CN106987909A - Cocoon cooking used additives in a kind of reeling silk production process - Google Patents

Cocoon cooking used additives in a kind of reeling silk production process Download PDF

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Publication number
CN106987909A
CN106987909A CN201710258047.1A CN201710258047A CN106987909A CN 106987909 A CN106987909 A CN 106987909A CN 201710258047 A CN201710258047 A CN 201710258047A CN 106987909 A CN106987909 A CN 106987909A
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CN
China
Prior art keywords
parts
agent
cocoon cooking
defoamer
cocoon
Prior art date
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Pending
Application number
CN201710258047.1A
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Chinese (zh)
Inventor
周光华
周培文
江来珍
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Qianshan County Longhua Silk Co Ltd
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Qianshan County Longhua Silk Co Ltd
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Publication date
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Priority to CN201710258047.1A priority Critical patent/CN106987909A/en
Publication of CN106987909A publication Critical patent/CN106987909A/en
Pending legal-status Critical Current

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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01CCHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
    • D01C3/00Treatment of animal material, e.g. chemical scouring of wool
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01CCHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
    • D01C3/00Treatment of animal material, e.g. chemical scouring of wool
    • D01C3/02De-gumming silk

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Animal Husbandry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Molecular Biology (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses cocoon cooking used additives in a kind of reeling silk production process, the described agent that attaches is made up of following components by following parts by weight, 3~5 parts of fatty alcohol, 3~5 parts of AEO, 5~8 parts of water-soluble monomer, 8~12 parts of phosphorylation agent, 1~1.5 part of mercerising soap lye, 0.1~0.5 part of defoamer.Instant invention overcomes the deficiencies in the prior art, composite assistant is applied to during cocoon cooking process, the comparative analysis auxiliary agent improves unwinding degree, the tensile strength of enhancing silk to permeating cocoon chamber in filature process of cocoon.

Description

Cocoon cooking used additives in a kind of reeling silk production process
Technical field
The present invention relates to filature production technical field, cocoon cooking used additives in a kind of reeling silk production process are particularly belonged to.
Background technology
Silk is obtained by silk weaving, and silk is obtained by silk cocoon filature cocoon cooking processing.Silk is extracted from silk cocoon Process is referred to as filature, filature cocoon cooking process mainly include mixed cocoon, shell cocoon, select silkworm, cocoon cooking, filature, rereeling, the process, reel silk from cocoons such as arrangement Silk production is commonly referred to as throwing.
The mode that filature is boiled usually using water, on the one hand using water high temperature kill cocoon in silkworm chrysalis, on the other hand because Silk is animal origin, containing a large amount of animal colloid albumens, by heating, makes wherein most colloid albumen soluble in water, from And separation fiber is played, smoothly extract the purpose of silk out.
Silk cocoon uses different cocoon cooking process and technical measures in filature production, and the quality to filature has a great impact, Only cooked cocoon could the good silk of reel silk from cocoons, the particularly influence to unwinding degree and silk production rate.China is more at present using the outer vacuum infiltration of machine With the technology progress throwing being cooked in machine, silk cocoon handles by vacuum infiltration water suction before being cooked, reaches cooked cocoon and fill Divide infiltration, proper mature (ripe) uniform, the cocoon outer layer that adequately protects hangs rough and internal layer and fall thread with middle internal layer, reduction is cooked.But, due to silk cocoon cocoon Layer is more, and water suction infiltration resistance is big, and cocoon layer water suction osmosis is small, therefore when vacuum infiltration absorbs water and handled, to temperature, pressure Power, time and traffic requirement are high, operating difficulties.
The content of the invention
It is an object of the invention to provide cocoon cooking used additives in a kind of reeling silk production process, prior art is overcome not Foot, composite assistant is applied to during cocoon cooking process, and the comparative analysis auxiliary agent is carried to permeating cocoon chamber in filature process of cocoon High reelability degree, strengthens the tensile strength of silk.
The technical solution adopted by the present invention is as follows:
Cocoon cooking used additives in a kind of reeling silk production process, described attaches agent by following components by following parts by weight numeral system Into 3~5 parts of fatty alcohol, 3~5 parts of AEO, 5~8 parts of water-soluble monomer, 8~12 parts of phosphorylation agent, silk 1~1.5 part of light soap lye, 0.1~0.5 part of defoamer.
Described 4 parts of fatty alcohol, 4 parts of AEO, 6 parts of water-soluble monomer, 10 parts of phosphorylation agent, mercerising 1.2 parts of soap lye, 0.3 part of defoamer.
Described water-soluble monomer is to be selected from acrylic acid, methacrylic acid, one or more kinds of combinations of cis-butenedioic anhydride.
Described phosphorylation agent is one or more of mixed in phosphorus pentoxide, phosphorus oxychloride or polyphosphoric acid Compound.
Described defoamer is in polyethers defoamer, higher alcohols defoamer, silicon class defoamer, polyether-modified silicon defoaming agent One or more of compositions.
A kind of method of filature cocoon cooking, after above-mentioned auxiliary agent is added, controls water temperature at 35~40 °, and under vacuum Carry out, cocoon cooking handles 2~3min, the addition of bleeding agent is the bleeding agent that 0.5~1kg is added per 100kg silk cocoons.
Compared with the prior art, beneficial effects of the present invention are as follows:
The present invention is using the combination of above-mentioned bleeding agent and cocoon cooking process, and it can fully permeate cocoon chamber immaculate, be conducive to The protection of silk, unwinding, cleannes, cleanliness can be improved relative to traditional cocoon cooking process, and consumption reduction adds the tension of silk Intensity, feel is soft and smooth glossy, and rough, raising production efficiency is hung in reduction.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, to the technology in the embodiment of the present invention Scheme is clearly and completely described, it is clear that described embodiment is a part of embodiment of the invention, rather than whole Embodiment.Based on the embodiment in the present invention, those of ordinary skill in the art are obtained under the premise of creative work is not made The every other embodiment obtained, belongs to the scope of protection of the invention.
Cocoon cooking used additives in a kind of reeling silk production process, described attaches agent by following components by following parts by weight numeral system Into described 4 parts of fatty alcohol, 4 parts of AEO, 6 parts of water-soluble monomer, 10 parts of phosphorylation agent, mercerising soap lye 1.2 parts, 0.3 part of defoamer;Described water-soluble monomer be selected from acrylic acid, methacrylic acid, one kind of cis-butenedioic anhydride or it is a kind of with On combination;Described phosphorylation agent is one or more of in phosphorus pentoxide, phosphorus oxychloride or polyphosphoric acid Mixture;Described defoamer is in polyethers defoamer, higher alcohols defoamer, silicon class defoamer, polyether-modified silicon defoaming agent One or more of compositions.
A kind of method of filature cocoon cooking, after above-mentioned auxiliary agent is added, controls water temperature at 35~40 °, and under vacuum Carry out, cocoon cooking handles 2~3min, the addition of bleeding agent is the bleeding agent that 0.5~1kg is added per 100kg silk cocoons;Profit of the invention With the combination of above-mentioned bleeding agent and cocoon cooking process, it can fully permeate cocoon chamber immaculate, be conducive to the protection of silk, relative to Traditional cocoon cooking process can improve unwinding, cleannes, cleanliness, and consumption reduction adds the tensile strength of silk, feel is soft and smooth light Rough, raising production efficiency is hung in pool, reduction.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality Body or operation make a distinction with another entity or operation, and not necessarily require or imply these entities or deposited between operating In any this actual relation or order.Moreover, term " comprising ", "comprising" or its any other variant are intended to Nonexcludability is included, so that process, method, article or equipment including a series of key elements not only will including those Element, but also other key elements including being not expressly set out, or also include being this process, method, article or equipment Intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that Also there is other identical element in process, method, article or equipment including the key element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although with reference to the foregoing embodiments The present invention is described in detail, it will be understood by those within the art that:It still can be to foregoing each implementation Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic;And these modification or Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.

Claims (6)

1. cocoon cooking used additives in a kind of reeling silk production process, it is characterised in that described attaches agent by following components by following heavy Amount number is made, 3~5 parts of fatty alcohol, 3~5 parts of AEO, 5~8 parts of water-soluble monomer, and phosphorylation agent 8~ 12 parts, 1~1.5 part of mercerising soap lye, 0.1~0.5 part of defoamer.
2. cocoon cooking used additives in reeling silk production process according to claim 1, it is characterised in that:Described 4 parts of fatty alcohol, 4 parts of AEO, 6 parts of water-soluble monomer, 10 parts of phosphorylation agent, 1.2 parts of mercerising soap lye, 0.3 part of defoamer.
3. cocoon cooking used additives in reeling silk production process according to claim 1, it is characterised in that:Described water-soluble monomer It is to be selected from acrylic acid, methacrylic acid, one or more kinds of combinations of cis-butenedioic anhydride.
4. cocoon cooking used additives in reeling silk production process according to claim 1, it is characterised in that:Described phosphorylation agent One or more of mixtures in phosphorus pentoxide, phosphorus oxychloride or polyphosphoric acid.
5. cocoon cooking used additives in reeling silk production process according to claim 1, it is characterised in that:Described defoamer is poly- One or more of compositions in ethers defoamer, higher alcohols defoamer, silicon class defoamer, polyether-modified silicon defoaming agent.
6. a kind of method that filature cocoon cooking is carried out using auxiliary agent as described in the appended claim 1, it is characterised in that:Adding above-mentioned help After agent, control water temperature is carried out at 35~40 °, and under vacuum, and cocoon cooking handles 2~3min, and the addition of bleeding agent is every 100kg silk cocoons add 0.5~1kg bleeding agent.
CN201710258047.1A 2017-04-19 2017-04-19 Cocoon cooking used additives in a kind of reeling silk production process Pending CN106987909A (en)

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Application Number Priority Date Filing Date Title
CN201710258047.1A CN106987909A (en) 2017-04-19 2017-04-19 Cocoon cooking used additives in a kind of reeling silk production process

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Application Number Priority Date Filing Date Title
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CN106987909A true CN106987909A (en) 2017-07-28

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107699961A (en) * 2017-11-27 2018-02-16 鹿寨县贵盛茧丝工贸有限公司 The method for improving fresh silk obvolvent
CN107805849A (en) * 2017-11-27 2018-03-16 鹿寨县贵盛茧丝工贸有限公司 Silk cocoon reels off raw silk from cocoons method
CN110042562A (en) * 2019-03-30 2019-07-23 浙江蚕缘家纺有限公司 A kind of tussah silk carding process
CN111101207A (en) * 2020-01-07 2020-05-05 圣凯科技产业(辽宁)有限公司 Degumming agent and preparation method thereof, silkworm cocoon degumming method and application

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102121135A (en) * 2011-04-07 2011-07-13 重庆市纤维检验局 Silk making method of transgenic colored cocoons
CN102586896A (en) * 2012-01-11 2012-07-18 广西工学院 Novel cocoon cooking aid and its application
CN103628319A (en) * 2013-12-02 2014-03-12 上林海润丝业有限公司 Penetrant and method for cooking silk reeling cocoon
CN104611923A (en) * 2015-01-23 2015-05-13 江苏金太阳纺织科技有限公司 Phosphate silkete penetrating agent and preparation method thereof
CN105002734A (en) * 2015-07-01 2015-10-28 广东灵捷制造化工有限公司 Degreasing and blenching auxiliary agent used for medical gauze one-step bath pretreatment, and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102121135A (en) * 2011-04-07 2011-07-13 重庆市纤维检验局 Silk making method of transgenic colored cocoons
CN102586896A (en) * 2012-01-11 2012-07-18 广西工学院 Novel cocoon cooking aid and its application
CN103628319A (en) * 2013-12-02 2014-03-12 上林海润丝业有限公司 Penetrant and method for cooking silk reeling cocoon
CN104611923A (en) * 2015-01-23 2015-05-13 江苏金太阳纺织科技有限公司 Phosphate silkete penetrating agent and preparation method thereof
CN105002734A (en) * 2015-07-01 2015-10-28 广东灵捷制造化工有限公司 Degreasing and blenching auxiliary agent used for medical gauze one-step bath pretreatment, and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107699961A (en) * 2017-11-27 2018-02-16 鹿寨县贵盛茧丝工贸有限公司 The method for improving fresh silk obvolvent
CN107805849A (en) * 2017-11-27 2018-03-16 鹿寨县贵盛茧丝工贸有限公司 Silk cocoon reels off raw silk from cocoons method
CN110042562A (en) * 2019-03-30 2019-07-23 浙江蚕缘家纺有限公司 A kind of tussah silk carding process
CN111101207A (en) * 2020-01-07 2020-05-05 圣凯科技产业(辽宁)有限公司 Degumming agent and preparation method thereof, silkworm cocoon degumming method and application

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