CN108651786A - A kind of preparation method of full nutritional sea buckthorn fruit juice - Google Patents
A kind of preparation method of full nutritional sea buckthorn fruit juice Download PDFInfo
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- CN108651786A CN108651786A CN201810474914.XA CN201810474914A CN108651786A CN 108651786 A CN108651786 A CN 108651786A CN 201810474914 A CN201810474914 A CN 201810474914A CN 108651786 A CN108651786 A CN 108651786A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
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Abstract
The present invention provides a kind of preparation methods of full nutritional sea buckthorn fruit juice, pass through：1. seabuckthorn seeds are extracted seabuckthorn seeds glue, for stablizing the emulsification of fruit oil and fruit juice, improving the stability of nutritional ingredient；2. sea-buckthorn leaf extract is added in fruit juice, one seabuckthorn tree of reduction, the fruit juice containing the full trophic function of sea-buckthorn are realized.
Description
Technical field
This patent is related to a kind of preparation method of hippophae rhamnoides nutrition fruit juice, belongs to field of food science.
Background technology
Sea-buckthorn (Hippophae rhamnoides L.) is Elaeangnaceae hippophae plant, also known as acid thorn, Da Pu (hide
Name), infuse its day dry (covering name), lucky sweat (Uygur's name) etc., be a kind of shrub, dungarunga or arbor, northwest China, northeast,
The area such as North China, southwest is widely distributed, enjoys " natural complex treasure-house ", " green gold ", " improve the ecological environment pioneer "
Laudatory title,《Chinese Pharmacopoeia》In with its fruit medicine, there is the effect of reinforcing spleen to promote digestion, cough-relieving apophlegmatic, Huoxue San " addiction.
Research confirms that sea-buckthorn has a very abundant nutritive value, rhizome, branches and leaves, fruit, seed of sea-buckthorn etc. it is all nutritious with
And medicinal ingredient.Seabuckthorn Oil contains a variety of nutrient substances necessary to human body, including a variety of unsaturated fatty acids, carrot
A variety of liposoluble vitamins and 36 kinds of flavonoids and polyphenols such as plain, carotenoid and its derivative, natural VE, also
There are nearly more than 160 kinds of life active compounds such as sterol, anthocyanidin, Quercetin, is a complete vital activity factor treasure-house, is pole
Good nutrient and healthcare products.Fructus hippophae can also squeeze the juice, rich in biologies such as flavone compound and procyanidine in residual residue
Active constituent.
Have numerous open source literature trials at present and prepare sea buckthorn juice, as patent 201610888220.1 provides a kind of tune
The preparation method of distribution type sea buckthorn juice, patent 201510096240.0 provide a kind of preparation method of fermented type sea buckthorn juice.
Sea-buckthorn, which will be prepared into, to be suitble to leisure to drink and has the fruit drink of certain trophism, the main problems are as follows：①
Mouthfeel.Sea buckthorn fruit taste itself is sour and astringent, and has a kind of special stink, does not meet consuming public for fruit drink
Mouthfeel is approved；2. Seabuckthorn Oil is easily layered.Fructus hippophae oil content is very high, and fruit juice is prepared again if oil is got rid of, and can lose nutrition
Ingredient；Fruit juice is easy to be layered again if retaining hippophae rhamnoides fruit oil；3. being also enriched in vitamin, aliphatic acid, flavonoids in Leaves of Hippophae L
Close object, triterpene, steroid compound, polyphenol, serotonin, tannin, trace element, polysaccharide, crude protein, crude fibre and amino acid
Equal nutriments, fruit juice very waste of resource is prepared only with fructus hippophae.
Invention content
The object of the present invention is to provide a kind of preparation methods of full nutritional sea buckthorn fruit juice, pass through：1. seabuckthorn seeds are extracted husky
Spine seed glue, for stablizing the emulsification of fruit oil and fruit juice, improving the stability of nutritional ingredient；2. sea-buckthorn leaf extract is added to fruit
In juice, one seabuckthorn tree of reduction, the fruit juice containing the full trophic function of sea-buckthorn are realized.
In order to achieve the object of the present invention, concrete operation step is as follows：
1, the extraction of seabuckthorn seeds glue
500g seabuckthorn seeds are taken, by mass volume ratio 1:5~1:8 be added pure water, 0~4 DEG C immersion 72~96h, 20000~
30000rpm smashes 3~5min, and heating water bath extracts 4~5h, 80~90 DEG C of temperature, and filtering takes filtrate；Again by volume 1:5
~1:8 are added pure water, and heating water bath extracts 4~5h, 80~90 DEG C of temperature, and filtering takes filtrate；It filtrate will merge twice, carry out
Concentration, 70~80 DEG C of temperature, vacuum degree ＜ 0.09MPa are added anhydrous until volume is 1/20~1/10 stopping concentration before concentration
Ethyl alcohol to ethanol content reaches 80~90%, 4 DEG C of alcohol precipitations and stays overnight, and filters to obtain solid precipitation, is lyophilized to obtain the final product.
2, the extraction of Leaves of Hippophae L
500g Leaves of Hippophae L is taken, 3~5min is smashed with 20000~30000rpm after drying, by mass volume ratio 1:5~1:8
Petroleum ether, 65~75 DEG C of extraction 2h is added, filtering takes filter residue；Filter residue is volatilized into petroleum ether, by mass volume ratio 1:5~1:8 add
Enter ethanol solution, concentration of alcohol 50%, 65~75 DEG C of 2~3h of extraction filter, take filtrate；Filtrate is concentrated, and temperature 60~
70 DEG C, vacuum degree ＜ 0.09MPa, until medicinal extract shape, medicinal extract is lyophilized without ethanol flavor to obtain the final product.
3, the preparation of full nutritional sea buckthorn fruit juice
The complete fructus hippophae of condition is taken, is squeezed the juice with juice extractor after cleaning, Seabuckthorn fruit plasmogen is obtained after being filtered to remove dregs.
The following raw material is taken by weight：80~100 parts of Seabuckthorn fruit plasmogen, 10~20 parts of white granulated sugar, 6~8 parts of seabuckthorn seeds glue, Leaves of Hippophae L carries
Take 3~5 parts of object, 3~5 parts of honey, 50~120 parts of water, 20~40 parts of other fruit juices.
Apple fumet, lemon juice, orange Normal juice or the sour-sweet fruit juice of other tastes can be selected in other fruit juices.
After mixing by each ingredient, homogeneous is carried out twice with high pressure homogenizer, first pass homogenization pressure is 300Bar, the
Two times homogenization pressures be 500Bar to get.
Based on method provided by the invention, other sweeteners can be selected on the basis of invention content, such as xylitol, sugarcane
Sugar, Aspartame, Sucralose, antierythrite, Momordia grosvenori aglycone, acesulfame potassium etc. replace white granulated sugar, and dosage is according to other sweeteners
Sugariness be adjusted；Conventional sterilization can also be added after processing step, as pasteurize, high-pressure pulse electric sterilization,
The methods of irradiation sterilization；The step of sterile filling can also be increased according to the form of product.
It is an advantage of the present invention that the seabuckthorn seeds glue contained using seabuckthorn seeds itself is as stabilizer, instead of common food
Product additive such as xanthans, carragheen, carboxymethyl cellulose etc. can play the emulsification of the Seabuckthorn Oil and moisture in stable fruit juice
System, and exogenous additive is not added, it has been truly realized no added pollution-free food；It is added to Leaves of Hippophae L extraction simultaneously
Object makes the nutritional ingredient of fruit juice increase, while also increasing the flavor of fruit juice, plays better health-care effect.
Specific implementation mode
The optimal extraction technology of 1 seabuckthorn seeds glue of embodiment
Seabuckthorn seeds are taken, pure water are added by certain solid-liquid ratio, 0~4 DEG C of immersion certain time, 20000~30000rpm smashes 3
~5min, heating water bath are extracted by certain temperature and time, and filtering takes filtrate；Second of extraction is carried out again, is filtered, is taken filtrate；
It filtrate will merge twice, be concentrated, 70~80 DEG C of temperature, vacuum degree ＜ 0.09MPa, until volume is 1/20~1/ before concentration
10 stop concentration, and addition absolute ethyl alcohol to ethanol content reaches 80~90%, 4 DEG C of alcohol precipitations and stays overnight, filters to obtain solid precipitation, freeze
It is dry.
Using the stablizing effect of seabuckthorn seeds glue as index, with solid-liquid ratio, soaking time, water-bath extraction time, water-bath extraction temperature
Degree is investigation factor, using L9(34) table designs orthogonal test, the extraction process of optimization seabuckthorn seeds glue, and carries out verification test.Cause
Element is shown in Table 1 with level.
1 factor of table and level
The stablizing effect of seabuckthorn seeds glue calculates as follows：
1. standing 48h observes delamination：Sea buckthorn juice conduct is added in the seabuckthorn seeds glue obtained according to different extraction routes
Stabilizer can obtain uniform, stiff fruit juice and see whether layering, not stratified score after 4 DEG C of refrigerators place 48h
It is 1, layering but can shakes up and be scored at 0, layering is unable to mixing after shaking and is scored at -1；
2. centrifugation observation delamination：Sea buckthorn juice is added as stabilization in the seabuckthorn seeds glue obtained according to different extraction routes
Agent can obtain uniform, stiff fruit juice and see whether layering after 1000rpm centrifuges 5min, not stratified to be scored at 1,
It is layered but can shake up and be scored at 0, layering is unable to mixing after shaking and is scored at -1；
3. score will be added twice, as total score.
According to result it is found that optimal extracting factor is A2B3C3D2, influence size of each factor to result is ordered as D
＞ C ＞ A ＞ B finally determine that optimal extraction process is solid-liquid ratio 1:5, soaking time 72h, extraction time 6h, Extracting temperature 80
℃。
The optimal extraction technology of 2 Leaves of Hippophae L of embodiment
Seabuckthorn seeds leaf is taken, 3~5min is smashed with 20000~30000rpm after drying, by mass volume ratio 1:5~1:8 add
Enter petroleum ether, 65~75 DEG C of extraction 2h, filtering takes filter residue；Filter residue is volatilized into petroleum ether, is added by certain mass volume ratio certain
The ethanol solution of concentration, under certain temperature water-bath extract certain time, filtering takes filtrate；Filtrate is concentrated, temperature 60~70
DEG C, vacuum degree ＜ 0.09MPa, until medicinal extract shape, medicinal extract is lyophilized without ethanol flavor to obtain the final product.
Using the recovery rate summation of the 6 kinds of flavone aglycones contained in Leaves of Hippophae L as index, carried with solid-liquid ratio, concentration of alcohol, water-bath
It is investigation factor to take time, water-bath Extracting temperature, using L9(34) table design orthogonal test, optimize the extraction process of Leaves of Hippophae L, and
Carry out verification test.Factor is shown in Table 2 with level.
2 factor of table and level
The recovery rate summation of flavone aglycone calculates as follows in Leaves of Hippophae L：Extract powder high performance liquid chromatography after freeze-drying
Method detect, be calculated catechin, rutin, myricetin, Quercetin, Kaempferol, Isorhamnetin content, content is added to obtain
Summation.
According to result it is found that optimal extracting factor is A2B1C3D2, influence size of each factor to result is ordered as B
＞ C ＞ D ＞ A finally determine that optimal extraction process is solid-liquid ratio 1:7, concentration of alcohol 50%, extraction time 6h, Extracting temperature 60
℃。
The stability test of 3 sea buckthorn juice of embodiment
The complete fructus hippophae of condition is taken, is squeezed the juice with juice extractor after cleaning, Seabuckthorn fruit plasmogen is obtained after being filtered to remove dregs.
The following raw material is taken by weight：80~100 parts of Seabuckthorn fruit plasmogen, 10~20 parts of white granulated sugar, stabilizer, sea-buckthorn leaf extract 3~5
Part, 3~5 parts of honey, 50~120 parts of water, 20~40 parts of other fruit juices.Apple fumet, lemon can be selected in other fruit juices
Lemon Normal juice, orange Normal juice or the sour-sweet fruit juice of other tastes.After mixing by each ingredient, it is carried out with high pressure homogenizer
Twice of matter, first pass homogenization pressure are 300Bar, second time homogenization pressure be 500Bar to get.
Wherein stabilizer selects the commercial stabilizer in a following table 3, and the seabuckthorn seeds glue voluntarily extracted is as a comparison.
From test result it is found that seabuckthorn seeds glue plays the effect for stablizing fruit juice well, and selects and come from sea-buckthorn sheet
The ingredient of body, than adding, other food additives are safer, more can be consumer receives.
The health-care effect of 4 sea buckthorn juice of embodiment
Sea buckthorn juice is prepared according to the step of invention content, the white granulated sugar in the 3rd step is only changed to 0.5~1 part of acesulfame potassium,
The fruit drink for diabetes patients is made.Choose hospitalization due to blood glucose increases in short term excessively of division of endocrinology of hospital
Patient 15, wherein 5 offer sea-buchthorn juice beverages, do not limit Ganderwa and number, at least drink 500mL daily, in hospital
After one week treatment observes blood sugar recovery situation；5 offer sea-buckthorn fruit protoplasms；The diet of other 5 maintenances hospital.
According to admission examination result and discharge inspection result, 5 glucose falls for taking sea buckthorn juice are apparent
Better than 5 for taking 5 of sea-buckthorn fruit protoplasm and compareing, either fasting blood-glucose or postprandial blood sugar, there is the apparent range of decrease,
Even there is the dose that 1 patient can reduce melbine to original half, remains to control blood glucose fluctuation in normal range (NR)
It is interior.For the compliance of patient, take sea buckthorn juice 5 patients indicate taste of juice it is sour-sweet tasty and refreshing, can a solution usually
Gluttonous beverage and the pain that cannot be drunk, and to hypoglycemic helpful effect；And 5 patients for taking sea-buckthorn fruit protoplasm indicate magma acid
It is puckery to be difficult to entrance, it is helped to hypoglycemic if not hearing, will not actively want to drink so difficult drink.Illustrate to use sea buckthorn juice
It is in good taste and helpful to treating as the fruit drink that diabetes patient can drink.
Claims (5)
1. a kind of preparation method of full nutritional sea buckthorn fruit juice, which is characterized in that pass through：1. seabuckthorn seeds are extracted seabuckthorn seeds glue, use
In stablize fruit oil and fruit juice emulsification, improve nutritional ingredient stability；2. sea-buckthorn leaf extract is added in fruit juice, realize
Restore a seabuckthorn tree, the fruit juice containing the full trophic function of sea-buckthorn.
2. the method as described in claim 1, which is characterized in that seabuckthorn seeds glue extracting method is as follows：500g seabuckthorn seeds are taken, by matter
Measure volume ratio 1:5~1:8 are added pure water, and 0~4 DEG C of immersion 72~96h, 20000~30000rpm smash 3~5min, and water-bath adds
4~5h of thermal extraction, 80~90 DEG C of temperature, filtering take filtrate；Again by volume 1:5~1:8 are added pure water, heating water bath extraction 4
~5h, 80~90 DEG C of temperature, filtering take filtrate；It filtrate will merge twice, be concentrated, 70~80 DEG C of temperature, vacuum degree ＜
0.09MPa, until volume is 1/20~1/10 to stop concentration before concentration, be added absolute ethyl alcohol to ethanol content reach 80~
90%, 4 DEG C of alcohol precipitations are stayed overnight, and are filtered to obtain solid precipitation, are lyophilized to obtain the final product.
3. the method as described in claim 1, which is characterized in that Leaves of Hippophae L extracting method is as follows：500g Leaves of Hippophae L is taken, after drying
3~5min is smashed with 20000~30000rpm, by mass volume ratio 1:5~1:8 are added petroleum ether, 65~75 DEG C of extraction 2h, mistake
Filter, takes filter residue；Filter residue is volatilized into petroleum ether, by mass volume ratio 1:5~1:8 addition ethanol solutions, concentration of alcohol 50%, 65
~75 DEG C of 2~3h of extraction, filtering take filtrate；Filtrate is concentrated, 60~70 DEG C of temperature, vacuum degree ＜ 0.09MPa, until medicinal extract
Shape, medicinal extract are lyophilized without ethanol flavor to obtain the final product.
4. the method as described in claim 1, which is characterized in that the preparation method of fruit juice is as follows：The complete fructus hippophae of condition is taken,
It is squeezed the juice with juice extractor after cleaning, Seabuckthorn fruit plasmogen is obtained after being filtered to remove dregs；The following raw material is taken by weight：Sea-buckthorn is former
80~100 parts of slurry, 10~20 parts of white granulated sugar, 6~8 parts of seabuckthorn seeds glue, 3~5 parts of sea-buckthorn leaf extract, 3~5 parts of honey, water 50
~120 parts, 20~40 parts of other fruit juices；Other fruit juices can be selected apple fumet, lemon juice, orange Normal juice or its
The sour-sweet fruit juice of his taste；After mixing by each ingredient, homogeneous is carried out twice with high pressure homogenizer, first pass homogeneous pressure
Power is 300Bar, second time homogenization pressure be 500Bar to get.
5. the method as described in claim 1, it is characterized in that, other sweeteners may be selected in the white granulated sugar in claim 4, such as wood
The replacements such as sugar alcohol, sucrose, Aspartame, Sucralose, antierythrite, Momordia grosvenori aglycone, acesulfame potassium, dosage is according to other sweeteners
Sugariness be adjusted；Conventional sterilization can also be added after processing step, as pasteurize, high-pressure pulse electric sterilization,
The methods of irradiation sterilization；The step of sterile filling can also be increased according to the form of product.
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| CN201810474914.XA CN108651786A (en) | 2018-05-17 | 2018-05-17 | A kind of preparation method of full nutritional sea buckthorn fruit juice |
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| CN201810474914.XA CN108651786A (en) | 2018-05-17 | 2018-05-17 | A kind of preparation method of full nutritional sea buckthorn fruit juice |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113180114A (en) * | 2021-04-22 | 2021-07-30 | 成都中医药大学 | Sea-buckthorn milk tablet and preparation method thereof |
| CN114304449A (en) * | 2020-09-24 | 2022-04-12 | 赵英 | Sea-buckthorn juice and preparation method thereof |
| CN114668089A (en) * | 2022-03-09 | 2022-06-28 | 山东省食品发酵工业研究设计院 | Production method for preventing oil floating of sea buckthorn fruit beverage |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114304449A (en) * | 2020-09-24 | 2022-04-12 | 赵英 | Sea-buckthorn juice and preparation method thereof |
| CN113180114A (en) * | 2021-04-22 | 2021-07-30 | 成都中医药大学 | Sea-buckthorn milk tablet and preparation method thereof |
| CN114668089A (en) * | 2022-03-09 | 2022-06-28 | 山东省食品发酵工业研究设计院 | Production method for preventing oil floating of sea buckthorn fruit beverage |
| CN114668089B (en) * | 2022-03-09 | 2024-02-02 | 山东省食品发酵工业研究设计院 | Production method for preventing sea buckthorn fruit beverage grease from floating upwards |
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