CN108719350A - Sunstroke prevention mosquito-repellent essential oil and preparation method thereof and application method - Google Patents
Sunstroke prevention mosquito-repellent essential oil and preparation method thereof and application method Download PDFInfo
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- CN108719350A CN108719350A CN201810605468.1A CN201810605468A CN108719350A CN 108719350 A CN108719350 A CN 108719350A CN 201810605468 A CN201810605468 A CN 201810605468A CN 108719350 A CN108719350 A CN 108719350A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01M—CATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
- A01M29/00—Scaring or repelling devices, e.g. bird-scaring apparatus
- A01M29/12—Scaring or repelling devices, e.g. bird-scaring apparatus using odoriferous substances, e.g. aromas, pheromones or chemical agents
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Agronomy & Crop Science (AREA)
- Botany (AREA)
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Abstract
The invention discloses a kind of sunstroke prevention mosquito-repellent essential oil and preparation method thereof and application methods.The sunstroke prevention mosquito-repellent essential oil includes the raw material of following mass fraction：0-10 parts of palchouli oil, 0-10 parts of Blumea oil, 0-10 parts of elsholtzia oil, 0-10 parts of Herba Eupatorii Fortunei oil, 0-10 parts of caryophyllus oil, 0-10 parts of Oleum Citri Reticulatae, 0-10 parts of peppermint oil.Sunstroke prevention mosquito-repellent essential oil preparation method letter provided by the invention is extremely simple, and under vacuum, raw material is uniformly mixed.In use, sunstroke prevention mosquito-repellent essential oil is instilled in fumigating machine, evaporated by way of atomization.Compared to the prior art, sunstroke prevention mosquito-repellent essential oil repelling effect of the invention is good, while also having effects that certain sunstroke prevention clearing damp, refreshing the mind.
Description
Technical field
The present invention relates to chemical technical field of daily necessities, and in particular to a kind of sunstroke prevention mosquito-repellent essential oil and preparation method thereof and makes
Use method.
Background technology
Since ancient times, people just understand smokes combustion mosquito repellent using various natural plant materials, such as Mozzie buster, argy wormwood, peppermint, smokes
Clothing grass etc., this is because including the natural flavoring ingredients of mosquito repellent function in these plants.With the development of chemical industry, people
Natural perfume material is extracted from these plants, i.e., various plants essential oils achieve the purpose that mosquito repellent using these plants essential oils.Together
Shi Yinwei plants essential oil fragrant odours have and diseases preventions, the health-care effect such as purify air, refresh the mind, is antifatigue, caused people
Very big concern.But not only mosquito repellent is inefficient for single essential oil component, fragrance is also difficult to be received by many people,
It is difficult to be used more widely.
Accordingly, it is desirable to provide a kind of new plants essential oil solves the above problems.
Invention content
The purpose of the present invention is overcoming above-mentioned technical problem, it is good to provide a kind of mosquito repellent, at the same also have certain sunstroke prevention clearing damp,
Plants essential oil of the effect that refreshes the mind and preparation method thereof and application method.
Technical scheme is as follows：
A kind of sunstroke prevention mosquito-repellent essential oil comprising the raw material of following mass fraction：0-10 parts of palchouli oil, 0-10 parts of Blumea oil,
0-10 parts of elsholtzia oil, 0-10 parts of Herba Eupatorii Fortunei oil, 0-10 parts of caryophyllus oil, 0-10 parts of Oleum Citri Reticulatae, 0-10 parts of peppermint oil.
Preferably, the sunstroke prevention mosquito-repellent essential oil includes the raw material of following mass fraction：8 parts of palchouli oil, 8 parts of Blumea oil are fragrant
8 parts of Ru oil, 8 parts of Herba Eupatorii Fortunei oil, 5 parts of caryophyllus oil, 5 parts of Oleum Citri Reticulatae, 5 parts of peppermint oil.
Preferably, the sunstroke prevention mosquito-repellent essential oil includes the raw material of following mass fraction：8 parts of palchouli oil, 8 parts of Blumea oil are fragrant
8 parts of Ru oil, 8 parts of Herba Eupatorii Fortunei oil, 8 parts of caryophyllus oil, 8 parts of Oleum Citri Reticulatae, 8 parts of peppermint oil.
Plants essential oil has multiple efficacies, as safely and effectively additive, be widely used in medicine, food,
Among health products and cosmetics：
Palchouli oil can be eliminated drowsiness, inspire enthusiasm；
Blumea oil has effects that warming and activating meridian, qi and activate blood circulation；
Elsholtzia oil has the function of eliminating summer heat and remove dampness；
Herba Eupatorii Fortunei oil fragrant odour has dampness elimination, appetizing of being amusing, delivers the effect of relieving summer-heat；
Caryophyllus oil can promote blood circulation, and sterilize expelling parasite；
Oleum Citri Reticulatae can eliminate headache, clearing damp resolving sputum；
Peppermint oil has the function of refreshing the mind, dispels summer-heat and damp.
The present invention also provides a kind of preparation methods of sunstroke prevention mosquito-repellent essential oil comprising following steps：
Raw material is weighed according to proportioning, wherein raw material proportioning is：0-10 parts of palchouli oil, 0-10 parts of Blumea oil, elsholtzia oil 0-10
Part, 0-10 parts of Herba Eupatorii Fortunei oil, 0-10 parts of caryophyllus oil, 0-10 parts of Oleum Citri Reticulatae, 0-10 parts of peppermint oil；
Under vacuum, raw material is uniformly mixed.
Preferably, the palchouli oil is made using organic solvent extraction；The Blumea oil and Herba Eupatorii Fortunei oil use CO2It is super to face
Boundary's extraction is made；The elsholtzia oil, caryophyllus oil and peppermint oil are made using ultrasonic wave assisted extraction method；The Oleum Citri Reticulatae uses
Steam distillation is made.
Preferably, in the organic solvent extraction of the palchouli oil, use petroleum ether for solvent, petroleum ether dosage is 3~5
It measures again, Extracting temperature is 40~45 DEG C, and extraction is multiple.
Preferably, the CO of the Blumea oil2In supercritical extraction, extracting pressure 20Mpa, extraction temperature is 30~35
DEG C, extraction time is 100~120min, CO2Flow is 24kg/h, and separating pressure 8Mpa, separation temperature is 50~55 DEG C；Institute
State the CO of Herba Eupatorii Fortunei oil2In supercritical extraction, extracting pressure 15MPa, extraction temperature is 30~35 DEG C, extraction time 60-
90min, CO2Flow is 20kg/h, and separating pressure 7-8Mpa, separation temperature is 55~60 DEG C.
Preferably, in the ultrasonic wave assisted extraction method of the elsholtzia oil, use petroleum ether for solvent, liquid ratio 12.1mL/
G, 50~60 DEG C of ultrasonic temperature, ultrasonic time are 30~60min；
In the ultrasonic wave assisted extraction method of the caryophyllus oil, being impregnated using 75% ethyl alcohol, ultrasonic time is 60~90min,
Ultrasonic temperature is 65~70 DEG C, the concentrate that rotary evaporation is precipitated to no ethyl alcohol, solid-liquid ratio 1:20, then should with n-hexane extraction
Concentrate evaporates n-hexane, obtains caryophyllus oil；
In the ultrasonic wave assisted extraction method of the peppermint oil, distillation time is 120~135min, ultrasonic power 300`
400W, ultrasonic treatment time are 10~20min.
Preferably, in the steam distillation of the Oleum Citri Reticulatae, first by tangerine peel powder at coarse powder, then plus 6~8 times are measured water
1~2h is impregnated, 5~6h is finally extracted.
The present invention also provides a kind of application methods of sunstroke prevention mosquito-repellent essential oil simultaneously, and sunstroke prevention mosquito-repellent essential oil described above is instilled
In fumigating machine, evaporated by way of atomization.
Compared to the prior art, sunstroke prevention mosquito-repellent essential oil provided by the invention and preparation method thereof and application method have following
Advantageous effect：
One, it uses natural plant essential oils to be mixed for raw material, is free of insecticide, long-time service will not generate human body secondary
Effect, safely and effectively；
Two, there is good sunstroke prevention, repelling effect, repelling effect is lasting, is suitble to hot summer；
Three, also have the effect of it is certain dispel summer-heat and damp, refresh the mind, be conducive to health；
Four, have the effect of certain pleasant mental and body, used in combination with fumigating machine, it is applicable at home, interior, Office Area
Domain and all kinds of public domains for needing mosquito repellent；
Five, raw material essential oil is obtained using various novel energy-efficient extracting methods, superior in quality, yield is high；
Six, the preparation method of the sunstroke prevention mosquito-repellent essential oil is simple, can produce in enormous quantities；
Seven, Brown Glass Brown glass bottles and jars only avoid light place may be used in the sunstroke prevention mosquito-repellent essential oil, and store method is simple, and is on a small quantity
The effect of mosquito repellent is can reach, use easy to carry meets modern Man's Demands.
Specific implementation mode
With reference to embodiment, the present invention is described in further detail, and embodiments of the present invention are not limited thereto.
Table 1 is please referred to, each raw material presses the proportioning figure of mass fraction in the sunstroke prevention mosquito-repellent essential oil for being 1-5 of the embodiment of the present invention.
Raw material proportioning figure in the sunstroke prevention mosquito-repellent essential oil of 1 embodiment 1-5 of table
Wherein, palchouli oil is made using organic solvent extraction, specially：Using petroleum ether as solvent, wrinkled giant hyssop is dissolved in molten
In agent, the dosage of solvent petroleum ether is 5 times of wrinkled giant hyssop, is then extracted at least 4 times at 40 DEG C of temperature, obtains palchouli oil., due to
Overall process does not have to organic solvent, therefore extract absolutely not residual solvent, at the same also prevent extraction process to the murder by poisoning of human body and
Pollution to environment, be 100% it is pure natural；
Blumea oil uses CO2Supercritical extraction is made, specially：It is added in autoclave after folium artemisiae argyi is crushed, toward high pressure
The CO of pressurization is passed through in kettle2Fluid, flow 24kg/h extract 100min under conditions of pressure 20MPa, 30 DEG C of temperature；
Then the fluid for carrying extract enters separating still, is detached under conditions of pressure 8Mpa, 55 DEG C of temperature, you can ended
Leaf essential oil.
Herba Eupatorii Fortunei oil uses CO2Supercritical extraction is made, specially：It is added in autoclave after eupatorium is crushed, toward high pressure
The CO of pressurization is passed through in kettle2Fluid, flow 20kg/h extract 80min under conditions of pressure 15MPa, 32 DEG C of temperature；So
The fluid for carrying extract afterwards enters separating still, is detached under conditions of pressure 8Mpa, temperature 60 C, you can obtain eupatorium
Essential oil.
Elsholtzia oil is made using ultrasonic wave assisted extraction method, specially：Elscholtiza and petroleum ether are pressed into liquid ratio 12.1mL/g
Mixing, immersion start ultrasonic vibration, ultrasonic time 31min after a certain period of time, and ultrasonic temperature is 56.8 DEG C；Filtering, by filtrate
Rotary evaporation to petroleum ether volatilizes, you can obtains elsholtzia oil.
Caryophyllus oil is made using ultrasonic wave assisted extraction method, specially：Cloves is impregnated using 75% ethyl alcohol, it is then ultrasonic
Concussion, ultrasonic time 90min, ultrasonic temperature are 65 DEG C；The concentrate that filtrate rotary evaporation is precipitated to no ethyl alcohol after filtering,
Solid-liquid ratio is 1:20, then with the n-hexane extraction concentrate, evaporate n-hexane, obtain caryophyllus oil.
Peppermint oil is made using ultrasonic wave assisted extraction method, specially：Dried peppermint leaf merging high speed disintegrator is crushed, mistake
Sieve, is poured into reagent bottle, with 10 times of distilled water immersions, seals, then handled with ultrasonic cell disrupte machine, ultrasonic power 300-
400W, sonication times are 10~20min；Steam distillation is carried out after processing, distillation time is 120~135min, is distilled out
Sample with ether extract volatile oil, then be added 5g anhydrous sodium sulfates slough moisture in ether, be filtered to remove anhydrous sodium sulfate,
60 DEG C of water-baths remove ether to get Herba Menthae Haplocalycis volatile oil again.
Oleum Citri Reticulatae is made using steam distillation, specially：By tangerine peel powder at coarse powder, 6 times of amount water are added to impregnate 1h, then
6h is distilled, separates grease after placing cooling, which is Oleum Citri Reticulatae.
The preparation method of sunstroke prevention mosquito-repellent essential oil described in above-described embodiment 1-5 is：Raw material is weighed according to proportioning, it then will be former
Material mixes, and under vacuum, is uniformly mixed with 100r/min rotating speeds stirring 20min, finally will after mixing
Essential oil composition is fitted into Brown Glass Brown glass bottles and jars only, for using.
In use, the sunstroke prevention mosquito-repellent essential oil of the present invention is instilled in fumigating machine, is evaporated, reached by way of atomization
Sunstroke prevention mosquito repellent refreshes the mind and other effects.
Experimental verification：
One, repelling effect is verified
Repelling effect is tested using cylinder method, the transparent cylinder of three diameters about 21cm length about 43cm is connected, successively
Labeled as No.1 cylinder, No. two cylinders and No. three cylinders；It is separated with baffle between three cylinders and both sides is blocked with baffle, No.1 circle
Cylinder is sealed with gauze of breathing freely, and No. two cylinders are put into 100 experiment mosquitoes in advance, and No. three cylinders are put into test essential oil and close with baffle
Envelope.After being put into test essential oil smaple 2min, while two block baffles opened between three cylinders are taken out, baffle is turned back to, then remembered by 10min
Record the mosquito quantity in No.1 cylinder and No. three cylinders.
Calculating mosquito repellent rate, mosquito repellent rate=100% × (- No. three cylinder mosquito numbers of No.1 cylinder mosquito number)/No.1 cylinder mosquito number,
Each experiment is repeated 3 times and records test data, calculates its average mosquito repellent rate.
One group of comparative example is set, repelling effect more of the present invention is observed, comparative example is certain commercially available brand mosquito-repellent essential oil.
Experimental result：
2 repelling effect of table compares
It is verified by Experimental comparison, repelling effect of the invention is good, and the repelling effect of the embodiment of the present invention is substantially better than
The repelling effect of certain commercially available brand mosquito-repellent essential oil, and the repelling effect of embodiment 4 meets consumer for driving 80% or more
The demand of mosquito effect, while can be according to the proportion for adjusting each raw material essential oil, to configure the mosquito repellent with diverse fragrant flavour
Essential oil meets the needs of consumer is for fragrance.
Two, sunstroke prevention clearing damp, refresh the mind compliance test result
Using questionnaire method to the sunstroke prevention clearing damp of the present invention, refresh the mind and other effects and to evaluate, invite 100 aspirations
Person is using it is evaluated after the sunstroke prevention mosquito-repellent essential oil 15min of the embodiment of the present invention 4, and questionnaire result is averaged, questionnaire tune
The fruit that comes to an end is as shown in table 3 below：
Table 3
As known from Table 3, sunstroke prevention mosquito-repellent essential oil of the invention has certain fragrant therapeutic effect, the effect of certain sunstroke prevention clearing damp
Fruit, the very good effect that refreshes the mind, and can effective mosquito repellent, being suitable for hot summer uses.
Compared to the prior art, sunstroke prevention mosquito-repellent essential oil provided by the invention and preparation method thereof and application method have following
Advantageous effect：
One, it uses natural plant essential oils to be mixed for raw material, is free of insecticide, long-time service will not generate human body secondary
Effect, safely and effectively；
Two, there is good sunstroke prevention, repelling effect, repelling effect is lasting, is suitble to hot summer；
Three, also have the effect of it is certain dispel summer-heat and damp, refresh the mind, be conducive to health；
Four, have the effect of certain pleasant mental and body, used in combination with fumigating machine, it is applicable at home, interior, Office Area
Domain and all kinds of public domains for needing mosquito repellent；
Five, raw material essential oil is obtained using various novel energy-efficient extracting methods, superior in quality, yield is high；
Six, the preparation method of the sunstroke prevention mosquito-repellent essential oil is simple, can produce in enormous quantities；
Seven, Brown Glass Brown glass bottles and jars only avoid light place may be used in the sunstroke prevention mosquito-repellent essential oil, and store method is simple, and is on a small quantity
The effect of mosquito repellent is can reach, use easy to carry meets modern Man's Demands.
Example the above is only the implementation of the present invention is not intended to limit the scope of the invention, every to utilize this hair
Equivalent structure or equivalent flow shift made by bright description is applied directly or indirectly in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (10)
1. a kind of sunstroke prevention mosquito-repellent essential oil, which is characterized in that include the raw material of following mass fraction：0-10 parts of palchouli oil, Blumea oil
0-10 parts, 0-10 parts of elsholtzia oil, 0-10 parts of Herba Eupatorii Fortunei oil, 0-10 parts of caryophyllus oil, 0-10 parts of Oleum Citri Reticulatae, 0-10 parts of peppermint oil.
2. sunstroke prevention mosquito-repellent essential oil according to claim 1, which is characterized in that include the raw material of following mass fraction：Wrinkled giant hyssop
8 parts of oil, 8 parts of Blumea oil, 8 parts of elsholtzia oil, 8 parts of Herba Eupatorii Fortunei oil, 5 parts of caryophyllus oil, 5 parts of Oleum Citri Reticulatae, 5 parts of peppermint oil.
3. sunstroke prevention mosquito-repellent essential oil according to claim 1, which is characterized in that include the raw material of following mass fraction：Wrinkled giant hyssop
8 parts of oil, 8 parts of Blumea oil, 8 parts of elsholtzia oil, 8 parts of Herba Eupatorii Fortunei oil, 8 parts of caryophyllus oil, 8 parts of Oleum Citri Reticulatae, 8 parts of peppermint oil.
4. a kind of preparation method of sunstroke prevention mosquito-repellent essential oil, which is characterized in that include the following steps：
Raw material is weighed according to proportioning, wherein raw material proportioning is：0-10 parts of palchouli oil, 0-10 parts of Blumea oil, 0-10 parts of elsholtzia oil are worn
Blue 0-10 parts of oil, 0-10 parts of caryophyllus oil, 0-10 parts of Oleum Citri Reticulatae, 0-10 parts of peppermint oil；
Under vacuum, raw material is uniformly mixed.
5. the preparation method of sunstroke prevention mosquito-repellent essential oil according to claim 4, which is characterized in that the palchouli oil is using organic
Solvent extraction method is made；The Blumea oil and Herba Eupatorii Fortunei oil use CO2Supercritical extraction is made；The elsholtzia oil, caryophyllus oil and
Peppermint oil is made using ultrasonic wave assisted extraction method；The Oleum Citri Reticulatae is made using steam distillation.
6. the preparation method of sunstroke prevention mosquito-repellent essential oil according to claim 5, which is characterized in that the palchouli oil it is organic molten
In agent extraction method, use petroleum ether for solvent, petroleum ether dosage is 3~5 times of amounts, and Extracting temperature is 40~45 DEG C, and extraction is multiple.
7. the preparation method of sunstroke prevention mosquito-repellent essential oil according to claim 5, which is characterized in that the CO of the Blumea oil2It is super to face
In boundary's extraction, extracting pressure 20MPa, extraction temperature is 30~35 DEG C, and extraction time is 100~120min, CO2Flow is
24kg/h, separating pressure 8Mpa, separation temperature are 50~55 DEG C；The CO of the Herba Eupatorii Fortunei oil2In supercritical extraction, extraction pressure
Power is 15MPa, and extraction temperature is 30~35 DEG C, extraction time 60-90min, CO2Flow is 20kg/h, separating pressure 7-
8Mpa, separation temperature are 55~60 DEG C.
8. the preparation method of sunstroke prevention mosquito-repellent essential oil according to claim 5, which is characterized in that the ultrasonic wave of the elsholtzia oil
In assisted extraction method, use petroleum ether for solvent, liquid ratio 12.1mL/g, 50~60 DEG C of ultrasonic temperature, ultrasonic time be 30~
60min；
It in the ultrasonic wave assisted extraction method of the caryophyllus oil, is impregnated using 75% ethyl alcohol, ultrasonic time is 60~90min, ultrasound
Temperature is 65~70 DEG C, the concentrate that rotary evaporation is precipitated to no ethyl alcohol, solid-liquid ratio 1:20, then with the n-hexane extraction concentration
Liquid evaporates n-hexane, obtains caryophyllus oil；
In the ultrasonic wave assisted extraction method of the peppermint oil, distillation time is 120~135min, ultrasonic power 300-
400W, sonication times are 10~20min.
9. the preparation method of sunstroke prevention mosquito-repellent essential oil according to claim 5, which is characterized in that the vapor of the Oleum Citri Reticulatae
In the way of distillation, tangerine peel powder adds 6~8 times of amount water to impregnate 1~2h, distills 5~6h at coarse powder.
10. a kind of application method based on sunstroke prevention mosquito-repellent essential oil described in claim 1, which is characterized in that drive the sunstroke prevention
Mosquito essential oil instills in fumigating machine, is evaporated by way of atomization.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112262858A (en) * | 2020-09-30 | 2021-01-26 | 深圳市妇幼保健院 | Mosquito-repellent essential oil |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103230351A (en) * | 2013-04-28 | 2013-08-07 | 马瑞 | All natural mosquito repel |
| CN103585540A (en) * | 2013-08-31 | 2014-02-19 | 云南中医学院 | Incense-fumigating oil of rhizoma atractylodis and folium artemisiae argyi |
| CN104585255A (en) * | 2015-01-05 | 2015-05-06 | 刘向上 | Mosquito-repelling bactericide |
| CN106266685A (en) * | 2016-08-27 | 2017-01-04 | 广东罗浮山国药股份有限公司 | A kind of compound essential Oil and preparation method thereof |
| CN106577841A (en) * | 2017-01-05 | 2017-04-26 | 殷林勇 | Electric heating type Chinese mugwort essential oil mosquito repellent |
| CN107343865A (en) * | 2017-08-03 | 2017-11-14 | 成都煜泉绿健科技有限公司 | A kind of compound volatile oil and preparation method thereof, application |
-
2018
- 2018-06-13 CN CN201810605468.1A patent/CN108719350A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103230351A (en) * | 2013-04-28 | 2013-08-07 | 马瑞 | All natural mosquito repel |
| CN103585540A (en) * | 2013-08-31 | 2014-02-19 | 云南中医学院 | Incense-fumigating oil of rhizoma atractylodis and folium artemisiae argyi |
| CN104585255A (en) * | 2015-01-05 | 2015-05-06 | 刘向上 | Mosquito-repelling bactericide |
| CN106266685A (en) * | 2016-08-27 | 2017-01-04 | 广东罗浮山国药股份有限公司 | A kind of compound essential Oil and preparation method thereof |
| CN106577841A (en) * | 2017-01-05 | 2017-04-26 | 殷林勇 | Electric heating type Chinese mugwort essential oil mosquito repellent |
| CN107343865A (en) * | 2017-08-03 | 2017-11-14 | 成都煜泉绿健科技有限公司 | A kind of compound volatile oil and preparation method thereof, application |
Non-Patent Citations (2)
| Title |
|---|
| 尹莲: "《天然药物化学 新世纪第2版》", 31 July 2017, 中国中医药出版社 * |
| 张卫明: "《芳香疗法和芳疗植物》", 31 August 2009, 东南大学出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112262858A (en) * | 2020-09-30 | 2021-01-26 | 深圳市妇幼保健院 | Mosquito-repellent essential oil |
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