CN108587476A - A kind of preparation method of steel polishing agent - Google Patents
A kind of preparation method of steel polishing agent Download PDFInfo
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- CN108587476A CN108587476A CN201810515218.9A CN201810515218A CN108587476A CN 108587476 A CN108587476 A CN 108587476A CN 201810515218 A CN201810515218 A CN 201810515218A CN 108587476 A CN108587476 A CN 108587476A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
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Abstract
The invention discloses a kind of preparation methods of steel polishing agent, belong to steel surface processing technology field.The present invention is using flyash, rich aluminium clay as raw material, through alkali soluble activation, hydro-thermal, colloidal sol, molecular sieve is made, high-dispersion load structure, it plays a role to aluminium ion, iron ion and provides good dispersed encapsulated, abrasive material decentralized medium makes nano level abrasive particle be fixed in polymeric gel structure, injury of the abrasive particle surface imperfection hard structure to stainless steel work-piece surface is reduced, the workpiece surface glossiness in polishing process is effectively improved；Graft modification SiO2Liquid coated alumina, the irregular structures such as the corner angle on its surface and protrusion are improved, surface becomes more mellow and fuller, to effectively reduce the damage of the structures to stainless steel surface such as the corner angle of hard and protrusion in polishing process, improves the glossiness on the stainless steel work-piece surface in polishing process.The present invention solves the problems, such as bad to workpiece surface glossiness in polishing process for current steel polishing agent.
Description
Technical field
The invention belongs to steel surface processing technology fields, more particularly to a kind of preparation method of steel polishing agent.
Background technology
Polishing refers to so that workpiece surface roughness is reduced using the effect of machinery, chemistry or electrochemistry, bright with acquisition,
The processing method of flat surface.It is to be carried out to workpiece surface using flexible polishing tool and abrasive grain or other polishing mediums
Modification processing.Polishing cannot improve the dimensional accuracy or geometrical precision of workpiece, but to obtain smooth surface or specular light
For the purpose of pool, sometimes also eliminating gloss (delustring).Usually using polishing wheel as polishing tool.Polishing wheel generally uses multilayer sail
Cloth, felt or leather fold, and both sides are clamped with circular metal plate, and wheel rim coating is uniformly mixed by micron power and grease etc.
Made of polishing agent.Although present conventional use of metal polish, polishing performance have been able to meet and generally require, still
Still have much room for improvement to further improve performance, be also required into one simultaneously for the glossiness retentivity of steel surface after polishing
Step improves.
Steel-product in use, due to oxidation, humidity in air or contacts chemical substance and corrosive gas etc.
Reason causes steel-product surface corrosion, attachment foul greasy dirt situation usually to be used to increase steel-product any surface finish
The steel detergent or steel polishing agent of chemistry are handled.Steel polishing agent is one of important procedure of metal surface processing,
Chemical substance for belonging to part surface polishing.It is divided into paste and liquid.Paste general types have：White antiscuffing paste, green
Antiscuffing paste, red antiscuffing paste, paste polish etc..
Liquid metals polishing agent product typically contains strong acid or phosphate, pollutes environment and cleaning efficiency is low.
Solid steel antiscuffing paste is with the minerals such as fine gtinding sand, aluminium oxide and burnishing oil, specially treated and high speed
Toothpaste body made of emulsification, belongs to fine chemical product, is subject to and does not finely do a variety of granularities.Effect：Steel surface decontamination is thrown
Light, the artificial effect polished with metal surface protection.Import and two kinds domestic can be divided into.There are many imported and famous brand, and appearance is beautiful,
But price is very expensive.It is polished for high-grade mold, precision instrument or part decontamination.Domestic, steel surface fine gtinding is polished
Cream, import primary raw material and technique are nursed, it is easy to use to be process toothpaste-like using high speed emulsification.Due to cheap,
Various steel surfaces are widely used in, decontamination is polished, nursed, and because abrasive sand is finer and smoother, and is hand polish, generally will not be
Steel surface is left a trace, and can reach bright such as new appearance, and cream is polished according to bright stock and oxide mass, content, steel
Also there is quick clean bright cream and commonly polish two kinds of cream.Currently there are steel polishing agent in use, often first
The operations such as surface is cleaned and polished, so that steel surface is clean and brightness is higher, the product is used to improve
The quality of equipment obtained etc..However in the prior art, often the operations such as cleaning and polishing of steel surface are by artificial
The realizations such as polishing, it is not only time-consuming and laborious, production efficiency is substantially reduced, and the effect of manual polishing is heavily dependent on behaviour
Make the proficiency of personnel, therefore, often causes the metal quality after cleaning irregular.
Invention content
The technical problems to be solved by the invention：For current steel polishing agent to workpiece surface gloss in polishing process
Bad problem is spent, a kind of preparation method of steel polishing agent is provided.
In order to solve the above technical problems, the present invention is using technical solution as described below：
A kind of preparation method of steel polishing agent includes the following steps：
（1）In 40 ~ 60 DEG C, base-material in mass ratio 1 is taken：3 ~ 5 are added sodium hydroxide solution, and 30 ~ 45min is mixed, is heated to
90 ~ 100 DEG C, mixed liquor is obtained, 30 ~ 40% silica gel of mixed liquor quality, the hydrogen of mixed liquor quality 25 ~ 35% are added into mixed liquor
Aluminium oxide is uniformly mixed, obtains colloidal sol, take colloidal sol in mass ratio 1:0.1 is added hexadecyltrimethylammonium chloride, is uniformly mixed,
85 ~ 100 DEG C are warming up to, 1 ~ 2h is stood, filtering takes filter residue with 2 ~ 4 times of deionized water cleanings of filter residue quality, by the filter residue after washing
In 85 ~ 100 DEG C of dryings, dried object is obtained, takes dried object with 600 ~ 700 DEG C of 3 ~ 5h of roasting, obtains calcining matter, it is spare；
（2）In mass ratio 1：3 ~ 5 take 3- (methacryloxypropyl) propyl trimethoxy silicane that Nano-meter SiO_2 is added2/ ethyl alcohol disperses
Liquid, in 40 ~ 50 DEG C, stirring 20 ~ for 24 hours, improved silica dispersion liquid is obtained, methyl methacrylate in mass ratio 1 is taken：2 ~ 4 add
Enter improved silica dispersion liquid, is uniformly mixed, rotary evaporation is dried under vacuum to the 30 ~ 40% of original volume, obtains concentrate, takes dense
Contracting liquid in mass ratio 2：0.3 ~ 0.8 is added methyl methacrylate, and mixing obtains monomer dispersion liquid；
（3）In 20 ~ 25 DEG C, monomer dispersion liquid is taken, 15 ~ 20% over cure potassium of monomer dispersion liquid quality is added, is mixed equal
It is even, 90 ~ 100 DEG C of 1 ~ 2h of maintenance are warming up to, 40 ~ 50 DEG C of 12 ~ 15h of maintenance is cooled to, obtains base fluid；
（4）According to the mass fraction, 40 ~ 60 parts of steps are taken successively（1）In spare calcining matter, 50 ~ 70 parts of base fluids, 20 ~ 40
Part copper-bath, 15 ~ 30 parts of aluminium oxide, 10 ~ 15 parts of solubilizer, 20 ~ 30 parts of surfactants, 4 ~ 10 parts of citric acids, 5 ~ 12
Part oxalic acid, after first mixing bulking agent, surfactant, citric acid, oxalic acid, aluminium oxide, it is mixed to add calcining matter for heating melting
It closes, stirs 30 ~ 45min, ultrasonic wave disperses 15 ~ 25min, obtains dispersion molten liquid, takes dispersion molten liquid, injection molding to be cooled and shaped, takes off
Mould is to get steel polishing agent.
The step（1）In base-material：Take flyash, rich aluminium clay, sodium carbonate in mass ratio 1:1~3:0.3 mixing, i.e.,
Obtain base-material.
The step（4）In solubilizer：In mass ratio 2:1:1:4 ~ 6 polyethylene glycol, Emulsifier EL-60, tween
80, absolute ethyl alcohol mixing is to get solubilizer.
The step（4）In surfactant：In mass ratio 2:1 ~ 2 takes fatty alcohol polyoxyethylene ether, detergent alkylate
Sodium sulfonate mixes to get surfactant.
Compared with other methods, advantageous effects are the present invention：
Using flyash, rich aluminium clay as raw material, through alkali soluble activation, hydro-thermal, colloidal sol, molecular sieve, high-dispersion load is made in the present invention
Structure, plays a role to aluminium ion, iron ion and provides good dispersed encapsulated, and abrasive material decentralized medium makes nano level abrasive material
Particle is fixed in polymeric gel structure, and in preparation process, the presence of gel network structure can effectively avoid product and exist
The reunion of nanometer abrasive particle, makes its polishing performance be improved, in addition, the high score of toughness during preparation, storage and use
Sub- gel can reduce injury of the abrasive particle surface imperfection hard structure to stainless steel work-piece surface, effectively improve polished
Workpiece surface glossiness in journey；Graft modification SiO2Liquid coated alumina, the irregular structures such as the corner angle on surface and protrusion obtain
To improvement, surface becomes more mellow and fuller, so as to effectively reduce in polishing process the structures such as the corner angle of hard and protrusion to stainless
The damage of steel surface, and the hardness of silica is lower for aluminium oxide, oxidation aluminium surface coat one layer of hardness compared with
After low silicon dioxide layer, the glossiness on the stainless steel work-piece surface in polishing process can be effectively improved.
Specific implementation mode
Nano-meter SiO_22/ alcohol dispersion liquid：It is purchased from Xuancheng Jingrui New Material Co., Ltd..
Base-material：Take flyash, rich aluminium clay, sodium carbonate in mass ratio 1:1~3:0.3 mixing is to get base-material.
Solubilizer：In mass ratio 2:1:1:4 ~ 6 polyethylene glycol, Emulsifier EL-60, Tween 80, absolute ethyl alcohol mixing,
Up to solubilizer.
Surfactant：In mass ratio 2:1 ~ 2 take fatty alcohol polyoxyethylene ether, neopelex mixing to get
Surfactant.
A kind of preparation method of steel polishing agent, includes the following steps：
（1）In 40 ~ 60 DEG C of water-bath, base-material in mass ratio 1 is taken：3 ~ 5 are added the sodium hydroxide solution that mass fraction is 40%, with 150
~ 180r/min be mixed 30 ~ 45min, after be heated to 90 ~ 100 DEG C, obtain mixed liquor, into mixed liquor be added mixed liquor quality
30 ~ 40% silica gel, mixed liquor quality 25 ~ 35% aluminium hydroxide, be uniformly mixed, obtain colloidal sol, take colloidal sol in mass ratio 1:0.1
Hexadecyltrimethylammonium chloride is added, is uniformly mixed, is warming up to 85 ~ 100 DEG C, stands 1 ~ 2h, filtering takes filter residue with filter residue matter
Amount 2 ~ 4 times of deionized waters cleaning, after by the filter residue after washing move to 85 ~ 100 DEG C of drying boxes dry to water content 1% hereinafter,
Dried object takes dried object, with 600 ~ 700 DEG C of 3 ~ 5h of roasting, to obtain calcining matter in Muffle furnace, spare；
（2）In mass ratio 1：3 ~ 5 take 3- (methacryloxypropyl) propyl trimethoxy silicane that Nano-meter SiO_2 is added2/ ethyl alcohol disperses
Liquid, in 40 ~ 50 DEG C, stirring 20 ~ for 24 hours, improved silica dispersion liquid is obtained, methyl methacrylate in mass ratio 1 is taken：2 ~ 4 add
Enter improved silica dispersion liquid, is uniformly mixed, rotary evaporation is dried under vacuum to the 30 ~ 40% of original volume, obtains concentrate, takes dense
Contracting liquid in mass ratio 2：0.3 ~ 0.8 is added methyl methacrylate, and mixing obtains monomer dispersion liquid；
（3）20 ~ 25 DEG C are bathed in grease, takes monomer dispersion liquid, 15 ~ 20% over cure potassium of monomer dispersion liquid quality, mixing is added
Stir evenly, 90 ~ 100 DEG C of 1 ~ 2h of maintenance be warming up to 5 ~ 10 DEG C/min rates, after be cooled to 40 with 10 ~ 15 DEG C/min rates ~
50 DEG C of 12 ~ 15h of maintenance, obtain base fluid；
（4）According to the mass fraction, it is 20 ~ 30% to take 40 ~ 60 parts of calcining matters, 50 ~ 70 parts of base fluids, 20 ~ 40 parts of mass fractions successively
Copper-bath, 15 ~ 30 parts of aluminium oxide, 10 ~ 15 parts of solubilizer, 20 ~ 30 parts of surfactants, 4 ~ 10 parts of citric acids, 5 ~ 12 parts
Oxalic acid, after first mixing bulking agent, surfactant, citric acid, oxalic acid, aluminium oxide, it is mixed to add calcining matter for heating melting
It closes, 30 ~ 45min is stirred with 220 ~ 250r/min, ultrasonic wave disperses 15 ~ 25min, obtains dispersion molten liquid, take dispersion molten liquid, notes
Mould is cooled and shaped, and is demoulded to get steel polishing agent.
Embodiment 1
Nano-meter SiO_22/ alcohol dispersion liquid：It is purchased from Xuancheng Jingrui New Material Co., Ltd..
Base-material：Take flyash, rich aluminium clay, sodium carbonate in mass ratio 1:1:0.3 mixing is to get base-material.
Solubilizer：In mass ratio 2:1:1:4 polyethylene glycol, Emulsifier EL-60, Tween 80, absolute ethyl alcohol mixing, i.e.,
Obtain solubilizer.
Surfactant：In mass ratio 2:1 takes fatty alcohol polyoxyethylene ether, neopelex mixing to get table
Face activating agent.
A kind of preparation method of steel polishing agent, includes the following steps：
（1）In 40 DEG C of water-bath, base-material in mass ratio 1 is taken：3 are added the sodium hydroxide solution that mass fraction is 40%, with 150r/min
Be mixed 30min, after be heated to 90 DEG C, obtain mixed liquor, into mixed liquor be added mixed liquor quality 30% silica gel, mixing
The aluminium hydroxide of liquid quality 25% is uniformly mixed, obtains colloidal sol, take colloidal sol in mass ratio 1:0.1 is added cetyl trimethyl chlorination
Ammonium is uniformly mixed, is warming up to 85 DEG C, stands 1h, filtering, takes filter residue with the 2 times of deionized waters cleanings of filter residue quality, after will be after washing
Filter residue move to 85 DEG C of drying boxes dry to water content 1% hereinafter, dried object, take dried object to be roasted with 600 DEG C in Muffle furnace
3h obtains calcining matter, spare；
（2）In mass ratio 1：3 take 3- (methacryloxypropyl) propyl trimethoxy silicane that Nano-meter SiO_2 is added2/ alcohol dispersion liquid,
In 40 DEG C, 20h is stirred, improved silica dispersion liquid is obtained, takes methyl methacrylate in mass ratio 1：2 ~ 4 are added modified dioxy
SiClx dispersion liquid is uniformly mixed, and rotary evaporation is dried under vacuum to the 30 ~ 40% of original volume, obtains concentrate, takes concentrate by quality
Than 2：0.3 is added methyl methacrylate, and mixing obtains monomer dispersion liquid；
（3）20 DEG C are bathed in grease, takes monomer dispersion liquid, 15% over cure potassium of monomer dispersion liquid quality is added, is mixed equal
It is even, with 5 DEG C/min rates be warming up to 90 DEG C maintenance 1h, after with 10 DEG C/min rates be cooled to 40 DEG C maintenance 12h, obtain base fluid；
（4）According to the mass fraction, take successively 40 parts of calcining matters, 50 parts of base fluids, the copper-bath that 20 parts of mass fractions are 20%,
15 parts of aluminium oxide, 10 parts of solubilizer, 20 parts of surfactants, 4 parts of citric acids, 5 parts of oxalic acid, first by bulking agent, surfactant,
After citric acid, oxalic acid, aluminium oxide mixing, heating melting adds calcining matter mixing, and 30min, ultrasonic wave are stirred with 220r/min
Disperse 15min, obtain dispersion molten liquid, takes dispersion molten liquid, injection molding to be cooled and shaped, demould to get steel polishing agent.
Embodiment 2
Nano-meter SiO_22/ alcohol dispersion liquid：It is purchased from Xuancheng Jingrui New Material Co., Ltd..
Base-material：Take flyash, rich aluminium clay, sodium carbonate in mass ratio 1:2:0.3 mixing is to get base-material.
Solubilizer：In mass ratio 2:1:1:5 polyethylene glycol, Emulsifier EL-60, Tween 80, absolute ethyl alcohol mixing, i.e.,
Obtain solubilizer.
Surfactant：In mass ratio 2:1.5 take fatty alcohol polyoxyethylene ether, neopelex mixing to get
Surfactant.
A kind of preparation method of steel polishing agent, includes the following steps：
（1）In 50 DEG C of water-bath, base-material in mass ratio 1 is taken：4 are added the sodium hydroxide solution that mass fraction is 40%, with 165r/min
Be mixed 38min, after be heated to 95 DEG C, obtain mixed liquor, into mixed liquor be added mixed liquor quality 35% silica gel, mixing
The aluminium hydroxide of liquid quality 30% is uniformly mixed, obtains colloidal sol, take colloidal sol in mass ratio 1:0.1 is added cetyl trimethyl chlorination
Ammonium is uniformly mixed, is warming up to 95 DEG C, stands 1.5h, filtering, takes filter residue with the 3 times of deionized waters cleanings of filter residue quality, after will washing
Filter residue afterwards move to 95 DEG C of drying boxes dry to water content 1% hereinafter, dried object, take dried object to be roasted with 650 DEG C in Muffle furnace
4h is burnt, calcining matter is obtained, it is spare；
（2）In mass ratio 1：4 take 3- (methacryloxypropyl) propyl trimethoxy silicane that Nano-meter SiO_2 is added2/ alcohol dispersion liquid,
In 45 DEG C of water-bath, 22h is stirred with 240r/min, improved silica dispersion liquid is obtained, takes methyl methacrylate in mass ratio 1：3
Improved silica dispersion liquid is added, is uniformly mixed, rotary evaporation is dried under vacuum to the 35% of original volume, to concentrate, takes dense
Contracting liquid in mass ratio 2：0.5 is added methyl methacrylate, obtains monomer dispersion liquid；
（3）23 DEG C are bathed in grease, takes monomer dispersion liquid, 18% over cure potassium of monomer dispersion liquid quality is added, is mixed equal
It is even, with 8 DEG C/min rates be warming up to 95 DEG C maintenance 1.5h, after with 13 DEG C/min rates be cooled to 45 DEG C maintenance 13h, obtain base fluid；
（4）According to the mass fraction, take successively 50 parts of calcining matters, 60 parts of base fluids, the copper-bath that 30 parts of mass fractions are 25%,
23 parts of aluminium oxide, 13 parts of solubilizer, 25 parts of surfactants, 7 parts of citric acids, 8 parts of oxalic acid, first by bulking agent, surfactant,
After citric acid, oxalic acid, aluminium oxide mixing, heating melting adds calcining matter mixing, and 38min, ultrasonic wave are stirred with 235r/min
Disperse 20min, obtain dispersion molten liquid, takes dispersion molten liquid, injection molding to be cooled and shaped, demould to get steel polishing agent.
Embodiment 3
Nano-meter SiO_22/ alcohol dispersion liquid：It is purchased from Xuancheng Jingrui New Material Co., Ltd..
Base-material：Take flyash, rich aluminium clay, sodium carbonate in mass ratio 1:3:0.3 mixing is to get base-material.
Solubilizer：In mass ratio 2:1:1:6 polyethylene glycol, Emulsifier EL-60, Tween 80, absolute ethyl alcohol mixing, i.e.,
Obtain solubilizer.
Surfactant：In mass ratio 2:2 take fatty alcohol polyoxyethylene ether, neopelex mixing to get table
Face activating agent.
A kind of preparation method of steel polishing agent, includes the following steps：
（1）In 60 DEG C of water-bath, base-material in mass ratio 1 is taken：5 are added the sodium hydroxide solution that mass fraction is 40%, with 180r/min
Be mixed 45min, after be heated to 100 DEG C, obtain mixed liquor, into mixed liquor be added mixed liquor quality 40% silica gel, mixing
The aluminium hydroxide of liquid quality 35% is uniformly mixed, obtains colloidal sol, take colloidal sol in mass ratio 1:0.1 is added cetyl trimethyl chlorination
Ammonium is uniformly mixed, is warming up to 100 DEG C, stands 2h, filtering, takes filter residue with the 4 times of deionized waters cleanings of filter residue quality, after will washing
Filter residue afterwards move to 100 DEG C of drying boxes dry to water content 1% hereinafter, dried object, take dried object in Muffle furnace with 700 DEG C
5h is roasted, calcining matter is obtained, it is spare；
（2）In mass ratio 1：5 take 3- (methacryloxypropyl) propyl trimethoxy silicane that Nano-meter SiO_2 is added2/ alcohol dispersion liquid,
For 24 hours with 250r/min stirrings improved silica dispersion liquid is obtained, methyl methacrylate in mass ratio 1 is taken in 50 DEG C of water-bath：4
Improved silica dispersion liquid is added, is uniformly mixed, rotary evaporation is dried under vacuum to the 40% of original volume, to concentrate, takes dense
Contracting liquid in mass ratio 2：0.8 is added methyl methacrylate, obtains monomer dispersion liquid；
（3）25 DEG C are bathed in grease, takes monomer dispersion liquid, 20% over cure potassium of monomer dispersion liquid quality is added, is mixed equal
It is even, with 10 DEG C/min rates be warming up to 100 DEG C maintenance 2h, after with 15 DEG C/min rates be cooled to 50 DEG C maintenance 15h, obtain base fluid；
（4）According to the mass fraction, take successively 60 parts of calcining matters, 70 parts of base fluids, the copper-bath that 40 parts of mass fractions are 30%,
30 parts of aluminium oxide, 15 parts of solubilizer, 30 parts of surfactants, 10 parts of citric acids, 12 parts of oxalic acid, first by bulking agent, surface-active
After agent, citric acid, oxalic acid, aluminium oxide mixing, heating melting adds calcining matter mixing, stirs 45min with 250r/min, surpasses
Sound wave disperses 25min, obtains dispersion molten liquid, takes dispersion molten liquid, injection molding to be cooled and shaped, demoulds to get steel polishing agent.
Comparative example：The steel polishing agent of Dongguan City company production
The steel polishing agent that embodiment 1,2,3 and comparative example are prepared is tested for the property, aluminum alloy surface is thrown
Phototesting, and performance comparison is carried out with existing common polishing agent, test result is recorded in table 1.
Table 1：
In summary, glossiness is imitated after a polish for steel polishing agent produced by the present invention it can be seen from detection data in upper table
Fruit is stronger, and smoothness is more smooth and the retention time is long, has broad application prospects.
Claims (4)
1. a kind of preparation method of steel polishing agent, which is characterized in that the preparation method includes the following steps：
In 40 ~ 60 DEG C, base-material in mass ratio 1 is taken：3 ~ 5 are added sodium hydroxide solution, are mixed, are heated to 90 ~ 100 DEG C, obtain
Mixed liquor, the silica gel of mixed liquor quality 30 ~ 40%, the aluminium hydroxide of mixed liquor quality 25 ~ 35% are added into mixed liquor, and mixing is equal
It is even, colloidal sol is obtained, colloidal sol in mass ratio 1 is taken:0.1 is added hexadecyltrimethylammonium chloride, is uniformly mixed, is warming up to 85 ~ 100
DEG C, 1 ~ 2h is stood, filtering takes filter residue with 2 ~ 4 times of deionized water cleanings of filter residue quality, and the filter residue after washing is dry in 85 ~ 100 DEG C
It is dry, dried object is obtained, takes dried object with 600 ~ 700 DEG C of 3 ~ 5h of roasting, obtains calcining matter, it is spare；
（2）In mass ratio 1：3 ~ 5 take 3- (methacryloxypropyl) propyl trimethoxy silicane that Nano-meter SiO_2 is added2/ alcohol dispersion liquid,
In 40 ~ 50 DEG C, stirring 20 ~ for 24 hours, improved silica dispersion liquid is obtained, methyl methacrylate in mass ratio 1 is taken：2 ~ 4 additions change
Property silica dispersions, be uniformly mixed, rotary evaporation is dried under vacuum to the 30 ~ 40% of original volume, obtains concentrate, takes concentrate
In mass ratio 2：0.3 ~ 0.8 is added methyl methacrylate, and mixing obtains monomer dispersion liquid；
（3）In 20 ~ 25 DEG C, monomer dispersion liquid is taken, 15 ~ 20% over cure potassium of monomer dispersion liquid quality is added, is mixed equal
It is even, 90 ~ 100 DEG C of 1 ~ 2h are warming up to, 40 ~ 50 DEG C of 12 ~ 15h is cooled to, obtains base fluid；
（4）According to the mass fraction, 40 ~ 60 parts of steps are taken successively（1）In spare calcining matter, 50 ~ 70 parts of base fluids, 20 ~ 40
Part copper-bath, 15 ~ 30 parts of aluminium oxide, 10 ~ 15 parts of solubilizer, 20 ~ 30 parts of surfactants, 4 ~ 10 parts of citric acids, 5 ~ 12
Part oxalic acid, after first mixing solubilizer, surfactant, citric acid, oxalic acid, aluminium oxide, it is mixed to add calcining matter for heating melting
Stirring is closed, dispersion molten liquid is obtained, takes dispersion molten liquid, injection molding to be cooled and shaped, demoulds to get steel polishing agent.
2. the preparation method of steel polishing agent according to claim 1, which is characterized in that the step（1）In base-material：It takes
Flyash, rich aluminium clay, sodium carbonate in mass ratio 1:1~3:0.3 mixing is to get base-material.
3. the preparation method of steel polishing agent according to claim 1, which is characterized in that the step（4）In solubilizer：
In mass ratio 2:1:1:4 ~ 6 polyethylene glycol, Emulsifier EL-60, Tween 80, absolute ethyl alcohol mixing are to get solubilizer.
4. the preparation method of steel polishing agent according to claim 1, which is characterized in that the step（4）In surface live
Property agent：In mass ratio 2:1 ~ 2 takes fatty alcohol polyoxyethylene ether, neopelex mixing to get surfactant.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114163931A (en) * | 2021-12-09 | 2022-03-11 | 深圳市拍档科技有限公司 | Aluminum alloy liquid fine polishing wax and preparation method thereof |
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| US20080085412A1 (en) * | 2006-10-04 | 2008-04-10 | Ortiz C Yolanda | Silica-coated metal oxide sols having variable metal oxide to silica ratio |
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| CN103436183A (en) * | 2013-08-31 | 2013-12-11 | 青岛承天伟业机械制造有限公司 | Environment-friendly chemico-mechanical polishing liquid for dielectric layer materials |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114163931A (en) * | 2021-12-09 | 2022-03-11 | 深圳市拍档科技有限公司 | Aluminum alloy liquid fine polishing wax and preparation method thereof |
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Application publication date: 20180928 |