CN108669102A - A kind of preparation method of the disease control liquid of purple willow growth - Google Patents
A kind of preparation method of the disease control liquid of purple willow growth Download PDFInfo
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- CN108669102A CN108669102A CN201810669412.2A CN201810669412A CN108669102A CN 108669102 A CN108669102 A CN 108669102A CN 201810669412 A CN201810669412 A CN 201810669412A CN 108669102 A CN108669102 A CN 108669102A
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- processing
- purple willow
- disease control
- control liquid
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/10—Apiaceae or Umbelliferae [Carrot family], e.g. parsley, caraway, dill, lovage, fennel or snakebed
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/32—Ranunculaceae [Buttercup family], e.g. hepatica, hydrastis or goldenseal
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
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- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
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- Biotechnology (AREA)
- Agronomy & Crop Science (AREA)
- Mycology (AREA)
- Plant Pathology (AREA)
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of preparation methods of the disease control liquid of purple willow growth, include the following steps：（1）Raw material weighs,（2）Raw material frying processing,（3）Extraction process.The present invention provides a kind of preparation methods of disease control liquid, overall step is simple, it is convenient to prepare, wherein using a variety of Chinese herbal medicines as raw material, extracts active ingredient jointly, there is control effect to the multiple diseases of purple willow growth, and prevention liquid obtained is safe and non-toxic, is not likely to produce drug resistance, drug effect is continual and steady, and rust, dead leaf disease, the incidence of root rot being easy to get in can growing purple willow are down to 3% or less, significantly improve the quality of growth and the benefit of plantation, great application value.
Description
Technical field
The invention belongs to purple willow planting technology fields, and in particular to a kind of preparation side of the disease control liquid of purple willow growth
Method.
Background technology
Wicker plaiting article is one of folks of china traditional handicraft product, is a kind of environment-friendly natural material that can be used in numerous areas
Material.People are intended only as common daily utility in ancient times, after 20th century decades just gradually rise, also gradually at
For the project of selected areas of China foreign exchange earning.
Purple willow is the common raw material of wicker plaiting article, and quality and yield affects the development of wicker plaiting article industry.Many plantations now
Purple willow is planted to provide raw material for willow-plaited process product in family, and purple willow can be corroded in growth course by multiple diseases, into
And the yield of plantation is affected, while going mouldy etc. of generating influences whether the yield rate subsequently woven and quality, therefore planting
When reduce well the incidence of disease for plant and wicker plaiting article industry for all have significance.
Invention content
The purpose of the present invention is for existing problem, provide a kind of preparation side of the disease control liquid of purple willow growth
Method.
The present invention is achieved by the following technical solutions：
A kind of preparation method of the disease control liquid of purple willow growth, includes the following steps：
（1）Raw material weighs：
Following substance is weighed by corresponding parts by weight：7 ~ 10 parts of lepidium seeds, 3 ~ 5 portions of tussilagoes, 4 ~ 6 portions of butterflybush flowers, 10 ~ 14 portions of henon bamboos
Leaf, 5 ~ 8 parts of ginkgo leaves, 4 ~ 7 parts of frutus cnidiis, 6 ~ 9 parts of chrysanthemums, 8 ~ 12 portions of coptiss；
（2）Raw material frying is handled：
A. first lepidium seed, tussilago, butterflybush flower, lophatherum gracile are put into jointly in the marmite for filling rice, continuous stir-frying processing
It is taken out after 40 ~ 45min, it is spare to obtain mixture A after elimination rice；
B. ginkgo leaf, frutus cnidii, chrysanthemum, the coptis are put into jointly in the marmite for filling river sand, the processing 35 that constantly stir-fries ~
It is taken out after 40min, it is spare to obtain mixture B after elimination river sand；
（3）Extraction process：
A. first by step（2）The mixture A and mixture B of gained are put into pot after processing, and 4 ~ 6 times of its gross mass is then added
Clear water, heating boiling boil 1 ~ 2h of processing after filter, obtain first-time filtrate and filter residue be spare；
B. after the filter residue obtained by operation a being put into ethanol solution constantly 10 ~ 14h of reflux extraction processing, leaching liquor is taken out
It is spare；
C. the leaching liquor obtained by first-time filtrate and operation b obtained by a will be operated to mix jointly, after 1 ~ 1.5h of sonic oscillation processing i.e.
It can.
Further, step（2）Temperature when operating the stir-frying processing described in a in control marmite is 90 ~ 95 DEG C.
Further, step（2）Temperature when operating the stir-frying processing described in b in control marmite is 95 ~ 100 DEG C.
Further, step（3）Operate c described in sonic oscillation processing when control ultrasonic wave frequency be 500 ~
550kHz。
The present invention has the following advantages compared with prior art：
The present invention provides a kind of preparation methods of disease control liquid, and overall step is simple, and it is convenient to prepare, wherein with a variety of medium-height grass
Medicine is raw material, extracts active ingredient jointly, has control effect to the multiple diseases of purple willow growth, and prevention liquid obtained is pacified
Atoxic is not likely to produce drug resistance, and drug effect is continual and steady, the hair of the rust, dead leaf disease, root rot that are easy to get in can growing purple willow
Raw rate is down to 3% hereinafter, significantly improve the quality of growth and the benefit of plantation, great application value.
Specific implementation mode
Embodiment 1
A kind of preparation method of the disease control liquid of purple willow growth, includes the following steps：
（1）Raw material weighs：
Following substance is weighed by corresponding parts by weight：7 parts of lepidium seeds, 3 portions of tussilagoes, 4 portions of butterflybush flowers, 10 portions of lophatherum graciles, 5 portions of ginkgoes
Leaf, 4 parts of frutus cnidiis, 6 parts of chrysanthemums, 8 portions of coptiss；
（2）Raw material frying is handled：
A. first lepidium seed, tussilago, butterflybush flower, lophatherum gracile are put into jointly in the marmite for filling rice, continuous stir-frying processing
It is taken out after 40min, it is spare to obtain mixture A after elimination rice；
B. ginkgo leaf, frutus cnidii, chrysanthemum, the coptis are put into jointly in the marmite for filling river sand, after constantly stir-frying processing 35min
It takes out, it is spare to obtain mixture B after elimination river sand；
（3）Extraction process：
A. first by step（2）The mixture A and mixture B of gained are put into pot after processing, and 4 times of its gross mass is then added
Clear water, heating boiling filter after boiling processing 1h, obtain first-time filtrate and filter residue is spare；
B. after the filter residue obtained by operation a being put into ethanol solution constantly reflux extraction processing 10h, leaching liquor is taken out standby
With；
C. the first-time filtrate obtained by a will be operated and the leaching liquor obtained by operation b mixes jointly, after sonic oscillation handles 1h.
Further, step（2）Temperature when operating the stir-frying processing described in a in control marmite is 90 DEG C.
Further, step（2）Temperature when operating the stir-frying processing described in b in control marmite is 95 DEG C.
Further, step（3）The frequency of control ultrasonic wave is 500kHz when operating the sonic oscillation processing described in c.
Embodiment 2
A kind of preparation method of the disease control liquid of purple willow growth, includes the following steps：
（1）Raw material weighs：
Following substance is weighed by corresponding parts by weight：9 parts of lepidium seeds, 4 portions of tussilagoes, 5 portions of butterflybush flowers, 12 portions of lophatherum graciles, 7 portions of ginkgoes
Leaf, 6 parts of frutus cnidiis, 8 parts of chrysanthemums, 10 portions of coptiss；
（2）Raw material frying is handled：
A. first lepidium seed, tussilago, butterflybush flower, lophatherum gracile are put into jointly in the marmite for filling rice, continuous stir-frying processing
It is taken out after 43min, it is spare to obtain mixture A after elimination rice；
B. ginkgo leaf, frutus cnidii, chrysanthemum, the coptis are put into jointly in the marmite for filling river sand, after constantly stir-frying processing 37min
It takes out, it is spare to obtain mixture B after elimination river sand；
（3）Extraction process：
A. first by step（2）The mixture A and mixture B of gained are put into pot after processing, and 5 times of its gross mass is then added
Clear water, heating boiling filter after boiling processing 1.5h, obtain first-time filtrate and filter residue is spare；
B. after the filter residue obtained by operation a being put into ethanol solution constantly reflux extraction processing 12h, leaching liquor is taken out standby
With；
C. the leaching liquor obtained by first-time filtrate and operation b obtained by a will be operated to mix jointly, after sonic oscillation processing 1.3h i.e.
It can.
Further, step（2）Temperature when operating the stir-frying processing described in a in control marmite is 92 DEG C.
Further, step（2）Temperature when operating the stir-frying processing described in b in control marmite is 97 DEG C.
Further, step（3）The frequency of control ultrasonic wave is 530kHz when operating the sonic oscillation processing described in c.
Embodiment 3
A kind of preparation method of the disease control liquid of purple willow growth, includes the following steps：
（1）Raw material weighs：
Following substance is weighed by corresponding parts by weight：10 parts of lepidium seeds, 5 portions of tussilagoes, 6 portions of butterflybush flowers, 14 portions of lophatherum graciles, 8 parts of silver
Apricot leaf, 7 parts of frutus cnidiis, 9 parts of chrysanthemums, 12 portions of coptiss；
（2）Raw material frying is handled：
A. first lepidium seed, tussilago, butterflybush flower, lophatherum gracile are put into jointly in the marmite for filling rice, continuous stir-frying processing
It is taken out after 45min, it is spare to obtain mixture A after elimination rice；
B. ginkgo leaf, frutus cnidii, chrysanthemum, the coptis are put into jointly in the marmite for filling river sand, after constantly stir-frying processing 40min
It takes out, it is spare to obtain mixture B after elimination river sand；
（3）Extraction process：
A. first by step（2）The mixture A and mixture B of gained are put into pot after processing, and 6 times of its gross mass is then added
Clear water, heating boiling filter after boiling processing 2h, obtain first-time filtrate and filter residue is spare；
B. after the filter residue obtained by operation a being put into ethanol solution constantly reflux extraction processing 14h, leaching liquor is taken out standby
With；
C. the leaching liquor obtained by first-time filtrate and operation b obtained by a will be operated to mix jointly, after sonic oscillation processing 1.5h i.e.
It can.
Further, step（2）Temperature when operating the stir-frying processing described in a in control marmite is 95 DEG C.
Further, step（2）Temperature when operating the stir-frying processing described in b in control marmite is 100 DEG C.
Further, step（3）The frequency of control ultrasonic wave is 550kHz when operating the sonic oscillation processing described in c.
The present invention, up to 97% or more, can significantly improve the quality of purple willow growth, by Qi to the control rate of purple willow Common Diseases
The planting benefit of willow increases 25% or more, great application value.
Claims (4)
1. a kind of preparation method of the disease control liquid of purple willow growth, which is characterized in that include the following steps：
（1）Raw material weighs：
Following substance is weighed by corresponding parts by weight：7 ~ 10 parts of lepidium seeds, 3 ~ 5 portions of tussilagoes, 4 ~ 6 portions of butterflybush flowers, 10 ~ 14 portions of henon bamboos
Leaf, 5 ~ 8 parts of ginkgo leaves, 4 ~ 7 parts of frutus cnidiis, 6 ~ 9 parts of chrysanthemums, 8 ~ 12 portions of coptiss；
（2）Raw material frying is handled：
A. first lepidium seed, tussilago, butterflybush flower, lophatherum gracile are put into jointly in the marmite for filling rice, continuous stir-frying processing
It is taken out after 40 ~ 45min, it is spare to obtain mixture A after elimination rice；
B. ginkgo leaf, frutus cnidii, chrysanthemum, the coptis are put into jointly in the marmite for filling river sand, the processing 35 that constantly stir-fries ~
It is taken out after 40min, it is spare to obtain mixture B after elimination river sand；
（3）Extraction process：
A. first by step（2）The mixture A and mixture B of gained are put into pot after processing, and 4 ~ 6 times of its gross mass is then added
Clear water, heating boiling boil 1 ~ 2h of processing after filter, obtain first-time filtrate and filter residue be spare；
B. after the filter residue obtained by operation a being put into ethanol solution constantly 10 ~ 14h of reflux extraction processing, leaching liquor is taken out
It is spare；
C. the leaching liquor obtained by first-time filtrate and operation b obtained by a will be operated to mix jointly, after 1 ~ 1.5h of sonic oscillation processing i.e.
It can.
2. a kind of preparation method of the disease control liquid of purple willow growth according to claim 1, which is characterized in that step
（2）Temperature when operating the stir-frying processing described in a in control marmite is 90 ~ 95 DEG C.
3. a kind of preparation method of the disease control liquid of purple willow growth according to claim 1, which is characterized in that step
（2）Temperature when operating the stir-frying processing described in b in control marmite is 95 ~ 100 DEG C.
4. a kind of preparation method of the disease control liquid of purple willow growth according to claim 1, which is characterized in that step
（3）The frequency of control ultrasonic wave is 500 ~ 550kHz when operating the sonic oscillation processing described in c.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810669412.2A CN108669102A (en) | 2018-06-26 | 2018-06-26 | A kind of preparation method of the disease control liquid of purple willow growth |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810669412.2A CN108669102A (en) | 2018-06-26 | 2018-06-26 | A kind of preparation method of the disease control liquid of purple willow growth |
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| Publication Number | Publication Date |
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| CN108669102A true CN108669102A (en) | 2018-10-19 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810669412.2A Pending CN108669102A (en) | 2018-06-26 | 2018-06-26 | A kind of preparation method of the disease control liquid of purple willow growth |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110326626A (en) * | 2019-08-05 | 2019-10-15 | 云南中医药大学 | The new application of lepidium seed volatile oil |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104782685A (en) * | 2015-03-24 | 2015-07-22 | 阜南县永兴工艺品有限公司 | Medicine for treating salix purpurea yellows |
| CN108049170A (en) * | 2017-12-22 | 2018-05-18 | 阜阳皖春家俬有限公司 | A kind of additive for promoting palm mattress mildew and insect proof characteristic |
-
2018
- 2018-06-26 CN CN201810669412.2A patent/CN108669102A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104782685A (en) * | 2015-03-24 | 2015-07-22 | 阜南县永兴工艺品有限公司 | Medicine for treating salix purpurea yellows |
| CN108049170A (en) * | 2017-12-22 | 2018-05-18 | 阜阳皖春家俬有限公司 | A kind of additive for promoting palm mattress mildew and insect proof characteristic |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110326626A (en) * | 2019-08-05 | 2019-10-15 | 云南中医药大学 | The new application of lepidium seed volatile oil |
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Application publication date: 20181019 |