CN106700948A - Antibacterial artificial stone polishing liquid - Google Patents
Antibacterial artificial stone polishing liquid Download PDFInfo
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- CN106700948A CN106700948A CN201611246733.9A CN201611246733A CN106700948A CN 106700948 A CN106700948 A CN 106700948A CN 201611246733 A CN201611246733 A CN 201611246733A CN 106700948 A CN106700948 A CN 106700948A
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- Prior art keywords
- parts
- artificial stone
- agent
- nano
- antimicrobial form
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/06—Other polishing compositions
- C09G1/08—Other polishing compositions based on wax
- C09G1/10—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin
- C09G1/12—Other polishing compositions based on wax based on mixtures of wax and natural or synthetic resin mixtures of wax and silicon-containing polycondensates
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
Abstract
The invention discloses an antibacterial artificial stone polishing liquid, and belongs to the technical field of polishing agents. The antibacterial artificial stone polishing liquid comprises a joint mixture, a light brightening agent, an antibacterial agent, a lubricant, an antifouling agent, a pH regulator, a surfactant and deionized water, and the antibacterial agent is a liquid formed by dispersing one or more of polyethylene glycol coated nano-silver, nanometer silver oxide, nanometer titanium dioxide, nano-zinc and nanometer zinc oxide. The polishing liquid has the advantages of lasting antibacterial effect, high stone glossiness, strong durability, and convenience in use.
Description
Technical field
The invention belongs to polishing fluid production technical field, and in particular to a kind of artificial stone's polishing with anti-microbial property
Liquid.
Background technology
Artificial stone is, with unsaturated polyester (UP) resin as adhesive, to be equipped with natural marble or calcite, dolomite, silicon
The inorganic powders such as sand, glass dust, and appropriate fire retardant, color etc., through dispensing mixing, porcelain casting, vibrocompression, extruding etc.
Method forming and hardening is made.Compared with lithotome, artificial stone has beautiful in colour, highly polished, color uniformity, resists
Press wear-resisting, good toughness, compact structure, sturdy and durable, light specific gravity, do not absorb water, resistant to corrosion weathering, aberration are small, colour-fast, radioactivity
Low advantage, the advantage with comprehensive utilization of resources has immeasurable effect in terms of environmental protection and energy saving, is also qualified
Building materials Green Product, it has also become the first-selected finishing material of modern architecture.Artificial stone when in use between long afterwards, it may appear that
Glossiness is decreased obviously, breed bacteria, generation are gone mouldy problem is, it is necessary to put into manpower and materials to stone material cleaning, sterilized, effect is but
It is undesirable.
At present, the polishing method to artificial stone mainly has physics to polish and two methods of chemical polishing.Physics polishing master
If being polished stone surface using sand paper, then glaze finish paint is coated, it is recovered light；Chemical polishing is mainly is thrown using some
Photo etching is surface-treated to artificial stone, its brightness and durability is all restored.Because the use of polishing agent is more convenient,
At present, the polishing agent on the market for artificial stone is widely loved by consumers.
Research for artificial stone's polishing agent prescription is also a lot.Such as patent of invention " polished bricks, stone material, artificial stone renovation
With polishing agent " (application number：2010101117991.3) disclose a kind of comprising compositions such as fluorine-containing auxiliary agent, nano silicons
Polishing agent, the polishing agent has the advantages that removal brick body surface foul, recovers stone material color and luster, improves durability；Patent of invention " one
Kind nanometer burnishing liquid, antiscuffing paste and preparation method thereof " (application number 201410746951.3) discloses one kind comprising organosilicon, silicon
The preparation method of colloidal sol, the polishing fluid of wax emulsion, has the advantages that to improve stone surface microstructure, reaches mirror effect；Hair
A kind of bright Patent Application Publication " stone polishing agent " (application number：201610275102.3) disclose it is a kind of by abrasive material, sodium oxalate,
Prodan, paraffin etc. can produce crystallizing layer into the polishing agent being grouped into stone surface, lift stone material glossiness.But almost
Polishing fluid function is all relatively simple, while smoothness, the brightness of stone surface is strengthened, without the corresponding function of increase.
The disclosure of background above technology contents is only used for auxiliary and understands inventive concept of the invention and technical scheme, and it is not
Necessarily belong in the prior art of present patent application, the applying date of the above in present patent application is being shown without tangible proof
In the case of disclosed, above-mentioned background technology should not be taken to evaluate the novelty and creativeness of the application.
The content of the invention
In order to overcome the deficiencies in the prior art, the present invention provides a kind of antimicrobial form artificial stone polishing fluid, artificial to realize
Stone polishing liquid is while polishing stone material surface action is played, moreover it is possible to play antibiotic effect.
In order to solve the above technical problems, the present invention uses following technical scheme：
A kind of antimicrobial form artificial stone polishing fluid, in units of weight portion, including following raw material：3~18 parts of gap filler, increasing
6~22 parts of photo etching, 0.2~6 part of lubricant, 4~16 parts of anti-fouling agent, 0.3~3.6 part of pH adjusting agent, surfactant 1~7.5
Part, 0.5~4 part of antiseptic, 40~140 parts of deionized water.
Preferably, the antimicrobial form artificial stone polishing fluid, in units of weight portion, including following raw material：Gap filler 5~
16 parts, 9~18 parts of optical brightener, 0.85~5.5 part of lubricant, 5~14 parts of anti-fouling agent, 0.8~2.6 part of pH adjusting agent, surface live
2.2~6 parts of agent of property, 1~3.5 part of antiseptic, 55~125 parts of deionized water.
Preferably, the antimicrobial form artificial stone polishing fluid, in units of weight portion, including following raw material：Gap filler 8~
12 parts, 12~16 parts of optical brightener, 1.8~4 parts of lubricant, 7~12 parts of anti-fouling agent, 1.4~2 parts of pH adjusting agent, surfactant 3
~4.8 parts, 1.5~3 parts of antiseptic, 80~110 parts of deionized water.
Preferably, the gap filler is mixed by one or more in nano silicon, phosphate, carbonate or silicate
Compound is constituted.
Preferably, the optical brightener is by one or more emulsifications in Brazil wax, beeswax, plate wax or atoleine
Liquid composition.
Preferably, the lubricant is the one kind in ethylene glycol and glycerol mixture, dimethicone or amido silicon oil
Or several mix.
Preferably, the anti-fouling agent is by butyl acrylate, methyl acrylate, acrylic acid, methacrylate, metering system
One or more in sour ten difluoro heptyl esters, full-fluorine octyl sulfuryl fluoride or 20-800 viscosity hydroxy silicone oil are polymerized.
Preferably, the pH adjusting agent by triethanolamine, ammoniacal liquor, sodium hydroxide solution, hydrochloric acid one or more mixing
Form.
Preferably, the antiseptic by coated with polyethylene glycol Nano Silver, nano phase ag_2 o, nano titanium oxide, Nano-Zinc,
The liquid composition of one or more dispersed mixtures in nano zine oxide.
It is highly preferred that the preparation method of the coated with polyethylene glycol nanometer silver type antibacterial agent is：Weigh 100~250g go from
There-necked flask is placed in frequency and is by sub- water, 20~60g polyethylene glycol, 5~30g silver nitrate solutiones in 500mL there-necked flasks
6000~80000Hz, 5~15min of ultrasonic vibration, then under 40~90 DEG C of water-baths, the machine in the case where rotating speed is 200~8000r/min
After tool stirs 3~15min, it is adjusted to stir speed (S.S.) 800~3000r/min and is slowly added dropwise pH adjusting agent adjust to solution ph
It is 7~10, natural cooling after 30~120min of reaction after 10~30min of centrifugation, by the filtering of separated out sediment, is air-dried, as
Coated with polyethylene glycol nanometer silver type antibacterial agent.
The invention has the advantages that：
(1) antimicrobial form artificial stone polishing fluid of the present invention, using coated with polyethylene glycol Nano Silver, nano oxidized
, used as antimicrobial component, its antibiotic property persistently, can effectively suppress stone material table for silver, nano titanium oxide, Nano-Zinc, nano zine oxide
Face bacterium, mould grow；
(2) antimicrobial form artificial stone polishing fluid of the present invention, with antibacterial, it is antifouling, add lustre to, U.S. seam etc. it is comprehensive
Can, used on artificial stone surface, the effect of long-acting anti-soil, antibacterial can be played.
Specific embodiment
The present invention is described in further detail with reference to specific embodiment.It is emphasized that the description below is only
Only it is exemplary, rather than in order to limit the scope of the present invention and its application.
In embodiment, the antimicrobial form artificial stone polishing fluid, in units of weight portion, including following raw material：Joint filling
3~18 parts of agent, 6~22 parts of optical brightener, 0.2~6 part of lubricant, 4~16 parts of anti-fouling agent, 0.3~3.6 part of pH adjusting agent, surface
1~7.5 part of activating agent, 0.5~4 part of antiseptic, 40~140 parts of deionized water.
The gap filler is by one or more the mixture groups in nano silicon, phosphate, carbonate or silicate
Into.
The optical brightener is emulsified by one or more in Brazil wax, beeswax, plate wax or atoleine
Liquid is constituted.
The lubricant is mixed by one or more in ethylene glycol, glycerine, dimethicone or amido silicon oil.
The anti-fouling agent is by butyl acrylate, methyl acrylate, acrylic acid, methacrylate, methacrylic acid 12
One or more in fluorine heptyl ester, full-fluorine octyl sulfuryl fluoride or 20-800 viscosity hydroxy silicone oil are polymerized.
The pH adjusting agent is mixed by one or more of triethanolamine, ammoniacal liquor, sodium hydroxide solution, hydrochloric acid.
The surfactant is sodium n-alkylbenzenesulfonate, sodium sulfate of polyethenoxy ether of fatty alcohol.
The antiseptic is by coated with polyethylene glycol Nano Silver, nano phase ag_2 o, nano titanium oxide, Nano-Zinc, nano oxygen
Change the liquid composition of one or more dispersed mixtures in zinc.
The preparation method of coated with polyethylene glycol nanometer silver type antibacterial agent is：Weigh 100~250g deionized waters, 20~
60g polyethylene glycol, 5~30g silver nitrate solutiones in 500mL there-necked flasks, and by there-necked flask be placed in frequency for 6000~
80000Hz 5~15min of ultrasonic vibration, then under 40~90 DEG C of water-baths, the mechanical agitation in the case where rotating speed is 200~8000r/min
After 3~15min, by stir speed (S.S.) be adjusted to 800~3000r/min and be slowly added dropwise pH adjusting agent adjust to solution ph be 7~
10, natural cooling after 30~120min of reaction after 10~30min of centrifugation, by the filtering of separated out sediment, is air-dried, as poly- second
Glycol coats nanometer silver type antibacterial agent.
Embodiment 1：
A kind of antimicrobial form artificial stone polishing fluid, in units of weight portion, including following raw material：5 parts of gap filler, optical brightener
8 parts, 0.6 part of lubricant, 8 parts of anti-fouling agent, 0.9 part of pH adjusting agent, 2 parts of sodium n-alkylbenzenesulfonate, 1.2 parts of antiseptic, go from
45 parts of sub- water.
The gap filler is 3 parts of nano silicons and 2 parts of phosphate mixts.
The optical brightener is the liquid of Brazil wax emulsification.
The lubricant is 0.3 part of ethylene glycol and 0.3 part of simethicone mixture.
The anti-fouling agent is butyl polyacrylate.
The pH adjusting agent is 0.6 part of triethanolamine and 0.3 part of hydrochloric acid mixture.
The antiseptic is coated with polyethylene glycol Nano silver solution.
The preparation method of coated with polyethylene glycol nanometer silver type antibacterial agent is：Weigh the poly- second two of 100g deionized waters, 20g
There-necked flask is placed in frequency for 6000Hz ultrasonic vibration 15min by alcohol, 5g silver nitrate solutiones in 500mL there-necked flasks, is connect
Under 40 DEG C of water-baths, after mechanical agitation 3min under rotating speed is 8000r/min, stir speed (S.S.) is adjusted to 800r/min simultaneously slow
It is 7.5 pH adjusting agent to be added dropwise and adjusts to solution ph, and natural cooling after reaction 30min after centrifugation 10min, will separate out precipitation
Thing is filtered, air-dried, as coated with polyethylene glycol nanometer silver type antibacterial agent.
Embodiment 2
A kind of antimicrobial form artificial stone polishing fluid, in units of weight portion, including following raw material：18 parts of gap filler, add lustre to
21 parts of agent, 5.5 parts of lubricant, 15 parts of anti-fouling agent, 3 parts of pH adjusting agent, 6.5 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, antiseptic
3.6 parts, 140 parts of deionized water.
The gap filler is 10 parts of nano silicons, 5 parts of carbonate and 3 parts of silicate mixtures.
The optical brightener is that the liquid of 14 parts of Brazil waxs and the emulsification of 7 parts of beeswaxs is mixed.
The lubricant is mixed for 2.5 parts of ethylene glycol, 2 parts of glycerine and 1 part of amido silicon oil.
The anti-fouling agent is 10 parts of PMAs and 5 parts of poly- fluorine octyl group sulfuryl fluorides.
The pH adjusting agent is that 1.8 parts of ammoniacal liquor and 1.2 parts of mixed in hydrochloric acid are formed.
The antiseptic is 2.2 parts of coated with polyethylene glycol Nano Silvers, 1.4 parts of coated with polyethylene glycol nano titanium oxide dispersions
Mixture liquid.
The preparation method of coated with polyethylene glycol nanometer silver type antibacterial agent is：Weigh the poly- second of 250g deionized waters, 260g
There-necked flask is placed in frequency for 80000Hz ultrasonic vibrations by glycol, 30g silver nitrate solutiones in 500mL there-necked flasks
5min, then under 90 DEG C of water-baths, after mechanical agitation 3min under rotating speed is 8000r/min, 3000r/ is adjusted to by stir speed (S.S.)
Min and be slowly added dropwise pH adjusting agent adjust to solution ph be 9.8, reaction 120min after natural cooling, centrifugation 30min after, will
Separated out sediment is filtered, air-dried, as coated with polyethylene glycol nanometer silver type antibacterial agent.
Embodiment 3
A kind of antimicrobial form artificial stone polishing fluid, in units of weight portion, including following raw material：10 parts of gap filler, add lustre to
14 parts of agent, 3 parts of lubricant, 11 parts of anti-fouling agent, 1.8 parts of pH adjusting agent, 3.5 parts of sodium n-alkylbenzenesulfonate, 2.5 parts of antiseptic,
100 parts of deionized water.
The gap filler is 6 parts of nano silicons, 2 parts of phosphate, 2 parts of silicate mixing compositions.
The optical brightener is that the liquid of 8 parts of beeswaxs, 2 parts of plate waxes and 4 parts of atoleine emulsifications is mixed.
The lubricant is that 2 parts of glycerine and 1 part of dimethicone are mixed.
The anti-fouling agent is 6 parts of polyacrylic acid, 3 parts of polymethacrylates, 2 parts of difluoro heptyl esters of polymethylacrylic acid ten.
The pH adjusting agent is formed for 0.6 part of triethanolamine, 0.3 part of sodium hydroxide solution, 0.9 part of mixed in hydrochloric acid.
The antiseptic is 1.5 parts of coated with polyethylene glycol Nano Silvers, 1 part of coated with polyethylene glycol Nano-Zinc dispersion mixing thing liquid
Body.
The preparation method of coated with polyethylene glycol nanometer silver type antibacterial agent is：Weigh the poly- second two of 150g deionized waters, 40g
There-necked flask is placed in frequency for 70000Hz ultrasonic vibration 10min by alcohol, 20g silver nitrate solutiones in 500mL there-necked flasks,
Then under 60 DEG C of water-baths, after mechanical agitation 7min under rotating speed is 3000r/min, stir speed (S.S.) is adjusted to 1500r/min simultaneously
It is 8.6 to be slowly added dropwise pH adjusting agent and adjust to solution ph, and natural cooling after reaction 70min after centrifugation 20min, will be separated out
Sediment is filtered, air-dried, as coated with polyethylene glycol nanometer silver type antibacterial agent.
In order to beneficial effects of the present invention are described in more detail, verified by following contrast experiment：
One piece of area of certain family is chosen for 4m2, rectangular artificial marble kitchen countertop be sample, the mesa surfaces mill
Damage, soiled condition are uniform.The table top is evenly dividing two parts A and B for area equation, midfeather 10cm.A table tops are used
Once, B table tops are polished once using commercially available polishing fluid 20mL, are entered immediately for polishing fluid 20mL polishings described in the embodiment of the present invention 1
Row test, record, randomly select 0.2m on table top2Sampling experimental；After the marble countertop was through routine use 10 days, re-start
Test, record and sampling experimental.
The experimental data of record table top A and B, it is as shown in the table：
As can be seen here, polishing fluid of the invention, can lift and keep artificial stone's surface brightness, kill stone surface
Bacterium and long-acting suppression bacteria breed.
The specific implementation of the invention is not to be limited to these illustrations for above content, is led for technology belonging to the present invention
For the those of ordinary skill in domain, without departing from the inventive concept of the premise, some simple deduction or replace can also be made,
The scope of patent protection that the claims of the present invention by being submitted to determine should be all considered as belonging to.
Claims (10)
1. a kind of antimicrobial form artificial stone polishing fluid, it is characterised in that in units of weight portion, including following raw material：Gap filler 3
~18 parts, 6~22 parts of optical brightener, 0.2~6 part of lubricant, 4~16 parts of anti-fouling agent, 0.3~3.6 part of pH adjusting agent, surface-active
1~7.5 part of agent, 0.5~4 part of antiseptic, 40~140 parts of deionized water.
2. antimicrobial form artificial stone polishing fluid according to claim 1, it is characterised in that in units of weight portion, including
Following raw material：5~16 parts of gap filler, 9~18 parts of optical brightener, 0.85~5.5 part of lubricant, 5~14 parts of anti-fouling agent, pH adjusting agent
0.8~2.6 part, 2.2~6 parts of surfactant, 1~3.5 part of antiseptic, 55~125 parts of deionized water.
3. antimicrobial form artificial stone polishing fluid according to claim 2, it is characterised in that in units of weight portion, including
Following raw material：8~12 parts of gap filler, 12~16 parts of optical brightener, 1.8~4 parts of lubricant, 7~12 parts of anti-fouling agent, pH adjusting agent
1.4~2 parts, 3~4.8 parts of surfactant, 1.5~3 parts of antiseptic, 80~110 parts of deionized water.
4. the antimicrobial form artificial stone's polishing fluid according to any one of claims 1 to 3, it is characterised in that the gap filler
It is made up of one or more mixtures in nano silicon, phosphate, carbonate or silicate.
5. the antimicrobial form artificial stone's polishing fluid according to any one of claims 1 to 3, it is characterised in that the optical brightener
The liquid emulsified by one or more in Brazil wax, beeswax, plate wax or atoleine is constituted.
6. the antimicrobial form artificial stone's polishing fluid according to any one of claims 1 to 3, it is characterised in that the lubricant
Mixed by one or more in ethylene glycol, glycerine, dimethicone or amido silicon oil.
7. the antimicrobial form artificial stone's polishing fluid according to any one of claims 1 to 3, it is characterised in that the anti-fouling agent
By butyl acrylate, methyl acrylate, acrylic acid, methacrylate, dodecafluoroheptyl methacrylate, perfluoro capryl sulphonyl
One or more in fluorine or 20-800 viscosity hydroxy silicone oil are polymerized.
8. the antimicrobial form polishing of artificial stone liquid according to any one of claims 1 to 3, it is characterised in that the pH adjusting agent
Mixed by triethanolamine, ammoniacal liquor, sodium hydroxide solution, hydrochloric acid one or more.
9. the antimicrobial form polishing of artificial stone liquid according to any one of claims 1 to 3, it is characterised in that the antiseptic by
One or more points in coated with polyethylene glycol Nano Silver, nano phase ag_2 o, nano titanium oxide, Nano-Zinc, nano zine oxide
The liquid composition of scattered mixture.
10. antimicrobial form artificial stone polishing fluid according to claim 9, it is characterised in that the coated with polyethylene glycol is received
Rice silver type antibacterial agent preparation method be：Weigh 100~250g deionized waters, 20~60g polyethylene glycol, 5~30g silver nitrates molten
There-necked flask is placed in frequency for 6000~80000Hz, 5~15min of ultrasonic vibration by liquid in 500mL there-necked flasks, then
Under 40~90 DEG C of water-baths, after 3~15min of mechanical agitation under rotating speed is 200~8000r/min, stir speed (S.S.) is adjusted to 800
~3000r/min and be slowly added dropwise pH adjusting agent adjust to solution ph be 7~10, reaction 30~120min after natural cooling,
After 10~30min of centrifugation, by the filtering of separated out sediment, air-dry, as coated with polyethylene glycol nanometer silver type antibacterial agent.
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| CN201611246733.9A CN106700948A (en) | 2016-12-29 | 2016-12-29 | Antibacterial artificial stone polishing liquid |
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| CN201611246733.9A CN106700948A (en) | 2016-12-29 | 2016-12-29 | Antibacterial artificial stone polishing liquid |
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Cited By (10)
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| CN107828341A (en) * | 2017-11-17 | 2018-03-23 | 枣庄市博源人造石有限公司 | A kind of antimicrobial form artificial stone polishing fluid and preparation method thereof |
| CN108003794A (en) * | 2017-12-11 | 2018-05-08 | 合众（佛山）化工有限公司 | A kind of ceramic polished liquid of photocatalyst type |
| CN110016294A (en) * | 2019-04-15 | 2019-07-16 | 广西利升石业有限公司 | A kind of antibacterial polishing fluid and preparation method thereof based on stone polishing |
| CN110157338A (en) * | 2019-07-03 | 2019-08-23 | 郑州石宝宝科技有限公司 | A kind of surface coating formula antiscuffing paste for lithotome |
| CN110587491A (en) * | 2019-09-28 | 2019-12-20 | 深圳市佰石特石业有限公司 | Marble leather surface treatment process |
| CN111099921A (en) * | 2019-12-26 | 2020-05-05 | 广东萨米特陶瓷有限公司 | Ceramic product applied by combining polished surface micropores with nano material and manufacturing method thereof |
| CN111730729A (en) * | 2020-08-03 | 2020-10-02 | 佛山市东鹏陶瓷发展有限公司 | Preparation method of antibacterial and bacteriostatic glazed tile and preparation method of nano antibacterial liquid thereof |
| CN115772449A (en) * | 2022-12-07 | 2023-03-10 | 上海达潮工贸有限公司 | Cleaning agent for renovating treatment of exterior wall stone and preparation method thereof |
| CN115785821A (en) * | 2022-11-17 | 2023-03-14 | 佛山市雅伦高科石业有限公司 | Stone polishing agent and preparation method thereof |
| CN117384549A (en) * | 2023-12-12 | 2024-01-12 | 广东纳德新材料有限公司 | Polishing nano-liquid for softening abrasive wax residues, and preparation method and application thereof |
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| CN107828341A (en) * | 2017-11-17 | 2018-03-23 | 枣庄市博源人造石有限公司 | A kind of antimicrobial form artificial stone polishing fluid and preparation method thereof |
| CN108003794A (en) * | 2017-12-11 | 2018-05-08 | 合众（佛山）化工有限公司 | A kind of ceramic polished liquid of photocatalyst type |
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