CN108839171A - A kind of preparation method of purple willow branch combined processing liquid - Google Patents

A kind of preparation method of purple willow branch combined processing liquid Download PDF

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Publication number
CN108839171A
CN108839171A CN201810658653.7A CN201810658653A CN108839171A CN 108839171 A CN108839171 A CN 108839171A CN 201810658653 A CN201810658653 A CN 201810658653A CN 108839171 A CN108839171 A CN 108839171A
Authority
CN
China
Prior art keywords
parts
processing liquid
purple willow
combined processing
willow branch
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810658653.7A
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Chinese (zh)
Inventor
宋迎楼
宋运宁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ANHUI HONGRUN ARTS AND CRAFTS Co Ltd
Original Assignee
ANHUI HONGRUN ARTS AND CRAFTS Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ANHUI HONGRUN ARTS AND CRAFTS Co Ltd filed Critical ANHUI HONGRUN ARTS AND CRAFTS Co Ltd
Priority to CN201810658653.7A priority Critical patent/CN108839171A/en
Publication of CN108839171A publication Critical patent/CN108839171A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/007Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process employing compositions comprising nanoparticles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/06Softening or hardening of wood
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • B27K9/002Cane, bamboo
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment
    • B27K2240/20Removing fungi, molds or insects

Abstract

The invention discloses a kind of purple willow branch combined processing liquid, by following material composition:Chinese medicine extract, sodium tetraborate, epoxidized soybean oil, microcrystalline wax, ethylene glycol, cetyl benzenesulfonic acid sodium, calgon, nano-titanium dioxide, deionized water.The present invention provides a kind of combined processing liquid, each material composition collocation is reasonable, formulated is convenient, combined processing liquid obtained can not only be obviously improved the mould proof characteristic of purple willow branch, further sofening treatment can be carried out to purple willow branch again, knitting property is improved, finally the service life of purple willow branch can be extended 35% or so, great popularizing value.

Description

A kind of preparation method of purple willow branch combined processing liquid
Technical field
The invention belongs to wicker plaiting article working process technical fields, and in particular to a kind of preparation of purple willow branch combined processing liquid Method.
Background technique
Wicker products are apparatus and craftwork common in people's life.Wherein purple willow is braiding common in wicker products Raw material, strong but pliable in texture, figure is longer, feel is smooth, and preferably, intensity and toughness are all higher, are very suitable for as wicker plaiting article for elasticity Raw material, but hardness is larger after purple willow is dry, should not weave, and purple willow is easy to damage by worms, is mouldy, influences making for product With.
Summary of the invention
The purpose of the present invention is being directed to existing problem, a kind of preparation side of purple willow branch combined processing liquid is provided Method.
The present invention is achieved by the following technical solutions:
A kind of purple willow branch combined processing liquid, by the material composition of following parts by weight:
15 ~ 20 parts of Chinese medicine extracts, 6 ~ 9 parts of sodium tetraborates, 13 ~ 17 parts of epoxidized soybean oils, 3 ~ 6 parts of microcrystalline waxes, 8 ~ 13 parts of second Glycol, 1 ~ 4 part of cetyl benzenesulfonic acid sodium, 2 ~ 5 parts of calgons, 7 ~ 11 parts of nano-titanium dioxides, 300 ~ 350 parts of deionizations Water.
Preferably, by the material composition of following parts by weight:
16 ~ 19 parts of Chinese medicine extracts, 7 ~ 8 parts of sodium tetraborates, 14 ~ 16 parts of epoxidized soybean oils, 4 ~ 5 parts of microcrystalline waxes, 9 ~ 12 parts of second Glycol, 2 ~ 3 parts of cetyl benzenesulfonic acid sodiums, 3 ~ 4 parts of calgons, 8 ~ 10 parts of nano-titanium dioxides, 310 ~ 340 parts of deionizations Water.
Preferably, by the material composition of following parts by weight:
18 parts of Chinese medicine extracts, 7.5 parts of sodium tetraborates, 15 parts of epoxidized soybean oils, 4.5 parts of microcrystalline waxes, 11 parts of ethylene glycol, 2.6 Part cetyl benzenesulfonic acid sodium, 3.4 parts of calgons, 9 parts of nano-titanium dioxides, 325 parts of deionized waters.
Further, the preparation method of the Chinese medicine extract is:By folium cortex eucommiae, Longtube Ground Ivy Herb, Fructus Forsythiae, myrobalan it is corresponding according to Weight ratio 4 ~ 6:5~8:2~5:7 ~ 10, which carry out mixing, is put into pot, and the clear water of 4 ~ 5 times of its gross mass is then added into pot, adds Heat boiling is filtered after boiling 1 ~ 2h of processing, after gained filtrate to be finally concentrated into the 1/6 of original volume.
Further, the grain diameter of the nano-titanium dioxide is 20 ~ 70nm.
A kind of preparation method of purple willow branch combined processing liquid, specifically puts into stirring for all substances ingredient jointly In tank, ultrasonic vibration takes out after handling 2 ~ 3h.
Further, the ultrasonic frequency when ultrasonic vibration is handled is 280 ~ 320kHz.
The present invention has the following advantages that compared with prior art:
The present invention provides a kind of combined processing liquid, rationally, formulated is convenient, combined processing obtained for each material composition collocation Liquid can not only be obviously improved the mould proof characteristic of purple willow branch, and can carry out further sofening treatment to purple willow branch, be promoted The service life of purple willow branch can finally be extended 35% or so, great popularizing value by knitting property.
Specific embodiment
Embodiment 1
A kind of purple willow branch combined processing liquid, by the material composition of following parts by weight:
15 parts of Chinese medicine extracts, 6 parts of sodium tetraborates, 13 parts of epoxidized soybean oils, 3 parts of microcrystalline waxes, 8 parts of ethylene glycol, 1 part of hexadecane Base benzene sulfonic acid sodium salt, 2 parts of calgons, 7 parts of nano-titanium dioxides, 300 parts of deionized waters.
Further, the preparation method of the Chinese medicine extract is:By folium cortex eucommiae, Longtube Ground Ivy Herb, Fructus Forsythiae, myrobalan it is corresponding according to Weight ratio 4:5:2:7, which carry out mixing, is put into pot, and the clear water of 4 times of its gross mass is then added into pot, and processing is boiled in heating boiling It is filtered after 1h, after gained filtrate to be finally concentrated into the 1/6 of original volume.
Further, the grain diameter of the nano-titanium dioxide is 20 ~ 70nm.
A kind of preparation method of purple willow branch combined processing liquid, specifically puts into stirring for all substances ingredient jointly In tank, ultrasonic vibration takes out after handling 2h.
Further, the ultrasonic frequency when ultrasonic vibration is handled is 280kHz.
Embodiment 2
A kind of purple willow branch combined processing liquid, by the material composition of following parts by weight:
18 parts of Chinese medicine extracts, 7.5 parts of sodium tetraborates, 15 parts of epoxidized soybean oils, 4.5 parts of microcrystalline waxes, 11 parts of ethylene glycol, 2.6 Part cetyl benzenesulfonic acid sodium, 3.4 parts of calgons, 9 parts of nano-titanium dioxides, 325 parts of deionized waters.
Further, the preparation method of the Chinese medicine extract is:By folium cortex eucommiae, Longtube Ground Ivy Herb, Fructus Forsythiae, myrobalan it is corresponding according to Weight ratio 5:7:4:9, which carry out mixing, is put into pot, and the clear water of 4.6 times of its gross mass is then added into pot, and place is boiled in heating boiling It is filtered after reason 1.5h, after gained filtrate to be finally concentrated into the 1/6 of original volume.
Further, the grain diameter of the nano-titanium dioxide is 20 ~ 70nm.
A kind of preparation method of purple willow branch combined processing liquid, specifically puts into stirring for all substances ingredient jointly In tank, ultrasonic vibration takes out after handling 2.5h.
Further, the ultrasonic frequency when ultrasonic vibration is handled is 300kHz.
Embodiment 3
A kind of purple willow branch combined processing liquid, by the material composition of following parts by weight:
20 parts of Chinese medicine extracts, 9 parts of sodium tetraborates, 17 parts of epoxidized soybean oils, 6 parts of microcrystalline waxes, 13 parts of ethylene glycol, 4 part 16 Sodium alkyl benzene sulfonate, 5 parts of calgons, 11 parts of nano-titanium dioxides, 350 parts of deionized waters.
Further, the preparation method of the Chinese medicine extract is:By folium cortex eucommiae, Longtube Ground Ivy Herb, Fructus Forsythiae, myrobalan it is corresponding according to Weight ratio 6:8:5:10, which carry out mixing, is put into pot, and the clear water of 5 times of its gross mass is then added into pot, and processing is boiled in heating boiling It is filtered after 2h, after gained filtrate to be finally concentrated into the 1/6 of original volume.
Further, the grain diameter of the nano-titanium dioxide is 20 ~ 70nm.
A kind of preparation method of purple willow branch combined processing liquid, specifically puts into stirring for all substances ingredient jointly In tank, ultrasonic vibration takes out after handling 3h.
Further, the ultrasonic frequency when ultrasonic vibration is handled is 320kHz.

Claims (7)

1. a kind of purple willow branch combined processing liquid, which is characterized in that by the material composition of following parts by weight:
15 ~ 20 parts of Chinese medicine extracts, 6 ~ 9 parts of sodium tetraborates, 13 ~ 17 parts of epoxidized soybean oils, 3 ~ 6 parts of microcrystalline waxes, 8 ~ 13 parts of second Glycol, 1 ~ 4 part of cetyl benzenesulfonic acid sodium, 2 ~ 5 parts of calgons, 7 ~ 11 parts of nano-titanium dioxides, 300 ~ 350 parts of deionizations Water.
2. a kind of purple willow branch combined processing liquid according to claim 1, which is characterized in that by the object of following parts by weight Matter composition:
16 ~ 19 parts of Chinese medicine extracts, 7 ~ 8 parts of sodium tetraborates, 14 ~ 16 parts of epoxidized soybean oils, 4 ~ 5 parts of microcrystalline waxes, 9 ~ 12 parts of second Glycol, 2 ~ 3 parts of cetyl benzenesulfonic acid sodiums, 3 ~ 4 parts of calgons, 8 ~ 10 parts of nano-titanium dioxides, 310 ~ 340 parts of deionizations Water.
3. a kind of purple willow branch combined processing liquid according to claim 1, which is characterized in that by the object of following parts by weight Matter composition:
18 parts of Chinese medicine extracts, 7.5 parts of sodium tetraborates, 15 parts of epoxidized soybean oils, 4.5 parts of microcrystalline waxes, 11 parts of ethylene glycol, 2.6 Part cetyl benzenesulfonic acid sodium, 3.4 parts of calgons, 9 parts of nano-titanium dioxides, 325 parts of deionized waters.
4. a kind of purple willow branch combined processing liquid described according to claim 1 ~ any one of 3, which is characterized in that described The preparation method of Chinese medicine extract is:Folium cortex eucommiae, Longtube Ground Ivy Herb, Fructus Forsythiae, myrobalan is corresponding according to weight ratio 4 ~ 6:5~8:2~5:7~ 10, which carry out mixing, is put into pot, and the clear water of 4 ~ 5 times of its gross mass is then added into pot, and mistake after 1 ~ 2h of processing is boiled in heating boiling Filter, after gained filtrate to be finally concentrated into the 1/6 of original volume.
5. a kind of purple willow branch combined processing liquid described according to claim 1 ~ any one of 3, which is characterized in that described The grain diameter of nano-titanium dioxide is 20 ~ 70nm.
6. a kind of preparation method of the purple willow branch with combined processing liquid as described in any one of claim 1 ~ 3, feature It is, specifically puts into all substances ingredient in agitator tank jointly, ultrasonic vibration takes out after handling 2 ~ 3h.
7. a kind of preparation method of purple willow branch combined processing liquid according to claim 6, which is characterized in that described super Ultrasonic frequency when processing is swung in acoustic shock is 280 ~ 320kHz.
CN201810658653.7A 2018-06-25 2018-06-25 A kind of preparation method of purple willow branch combined processing liquid Pending CN108839171A (en)

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Application Number Priority Date Filing Date Title
CN201810658653.7A CN108839171A (en) 2018-06-25 2018-06-25 A kind of preparation method of purple willow branch combined processing liquid

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Application Number Priority Date Filing Date Title
CN201810658653.7A CN108839171A (en) 2018-06-25 2018-06-25 A kind of preparation method of purple willow branch combined processing liquid

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CN108839171A true CN108839171A (en) 2018-11-20

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110039627A (en) * 2019-05-06 2019-07-23 北京林业大学 One vegetable oil/wax multiple emulsion waterproofing wood agent preparation method

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104308926A (en) * 2014-10-20 2015-01-28 安徽宏润工艺品有限公司 Wicker treating agent
CN106335116A (en) * 2016-08-27 2017-01-18 安徽省阜南志峰工艺品有限公司 Anti-ultraviolet and anti-aging treatment agent and preparing method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104308926A (en) * 2014-10-20 2015-01-28 安徽宏润工艺品有限公司 Wicker treating agent
CN106335116A (en) * 2016-08-27 2017-01-18 安徽省阜南志峰工艺品有限公司 Anti-ultraviolet and anti-aging treatment agent and preparing method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110039627A (en) * 2019-05-06 2019-07-23 北京林业大学 One vegetable oil/wax multiple emulsion waterproofing wood agent preparation method
CN110039627B (en) * 2019-05-06 2021-04-02 北京林业大学 Preparation method of vegetable oil/wax composite emulsion wood waterproofing agent

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Application publication date: 20181120