, places 6-10 hour in 30-40 ℃ behind the stirring and evenly mixing;
D. add NaOH and regulate pH value, stir salinization and made the adsorbent aqueous solution in 2 hours.
3. the method for reduction dry sensation of cigarette smoke according to claim 3 is characterized in that, described the heating of step b is 90-120 ℃.
4. the method for reduction dry sensation of cigarette smoke according to claim 3 is characterized in that, the pH value of the described adjusting of steps d is 7-10.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008102337705A CN101438851B (en) | 2008-12-29 | 2008-12-29 | Method for reducing dry sensation of cigarette smoke |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008102337705A CN101438851B (en) | 2008-12-29 | 2008-12-29 | Method for reducing dry sensation of cigarette smoke |
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| Publication Number | Publication Date |
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| CN101438851A CN101438851A (en) | 2009-05-27 |
| CN101438851B true CN101438851B (en) | 2011-08-31 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2008102337705A Active CN101438851B (en) | 2008-12-29 | 2008-12-29 | Method for reducing dry sensation of cigarette smoke |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102499468A (en) * | 2011-11-17 | 2012-06-20 | 云南中烟昆船瑞升科技有限公司 | Method capable of remarkably increasing softness and absorptivity of papermaking-method reconstituted tobaccos |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1087245A (en) * | 1992-11-27 | 1994-06-01 | 中国有色金属工业总公司昆明贵金属研究所 | Additive for filter tip of cigarette and preparation thereof and adding method |
| CN1100003A (en) * | 1993-09-05 | 1995-03-15 | 青岛建筑工程学院 | Compound adsorbent and its preparing process |
| CN101115408A (en) * | 2005-02-04 | 2008-01-30 | 菲利普莫里斯生产公司 | Flavour capsule for enhanced flavour delivery in cigarettes |
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2008
- 2008-12-29 CN CN2008102337705A patent/CN101438851B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1087245A (en) * | 1992-11-27 | 1994-06-01 | 中国有色金属工业总公司昆明贵金属研究所 | Additive for filter tip of cigarette and preparation thereof and adding method |
| CN1100003A (en) * | 1993-09-05 | 1995-03-15 | 青岛建筑工程学院 | Compound adsorbent and its preparing process |
| CN101115408A (en) * | 2005-02-04 | 2008-01-30 | 菲利普莫里斯生产公司 | Flavour capsule for enhanced flavour delivery in cigarettes |
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| CN101438851A (en) | 2009-05-27 |
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