CN108685057A - A kind of preparation method of propolis red date instant powder - Google Patents

A kind of preparation method of propolis red date instant powder Download PDF

Info

Publication number
CN108685057A
CN108685057A CN201810491654.7A CN201810491654A CN108685057A CN 108685057 A CN108685057 A CN 108685057A CN 201810491654 A CN201810491654 A CN 201810491654A CN 108685057 A CN108685057 A CN 108685057A
Authority
CN
China
Prior art keywords
propolis
jujube
preparation
gauze
filtered
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201810491654.7A
Other languages
Chinese (zh)
Inventor
秦义山
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wuhu Haoyikuai Food Co Ltd Sanshan Branch
Original Assignee
Wuhu Haoyikuai Food Co Ltd Sanshan Branch
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wuhu Haoyikuai Food Co Ltd Sanshan Branch filed Critical Wuhu Haoyikuai Food Co Ltd Sanshan Branch
Priority to CN201810491654.7A priority Critical patent/CN108685057A/en
Publication of CN108685057A publication Critical patent/CN108685057A/en
Withdrawn legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L19/00Products from fruits or vegetables; Preparation or treatment thereof
    • A23L19/01Instant products; Powders; Flakes; Granules
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L19/00Products from fruits or vegetables; Preparation or treatment thereof
    • A23L19/09Mashed or comminuted products, e.g. pulp, purée, sauce, or products made therefrom, e.g. snacks
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L21/00Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
    • A23L21/20Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23PSHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00Shaping or working of foodstuffs characterised by the products
    • A23P10/20Agglomerating; Granulating; Tabletting
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Jellies, Jams, And Syrups (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

A kind of preparation method of propolis red date instant powder, belongs to bee glue powder preparing technical field, including:Prepare jujube juice, propolis Freezing smashing, porcelain mortar grinding slightly carry, normal-temperature superhigh pressure extract, by jujube juice propolis extract mix mixed liquor, concentration, be freeze-dried propolis coarse powder, smash to obtain propolis micro mist.The product of the present invention not only improves the aesthetic quality of propolis product, and provides approach for the application field for further widening propolis product.Jujube can improve the undesirable mouthfeel of propolis well, and product has apparent jujube fragrance, without any undesirable pungent taste.The problems such as the problem of present invention is first slightly carried with ethyl alcohol, then through ultra high pressure extraction, can improve the utilization rate and flour extraction of propolis, and use ultra high pressure extraction overcomes Microwave Extraction uneven heating and ultrasonic wave extraction power consumption are big, noise.The propolis micro powder granule of the present invention is small, and average grain diameter is less than 70 μm, and regular shape, uniformity is good, and surface is smooth.

Description

A kind of preparation method of propolis red date instant powder
Technical field
The invention belongs to bee glue powder preparing technical fields, and in particular to a kind of preparation method of propolis red date instant powder.
Background technology
Propolis (propolis) is the resin setting the positions such as bud, bark acquire of the honeybee from plant, is blended into the tongue of honeybee The glandular secretions object such as gland, wax gland, through a kind of colloid substance made of honeybee process change.Recent study finds that propolis has Anticancer, protection liver, improves body's immunity and a variety of biological functions such as anti-oxidant at anti-sex pheromone, thus by The common concern of whole world various countries businessman.Propolis glue is classified as and can add in the material list of health food by China, is The utilization of propolis provide the guarantee in policy.
Functional components in propolis are extracted often using ethyl alcohol as solvent using the method for standing or being heated to reflux, but The shortcomings of this method is high with temperature there are extraction time length, is broken so as to cause the molten functional materials of flavonoids alcohol by different degrees of It is bad.In addition, the methods of microwave, ultrasonic wave are applied the extraction in propolis by somebody, but it is at laboratory's stage now.Microwave Extraction is substantially heating extraction, and there are problems that uneven heating.Although ultrasonic wave extraction has also carried out more research, But it only rests on laboratory scale, since its power consumption is big, the problems such as noise, makes it difficult to realize industrially scalable life Production.
Currently, both at home and abroad propolis product have it is tens of in, it is in the majority as the product of carrier using alcohol.This kind of product is because containing highly concentrated The alcohol of degree, takes extremely inconvenient, and many products have strong impulse taste, and consumer is difficult to entrance, and some consumers are to wine Smart allergy cannot be taken containing spirituous propolis product, and further applying for propolis is limited.Therefore exploitation aesthetic quality it is good, Propolis product with healthcare function is imperative.
Invention content
In order to solve the problems in the existing technology, the present invention provides a kind of preparation sides of propolis red date instant powder Method improves the aesthetic quality of propolis product, and propolis micro powder granule obtained is uniform.
The present invention uses following technical scheme:
A kind of preparation method of propolis red date instant powder, includes the following steps:
Step 1:It after the selected removal disease pest fruit of jujube, rotten fruit and underdone drying shrinkage fruit, cleans up, in 65 DEG C of drying Surface moisture removes jujube core with card punch, and jujube meat is cut into the bulk of 0.5cm square, and the water that jujube meat weighs 6 times, heating stirring is added After uniformly, using by pectase and cellulase in mass ratio 1:The mixed enzyme of 2 compositions carries out enzymolysis extraction of the juice, temperature 40 to jujube DEG C, extraction time 4h, enzyme dosage 2400mg/L, filter to obtain jujube juice;
Step 2:Propolis is freezed into 2-3h under the conditions of -80 DEG C, smashes it through 40 mesh sieve, bottling is spare;
Step 3:The ethanol solution that the propolis 5g that Freezing smashing of learning from else's experience is crossed is 70% with 25mL volumetric concentrations in porcelain mortar It is ground into paste, and is put into container and seals, is impregnated at room temperature for 24 hours, filtered through gauze, filter residue adds same volume and concentration Ethyl alcohol extracts 2 times repeatedly, merging filtrate;
Step 4:Filtrate is dissolved in the ethanol solution that 175mL volumetric concentrations are 70%, impregnates 48h, timing agitation, room temperature Super-pressure 350-400Mpa extracts 2-10min, and filtered through gauze obtains propolis extract;
Step 5:By jujube juice, propolis extract and gelatin in mass ratio 100:300:1 ratio mixing, obtains mixed liquor;
Step 6:Mixed liquor is concentrated into 40min for 60-70 DEG C in Rotary Evaporators, concentrate is obtained, is poured out after recycling ethyl alcohol Medicinal extract;
Step 7:Concentrate is freeze-dried at -45 DEG C and is warming up to 40 DEG C after 48h and makes water sublimed, obtains propolis coarse powder;
Step 8:Propolis coarse powder is put into Baily pulverizer, dry pulverization process is carried out to it, 15min is crushed at -20 DEG C and is obtained Propolis micro mist.
Preferably, the propolis micro mist average grain diameter described in step 8 is less than 70 μm.
Preferably, the super-pressure 350MPa described in step 4 extracts 2min.
Preferably, the filtering described in step 1 is to use three layers of filtered through gauze.
Preferably, the filtered through gauze described in step 3 is to use two layers of filtered through gauze.
Preferably, the filtered through gauze described in step 4 is to use 8-12 layers of filtered through gauze.
Preferably, the timing agitation described in step 4 is primary every 4h stirrings.
The beneficial effects of the present invention are:
1) product of the invention not only improves the aesthetic quality of propolis product, and further to widen propolis product Application field provides approach.Jujube can improve the undesirable mouthfeel of propolis well, and product has apparent jujube fragrance, Without any undesirable pungent taste.
2) present invention is first slightly carried with ethyl alcohol, then through ultra high pressure extraction, can improve the utilization rate and flour extraction of propolis, and is adopted The problems such as the problem of overcoming Microwave Extraction uneven heating with ultra high pressure extraction and ultrasonic wave extraction power consumption are big, noise.
3) propolis micro powder granule of the invention is small, and average grain diameter is less than 70 μm, and regular shape, uniformity is good, and table Face is smooth, and powder characteristics is better than propolis coarse powder.
4) present invention is extracted using the ethyl alcohol of volumetric concentration 70%, and extract has physiological activity.
5) rate is digested and absorbed by what superfine communication technique can improve propolis.
Specific implementation mode
With reference to embodiments, the technical solution in the present invention is clearly and completely described.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.
Embodiment 1
A kind of preparation method of propolis red date instant powder, includes the following steps:
Step 1:It after the selected removal disease pest fruit of jujube, rotten fruit and underdone drying shrinkage fruit, cleans up, in 65 DEG C of drying Surface moisture removes jujube core with card punch, and jujube meat is cut into the bulk of 0.5cm square, and the water that jujube meat weighs 6 times, heating stirring is added After uniformly, using by pectase and cellulase in mass ratio 1:The mixed enzyme of 2 compositions carries out enzymolysis extraction of the juice, temperature 40 to jujube DEG C, extraction time 4h, enzyme dosage 2400mg/L, filter to obtain jujube juice;
Step 2:Propolis is freezed into 2h under the conditions of -80 DEG C, smashes it through 40 mesh sieve, bottling is spare;
Step 3:The ethanol solution that the propolis 5g that Freezing smashing of learning from else's experience is crossed is 70% with 25mL volumetric concentrations in porcelain mortar It is ground into paste, and is put into container and seals, is impregnated at room temperature for 24 hours, filtered through gauze, filter residue adds same volume and concentration Ethyl alcohol extracts 2 times repeatedly, merging filtrate;
Step 4:Filtrate is dissolved in the ethanol solution that 175mL volumetric concentrations are 70%, impregnates 48h, timing agitation, room temperature Super-pressure 350Mpa extracts 2min, and filtered through gauze obtains propolis extract;
Step 5:By jujube juice, propolis extract and gelatin in mass ratio 100:300:1 ratio mixing, obtains mixed liquor;
Step 6:Mixed liquor is concentrated into 40min for 60 DEG C in Rotary Evaporators, concentrate is obtained, leaching is poured out after recycling ethyl alcohol Cream;
Step 7:Concentrate is freeze-dried at -45 DEG C and is warming up to 40 DEG C after 48h and makes water sublimed, obtains propolis coarse powder;
Step 8:Propolis coarse powder is put into Baily pulverizer, dry pulverization process is carried out to it, 15min is crushed at -20 DEG C and is obtained Propolis micro mist.
Propolis micro mist average grain diameter described in step 8 is less than 70 μm;Filtering described in step 1 is to use three layers of yarn Cloth filters;Filtered through gauze described in step 3 is to use two layers of filtered through gauze;Filtered through gauze described in step 4 is to use 8 Layer filtered through gauze;Timing agitation described in step 4 is primary every 4h stirrings.
Embodiment 2
A kind of preparation method of propolis red date instant powder, includes the following steps:
Step 1:It after the selected removal disease pest fruit of jujube, rotten fruit and underdone drying shrinkage fruit, cleans up, in 65 DEG C of drying Surface moisture removes jujube core with card punch, and jujube meat is cut into the bulk of 0.5cm square, and the water that jujube meat weighs 6 times, heating stirring is added After uniformly, using by pectase and cellulase in mass ratio 1:The mixed enzyme of 2 compositions carries out enzymolysis extraction of the juice, temperature 40 to jujube DEG C, extraction time 4h, enzyme dosage 2400mg/L, filter to obtain jujube juice;
Step 2:Propolis is freezed into 3h under the conditions of -80 DEG C, smashes it through 40 mesh sieve, bottling is spare;
Step 3:The ethanol solution that the propolis 5g that Freezing smashing of learning from else's experience is crossed is 70% with 25mL volumetric concentrations in porcelain mortar It is ground into paste, and is put into container and seals, is impregnated at room temperature for 24 hours, filtered through gauze, filter residue adds same volume and concentration Ethyl alcohol extracts 2 times repeatedly, merging filtrate;
Step 4:Filtrate is dissolved in the ethanol solution that 175mL volumetric concentrations are 70%, impregnates 48h, timing agitation, room temperature Super-pressure 400Mpa extracts 10min, and filtered through gauze obtains propolis extract;
Step 5:By jujube juice, propolis extract and gelatin in mass ratio 100:300:1 ratio mixing, obtains mixed liquor;
Step 6:Mixed liquor is concentrated into 40min for 70 DEG C in Rotary Evaporators, concentrate is obtained, leaching is poured out after recycling ethyl alcohol Cream;
Step 7:Concentrate is freeze-dried at -45 DEG C and is warming up to 40 DEG C after 48h and makes water sublimed, obtains propolis coarse powder;
Step 8:Propolis coarse powder is put into Baily pulverizer, dry pulverization process is carried out to it, 15min is crushed at -20 DEG C and is obtained Propolis micro mist.
Propolis micro mist average grain diameter described in step 8 is less than 70 μm;Filtering described in step 1 is to use three layers of yarn Cloth filters;Filtered through gauze described in step 3 is to use two layers of filtered through gauze;Filtered through gauze described in step 4 is to use 12 layers of filtered through gauze;Timing agitation described in step 4 is primary every 4h stirrings.
The present invention is exemplarily described above, it is clear that present invention specific implementation is not subject to the restrictions described above, As long as using the improvement of the various unsubstantialities of inventive concept and technical scheme of the present invention progress, or not improved this is sent out Bright design and technical solution directly applies to other occasions, within protection scope of the present invention.The protection of the present invention Range should be determined by the scope of protection defined in the claims.

Claims (7)

1. a kind of preparation method of propolis red date instant powder, which is characterized in that include the following steps:
Step 1:It after the selected removal disease pest fruit of jujube, rotten fruit and underdone drying shrinkage fruit, cleans up, surface is dried in 65 DEG C Moisture removes jujube core with card punch, and jujube meat is cut into the bulk of 0.5cm square, and the water that jujube meat weighs 6 times is added, and heating stirring is uniform Afterwards, using by pectase and cellulase in mass ratio 1:The mixed enzymes of 2 compositions carry out enzymolysis extraction of the juice to jujube, 40 DEG C of temperature, Extraction time 4h, enzyme dosage 2400mg/L, filter to obtain jujube juice;
Step 2:Propolis is freezed into 2-3h under the conditions of -80 DEG C, smashes it through 40 mesh sieve, bottling is spare;
Step 3:The ethanol solution that the propolis 5g that Freezing smashing of learning from else's experience is crossed is 70% with 25mL volumetric concentrations in porcelain mortar is ground into Paste, and be put into container and seal, it impregnates at room temperature for 24 hours, filtered through gauze, filter residue adds the ethyl alcohol of same volume and concentration It extracts 2 times repeatedly, merging filtrate;
Step 4:Filtrate is dissolved in the ethanol solution that 175mL volumetric concentrations are 70%, impregnates 48h, timing agitation, room temperature superelevation 350-400Mpa is pressed to extract 2-10min, filtered through gauze obtains propolis extract;
Step 5:By jujube juice, propolis extract and gelatin in mass ratio 100:300:1 ratio mixing, obtains mixed liquor;
Step 6:Mixed liquor is concentrated into 40min for 60-70 DEG C in Rotary Evaporators, concentrate is obtained, leaching is poured out after recycling ethyl alcohol Cream;
Step 7:Concentrate is freeze-dried at -45 DEG C and is warming up to 40 DEG C after 48h and makes water sublimed, obtains propolis coarse powder;
Step 8:Propolis coarse powder is put into Baily pulverizer, dry pulverization process is carried out to it, 15min is crushed at -20 DEG C and obtains propolis Micro mist.
2. a kind of preparation method of propolis red date instant powder according to claim 1, it is characterised in that:Described in step 8 Propolis micro mist average grain diameter be less than 70 μm.
3. a kind of preparation method of propolis red date instant powder according to claim 1, it is characterised in that:Described in step 4 Super-pressure 350MPa, extract 2min.
4. a kind of preparation method of propolis red date instant powder according to claim 1, it is characterised in that:Described in step 1 Filtering be use three layers of filtered through gauze.
5. a kind of preparation method of propolis red date instant powder according to claim 1, it is characterised in that:Described in step 3 Filtered through gauze be use two layers of filtered through gauze.
6. a kind of preparation method of propolis red date instant powder according to claim 1, it is characterised in that:Described in step 4 Filtered through gauze be use 8-12 layers of filtered through gauze.
7. a kind of preparation method of propolis red date instant powder according to claim 1, it is characterised in that:Described in step 4 Timing agitation be primary every 4h stirrings.
CN201810491654.7A 2018-05-22 2018-05-22 A kind of preparation method of propolis red date instant powder Withdrawn CN108685057A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810491654.7A CN108685057A (en) 2018-05-22 2018-05-22 A kind of preparation method of propolis red date instant powder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810491654.7A CN108685057A (en) 2018-05-22 2018-05-22 A kind of preparation method of propolis red date instant powder

Publications (1)

Publication Number Publication Date
CN108685057A true CN108685057A (en) 2018-10-23

Family

ID=63846760

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810491654.7A Withdrawn CN108685057A (en) 2018-05-22 2018-05-22 A kind of preparation method of propolis red date instant powder

Country Status (1)

Country Link
CN (1) CN108685057A (en)

Similar Documents

Publication Publication Date Title
CN101948897B (en) Method for extracting shinyleaf yellowhorn oil, shinyleaf yellowhorn polysaccharide and shinyleaf yellowhorn protolysate peptide from shinyleaf yellowhorn
CN101099513B (en) Cordyceps sinensis dried milk slices and producing method thereof
CN105076612A (en) Preparation method of instant tangerine peel oil tea powder and product of instant tangerine peel oil tea powder
CN103387919A (en) Production process of lucid ganoderma wine
CN104757191A (en) Enzymolysis technology used for preparing instant tea powder
CN104664539A (en) Production method of ginseng solid beverage
CN106085750A (en) A kind of processing method of Rhizoma Bistortae Radix ziziphi mauritianae health promoting wine
CN109170885A (en) A method of extracting ginseng effective component
CN101906169A (en) Process combination for preparing bletilla polysaccharide
CN104970418A (en) Production method for biological osmanthus by complex enzyme method
CN105379869A (en) Roxburgh rose black tea and preparation method thereof
CN105520156A (en) Preparation method of grape seed soluble dietary fiber
CN107281264A (en) A kind of preparation method and Cortex cinnamomi japonici (Ramulus Cinnamomi) extract that Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is produced from cinnamomi cortex pulveratus residue
CN108685057A (en) A kind of preparation method of propolis red date instant powder
CN108354157A (en) A kind of preparation method of propolis micro mist
CN105211401A (en) A kind of beauty treatment flowers and plants protein tea and preparation method thereof
CN108685074A (en) A kind of preparation method of propolis purple sweet potato powder
CN109293728A (en) A kind of green low cost preparation method of high-purity tea saponin
CN109123321A (en) A kind of extraction and preparation process of apple polyphenol
CN104431093A (en) Instant highland barley tea and preparation method thereof
CN112175741A (en) Method for extracting tea saponin from tea seed cake
CN105462752A (en) Phellinus igniarius and folium mori rice wine and preparation method thereof
CN106343565A (en) Momordica grosvenori health food and preparing method thereof
CN101380337B (en) Low temperature dynamic extraction method of plant effective ingredient
CN108925725A (en) A kind of processing method of Hedge Prinsepia Nut caffein

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WW01 Invention patent application withdrawn after publication

Application publication date: 20181023

WW01 Invention patent application withdrawn after publication