CN100449057C - Composite modifying formed paper for filter-tip of cigarette and preparation method thereof - Google Patents
Composite modifying formed paper for filter-tip of cigarette and preparation method thereof Download PDFInfo
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- CN100449057C CN100449057C CNB2006101638710A CN200610163871A CN100449057C CN 100449057 C CN100449057 C CN 100449057C CN B2006101638710 A CNB2006101638710 A CN B2006101638710A CN 200610163871 A CN200610163871 A CN 200610163871A CN 100449057 C CN100449057 C CN 100449057C
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Abstract
The present invention discloses one kind of composite modified and shaped paper for cigarette filter tip. The composite modified and shaped paper is prepared through the following steps: preparing coating fluid, spraying or rolling the coating fluid in the amount of 1-10 wt% of paper onto the paper, stoving to eliminate excessive water, cutting to the required sizes and packing. The coating fluid consists of adhering material 3-30 weight portions, including agent 5-10 weight portions, demulsifier 5-10 weight portions, sweetening agent 5-10 weight portions, humidizer 5- 20 weight portions, fume pH regulator 2-8 weight portions, cigarette taste improver 10-30 weight portions, selective harm reducer 30-50 weight portions, and water in the amount to reach dry material content of 1-20 wt%.
Description
Technical field
The present invention relates to a kind of cigarette material, more particularly, is a kind of cigarette filter composite modifying formed paper, particularly a kind of cigarette filter compound coating fluid of forming paper.
Background technology
Forming paper claims filter rod paper again, belongs to industrial slim extraordinary stationery, is mainly used in the tobacco business cigarette filter and wraps up acetate silk.
In order to reduce the harm of smoking to human body, along with going deep into of tobacco business " reducing tar and reducing harm " policy, forming paper is effectively fallen harmful means as a kind of, is in industry more and more widely used.But the ventilation dilution of forming paper also brings a lot of negative effects to cigarette, as: flue gas moisture and fragrance component diffusion increase, and cause flue gas drying sense increase, the decay of fragrance concentration etc.In recent years, be the new function of exploitation forming paper, many application study persons have put in the modification work of forming paper, and have obtained certain achievement.For example: propose among the CN 1696401A by on forming paper, being coated with medical stone, active carbon, ion exchange resin, polysaccharide, natural, natural plants powder isoreactivity sorbing material coating, give the filter tip forming paper and have the function that reduces the cigarette harmful components, but its technology is only applicable to common forming paper.And for example: CN 1818210A proposes can to remove in the flue gas 40% CO and CO by add some coating that contain resin liquid, extracts of Chinese herbal medicine, sorbing material etc. on high porosity plug wrap paper
2, 80% hydrogen chloride, 70% acrolein and benzene reduce heavy metal and harmful components simultaneously, and can reach pharynx-clearing throat-benefiting, reduce oral peculiar smell, improve the effect of excitant and mouthfeel.But this technology can influence the air permeability of high porosity plug wrap paper, and the more residual harmful organic compound in liquid-solidization of synthetic resin back also brings hidden danger to cigarette odor-absorbing and security.
Present forming paper study on the modification all concentrates on bonding material some sorbing materials is fixed on the forming paper reaching the harmful effect of falling, but there is no report for the correlative study that improves the cigarette organoleptic quality; It is high that the more common forming paper of high porosity plug wrap paper cost is wanted, the modifying formed paper that makes with preceding method, can reduce the air permeability of high porosity plug wrap paper, thereby reduce the cost performance of its use, and the correlative study of flue gas modification (as fragrance, assorted gas, harmony etc.) is not still had report yet.
Summary of the invention
The objective of the invention is effectively to avoid the negative effect of forming paper modification, a kind of composite modifying formed paper for filter-tip of cigarette is provided at deficiency of the prior art.
Purpose of the present invention is achieved by following technical proposals.
The invention provides a kind of composite modifying formed paper for filter-tip of cigarette, this composite modifying formed paper is prepared by following method: at first prepare coating fluid, utilize the gluing of spraying or roller coating to apply mode then, percentage is 1%～10% coating weight by weight, add on the forming paper, dry, evaporating surplus moisture, again forming paper is cut, is packed by required width and length, promptly get the cigarette filter modifying formed paper.
Wherein, the parts by weight of the raw material of described coating fluid composition are: 3～30 parts of binding materials, 5～10 parts of coalescence inclusion agents, broken 5～10 parts of agent with fixed attention, 5～10 parts of sweeteners, 5～20 parts of humidizers, 2～8 parts of flue gas pH value conditioning agents, 10～30 parts of cigarette odor-absorbing modifying agents, 30～50 parts of selective harm-reducing agent; The percetage by weight that adds water move to dry matter content is 1%～20%; Described binding material is selected from a kind of in polyethylene glycol, amphoteric starch, gum Arabic or the shitosan or their mixture; Described coalescence inclusion agents is selected from a kind of in stearic acid, bay ferment or the sucrose ester or their mixture; Describedly broken coagulate agent and be selected from a kind of in isoamyl alcohol, leaf-alcohol, 3-methylhexanoic acid or the isovaleric acid or their mixture; Described sweetener is selected from a kind of in stevioside, xylitol, sucrose or the honey or their mixture; Described humidizer is selected from a kind of in glycerine, propylene glycol, dimethyl sulfoxide (DMSO) or the dimethyl sulfone or their mixture; Described flue gas pH value conditioning agent is selected from a kind of in propionic acid, citric acid, tartaric acid, malic acid, gluconic acid, amino acid or the natural alkaline matter or their mixture; Described cigarette odor-absorbing modifying agent is selected from a kind of in tobacco extract, licorice, tomato extract, active aloe extract or the ammonium gluconate; Or their mixture; Described selective harm-reducing agent is selected from a kind of in active carbon, magnesium silicate, Tea Polyphenols or the cyclodextrin or their mixture.
The invention provides a kind of preparation method of composite modifying formed paper for filter-tip of cigarette, this method adopts the step of following order:
(1) described binding material is added water, dissolve under 90 ℃, the weight ratio of binding material and water is 1: 9;
(2) described selective harm-reducing agent is levigate to 200 order fine powders, and add in the gains of step (1);
(3) add described sweetener and humidizer;
(4) add described broken agent or coalescence inclusion agents, flue gas pH value conditioning agent and the cigarette odor-absorbing modifying agent of coagulating, the percetage by weight that adds water move to dry matter content then is 1%～20%, mixes, and promptly makes required coating fluid;
(5) with described coating fluid, by normal forming paper production technology, utilize the gluing of spraying or roller coating to apply mode, the percetage by weight that accounts for forming paper by dry basis is 1%～10% coating weight, add on the forming paper, dry, evaporating surplus moisture, again forming paper is cut, is packed by required width and length, promptly get the cigarette filter modifying formed paper.
Know-why of the present invention is:
Cigarette filter tip rod among the present invention with the forming paper modified compound additive by the force field in the filter rod in cigarette smoke, change aerocolloidal characteristic and composition, thereby reach the function of improving harmful components in cigarette smoking quality and the selectivity reducing cigarette fume.
When the cigarette flue gas aerosol particle collided, when the chemical composition of two particle is identical, or chemical composition was different but when dissolving mutually, because of the molecular separating force summation is far longer than potential barrier, coalescence takes place automatically.But different and when not dissolving mutually, the molecular separating force summation is less than potential barrier when chemical composition, coalescence can not take place automatically, need reduce interfacial tension between two particle by the coalescence inclusion agents.Cigarette filter tip rod of the present invention, enters in the cigarette smoke with diluent air under the dynamic force field action that pressure drop produces with the coalescence inclusion agents component in the forming paper modified compound additive, makes particulate generation coalescence, thereby is filtered.Consequently make the aerosol particle concentration step-down, harmful components such as aromatic degree of cigarette and tar are reduced, make the aerosol that enters the oral cavity form quadratic distribution simultaneously, make particle size become big slightly, flue gas feature according to cigarette, suitable coalescence inclusion agents and consumption thereof can make particulate be more evenly distributed, thereby improve the hamony and the comfort level of cigarette.
Cigarette filter of the present invention, enters in the cigarette smoke with diluent air under the dynamic force field action that pressure drop produces with the broken agent component of coagulating in the forming paper modified compound additive, and the aerosol macroparticle is separated.Aerosol particle concentration is increased, particle size is diminished slightly.According to the flue gas feature of different trade mark cigarette, suitable brokenly coagulate agent and can make the particulate size littler, it is more single, more even to distribute, thus the exquisiteness of raising cigarette smoke, property sent out and richness thoroughly.
Cigarette filter of the present invention, enters in the cigarette smoke with diluent air under the dynamic force field action that pressure drop produces with the sweetener component in the forming paper modified compound additive, can increase the sweet rhythm of flue gas and rich, and the oral cavity comfortableness is improved.
The humidizer component of cigarette filter of the present invention in the forming paper modified compound additive, under the dynamic force field action that pressure drop produces, the moisture of its absorption and self can enter cigarette smoke with diluent air, make flue gas keep enough moisture to enter the oral cavity, improved because the dried thorn sense of ventilating and bringing.
Cigarette filter of the present invention under the dynamic force field action that pressure drop produces, enters cigarette smoke with diluent air with the flue gas pH value conditioning agent component in the forming paper modified compound additive, and flue gas pH value is changed.Its result one optionally reduces the increment of the nicotine that causes because of ventilation, decreases by 50%, two, makes flue gas particle generation coalescence, filtration, thereby reduces flue gas concentration, and flue gas is softer.
The cigarette odor-absorbing modifying agent component of cigarette filter of the present invention in the forming paper modified compound additive, under the dynamic force field action that pressure drop produces, enter cigarette smoke with diluent air, thereby remedy the deficiency that the reduction of fractions to a common denominator brings, also can give cigarette special brand identity simultaneously.
Under the thrust of concentration difference, small size particles and gas molecule overcome the dynamic field of force of pressure drop generation and the resistance of decentralized medium or medium is done Brownian movement, contact with the selective harm-reducing agent component in the forming paper modified compound additive with cigarette filter tip rod of the present invention, thereby the generation selective absorption is as CO reduction by 20%, hydrogen chloride reduction by 50% etc.
Compared with prior art, the present invention has following beneficial effect:
(1) technology of the present invention is simple, is convenient to realize suitability for industrialized production;
(2) the present invention has remedied the defective of punching ventilation cigarette, has increased the damp sense of flue gas;
(3) the present invention can change aerocolloidal particle properties, thereby adjusts exquisiteness, hamony and the comfortableness of flue gas, can improve concentration, richness and the saturating property sent out of cigarette perfume (or spice) simultaneously;
(4) the present invention provides security higher cigarette products for the smoker;
(5) the invention provides a kind of new having and fall harmful function, can improve the composite modifying formed paper of cigarette sensible quality simultaneously, for the design or the maintenance of cigarette provides new thinking or means.
The specific embodiment:
By specific embodiment given below, can further be well understood to the present invention.But they are not limitation of the invention.
Except as otherwise noted, the percentage that is adopted among the present invention is percetage by weight.
Embodiment 1
15 kilograms of polyethylene glycol are added water, dissolve under 90 ℃, the weight ratio of binding material and water is 1: 9, and is stand-by; 40 kilograms of metal-metallic oxide modified activated carbons are levigate to 200 order fine powders, and add in the aqueous solution of described polyethylene glycol; Add 7 kilograms of steviosides, add 15 kilograms of 15 kilograms of isoamyl alcohol, 5 kilograms of propionic acid and licorices, the percetage by weight that adds water move to dry matter content then is 10%, mixes, and promptly makes required coating fluid; With described coating fluid, by normal forming paper production technology, utilize the gluing of spraying or roller coating to apply mode, percentage is that 6% coating weight is coated common forming paper by weight, dry, evaporating surplus moisture, again forming paper is cut, packed by certain width and length, promptly get the cigarette filter modifying formed paper.The gained modifying formed paper is used to not have filter tip ventilation cigarette, makes soft, the harmony that becomes of this cigarette smoke, and total particulate matter reduces by 35% simultaneously.
Embodiment 2
Repeat embodiment 1, following difference is arranged: take by weighing 5 kilograms of laruyl alcohols, 25 kilograms of sucrose esters, 8 kilograms of stearic acid, the percetage by weight that adds water move to dry matter content is 5%, mix, account for the spreading rate of forming paper quality 2.5% by dry basis, the gained modifying formed paper is applied to filter tip ventilation cigarette, makes soft, the harmony that becomes of this cigarette smoke, and total particulate matter reduces by 30% simultaneously.
Embodiment 3
Repeat embodiment 1, following difference is arranged: take by weighing 15 kilograms of isoamyl alcohol, 8 kilograms of 3-methylhexanoic acids, 3 kilograms of leaf-alcohols, 3 kilograms of isovaleric acid, the percetage by weight that adds water move to dry matter content is 4%, mix, account for the spreading rate of forming paper quality 2.0% by dry basis, the gained modifying formed paper is applied to make flue gas finer and smoother, pure and mild, and the fragrant richness of cigarette, the property sent out is improved thoroughly, makes nicotine reduce by 15% simultaneously.
Embodiment 4
Repeat embodiment 1, following difference is arranged: take by weighing 10 kilograms of synanthrin, 12 kilograms of xylitols, 14 kilograms of sucrose, 25 kilograms of honey, the percetage by weight that adds water move to dry matter content is 5%, mix, account for the spreading rate of forming paper quality 4.0% by dry basis, the gained modifying formed paper has increased the sweet sense of flue gas and rich, can cover bad assorted gas simultaneously.
Embodiment 5
Repeat embodiment 1, following difference is arranged: the percetage by weight that take by weighing 6 kilograms of glycerine, 15 kilograms of propylene glycol, 6 kilograms of dimethyl sulfoxide (DMSO)s, 8 kilograms of dimethyl sulfones, adds water move to dry matter content is 3%, mix, account for the spreading rate of forming paper quality 1.8% by dry basis, the gained modifying formed paper has increased the damp sense of flue gas, improve the comfort level of throat, remedied the dry problem of flue gas that reduction of fractions to a common denominator dilution brings.
Embodiment 6
Repeat embodiment 1, following difference is arranged: take by weighing 3 kilograms of propionic acid, 2 kilograms of malic acid, 5 kilograms of gluconic acids, 1 kilogram of citric acid, 2 kilograms in tartaric acid, 2 kilograms in amino acid, the percetage by weight that adds water move to dry matter content is 4%, mix, account for the spreading rate of forming paper quality 2.2% by dry basis, the gained modifying formed paper makes that flue gas is softer, mouthfeel is more comfortable.
Embodiment 7
Repeat embodiment 1, following difference is arranged: take by weighing 25 kilograms of tobacco extracts, 30 kilograms of licorices, 10 kilograms of tomato extracts, 15 kilograms of ammonium gluconates, the percetage by weight that adds water move to dry matter content is 3%, mix, account for the spreading rate of forming paper quality 2.0% by dry basis, the gained modifying formed paper can increase concentration, richness and the sweet sense of cigarette perfume (or spice), also is greatly improved on comfortableness simultaneously.
Embodiment 8
Repeat embodiment 1, following difference is arranged: take by weighing 10 kilograms of shitosans, 15 kilograms of polyethylene glycol, 8 kilograms of stearic acid, 8 kilograms of natural alkaline matters, 7 kilograms of amphoteric starches, 20 kilograms of metal-metallic oxide modified activated carbons, 20 kilograms of magnesium silicates, the percetage by weight that adds water move to dry matter content is 12%, mix, the spreading rate that accounts for forming paper quality 5.5% by dry basis is coated common forming paper, the gained modifying formed paper is used for non-ventilation filter tip cigarette, can reduce CO 20%, hydrogen chloride 50%.
Embodiment 9
Repeat embodiment 1, following difference is arranged: take by weighing 15 kilograms of gum Arabics, 10 kilograms of shitosans, 25 kilograms of sucrose esters, 10 kilograms of laruyl alcohols, 8 kilograms of stearic acid, the percetage by weight that adds water move to dry matter content is 3%, mix, the spreading rate that accounts for forming paper quality 2.5% by dry basis is coated common forming paper, and the gained modifying formed paper can make the fragrant coordination of cigarette cigarette, comfortable taste, and can reduce CO15%, total particulate matter 20%.
Embodiment 10
Repeat embodiment 1, following difference is arranged: take by weighing 20 kilograms of shitosans, 20 kilograms of sucrose esters, 15 kilograms of steviosides, 25 kilograms of honey, 6 kilograms of glycerine, 10 kilograms of malic acid, 8 kilograms of gluconic acids, 25 kilograms of tobacco extracts, 25 kilograms of licorices, 10 kilograms of ammonium gluconates, 15 kilograms of tomato extracts, 20 kilograms of metal-metallic oxide modified activated carbons, 15 kilograms of magnesium silicates, 15 kilograms of cyclodextrin, the percetage by weight that adds water move to dry matter content is 7%, mix, the spreading rate that accounts for common forming paper quality 3.2% by dry basis is coated common forming paper, the gained modifying formed paper is used for non-ventilation filter tip cigarette, can make the cigarette cigarette aromatic strongly fragrant, plentiful, sweet, reduce CO 20% simultaneously, total particulate matter 20%.
Embodiment 11
Repeat embodiment 1, following difference is arranged: take by weighing 15 kilograms of polyethylene glycol, 15 kilograms of shitosans, 8 kilograms of 3-methylhexanoic acids, 20 kilograms of steviosides, 30 kilograms of honey, 8 kilograms of dimethyl sulfoxide (DMSO)s, 10 kilograms of malic acid, 6 kilograms of propionic acid, 30 kilograms of licorices, the active aloe extract, 20 kilograms of metal-metallic oxide modified activated carbons, 15 kilograms of magnesium silicates, 10 kilograms of cyclodextrin, the percetage by weight that adds water move to dry matter content is 7%, mix, the spreading rate that accounts for forming paper quality 3.2% by dry basis is coated common forming paper, the gained modifying formed paper can make the cigarette cigarette fragrant fine and smooth, dense fragrance, plentiful, saturating sending out, sweet, coordinate, can reduce oral stimulation and residual, reduce CO 20% simultaneously.
Claims (2)
1. composite modifying formed paper for filter-tip of cigarette, this composite modifying formed paper is prepared by following method: at first prepare coating fluid, utilize the gluing of spraying or roller coating to apply mode then, percentage is 1%～10% coating weight by weight, add on the forming paper, dry, evaporating surplus moisture, again forming paper is cut, is packed by required width and length, promptly get the cigarette filter modifying formed paper; Wherein, the parts by weight of the raw material of described coating fluid composition are: 3～30 parts of binding materials, 5～10 parts of coalescence inclusion agents, broken 5～10 parts of agent with fixed attention, 5～10 parts of sweeteners, 5～20 parts of humidizers, 2～8 parts of flue gas pH value conditioning agents, 10～30 parts of cigarette odor-absorbing modifying agents, 30～50 parts of selective harm-reducing agent; The percetage by weight that adds water move to dry matter content is 1%～20%; Described binding material is selected from a kind of in polyethylene glycol, amphoteric starch, gum Arabic or the shitosan or their mixture; Described coalescence inclusion agents is selected from a kind of in stearic acid, laruyl alcohol or the sucrose ester or their mixture; Describedly broken coagulate agent and be selected from a kind of in isoamyl alcohol, leaf-alcohol, 3-methylhexanoic acid or the isovaleric acid or their mixture; Described sweetener is selected from a kind of in stevioside, xylitol, sucrose or the honey or their mixture; Described humidizer is selected from a kind of in glycerine, propylene glycol, dimethyl sulfoxide (DMSO) or the dimethyl sulfone or their mixture; Described flue gas pH value conditioning agent is selected from a kind of in propionic acid, citric acid, tartaric acid, malic acid, gluconic acid or the amino acid or their mixture; Described cigarette odor-absorbing modifying agent is selected from a kind of in tobacco extract, licorice, tomato extract, active aloe extract or the ammonium gluconate; Or their mixture; Described selective harm-reducing agent is selected from a kind of in active carbon, magnesium silicate, Tea Polyphenols or the cyclodextrin or their mixture.
2. the preparation method of the described composite modifying formed paper for filter-tip of cigarette of claim 1, this method adopts the step of following order:
(1) described binding material is added water, dissolve under 90 ℃, the weight ratio of binding material and water is 1: 9;
(2) described selective harm-reducing agent is levigate to 200 order fine powders, and add in the gains of step (1);
(3) add described sweetener and humidizer;
(4) add described broken agent, coalescence inclusion agents, flue gas pH value conditioning agent and the cigarette odor-absorbing modifying agent of coagulating, the percetage by weight that adds water move to dry matter content then is 1%～20%, mixes, and promptly makes required coating fluid;
(5) with described coating fluid, by normal forming paper production technology, utilize the gluing of spraying or roller coating to apply mode, the percetage by weight that accounts for forming paper by dry basis is 1%～10% coating weight, add on the forming paper, dry, evaporating surplus moisture, again forming paper is cut, is packed by required width and length, promptly get the cigarette filter modifying formed paper.
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| Application Number | Priority Date | Filing Date | Title |
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| CNB2006101638710A CN100449057C (en) | 2006-12-30 | 2006-12-30 | Composite modifying formed paper for filter-tip of cigarette and preparation method thereof |
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| CNB2006101638710A CN100449057C (en) | 2006-12-30 | 2006-12-30 | Composite modifying formed paper for filter-tip of cigarette and preparation method thereof |
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| CN100999884A CN100999884A (en) | 2007-07-18 |
| CN100449057C true CN100449057C (en) | 2009-01-07 |
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| CN101416775B (en) * | 2007-10-26 | 2011-10-26 | 武汉烟草(集团)有限公司 | Tomato gradual extraction and integrated utilization method in cigarette |
| CN101843360B (en) * | 2009-03-24 | 2012-10-10 | 湖北中烟工业有限责任公司 | Tobacco leaf laser drilling method capable of simultaneously reducing tar and CO in cigarettes |
| CN101716492B (en) * | 2009-12-17 | 2011-12-28 | 云南恩典科技产业发展有限公司 | Antibacterial adsorbent selectively adsorbing nicotine and carbon monoxide in smoke and application in wrap paper thereof |
| CN101721975B (en) * | 2009-12-17 | 2011-12-28 | 云南恩典科技产业发展有限公司 | Antimicrobial adsorbent for selectively absorbing tar and carbon monoxide in smoke and application thereof in wrap paper |
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| CN102261010A (en) * | 2011-07-22 | 2011-11-30 | 浙江舜浦纸业有限公司 | Method for producing paper |
| CN102433793B (en) * | 2011-10-20 | 2014-07-02 | 广东中烟工业有限责任公司 | Flavoring method for filter rod wrapping paper |
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| CN102517981B (en) * | 2011-11-03 | 2014-08-06 | 湖南中烟工业有限责任公司 | Cellulose paper capable of reducing content of hydrocyanic acid or volatile carbonyl compound in cigarette smoke and preparation and application thereof |
| CN102619134B (en) * | 2012-03-09 | 2014-07-02 | 广东中烟工业有限责任公司 | Aroma improvement method for filter stick forming paper |
| CN102839565B (en) * | 2012-09-11 | 2014-12-24 | 广东中烟工业有限责任公司 | Cigarette paper additive for reducing harmful ingredients of cigarette mainstream smoke and application thereof |
| CN103214991B (en) * | 2013-04-02 | 2015-01-28 | 大亚科技股份有限公司 | Polypropylene tip filter stick adhesive for modifying cigarettes and application thereof |
| CN103225233B (en) * | 2013-04-27 | 2014-12-03 | 红塔辽宁烟草有限责任公司 | Preparation method of lining paper improving cigarette physical humidity-keeping performance |
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