CN105400435A - Alkaline nano ceramic polishing solution and preparation method thereof - Google Patents
Alkaline nano ceramic polishing solution and preparation method thereof Download PDFInfo
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- CN105400435A CN105400435A CN201510993006.8A CN201510993006A CN105400435A CN 105400435 A CN105400435 A CN 105400435A CN 201510993006 A CN201510993006 A CN 201510993006A CN 105400435 A CN105400435 A CN 105400435A
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- polished liquid
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- 239000000919 ceramic Substances 0.000 title claims abstract description 89
- 238000005498 polishing Methods 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 74
- 239000000084 colloidal system Substances 0.000 claims abstract description 31
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 31
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 31
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 150000001282 organosilanes Chemical class 0.000 claims abstract description 14
- 239000002904 solvent Substances 0.000 claims abstract description 14
- 239000004094 surface-active agent Substances 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims description 62
- 239000003795 chemical substances by application Substances 0.000 claims description 17
- 239000013543 active substance Substances 0.000 claims description 16
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical group OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 15
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 15
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 238000005260 corrosion Methods 0.000 claims description 14
- 230000007797 corrosion Effects 0.000 claims description 14
- 108010053481 Antifreeze Proteins Proteins 0.000 claims description 13
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 13
- 230000002528 anti-freeze Effects 0.000 claims description 13
- 239000012530 fluid Substances 0.000 claims description 13
- 239000008187 granular material Substances 0.000 claims description 12
- 239000002245 particle Substances 0.000 claims description 12
- 239000012467 final product Substances 0.000 claims description 8
- 150000001412 amines Chemical group 0.000 claims description 7
- 239000000654 additive Substances 0.000 claims description 6
- 230000000996 additive effect Effects 0.000 claims description 6
- CPUDPFPXCZDNGI-UHFFFAOYSA-N triethoxy(methyl)silane Chemical compound CCO[Si](C)(OCC)OCC CPUDPFPXCZDNGI-UHFFFAOYSA-N 0.000 claims description 6
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 claims description 4
- RNMDNPCBIKJCQP-UHFFFAOYSA-N 5-nonyl-7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-ol Chemical compound C(CCCCCCCC)C1=C2C(=C(C=C1)O)O2 RNMDNPCBIKJCQP-UHFFFAOYSA-N 0.000 claims description 4
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 4
- TVJPBVNWVPUZBM-UHFFFAOYSA-N [diacetyloxy(methyl)silyl] acetate Chemical compound CC(=O)O[Si](C)(OC(C)=O)OC(C)=O TVJPBVNWVPUZBM-UHFFFAOYSA-N 0.000 claims description 4
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 4
- SBZXBUIDTXKZTM-UHFFFAOYSA-N diglyme Chemical compound COCCOCCOC SBZXBUIDTXKZTM-UHFFFAOYSA-N 0.000 claims description 4
- BFXIKLCIZHOAAZ-UHFFFAOYSA-N methyltrimethoxysilane Chemical compound CO[Si](C)(OC)OC BFXIKLCIZHOAAZ-UHFFFAOYSA-N 0.000 claims description 4
- -1 polyoxyethylene nonylphenol Polymers 0.000 claims description 4
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 4
- XYRAEZLPSATLHH-UHFFFAOYSA-N trisodium methoxy(trioxido)silane Chemical group [Na+].[Na+].[Na+].CO[Si]([O-])([O-])[O-] XYRAEZLPSATLHH-UHFFFAOYSA-N 0.000 claims description 4
- 229960004418 trolamine Drugs 0.000 claims description 4
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 claims description 3
- RNIHAPSVIGPAFF-UHFFFAOYSA-N Acrylamide-acrylic acid resin Chemical compound NC(=O)C=C.OC(=O)C=C RNIHAPSVIGPAFF-UHFFFAOYSA-N 0.000 claims description 3
- 229920006322 acrylamide copolymer Polymers 0.000 claims description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical group OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 3
- 239000003755 preservative agent Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 13
- 238000009776 industrial production Methods 0.000 abstract description 2
- 125000003277 amino group Chemical group 0.000 abstract 1
- 239000007822 coupling agent Substances 0.000 abstract 1
- 230000003373 anti-fouling effect Effects 0.000 description 4
- 239000011449 brick Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000002131 composite material Substances 0.000 description 2
- 239000004567 concrete Substances 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 1
- 230000009545 invasion Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 238000007517 polishing process Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000006748 scratching Methods 0.000 description 1
- 230000002393 scratching effect Effects 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
- Mechanical Treatment Of Semiconductor (AREA)
Abstract
The invention relates to an alkaline nano-ceramic polishing solution, which comprises silicon dioxide colloid and water, and further comprises at least one of the following components: an antifreezing solvent, an organosilane coupling agent and a surfactant; the surfactant is an amine surfactant and/or an ether surfactant. The alkaline nano-ceramic polishing solution can avoid the conditions of scratch and cloud point generated in the process of carrying out ultra-clean treatment on the ceramic by using the nano-ceramic polishing solution, and the preparation method is simple, easy to operate and convenient for industrial production.
Description
Technical field
The present invention relates to polishing fluid, be specifically related to ceramic polished liquid of a kind of alkaline nano and preparation method thereof.
Background technology
Super clean bright technology adopts a kind of special high precision polishing machine by the surface of nano-liquid droplet to polished tile, by repeatedly the exerting pressure of grinding head for polishing, polish, polishing, pore nano fluid better being penetrated into polished tile is inner, plug pore and the tiny crack of polished tile, form a kind of special, continuous print nanometer film, thus make polished tile have beautiful surface.And this surface energy effectively stops the invasion of pollutent, there is good antifouling property.Super clean bright technology is the most effectual way of current polished tile protective treatment, needs to use the super clean brilliant polish machine of high precision and nano material polishing fluid.At present, the super clean bright nanometer burnishing liquid of use is mainly alkalescence.Wherein, easily there is surperficial cloud point and the slight problem scratched in the polishing fluid of alkalescence in polishing process.
Summary of the invention
The object of the present invention is to provide a kind of ceramic polished liquid of alkaline nano that can solve traditional polishing fluid easily generation cloud point and scuffing in super clean bright treatment process, the present invention also provides the preparation method of the ceramic polished liquid of this alkaline nano.
For solving the problem, the technical solution adopted in the present invention is as follows:
The ceramic polished liquid of a kind of alkaline nano, comprise silicon dioxide colloid and water, described nano ceramics polishing fluid also comprises at least one in following component: anti-freeze type solvent, organo silane coupling agent and tensio-active agent; Described tensio-active agent is amine surfactants and/or ether surfactant.
In the present invention, preferred scheme is that the ceramic polished liquid of described alkaline nano also comprises additive, and described additive is alkaline corrosion agent, stain control agent and at least one of the preservatives.
In the present invention, preferred scheme is that the described ceramic polished liquid of alkaline nano is made up of the following component according to percent by weight: silicon dioxide colloid 30-80%, anti-freeze type solvent 0.1-2%, organo silane coupling agent 0.1-1.5%, tensio-active agent 0.1-2%, alkaline corrosion agent 0.6-0.9%, surplus is water.
In the present invention, preferred scheme is that the described ceramic polished liquid of alkaline nano is made by by the following component according to percent by weight: silicon dioxide colloid 40-60%, anti-freeze type solvent 0.3-1%, organo silane coupling agent 0.5-1%, tensio-active agent 0.3-1%, alkaline corrosion agent 0.6-0.9%, surplus is water.
In the present invention, preferred scheme is that described anti-freeze type solvent is selected from ethylene glycol, propylene glycol and glycerol; Described organo silane coupling agent is selected from sodium methyl silicate, methyltrimethoxy silane, Union carbide A-162 and methyl triacetoxysilane; Described tensio-active agent is selected from glycol ether, butyl glycol ether, diethylene glycol dimethyl ether, isomerous tridecanol polyoxyethylene ether, polyoxyethylene nonylphenol ether, diethanolamine, trolamine, acrylic acid-acrylamide copolymer and Soxylat A 25-7; Described silicon dioxide colloid is alkaline silica sol.
In the present invention, preferred scheme is the particle diameter of silica dioxide granule in described silicon dioxide colloid is 5-80nm.
In the present invention, preferred scheme is the particle diameter of silica dioxide granule in described silicon dioxide colloid is 10-50nm.
In the present invention, preferred scheme is the pH value of described ceramic polished liquid is 8-11.
In the present invention, preferred scheme is the pH value of described ceramic polished liquid is 9-10.
The present invention also provides the preparation method of the ceramic polished liquid of this alkaline nano, comprises the steps: each component of getting formula ratio, mixes, to obtain final product.
Compared with prior art, tool of the present invention has the following advantages: nano ceramics polishing fluid of the present invention, composite by each component, make the nano ceramics polishing fluid good properties obtained, at this nano ceramics polishing fluid of later use in the super clean bright treating processes of ceramic brick surface, the problem of cloud point and scuffing can be avoided, and there is very long storage time and work-ing life; In addition, preparation technology of the present invention is simple, easy to operate, is convenient to industrial production application.
Below in conjunction with embodiment, the present invention is described in detail.
Embodiment
The ceramic polished liquid of a kind of alkaline nano, comprise silicon dioxide colloid and water, described nano ceramics polishing fluid also comprises at least one in following component: anti-freeze type solvent, organo silane coupling agent and tensio-active agent; Described tensio-active agent is amine surfactants and/or ether surfactant.Wherein, amine surfactants can be amine substance monomer, also can be the multipolymer of amine substance, the molecular weight of the multipolymer of amine substance is preferably 100-8000; Ether surfactant can be ether material monomer, also can be the multipolymer of ether material, the molecular weight of the multipolymer of ether material is preferably 100-8000.
In the present invention, preferred scheme is that the ceramic polished liquid of described alkaline nano also comprises additive, and described additive is alkaline corrosion agent, stain control agent and at least one of the preservatives.
In the present invention, preferred scheme is that the described ceramic polished liquid of alkaline nano is made up of the following component according to percent by weight: silicon dioxide colloid 30-80%, anti-freeze type solvent 0.1-2%, organo silane coupling agent 0.1-1.5%, tensio-active agent 0.1-2%, alkaline corrosion agent 0.6-0.9%, surplus is water.
In the present invention, preferred scheme is that the described ceramic polished liquid of alkaline nano is made by by the following component according to percent by weight: silicon dioxide colloid 40-60%, anti-freeze type solvent 0.3-1%, organo silane coupling agent 0.5-1%, tensio-active agent 0.3-1%, alkaline corrosion agent 0.6-0.9%, surplus is water.
In the present invention, preferred scheme is that described anti-freeze type solvent is selected from ethylene glycol, propylene glycol and glycerol; Described organo silane coupling agent is selected from sodium methyl silicate, methyltrimethoxy silane, Union carbide A-162 and methyl triacetoxysilane; Described tensio-active agent is selected from glycol ether, butyl glycol ether, diethylene glycol dimethyl ether, isomerous tridecanol polyoxyethylene ether, polyoxyethylene nonylphenol ether, diethanolamine, trolamine, acrylic acid-acrylamide copolymer and Soxylat A 25-7; Described silicon dioxide colloid is alkaline silica sol.
In the present invention, preferred scheme is the particle diameter of silica dioxide granule in described silicon dioxide colloid is 5-80nm; Further preferably, the particle diameter of the silica dioxide granule in described silicon dioxide colloid is 10-50nm.
In the present invention, preferred scheme is the pH value of described ceramic polished liquid is 8-11; The pH value of further preferably described ceramic polished liquid is 9-10.
In embodiments of the invention 1-10, silicon dioxide colloid is alkaline silica sol (particle diameter of the silica dioxide granule in silicon dioxide colloid is 20-30nm), tensio-active agent is polyoxyethylene nonylphenol ether, anti-freeze type solvent is ethylene glycol, organo silane coupling agent is Union carbide A-162; The preparation method of the ceramic polished liquid of alkaline nano of each embodiment, comprises the steps: each component of getting formula ratio, mixes, to obtain final product.
Embodiment 1-10
Each component is got according to the formula in following table 1, mix, the ceramic polished liquid of alkaline nano of obtained embodiment 1-10 respectively, then the ceramic tile of same batch that certain company on the market produces is got, the ceramic polished liquid of embodiment 1-10 is adopted to carry out super clean bright process to above-mentioned ceramic tile respectively, above-mentioned 10 groups adopt identical super clean bright treatment process, then the ceramic brick surface after these 10 groups of process is observed, observe the photometric quantity that whether there is antifouling property (by observing whether there is cloud point), cut and detect ceramic tile surface, concrete outcome refers to following table 1:
The embodiment 1 ~ 10 that table 1 is the super clean bright nano ceramics polishing fluid of alkalescence of preparation and composite effect
As can be seen from upper table 1, this ceramic polished liquid be applied in ceramic polished in, gained pottery minute surface and anti-fouling effect better.
After above-mentioned ceramic polished liquid is stored 14 months, be applied in ceramic polished in, gained pottery minute surface and anti-fouling effect better, this ceramic polished liquid is long for storage time as seen.
Embodiment 11
The ceramic polished liquid of a kind of alkaline nano, the ceramic polished liquid of described alkaline nano is made up of the following component according to percent by weight: silicon dioxide colloid (particle diameter of the silica dioxide granule in silicon dioxide colloid is 20-30nm) 60%, propylene glycol 0.1%, sodium methyl silicate 0.1%, trolamine 0.1%, alkaline corrosion agent 0.7%, surplus is water.The preparation method of the ceramic polished liquid of this alkaline nano comprises the steps: each component of getting formula ratio, mixes, to obtain final product.
Embodiment 12
The ceramic polished liquid of a kind of alkaline nano, the ceramic polished liquid of described alkaline nano is made up of the following component according to percent by weight: silicon dioxide colloid (particle diameter of the silica dioxide granule in silicon dioxide colloid is 20-30nm) 48%, glycerol 2%, methyltrimethoxy silane 1.5%, diethanolamine 2%, alkaline corrosion agent 0.7%, surplus is water.The preparation method of the ceramic polished liquid of this alkaline nano comprises the steps: each component of getting formula ratio, mixes, to obtain final product.
Embodiment 13
The ceramic polished liquid of a kind of alkaline nano, the ceramic polished liquid of described alkaline nano is made up of the following component according to percent by weight: silicon dioxide colloid (particle diameter of the silica dioxide granule in silicon dioxide colloid is 20-30nm) 40%, ethylene glycol 0.3%, Union carbide A-162 0.5%, Soxylat A 25-7 (molecular weight 500-6000) 0.3%, alkaline corrosion agent 0.6%, surplus is water.The preparation method of the ceramic polished liquid of this alkaline nano comprises the steps: each component of getting formula ratio, mixes, to obtain final product.
Embodiment 14
The ceramic polished liquid of a kind of alkaline nano, the ceramic polished liquid of described alkaline nano is made up of the following component according to percent by weight: silicon dioxide colloid (particle diameter of the silica dioxide granule in silicon dioxide colloid is 20-30nm) 60%, propylene glycol 1%, methyl triacetoxysilane 1%, butyl glycol ether 1%, alkaline corrosion agent 0.9%, surplus is water.The preparation method of the ceramic polished liquid of this alkaline nano comprises the steps: each component of getting formula ratio, mixes, to obtain final product.
Embodiment 15
The ceramic polished liquid of a kind of alkaline nano, the ceramic polished liquid of described alkaline nano is made up of the following component according to percent by weight: silicon dioxide colloid (particle diameter of the silica dioxide granule in silicon dioxide colloid is 20-30nm) 55%, glycerol 0.6%, Union carbide A-162 0.8%, diethylene glycol dimethyl ether 0.7%, alkaline corrosion agent 0.9%, surplus is water.The preparation method of the ceramic polished liquid of this alkaline nano comprises the steps: each component of getting formula ratio, mixes, to obtain final product.
Experimental example
Get the ceramic polished liquid of alkaline nano of the present embodiment 11-15, and the nano ceramics polishing fluid of three company's productions on the market, be respectively A, B, C tri-groups; Then the ceramic tile of same batch that certain company on the market produces is got, then the ceramic polished liquid of alkaline nano of embodiment 11-15 and the ceramic polished liquid of A, B, C tri-groups is adopted to carry out super clean bright process to above-mentioned ceramic tile respectively, above-mentioned 8 groups adopt identical super clean bright treatment process, then the ceramic brick surface after these 8 groups of process is observed, observe and whether there is cloud point and scuffing, concrete outcome refers to following table 2:
Table 2: ceramic brick surface cloud point and the situation of scuffing recorder
As can be seen from data in upper table, the ceramic polished liquid of alkaline nano of the present invention, can avoid utilizing the situation occurring cloud point and scuffing when the ceramic polished liquid of this alkaline nano is follow-up carries out super clean bright treatment process to ceramic tile surface.
At room temperature preserve the ceramic polished liquid of alkaline nano of embodiment 11-15, preserve 1.5 years, when 3rd month, the 6th month, the 9th month, the 12nd month, the 14th month and 15th month, the ceramic polished liquid of alkaline nano getting these 5 embodiments respectively carried out super clean bright process to above-mentioned ceramic tile.Found that, 14th month time, after adopting the ceramic polished liquid of the various embodiments described above alkaline nano to carry out super clean bright process to above-mentioned ceramic tile, ceramic surface is without cloud point, without scratching; 15th month time, utilizing the ceramic tile surface of the alkaline nano ceramic polished liquid process of embodiment 14,15 to have slight scuffing, a small amount of cloud point, all there is not this situation in all the other embodiments.
Above-mentioned embodiment is only the preferred embodiment of the present invention; can not limit the scope of protection of the invention with this, change and the replacement of any unsubstantiality that those skilled in the art does on basis of the present invention all belong to the present invention's scope required for protection.
Claims (10)
1. the ceramic polished liquid of alkaline nano, comprises silicon dioxide colloid and water, it is characterized in that described nano ceramics polishing fluid also comprises at least one in following component: anti-freeze type solvent, organo silane coupling agent and tensio-active agent; Described tensio-active agent is amine surfactants and/or ether surfactant.
2. the ceramic polished liquid of alkaline nano according to claim 1, is characterized in that: the ceramic polished liquid of described alkaline nano also comprises additive, and described additive is alkaline corrosion agent, stain control agent and at least one of the preservatives.
3. the ceramic polished liquid of alkaline nano according to claim 2, it is characterized in that being made up of the following component according to percent by weight: silicon dioxide colloid 30-80%, anti-freeze type solvent 0.1-2%, organo silane coupling agent 0.1-1.5%, tensio-active agent 0.1-2%, alkaline corrosion agent 0.6-0.9%, surplus is water.
4. the ceramic polished liquid of alkaline nano according to claim 3, it is characterized in that being made up of the following component according to percent by weight: silicon dioxide colloid 40-60%, anti-freeze type solvent 0.3-1%, organo silane coupling agent 0.5-1%, tensio-active agent 0.3-1%, alkaline corrosion agent 0.6-0.9%, surplus is water.
5. the ceramic polished liquid of alkaline nano according to claim 3, is characterized in that: described anti-freeze type solvent is selected from ethylene glycol, propylene glycol and glycerol; Described organo silane coupling agent is selected from sodium methyl silicate, methyltrimethoxy silane, Union carbide A-162 and methyl triacetoxysilane; Described tensio-active agent is selected from glycol ether, butyl glycol ether, diethylene glycol dimethyl ether, isomerous tridecanol polyoxyethylene ether, polyoxyethylene nonylphenol ether, diethanolamine, trolamine, acrylic acid-acrylamide copolymer and Soxylat A 25-7; Described silicon dioxide colloid is alkaline silica sol.
6. the ceramic polished liquid of alkaline nano according to claim 5, is characterized in that: the particle diameter of the silica dioxide granule in described silicon dioxide colloid is 5-80nm.
7. the ceramic polished liquid of alkaline nano according to claim 6, is characterized in that: the particle diameter of the silica dioxide granule in described silicon dioxide colloid is 10-50nm.
8. the ceramic polished liquid of alkaline nano according to claim 3, is characterized in that: the pH value of described ceramic polished liquid is 8-11.
9. the ceramic polished liquid of alkaline nano according to claim 8, is characterized in that: the pH value of described ceramic polished liquid is 9-10.
10. the preparation method of the ceramic polished liquid of the alkaline nano according to any one of claim 1-9, is characterized in that each component comprising the steps: to get formula ratio, mixes, to obtain final product.
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| CN108531087A (en) * | 2018-06-13 | 2018-09-14 | 李秋菊 | A kind of antifreeze polishing liquid and preparation method thereof |
| CN109111857A (en) * | 2018-09-06 | 2019-01-01 | 北京保利世达科技有限公司 | A kind of polishing fluid and its purposes for polishing 2.5D zirconia ceramics plate |
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