CN101843311A - Method for preparing hippophae rhamnoides seed micro powder capsules - Google Patents
Method for preparing hippophae rhamnoides seed micro powder capsules Download PDFInfo
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- CN101843311A CN101843311A CN201010163989A CN201010163989A CN101843311A CN 101843311 A CN101843311 A CN 101843311A CN 201010163989 A CN201010163989 A CN 201010163989A CN 201010163989 A CN201010163989 A CN 201010163989A CN 101843311 A CN101843311 A CN 101843311A
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Abstract
The invention relates to a method for preparing hippophae rhamnoides seed micro powder capsules. The method for preparing the hippophae rhamnoides seed micro powder capsules comprises the following steps of: performing vacuum drying on hippophae rhamnoides seeds; adding konjac glucomannan-acrylic graft copolymer (KAC) which serves as an anticaking agent into the hippophae rhamnoides seeds; performing low-temperature superfine pulverization on the mixture; and encapsulating the mixture, and performing irradiation sterilization at the temperature of 600 DEG C. The method has the advantages of making full use of the hippophae rhamnoides seeds, generating no by-products, keeping the primitivity of the hippophae rhamnoides seeds, avoiding destruction to heat-sensitive and unstable active ingredients, reserving the effective active ingredients and the original various nutritional ingredients in the hippophae rhamnoides seeds to the utmost extent, and being favorable for absorption. An adopted anti-caking agent can solve the problems that the superfine powder is aggregated easily and is difficult to disperse due to superfine particle sizes, and if the added content of the anti-caking agent is less, the anti-caking performance is higher so that the purity of the capsule hippophae rhamnoides seed powder reaches over 99.6 percent. Besides, the method for preparing the hippophae rhamnoides seed micro powder capsules is simple, has less equipment investments, a low production cost and no three wastes outputs, is suitable for application in hippophae rhamnoides producing areas with underdeveloped economy, and is environment-friendly industrialized technology.
Description
Technical field
The invention belongs to the natural plant health-care food processing technology field, be specifically related to the improvement of seabuckthorn seeds processing method.
Background technology
Sea-buckthorn (Hippophae rhamnoides.L) is the Elaeangnaceae hippophae plant.Contain multiple bioactive ingredients in the fruit of sea-buckthorn, limb, the blade to the human body beneficial, as flavonoids, terpene, steroidal class, vitamins, protein and amino acids, oil ﹠ fat acids, volatile oil, organic acid, sugar and trace element etc., be a kind of nutritious, plant that medical value is high.
Data shows that the content of Seabuckthorn Oil is 9%～18% in the Chinese sea buckthorn seed, and Seabuckthorm Seed Oil includes more than 140 kind of bioactive ingredients such as flavonoids, organic acid, alkaloid, sterols, triterpene class and multivitamin, amino acid.The processing and utilization of seabuckthorn seeds is the importance of sea-buckthorn deep processing.Mostly the domestic and international at present processing to seabuckthorn seeds is to adopt milling process, organic solvent extraction or supercritical CO
2Extracting process extracts Seabuckthorm Seed Oil; Milling process belongs to traditional oil expression method, and seabuckthorn seeds does not belong to high oil-containing material, and its oil pump capacity and oil quality all are very limited, existing how the employing; Organic solvent extraction can cause the problem of organic solvent residual and effective active composition loss in the Seabuckthorm Seed Oil, and a large amount of organic solvent waste liquid and waste gas are arranged aborning, and environment is polluted; Supercritical CO
2Extracting process is high to requirement height, the extraction equipment price of equipment precision, extraction cost is too high, has restricted the application of this technical method.
There are some researches show, seabuckthorn seeds is carried in the dregs of fat behind the oil and is contained the useful chemical composition of ten multiclass, but the nutritional labeling that particularly contains needed by human such as rich in protein, carbohydrate edible cellulose, potassium, magnesium, chromium, selenium and manganese, illustrate have in the seabuckthorn seeds many have bioactive material carry oil after still be retained in (chemical constitution study Fu of the comprehensive utilization of seabuckthorn seeds-seabuckthorn seeds dregs of fat builds " sea-buckthorns " 200619 (3) such as prosperous Tian Peng) in the dregs of fat.If the seabuckthorn seeds slag of carrying behind the oil is given it up, the serious wasting of resources will be caused.Also have and extract active ingredients such as flavones, Fructus Hippophae polysaccharide, the OPC (method of while grading extraction Hippophate flavone and Fructus Hippophae polysaccharide in the Chinese patent 200410017392.9 seabuckthorn seeds slags the seabuckthorn seeds slag of research after carrying oil; " Heilongjiang Bayi Agricultural Reclamation University's journals " such as Fructus Hippophae polysaccharide Study on extraction Yang Hong will; 200,810,176,033 1 kinds of methods of extracting OPC in the seabuckthorn seeds of Chinese patent); This class technical method is complex process, extraction cost height and have that the three wastes produce, have residual in the product and loss of effective components, be difficult to promote not only, the original just pettiness very of the content of these active components in the seabuckthorn seeds importantly, and all technology all are the extractions of single or several compositions, active ingredients are fully used, cause the serious waste of resource equally.
In sum, containing many effective active compositions in the seabuckthorn seeds, how to make full use of resource, improve the seabuckthorn seeds practical value, keep fully that the effective active composition reduces preparation cost simultaneously for human used in the seabuckthorn seeds, is basic point of departure of the present invention.
Summary of the invention
Purpose of the present invention just provides a kind of preparation method of hippophae rhamnoides seed micro powder capsules, makes that active ingredient can be fully utilized in the seabuckthorn seeds, keeps the effective active composition in the seabuckthorn seeds to greatest extent, can be absorbed and used fully again after edible; This preparation method is simple, equipment less investment, low, the no three wastes output of production cost, is adapted at the sea-buckthorn producing region application of economics of underdevelopment, is the industrialization technology of an environmental protection.
Hippophae rhamnoides seed micro powder capsules preparation method proposed by the invention, concrete steps comprise:
Step 1, will screen the seabuckthorn seeds of cleaning back (does not have assorted, dustless, nothing go mouldy), the employing vacuum drying method makes that moisture is 7%～10% in the seabuckthorn seeds; Its baking temperature is 50～60 ℃, and vacuum is 0.05～0.08MPa;
Step 2, the mass ratio by 2 ‰～3 ‰ in the seabuckthorn seeds of drying add konjaku glucomannan-acrylic acid graft copolymer (being anticaking agent), according to GB2760-2007 standard control interpolation process; Under temperature is-20 ℃～-30 ℃, granularity 〉=300 purpose conditions, adopt the low temperature ultramicro grinding;
Step 3, under aseptic condition, seabuckthorn seeds ultra micro powder adopted hard shell capsules dress capsule packing; The packing net content should meet the provisions of the relevant regulations issued by the State; Adopt
60C
0Irradiation sterilization, irradiation dose are 4～6kGy, and the every index of microorganism should meet the GB16740-1997 standard in the product of sterilization back.
By as can be seen above, the preparation method of hippophae rhamnoides seed micro powder capsules of the present invention has fully utilized seabuckthorn seeds, generates without any byproduct, has kept the ecosystem of seabuckthorn seeds, has kept the effective active composition in the seabuckthorn seeds to greatest extent; The hippophae rhamnoides seed micro powder capsules that makes preparation as health food have anti-oxidant, antifatigue, protect liver, regulate blood fat, antitumor, delay body aging, brain tonic and intelligence development, promote effects such as upgrowth and development of children.Because the present invention has adopted low temperature ultramicro grinding processing method, the material friability under low-temperature condition improves, is easy to pulverize, and can realize the breaking-wall cell pulverizing, and the material smashing fineness is reached more than 300 orders, is more conducive to absorb after human body is edible; And the technical process of vacuum dehydrating at lower temperature, irradiation sterilization has also been avoided high temperature and the organic solvent extracting method destruction to temperature-sensitive, labile active ingredient in the seabuckthorn seeds to greatest extent, has kept original nutrients in the seabuckthorn seeds.The anticaking agent that is adopted is konjaku glucomannan-acrylic acid graft copolymer (KAC), be the konjaku glucomannan of producing by natural konjaku (KGM) and acrylic graft-modified synthetic acquisition, hydrophilic radicals such as great amount of hydroxy group that it contains and carboxyl, have good moisture pick-up properties, can solve micro mist because of the meticulous problem of easily assembling caking, being difficult to disperse of granularity; The KAC that with the natural polysaccharide is raw material is environmentally friendly novel anticaking agent, and its addition still less, the resistive connection performance is more excellent, and the purity of capsule 's content-seabuckthorn seeds powder is reached more than 99.6%.In addition, preparation method of the present invention is simple, equipment less investment, low, the no three wastes output of production cost, is adapted at the sea-buckthorn producing region application of economics of underdevelopment, is the industrialization technology of an environmental protection.
The specific embodiment
The specific embodiment below in conjunction with the example in detail technical solution of the present invention.Konjaku glucomannan-the acrylic acid graft copolymer that adopts in the example (KAC) is produced for the sincere biotechnology of Wuhan power company, and the low temperature micronizer that adopts is the ZMD-6 type that Harbin nano medication chemistry equipment company produces.
Embodiment 1,
Step 1, adopt the double dust collection air-screen separator to remove impurity such as stone, fruit branch, pomace seabuckthorn seeds, change water spray Cleaning for High Capacity machine water again over to and clean, require seabuckthorn seeds after the selected cleaning do not have assorted, dustless, do not have and go mouldy;
Step 2, the seabuckthorn seeds after will cleaning adopt conventional vacuum drier to carry out drying, require baking temperature less than 60 ℃, vacuum 0.05～0.08MPa, the dried moisture of seabuckthorn seeds≤8%;
Step 3, in dried seabuckthorn seeds, add 3 ‰ anticaking agent KAC, according to GB2760-2007 " food add use sanitary standard " control interpolation process by mass ratio;
Step 4, the seabuckthorn seeds that will add anticaking agent adopt ZMD-6 type low temperature micronizer to pulverize, and requiring to pulverize temperature is-20 ℃, and the finished product granularity is 300 orders;
Step 5, with seabuckthorn seeds ultra micro powder encapsulated packing under aseptic condition of pulverizing, adopt the medical gelatin hard capsule case that meets version NF standard in 2000; The packing net content meets country's " quantification packing commodity supervision regulation ";
Step 6, the capsule employing that the seabuckthorn seeds powder will be housed
60C0 irradiation sterilization, irradiation dose are 6kGy; The every index of microorganism meets the requirement of country (GB16740-1997) health care (function) food universal standard in the product of sterilization back; Not loss of the content of its main active ingredient (as general flavone, OPC) after testing.
Embodiment 2,
Step 1, adopt the double dust collection air-screen separator to remove impurity such as stone, fruit branch, pomace seabuckthorn seeds, change water spray Cleaning for High Capacity machine water again over to and clean, require seabuckthorn seeds after the selected cleaning do not have assorted, dustless, do not have and go mouldy;
Step 2, the seabuckthorn seeds after will cleaning adopt conventional vacuum drier to carry out drying, require baking temperature less than 55 ℃, vacuum 0.05～0.08MPa, the dried moisture of seabuckthorn seeds＜10%;
Step 3, in dried seabuckthorn seeds, add 2 ‰ anticaking agent KAC, according to GB2760-2007 " food add use sanitary standard " control interpolation process by mass ratio;
Step 4, the seabuckthorn seeds that will add anticaking agent adopt ZMD-6 type low temperature micronizer to pulverize, and requiring to pulverize temperature is-25 ℃, and the finished product granularity is 350 orders;
Step 5, with seabuckthorn seeds ultra micro powder encapsulated packing under aseptic condition of pulverizing, adopt the medical gelatin hard capsule case that meets version NF standard in 2000; The packing net content meets country's " quantification packing commodity supervision regulation ";
Step 6, the capsule employing that the seabuckthorn seeds powder will be housed
60C
0Irradiation sterilization, irradiation dose are 4kGy; The every index of microorganism meets the requirement of country (GB16740-1997) health care (function) food universal standard in the product of sterilization back; Not loss of the content of its main active (as flavonoids, OPC) after testing.
Claims (3)
1. the preparation method of a hippophae rhamnoides seed micro powder capsules is characterized in that, concrete steps comprise:
Step 1, will screen the seabuckthorn seeds after cleaning, and adopt vacuum drying method to make that moisture is 7%～10% in the seabuckthorn seeds;
Step 2, the weight ratio by 2 ‰～3 ‰ in dried seabuckthorn seeds add konjaku glucomannan-acrylic acid graft copolymer; Adopt the low temperature ultramicro grinding to pulverize, make granularity 〉=300 orders;
Step 3, under aseptic condition, seabuckthorn seeds ultra micro powder is adorned capsule with hard shell capsules, adopt
60C0 irradiation sterilization, irradiation dose are 4～6kGy.
2. preparation method according to claim 1 is characterized in that, vacuum drying vacuum described in the step 1 is 0.05～0.08MPa, and baking temperature is 50～60 ℃.
3. preparation method according to claim 1 is characterized in that, the temperature of the ultramicro grinding of low temperature described in the step 2 is-20 ℃～-30 ℃.
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| CN201010163989A CN101843311A (en) | 2010-05-05 | 2010-05-05 | Method for preparing hippophae rhamnoides seed micro powder capsules |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105285558A (en) * | 2014-12-02 | 2016-02-03 | 山东黑尚莓生物技术发展股份有限公司 | Compound berry seed ultrafine powder and production method thereof |
| CN108651786A (en) * | 2018-05-17 | 2018-10-16 | 江南大学 | A kind of preparation method of full nutritional sea buckthorn fruit juice |
| CN109924488A (en) * | 2019-04-25 | 2019-06-25 | 璐炬． | A kind of acer truncatum seed and linseed compound cryosar Ultramicro-powder microcapsule preparation method |
| CN112293710A (en) * | 2020-10-29 | 2021-02-02 | 贾森 | Preparation method of composite micro-powder nutritional chewable tablet |
| CN116492269A (en) * | 2023-06-21 | 2023-07-28 | 美出莱(杭州)化妆品有限责任公司 | Peony seed superfine powder and freeze-dried powder prepared from peony seed superfine powder |
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| CN1309920A (en) * | 2000-02-20 | 2001-08-29 | 陈杰 | Sea-buckthorn seed kernel powder producing process |
| CN101579092A (en) * | 2009-06-22 | 2009-11-18 | 大连工业大学 | Method for producing active seabuckthorn freeze-drying powder and capsule thereof by using vacuum freeze-drying method |
| CN101670276A (en) * | 2009-09-30 | 2010-03-17 | 福建农林大学 | Amorphophallus glucomannan drying agent and preparation method thereof |
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2010
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| CN1309920A (en) * | 2000-02-20 | 2001-08-29 | 陈杰 | Sea-buckthorn seed kernel powder producing process |
| CN101579092A (en) * | 2009-06-22 | 2009-11-18 | 大连工业大学 | Method for producing active seabuckthorn freeze-drying powder and capsule thereof by using vacuum freeze-drying method |
| CN101670276A (en) * | 2009-09-30 | 2010-03-17 | 福建农林大学 | Amorphophallus glucomannan drying agent and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105285558A (en) * | 2014-12-02 | 2016-02-03 | 山东黑尚莓生物技术发展股份有限公司 | Compound berry seed ultrafine powder and production method thereof |
| CN108651786A (en) * | 2018-05-17 | 2018-10-16 | 江南大学 | A kind of preparation method of full nutritional sea buckthorn fruit juice |
| CN109924488A (en) * | 2019-04-25 | 2019-06-25 | 璐炬． | A kind of acer truncatum seed and linseed compound cryosar Ultramicro-powder microcapsule preparation method |
| CN112293710A (en) * | 2020-10-29 | 2021-02-02 | 贾森 | Preparation method of composite micro-powder nutritional chewable tablet |
| CN116492269A (en) * | 2023-06-21 | 2023-07-28 | 美出莱(杭州)化妆品有限责任公司 | Peony seed superfine powder and freeze-dried powder prepared from peony seed superfine powder |
| CN116492269B (en) * | 2023-06-21 | 2023-09-08 | 美出莱(杭州)化妆品有限责任公司 | Peony seed superfine powder and freeze-dried powder prepared from peony seed superfine powder |
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Application publication date: 20100929 |