CN107253250A - A kind of sofening treatment method of purple willow - Google Patents
A kind of sofening treatment method of purple willow Download PDFInfo
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- CN107253250A CN107253250A CN201710627039.XA CN201710627039A CN107253250A CN 107253250 A CN107253250 A CN 107253250A CN 201710627039 A CN201710627039 A CN 201710627039A CN 107253250 A CN107253250 A CN 107253250A
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- purple willow
- sofening treatment
- treatment method
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/06—Softening or hardening of wood
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/34—Organic impregnating agents
- B27K3/50—Mixtures of different organic impregnating agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/002—Cane, bamboo
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Fertilizers (AREA)
- Chemical And Physical Treatments For Wood And The Like (AREA)
Abstract
The invention discloses a kind of sofening treatment method of purple willow, comprise the following steps：（1）Purple willow processing,（2）Bating liquor preparation,（3）Sofening treatment.The present invention has carried out rational improvement to the sofening treatment technique of purple willow and handled, and holistic approach is simple, safety and environmental protection, effectively improves the softening quality and efficiency of purple willow, and is beneficial to the development that peach plants industry again.
Description
Technical field
The invention belongs to wicker plaiting article working process technical field, and in particular to a kind of sofening treatment method of purple willow.
Background technology
Funan County, is under the jurisdiction of Anhui Province's Fuyang City, area earlier is developed in category inland, on the Anhui Province northwestward, Huaihe River
Middle reaches joint portion north bank.Funan County have " famous-brand and high-quality special product county ", the title of " Natural resources reservoir ", be national grain-production great Xian, in
The unique agricultural in township, the whole nation of state's wicker plaiting article（Forestry）Recycling economy demonstration pilot project county, Funan is the township of national wicker plaiting article, wicker products
It is sold abroad.
Need to carry out sofening treatment in wicker plaiting article process, because the wicker hardness after harvesting naturally is higher, pliability is not up to
To the requirement needed for braiding, in order to shorten processing efficiency, lifting yield rate, then need to carry out softening process processing.At present for
Boiled more than the sofening treatment of wicker using water, water vapour is stifling etc., although its processing technology is simple, but sofening treatment effect not very
Ideal, in order to strengthen the effect of softening, people change the mode of single clear water softening, with the addition of in clear water acid, alkali etc. into
Point, it gets a promotion for the bating effect of wicker, but the multipair environment of the material composition added has harm, and it is handled after
The performances such as wicker pliability still need to further lifting.
The content of the invention
The purpose of the present invention is that there is provided a kind of sofening treatment method of purple willow the problem of being directed to existing.
The present invention is achieved by the following technical solutions：
A kind of sofening treatment method of purple willow, comprises the following steps：
（1）Purple willow is handled：
Boiling, peeling are first carried out to purple willow to handle, and are then dipped in salt solution and are taken after 15 ~ 20min of immersion treatment again
Go out, it is standby after finally being rinsed one time with clear water；
（2）Bating liquor is prepared：
A. take soil from peach plantation Tanaka, then mixed jointly with the clear water of 6 ~ 8 times of its gross mass, the scattered place of high-speed stirred
Manage and filtered after 45 ~ 50min, concentrate the filtrate to behind the 20 ~ 30% of original volume soil extract is standby；
B. by golden cypress, rhizoma menispermi, Folium Meliae, Buddha's hand, honeysuckle, cordate houttuynia according to weight than 15 ~ 18：5~7：8~10：3~5：2~
4：4 ~ 6 are mixed, and are then mixed jointly with the clear water of 5 ~ 7 times of its gross mass, and heating boiling is boiled and filtered after 1 ~ 2h of processing, by filtrate
Be concentrated into behind the 30 ~ 40% of original volume Chinese medicine extract is standby；
C. the soil extract obtained by a, the Chinese medicine extract obtained by operation b will be operated, and bleeding agent, clear water are according to weight ratio
13~15：4~7：0.1~0.2：80 ~ 90 are mixed, and bating liquor are obtained after stirring standby；
（3）Sofening treatment：
By step（1）Purple willow after processing is immersed in step（2）In the bating liquor of gained, heating keeps the temperature of bating liquor to be 75
~ 80 DEG C, handle taking-up after 30 ~ 40min and naturally cool to room temperature.
Further, step（1）Described in boiling processing be that purple willow is put into food steamer, with boiling water steam to purple willow steam
Boil 15 ~ 20min.
Further, step（1）Described in salt solution in salt mass fraction be 3 ~ 5%.
Further, step（2）Peach plantation field described in operation a is the continuous kind for having planted peach 6 years and the above
Plant field.
Further, step（2）Rotating speed when operating the high-speed stirred processing described in a is 1000 ~ 1200 revs/min.
Further, step（2）It is nonionic penetrant to operate the bleeding agent described in c.
It is with the addition of to be lifted in sofening treatment effect, existing method in clear water such as hydrochloric acid, phosphoric acid, ammoniacal liquor, sodium bicarbonate
Deng acid, alkali composition, in sofening treatment, mentioned component can promote half wood fibre to the wooden carry out soda acid etching of purple willow
Dissolution, promotes the softening of purple willow, but the waste liquid produced by after processing has to environment and also needs to repeatedly be gone before pollution, discharge
Dirt processing, the addition of mentioned component causes operating environment degree of safety not high, harm is easily brought to operator's health, above-mentioned in addition
Processing method is still undesirable for the bating effect of purple willow, especially for high-quality handicraft purple willow Feedstock treating when, its
Corresponding braid efficiency and yield rate be not high, and then have impact on overall economic benefit；The present invention by substantial amounts of experimental summary,
The composition of existing sofening treatment liquid is improved, specifically selection with the addition of soil extract and Chinese medicine extract into
Point, wherein soil extract is extracted in the soil for continuously having planted the plantation field of peach 6 years and the above, peach warp
After continuous plantation for many years, its root can secrete the compositions such as some phenolic acid class, terpene, ketone, the bioactive substance do not verified,
Some above-mentioned materials have from toxicity in itself for peach, are unfavorable for the growth of itself actually, especially when veteran age peach moves
When newly planting the peach that resistance is poor, the age of tree is low after removing again, its usual growth can be affected, the problem of easily depauperation occur, but
It is found by the applicant that above-mentioned substance is used to that in purple willow softening process good sofening treatment effect can be played, mentioned component is more by peach
Itself secretion, biological amalgamation is good, and the excitant to wood fibre is small, and effectively wood fibre can be produced in sofening treatment
The treatment effects such as esterification, etherificate, reduce the thermal softening temperature of wood fibre, in order to strengthen above-mentioned treatment effect, again well
It with the addition of bleeding agent and promote active ingredient to the infiltration inside purple willow, the Chinese medicine extract composition of addition improves bating liquor
Security, enhances the pest-resistant corrosion resistant performance of purple willow；And this method machine after bating liquor can directly discharge, environmental pollution
Plantation that is small, also can again being resigned from office and return home for peach with the peach plantation field soil blending after extraction, and influence peach in this soil
Some of growth have been removed from toxic component, the more conducively growth of peach, and the improvement for peach continuous cropping soil provides one
Plant new thinking.
The present invention has advantages below compared with prior art：
The present invention has carried out rational improvement to the sofening treatment technique of purple willow and handled, and holistic approach is simple, safety and environmental protection, effectively
The softening quality and efficiency of purple willow are improved, and is beneficial to the development that peach plants industry again.
Embodiment
Embodiment 1
A kind of sofening treatment method of purple willow, comprises the following steps：
（1）Purple willow is handled：
Boiling, peeling are first carried out to purple willow to handle, and are then dipped in salt solution after immersion treatment 15min and are taken out again,
It is standby after finally being rinsed one time with clear water；
（2）Bating liquor is prepared：
A. take soil from peach plantation Tanaka, then mixed jointly with the clear water of 6 times of its gross mass, high-speed stirred decentralized processing
Filtered after 45min, concentrate the filtrate to after the 20% of original volume soil extract is standby；
B. golden cypress, rhizoma menispermi, Folium Meliae, Buddha's hand, honeysuckle, cordate houttuynia are compared 15 according to weight：5：8：3：2：4 are mixed,
Then mixed jointly with the clear water of 5 times of its gross mass, heating boiling is filtered after boiling processing 1h, concentrates the filtrate to the 30% of original volume
It is standby that Chinese medicine extract is obtained afterwards；
C. the soil extract obtained by a, the Chinese medicine extract obtained by operation b will be operated, and bleeding agent, clear water are according to weight ratio
13：4：0.1：80 are mixed, and bating liquor are obtained after stirring standby；
（3）Sofening treatment：
By step（1）Purple willow after processing is immersed in step（2）In the bating liquor of gained, heating keeps the temperature of bating liquor to be 75
DEG C, taken out after processing 30min and naturally cool to room temperature.
Further, step（1）Described in boiling processing be that purple willow is put into food steamer, with boiling water steam to purple willow steam
Boil 15min.
Further, step（1）Described in salt solution in salt mass fraction be 3%.
Further, step（2）It is continuously to have planted the peach plantation field of 6 years to operate the peach plantation field described in a.
Further, step（2）Rotating speed when operating the high-speed stirred processing described in a is 1000 revs/min.
Further, step（2）It is nonionic penetrant to operate the bleeding agent described in c.
Embodiment 2
A kind of sofening treatment method of purple willow, comprises the following steps：
（1）Purple willow is handled：
Boiling, peeling are first carried out to purple willow to handle, and are then dipped in salt solution after immersion treatment 18min and are taken out again,
It is standby after finally being rinsed one time with clear water；
（2）Bating liquor is prepared：
A. take soil from peach plantation Tanaka, then mixed jointly with the clear water of 7 times of its gross mass, high-speed stirred decentralized processing
Filtered after 47min, concentrate the filtrate to after the 25% of original volume soil extract is standby；
B. golden cypress, rhizoma menispermi, Folium Meliae, Buddha's hand, honeysuckle, cordate houttuynia are compared 16 according to weight：6：9：4：3：5 are mixed,
Then mixed jointly with the clear water of 6 times of its gross mass, heating boiling is filtered after boiling processing 1.5h, concentrates the filtrate to original volume
Chinese medicine extract is obtained after 35% standby；
C. the soil extract obtained by a, the Chinese medicine extract obtained by operation b will be operated, and bleeding agent, clear water are according to weight ratio
14：3：0.15：85 are mixed, and bating liquor are obtained after stirring standby；
（3）Sofening treatment：
By step（1）Purple willow after processing is immersed in step（2）In the bating liquor of gained, heating keeps the temperature of bating liquor to be 77
DEG C, taken out after processing 36min and naturally cool to room temperature.
Further, step（1）Described in boiling processing be that purple willow is put into food steamer, with boiling water steam to purple willow steam
Boil 19min.
Further, step（1）Described in salt solution in salt mass fraction be 4%.
Further, step（2）It is continuously to have planted the peach plantation field of 7 years to operate the peach plantation field described in a.
Further, step（2）Rotating speed when operating the high-speed stirred processing described in a is 1100 revs/min.
Further, step（2）It is nonionic penetrant to operate the bleeding agent described in c.
Embodiment 3
A kind of sofening treatment method of purple willow, comprises the following steps：
（1）Purple willow is handled：
Boiling, peeling are first carried out to purple willow to handle, and are then dipped in salt solution after immersion treatment 20min and are taken out again,
It is standby after finally being rinsed one time with clear water；
（2）Bating liquor is prepared：
A. take soil from peach plantation Tanaka, then mixed jointly with the clear water of 8 times of its gross mass, high-speed stirred decentralized processing
Filtered after 50min, concentrate the filtrate to after the 30% of original volume soil extract is standby；
B. golden cypress, rhizoma menispermi, Folium Meliae, Buddha's hand, honeysuckle, cordate houttuynia are compared 18 according to weight：7：10： 5：4：6 are mixed
Close, then mixed jointly with the clear water of 7 times of its gross mass, heating boiling is filtered after boiling processing 2h, concentrates the filtrate to original volume
Chinese medicine extract is obtained after 40% standby；
C. the soil extract obtained by a, the Chinese medicine extract obtained by operation b will be operated, and bleeding agent, clear water are according to weight ratio
15：7：0.2：90 are mixed, and bating liquor are obtained after stirring standby；
（3）Sofening treatment：
By step（1）Purple willow after processing is immersed in step（2）In the bating liquor of gained, heating keeps the temperature of bating liquor to be 80
DEG C, taken out after processing 40min and naturally cool to room temperature.
Further, step（1）Described in boiling processing be that purple willow is put into food steamer, with boiling water steam to purple willow steam
Boil 20min.
Further, step（1）Described in salt solution in salt mass fraction be 5%.
Further, step（2）It is continuously to have planted the peach plantation field of 8 years to operate the peach plantation field described in a.
Further, step（2）Rotating speed when operating the high-speed stirred processing described in a is 1200 revs/min.
Further, step（2）It is nonionic penetrant to operate the bleeding agent described in c.
Comparative example 1
This comparative example 1 compared with Example 2, in step（2）Bating liquor prepare in, with etc. mass parts citric acid replace soil
Earth extract solution, for the preparation of bating liquor, method and step all same in addition.
Comparative example 2
This comparative example 2 compared with Example 2, in step（2）Bating liquor prepare in, with etc. mass parts ammoniacal liquor replace soil
Extract solution, for the preparation of bating liquor, method and step all same in addition.
Comparative example 3
This comparative example 3 compared with Example 2, in step（2）During bating liquor is prepared, the soil extract in bating liquor is saved
Composition, method and step all same in addition.
In order to contrast effect of the present invention, from same batch gather in fresh purple willow as experimental subjects, respectively with above-mentioned
Embodiment 2, comparative example 1, comparative example 2, the corresponding method of comparative example 3 carry out sofening treatment, blank control group
It is undressed original purple willow branch, performance test then is carried out to the purple willow branch after processing, specific correction data is as follows
Shown in table 1：
Table 1
| One-dimensional bending curvature radius average value（Without mould） | Weave yield rate（%） | |
| Embodiment 2 | 35.4 | 98.7 |
| Comparative example 1 | 46.2 | 95.0 |
| Comparative example 2 | 50.3 | 93.8 |
| Comparative example 3 | 70.1 | 80.3 |
| Blank control group | 124.6 | / |
Note：One-dimensional bending curvature radius average value described in upper table 1 refers to carry out Longitudinal compressing to the section of purple willow shoot tissue
Afterwards, then with SEM companies of Japan produce model JSM-5610LV SEM cell membrane tissue is detected and
, described one-dimensional bending curvature radius average value is smaller, shows that fibr tissue softening is more complete, corresponding processing operation softening
Effect is more preferable；Described braiding yield rate is that the purple willow branch after processing is normally woven, the yield rate that correspondence is made,
"/" represents not calculate.
Processing method of the present invention can effectively lift the softening quality of purple willow it can be seen from upper table 1, more existing common
Soda acid softening process quality more preferably, and the safer environmental protection of the inventive method, beneficial to promoting the use of.
Claims (6)
1. a kind of sofening treatment method of purple willow, it is characterised in that comprise the following steps：
（1）Purple willow is handled：
Boiling, peeling are first carried out to purple willow to handle, and are then dipped in salt solution and are taken after 15 ~ 20min of immersion treatment again
Go out, it is standby after finally being rinsed one time with clear water；
（2）Bating liquor is prepared：
A. take soil from peach plantation Tanaka, then mixed jointly with the clear water of 6 ~ 8 times of its gross mass, the scattered place of high-speed stirred
Manage and filtered after 45 ~ 50min, concentrate the filtrate to behind the 20 ~ 30% of original volume soil extract is standby；
B. by golden cypress, rhizoma menispermi, Folium Meliae, Buddha's hand, honeysuckle, cordate houttuynia according to weight than 15 ~ 18：5~7：8~10：3~5：2~
4：4 ~ 6 are mixed, and are then mixed jointly with the clear water of 5 ~ 7 times of its gross mass, and heating boiling is boiled and filtered after 1 ~ 2h of processing, by filtrate
Be concentrated into behind the 30 ~ 40% of original volume Chinese medicine extract is standby；
C. the soil extract obtained by a, the Chinese medicine extract obtained by operation b will be operated, and bleeding agent, clear water are according to weight ratio
13~15：4~7：0.1~0.2：80 ~ 90 are mixed, and bating liquor are obtained after stirring standby；
（3）Sofening treatment：
By step（1）Purple willow after processing is immersed in step（2）In the bating liquor of gained, heating keeps the temperature of bating liquor to be 75
~ 80 DEG C, handle taking-up after 30 ~ 40min and naturally cool to room temperature.
2. a kind of sofening treatment method of purple willow according to claim 1, it is characterised in that step（1）Described in steaming
It is that purple willow is put into food steamer to boil processing, with boiling water steam to 15 ~ 20min of purple willow boiling.
3. a kind of sofening treatment method of purple willow according to claim 1, it is characterised in that step（1）Described in food
The mass fraction of salt is 3 ~ 5% in salting liquid.
4. a kind of sofening treatment method of purple willow according to claim 1, it is characterised in that step（2）Operate described in a
Peach plantation field be the continuous plantation field for having planted peach 6 years and the above.
5. a kind of sofening treatment method of purple willow according to claim 1, it is characterised in that step（2）Operate described in a
High-speed stirred processing when rotating speed be 1000 ~ 1200 revs/min.
6. a kind of sofening treatment method of purple willow according to claim 1, it is characterised in that step（2）Operate described in c
Bleeding agent be nonionic penetrant.
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| CN201710627039.XA CN107253250A (en) | 2017-07-28 | 2017-07-28 | A kind of sofening treatment method of purple willow |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107839047A (en) * | 2017-11-24 | 2018-03-27 | 广西博白焕发工艺品有限公司 | A kind of method of mao bamboon bar dyeing |
| CN108943270A (en) * | 2018-07-30 | 2018-12-07 | 安徽华宇工艺品股份有限公司 | A kind of braiding softening method of purple willow |
| CN109159234A (en) * | 2018-09-25 | 2019-01-08 | 安徽省汉甲机电设备科技有限公司 | A kind of sofening treatment method of purple willow |
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| CN106182263A (en) * | 2016-07-13 | 2016-12-07 | 阜南县猛发工艺品有限公司 | A kind of aging wooden products processing method |
| CN106217526A (en) * | 2016-07-28 | 2016-12-14 | 安徽信达家居有限公司 | A kind of rattan processing method |
| CN106665704A (en) * | 2015-11-09 | 2017-05-17 | 阜南县宏泰工艺品有限公司 | Salix integra treatment agent and preparation method thereof |
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2017
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104441123A (en) * | 2014-09-25 | 2015-03-25 | 阜南县永兴工艺品有限公司 | Rattan processing method for willow artworks |
| CN106665704A (en) * | 2015-11-09 | 2017-05-17 | 阜南县宏泰工艺品有限公司 | Salix integra treatment agent and preparation method thereof |
| CN106182263A (en) * | 2016-07-13 | 2016-12-07 | 阜南县猛发工艺品有限公司 | A kind of aging wooden products processing method |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107839047A (en) * | 2017-11-24 | 2018-03-27 | 广西博白焕发工艺品有限公司 | A kind of method of mao bamboon bar dyeing |
| CN108943270A (en) * | 2018-07-30 | 2018-12-07 | 安徽华宇工艺品股份有限公司 | A kind of braiding softening method of purple willow |
| CN109159234A (en) * | 2018-09-25 | 2019-01-08 | 安徽省汉甲机电设备科技有限公司 | A kind of sofening treatment method of purple willow |
| CN109159234B (en) * | 2018-09-25 | 2020-06-19 | 阜南县艺达工艺品有限公司 | Softening treatment method of salix integra |
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