CN102150943A - Method for preparing mint tobacco flake threads - Google Patents

Method for preparing mint tobacco flake threads Download PDF

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Publication number
CN102150943A
CN102150943A CN201110075063XA CN201110075063A CN102150943A CN 102150943 A CN102150943 A CN 102150943A CN 201110075063X A CN201110075063X A CN 201110075063XA CN 201110075063 A CN201110075063 A CN 201110075063A CN 102150943 A CN102150943 A CN 102150943A
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China
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adsorbent
peppermint
tobacco
reconstituted tobacoo
mint
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CN201110075063XA
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CN102150943B (en
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穆小丽
任建新
罗嘉
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Abstract

The invention provides a method for preparing mint tobacco flake threads. The method comprises the following steps: a) utilizing an adsorbent to adsorb and fix mint so as to prepare a mint-containing adsorbent, wherein the mass ratio of the adsorbent to the mint is (5:1)-(15:1); b) mixing tobacco powder, an adhesive, water and the mint-containing adsorbent to prepare tobacco flake pulp, wherein the mint-containing adsorbent accounts for 20-25wt% of the tobacco flake threads, the tobacco powder accounts for 10-20wt% of the tobacco flake threads, and the adhesive accounts for 1-5wt% of the tobacco flake threads; and c) extruding the prepared flake pulp by utilizing a porous extruder so as to obtain flake threads, and drying to obtain the mint tobacco flake threads. The mint tobacco flake threads prepared by the method are mixed with tobacco threads to prepare mint type tobacco threads, so that the defects that the mint of the traditional tobacco is easily volatilized and the aroma (cool smell) of the mint is not released uniformly can be overcome, and the quality of the mint aroma (cool smell) of the tobacco is always consistent when the tobacco is smoked.

Description

A kind of preparation method of peppermint reconstituted tobacoo pipe tobacco
Technical field
The invention belongs to technical field of tobacco, relate to a kind of preparation method who contains adsorbent and a kind of peppermint reconstituted tobacoo pipe tobacco of peppermint.
Background technology
Traditional peppermint is added production technology in the pipe tobacco, complicated operation, loaded down with trivial details to.At first menthol is dissolved in the absolute alcohol, makes the menthol alcoholic solution of debita spissitudo, be sprayed onto in the pipe tobacco equably in proportion again and go.Adopt the cigarette products of menthol perfuming, minty note when burning and sucking (cold) flavor weakens rapidly with the increase of puff number, has arrived cigarette and has propped up end, and minty note (cold) flavor is very thin, can not obtain the suction sensation that minty note (cold) flavor evenly discharges, exist great igniting and sucking quality defective.
Reconstituted tobacoo is that the thin slice that utilizes offal, offal and smoked sheet etc. discarded in the cigarette process to make near tobacco leaf as raw material is used further to production of cigarettes.On the one hand, reconstituted tobacoo has maximally utilised tobacco material, and to reducing the consumption of raw materials of tobacco business, reducing cost and then saving aspect such as arable land all has positive role.On the other hand, reconstituted tobacoo has positive meaning aspect the tobacco product quality improving.Thin slice production has broken through the mode of simple twice laid, and beginning is improving the cigarette burning degree, improves the inherent quality of cigarette product, and the aspects such as harmful components that reduce in the cigarette play a major role.
Some scholar has carried out reinforced flavouring research in reconstituted tobacoo, the spices of interpolation, essence comprise natural baccy extract and monomer perfume material.The natural baccy extract has tobacco extract class material, and the monomer perfume material has vanillic aldehyde, diacetyl, Furanones and menthol or the like, and the interpolation of these perfume materials makes the using value of reconstituted tobacoo that large increase arranged.
The adsorbent filter tip generally adopts the microporous solids adsorbent that menthol is adsorbed, and the adsorbent that then will adsorb menthol adds in the filtering material, makes two compound or three composite filter tips.Normal temperature is menthol not desorption or a small amount of desorption of absorption down, only when flue gas during by this adsorbent menthol just be released.Chinese patent CN 1099957 has disclosed a kind of adsorbent of cigarette filter, and this adsorbent is the unformed manosil AS or the unformed aluminosilicate of certain specification, points out that this adsorbent has the ability of strong absorption and release spices.
Summary of the invention
Peppermint at traditional cigarette is volatile, the perfume (or spice) of peppermint (cold) flavor discharges uneven shortcoming, the invention provides a kind of adsorbent and a kind of peppermint reconstituted tobacoo pipe tobacco that contains peppermint, and the method for preparing the mint type cigarette pipe tobacco with this peppermint reconstituted tobacoo pipe tobacco is provided.This method is added peppermint reconstituted tobacoo pipe tobacco in the pipe tobacco to, has guaranteed that the quality of minty note (cold) flavor of cigarette is remained the same from beginning to end when suction.
The invention provides a kind of adsorbent that contains peppermint, the mass ratio of adsorbent and menthol is 5: 1-15: 1, and wherein adsorbent is one or several of silicic acid, sodium metasilicate, magnesium silicate, alumina silicate, starch.
This preparation of adsorbent method that contains peppermint is: adsorbent is positioned in the ethanol solution of menthol, adds hot reflux 1.5-2.5 hour, cooling is filtered, and descends dry 2.5-3.5 hour at 25-35 ℃.
The adsorbent preferred manufacturing procedure that contains peppermint is: adsorbent is positioned in the ethanol solution of menthol, added hot reflux 2 hours, be cooled to room temperature, filter, drying is 3 hours under 30 ℃.
The present invention also provides a kind of peppermint reconstituted tobacoo pipe tobacco, is made up of offal, adhesive and the above-mentioned adsorbent that contains peppermint; Wherein offal, adhesive and the described part by weight that contains the adsorbent of peppermint are: 1: (0.05-0.5): (1-2.5).
The preparation method of a kind of peppermint reconstituted tobacoo pipe tobacco of the present invention is:
A) with offal, adhesive, water and the described peppermint adsorbent that contains mix, make the reconstituted tobacoo slurry, the wherein said shared reconstituted tobacoo slurry of the adsorbent mass ratio that contains peppermint is 20%-25%, it is 10%-20% that offal accounts for reconstituted tobacoo slurry mass ratio, and the shared reconstituted tobacoo slurry of adhesive mass ratio is 1%-5%;
B) obtain sheet and shreds after the reconstituted tobacoo for preparing slurry is extruded with the micropore extruder, obtain peppermint reconstituted tobacoo pipe tobacco after the oven dry.
Wherein the adhesive described in the step a) is one or several of carboxymethyl cellulose, xanthans, carob, guar gum, shitosan.The bore of the micropore extruder described in the step b) is between 0.5mm-1.5mm.
After having obtained above-mentioned peppermint reconstituted tobacoo pipe tobacco according to method provided by the invention, itself and common pipe tobacco joined convert, obtain the mint type cigarette pipe tobacco, and be prepared into cigarette.
The prepared cigarette of peppermint reconstituted tobacoo pipe tobacco provided by the invention possesses following advantage:
1, easily stores, do not pollute the working environment and the production line of cigarette;
2, reduce the consumption of raw materials of tobacco, reduced production cost;
3, minty note (cold) flavor discharges evenly during cigarette burning;
4, prolonged the shelf life of mentholated cigarette.
The specific embodiment
The present invention is further illustrated according to specific embodiment below, but do not mean that restriction protection scope of the present invention.
Embodiment 1
Dry 25g magnesium silicate is positioned in the ethanol solution of 2.5g menthol, adds hot reflux 1.2 hours, is cooled to room temperature, filters, and drying is 3.5 hours under 28 ℃.The water that adds offal, 2.5g carboxymethyl cellulose and the 65g of 20g afterwards, fully obtain offal thin slice slurry behind the mixing, obtain the sheet and shreds of similar pipe tobacco after the thin slice for preparing slurry extruded with the micropore extruder of 0.8mm, obtain peppermint reconstituted tobacoo pipe tobacco after the oven dry.With peppermint reconstituted tobacoo pipe tobacco and the pipe tobacco mixing that obtains, make cigarette.The cigarette smoking result: cool sense is stronger, and fragrance ceases, basically identical before and after the suction.
Embodiment 2
Dry 18g alumina silicate is positioned in the ethanol solution of 3.0g menthol, adds hot reflux 1.5 hours, is cooled to room temperature, filters, and drying is 3 hours under 30 ℃.The water that adds offal, 1g carboxymethyl cellulose, 1.5g guar gum and the 50g of 12.5g afterwards, fully obtain offal thin slice slurry behind the mixing, obtain the sheet and shreds of similar pipe tobacco after the thin slice for preparing slurry extruded with the micropore extruder of 1.0mm, obtain peppermint reconstituted tobacoo pipe tobacco after the oven dry.With peppermint reconstituted tobacoo pipe tobacco and the pipe tobacco mixing that obtains, make cigarette.The cigarette smoking result: cool sense is strong, and fragrance ceases, basically identical before and after the suction
Embodiment 3
Dry 15g silicic acid is positioned in the ethanol solution of 1.25g menthol, adds hot reflux 2 hours, is cooled to room temperature, filters, and drying is 2.5 hours under 35 ℃.The water that adds offal, 1g carboxymethyl cellulose, 0.5g xanthans and the 40g of 10g afterwards, fully obtain offal thin slice slurry behind the mixing, obtain the sheet and shreds of similar pipe tobacco after the thin slice for preparing slurry extruded with the micropore extruder of 1.2mm, obtain peppermint reconstituted tobacoo pipe tobacco after the oven dry.With peppermint reconstituted tobacoo pipe tobacco and the pipe tobacco mixing that obtains, make cigarette.The cigarette smoking result: cool sense is stronger, and the fragrance breath is better, basically identical before and after the suction.

Claims (7)

1. an adsorbent that contains peppermint is characterized in that, the mass ratio of adsorbent and menthol is 5: 1-15: 1, and wherein said adsorbent is one or several of silicic acid, sodium metasilicate, magnesium silicate, alumina silicate, starch.
2. a kind of adsorbent that contains peppermint according to claim 1 is characterized in that the preparation method is: adsorbent is positioned in the ethanol solution of menthol, adds hot reflux 1.5-2.5 hour, cooling is filtered, and descends dry 2.5-3.5 hour at 25-35 ℃.
3. a kind of adsorbent that contains peppermint according to claim 2 is characterized in that the preparation method is: adsorbent is positioned in the ethanol solution of menthol, added hot reflux 2 hours, be cooled to room temperature, filter, drying is 3 hours under 30 ℃.
4. a peppermint reconstituted tobacoo pipe tobacco is characterized in that, forms by offal, adhesive with as the described adsorbent that contains peppermint of one of claim 1-3; Wherein offal, adhesive and the described part by weight that contains the adsorbent of peppermint are: 1: (0.05-0.5): (1-2.5).
5. a kind of peppermint reconstituted tobacoo pipe tobacco according to claim 4 is characterized in that the preparation method is:
A) with offal, adhesive, water and the described peppermint adsorbent that contains mix, make the reconstituted tobacoo slurry, the wherein said shared reconstituted tobacoo slurry of the adsorbent mass ratio that contains peppermint is 20%-25%, it is 10%-20% that offal accounts for reconstituted tobacoo slurry mass ratio, and the shared reconstituted tobacoo slurry of adhesive mass ratio is 1%-5%;
B) obtain sheet and shreds after the reconstituted tobacoo for preparing slurry is extruded with the micropore extruder, obtain peppermint reconstituted tobacoo pipe tobacco after the oven dry.
6. a kind of peppermint reconstituted tobacoo pipe tobacco according to claim 5 is characterized in that, described adhesive is one or several of carboxymethyl cellulose, xanthans, carob, guar gum, shitosan.
7. a kind of peppermint reconstituted tobacoo pipe tobacco according to claim 5 is characterized in that the bore of described micropore extruder is between 0.5mm-1.5mm.
CN 201110075063 2011-03-28 2011-03-28 Mint tobacco flake threads and method for preparing mint tobacco flake threads Active CN102150943B (en)

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102499432A (en) * 2011-10-14 2012-06-20 湖南中烟工业有限责任公司 Method of improving process-bearing property of volatile sweet spice in tobacco slice flavoring
CN102524941A (en) * 2012-01-17 2012-07-04 湖北中烟工业有限责任公司 Sheets capable of reducing tar content of cigarettes and manufacture method thereof
CN103300468A (en) * 2012-03-17 2013-09-18 福建中烟工业有限责任公司 Reinforced essence for baking aromatic tobacco and preparation method for reinforced essence
CN103637394A (en) * 2013-12-02 2014-03-19 中国烟草总公司重庆市公司烟草科学研究所 Preparation method of tobacco sheet shreds with banana taste
CN104877594A (en) * 2015-04-01 2015-09-02 湖南中烟工业有限责任公司 Adhesion agent for reconstituted tobacco leafs through slurry process
CN105533790A (en) * 2016-02-26 2016-05-04 贵州利生香中药科技有限公司 L-borneol tobacco sheet tobacco shreds and preparation method thereof
CN105533803A (en) * 2016-02-26 2016-05-04 贵州利生香中药科技有限公司 Cigarette filter tip containing medicine
CN106000293A (en) * 2016-06-24 2016-10-12 广东中烟工业有限责任公司 Preparation method and application of adsorbent
CN110432530A (en) * 2019-08-13 2019-11-12 湖北中烟工业有限责任公司 A kind of method for preparing slices suitable for low temperature cigarette

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10118153B1 (en) * 2018-08-07 2018-11-06 AAC Technologies Pte. Ltd. Gas absorbent particle and method for making same

Citations (2)

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Publication number Priority date Publication date Assignee Title
CN1099957A (en) * 1993-09-11 1995-03-15 中国烟草总公司郑州烟草研究院 Adsorbent for cigarette filter-tip
CN101319053A (en) * 2008-07-08 2008-12-10 江南大学 Method for preparing fatty acid stephanoporate starch ester and application thereof

Patent Citations (2)

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Publication number Priority date Publication date Assignee Title
CN1099957A (en) * 1993-09-11 1995-03-15 中国烟草总公司郑州烟草研究院 Adsorbent for cigarette filter-tip
CN101319053A (en) * 2008-07-08 2008-12-10 江南大学 Method for preparing fatty acid stephanoporate starch ester and application thereof

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102499432A (en) * 2011-10-14 2012-06-20 湖南中烟工业有限责任公司 Method of improving process-bearing property of volatile sweet spice in tobacco slice flavoring
CN102524941B (en) * 2012-01-17 2013-11-06 湖北中烟工业有限责任公司 Sheets capable of reducing tar content of cigarettes and manufacture method thereof
CN102524941A (en) * 2012-01-17 2012-07-04 湖北中烟工业有限责任公司 Sheets capable of reducing tar content of cigarettes and manufacture method thereof
CN103300468B (en) * 2012-03-17 2015-11-18 福建中烟工业有限责任公司 A kind of flavoring essence cured for Turkish tobaccos and preparation method thereof
CN103300468A (en) * 2012-03-17 2013-09-18 福建中烟工业有限责任公司 Reinforced essence for baking aromatic tobacco and preparation method for reinforced essence
CN103637394A (en) * 2013-12-02 2014-03-19 中国烟草总公司重庆市公司烟草科学研究所 Preparation method of tobacco sheet shreds with banana taste
CN104877594A (en) * 2015-04-01 2015-09-02 湖南中烟工业有限责任公司 Adhesion agent for reconstituted tobacco leafs through slurry process
CN104877594B (en) * 2015-04-01 2018-03-02 湖南中烟工业有限责任公司 A kind of thick slurry method reconstituted tobacco adhesive
CN105533790A (en) * 2016-02-26 2016-05-04 贵州利生香中药科技有限公司 L-borneol tobacco sheet tobacco shreds and preparation method thereof
CN105533803A (en) * 2016-02-26 2016-05-04 贵州利生香中药科技有限公司 Cigarette filter tip containing medicine
CN106000293A (en) * 2016-06-24 2016-10-12 广东中烟工业有限责任公司 Preparation method and application of adsorbent
CN106000293B (en) * 2016-06-24 2018-12-18 广东中烟工业有限责任公司 A kind of preparation method and application of adsorbent
CN110432530A (en) * 2019-08-13 2019-11-12 湖北中烟工业有限责任公司 A kind of method for preparing slices suitable for low temperature cigarette

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