CN108553353A - A kind of preparation method of river radix paeoniae rubra hydrosol - Google Patents
A kind of preparation method of river radix paeoniae rubra hydrosol Download PDFInfo
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- CN108553353A CN108553353A CN201810413610.2A CN201810413610A CN108553353A CN 108553353 A CN108553353 A CN 108553353A CN 201810413610 A CN201810413610 A CN 201810413610A CN 108553353 A CN108553353 A CN 108553353A
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- radix paeoniae
- paeoniae rubra
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- river radix
- hydrosol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Health & Medical Sciences (AREA)
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- Dermatology (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of river radix paeoniae rubra hydrosol, preparation method includes the following steps：(1) it pre-processes：Fresh material (river radix paeoniae rubra leaf, aloe) is cleaned up with deionized water, removing wherein goes mouldy, damages by worms, sick scar part, and removal of inclusions obtains pretreated material；(2) it crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；(3) it impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly；(4) it distills：Distillation still is sealed, is vacuumized；Then it is heated to deionized water boiling；Open ultrasonication；The condenser of distillation still, and the cooling water that circulates within the condenser are opened, starts to collect distillate；(5) it filters：The distillate of collection is stood at low temperature, then uses filter-cloth filtering, filtrate is obtained, appropriate preservative is added, you can.Obtained river radix paeoniae rubra hydrosol contains water-soluble active ingredient, stable quality.
Description
Technical field
The present invention relates to cosmetic fields, are specifically related to a kind of preparation method of river radix paeoniae rubra hydrosol.
Background technology
Insomnia is due to feelings will, diet internal injury, or after being ill and old, insufficiency of natural endowment, and the causes of disease such as have a guilty consicence cause the mind
Mistake is foster or confused and worried, so as to cause cannot often obtain a kind of illness that ortho is characterized；" agitation ", " depression " are usually
By modern metropolitan cities, people hangs over the corners of the mouth.Impetuous society, the mood of let us is also irritated to get up, operating pressure, emotion puzzlement, raw
Pressure living is ubiquitous.Many friends often can unexpectedly feel irritated in work and study life, little by little slight
Stimulation, will let us mood no longer stablize, always want to the unhealthy emotion for leading oneself off, it has been found that oneself can not lead off.
River radix paeoniae rubra is the dry root of ranunculaceae plant Chinese herbaceous peony or river radix paeoniae rubra, bitter in taste, is slightly cold, return liver warp.Main function is
Clearing heat and cooling blood, removing blood stasis and analgesics.For febrile virulent maculae, hematemesis and epistaxis, red eye, swell pain, liver-depressed hypochondrium pain, closed dysmenorrhea, abdominal mass abdominal pain,
Injury from falling down, carbuncle swells sore.In terms of nti-freckle, radix paeoniae rubra can play toxin expelling, weaken color spot, while improving endocrine effect.With
Have shown that river radix paeoniae rubra also toward research and have to inhibit blood platelet and erythrocyte aggregation, antithrombotic, antiatherosclerosis, cardioprotection and
The multiple pharmacological effects such as liver, antitumor.And the research of tranquilizing and allaying excitement is had not been reported.
Invention content
The technical problem to be solved in the present invention is to provide a kind of preparation methods of river radix paeoniae rubra hydrosol.
The technical solution to solve the above problems is as follows：
A kind of river radix paeoniae rubra hydrosol, preparation method include the following steps：
(1) it pre-processes：Fresh material (river radix paeoniae rubra leaf, aloe) is cleaned up with deionized water, removing wherein go mouldy,
It damages by worms, sick scar part, removal of inclusions obtains pretreated material；
(2) it crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
(3) it impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly；
(4) it distills：Distillation still is sealed, is vacuumized；Then it is heated to deionized water boiling；It opens at ultrasonic wave
Reason；The condenser of distillation still, and the cooling water that circulates within the condenser are opened, starts to collect distillate；
(5) it filters：The distillate of collection is stood at low temperature, then uses filter-cloth filtering, obtains filtrate, is added appropriate anti-
Rotten agent, you can.
In wherein some embodiments, the weight ratio of river radix paeoniae rubra leaf, aloe described in step (1) is (0.1-10)：
(0.1-10)。
In wherein some embodiments, the material described in step (1) further includes CORTEX PHELLODENDRI CHINENSE, tingia water lily；Preferably, institute
The river radix paeoniae rubra leaf stated, tingia water lily, CORTEX PHELLODENDRI CHINENSE, aloe weight ratio be (0.1-10)：(0.1-10)：(0.1-10)：(0.1-
10)。
In wherein some embodiments, the solid-liquid ratio that the deionization described in step (3) impregnates is (1：5)-(1：10) it, soaks
It is 1-2 hours to steep the time；
In wherein some embodiments, the pressure in kettle that is evacuated to described in step (4) is 0.05-0.1MPa；
In wherein some embodiments, the frequency of the ultrasonic wave described in step (4) is 30-60kHz, duration 5-
10 minutes；
In wherein some embodiments, the temperature of the standing described in step (5) is 1-5 DEG C, and the time is 12-24 hours；
The filter cloth mesh number is 1000-2000 mesh.
In wherein some embodiments, the preservative described in step (5) is hexylene glycol, and the additive amount of hexylene glycol is that river is red
The 3% of Chinese herbaceous peony hydrosol weight.
Second aspect of the present invention provides river radix paeoniae rubra hydrosol made from a kind of preparation method by mentioned earlier.
The advantageous effect that technical solution provided in an embodiment of the present invention is brought is：The preparation method of the present invention, before it is distilled
It is handled using ultrasonic wave, has been greatly facilitated extraction efficiency, increase the dissolution rate of river radix paeoniae rubra and active aloe ingredient.Ultrasonic wave
The cavitation effect brought is handled, river radix paeoniae rubra leaf and aloe cell can be made because instantaneously generating being broken due to running quickly and burst for cavitation bubble in aqueous solution
It splits, aqueous solution is made to penetrate into cell interior, improve the recovery rate of active material.In addition, the present invention also carries out low temperature to distillate
It stands and freezing and filtering, the macromolecular substances in distillate is made under low temperature to accelerate Precipitation, finally by filter cloth by precipitation
Microscopic precipitate filters out.The river radix paeoniae rubra hydrosol crossed through this process does not have the phenomenon that visible foreign is precipitated within the shelf-life.Cause
A variety of macromolecular substances such as the distillate of collection its complicated component, including vegetable protein, tannin, plant polyose.If not to receiving
The river radix paeoniae rubra hydrosol of collection is handled, and after placing a period of time, macromolecular substances gradually will be precipitated to form precipitation, seriously affect and disappear
The person of expense uses.In traditional hydrosol preparation process, often without filter operation, or room temperature filtering only is carried out to distillate, this
Hydrosol made from sample, often appearing in just has the phenomenon that visible foreign precipitation in the shelf-life.Its processing procedure of preparation method of the present invention
It merged immersion, ultrasound, distillation, stood a variety of processing means such as filtering, Cord blood and filter at low temperature, while having used specific ginseng
Several treatment conditions prepare river radix paeoniae rubra hydrosol, and obtained river radix paeoniae rubra hydrosol contains water-soluble active ingredient, stable quality, no
Sediment, appearance transparent clarification is easily precipitated, while also having effects that replenishing water and preserving moisture, tranquilizing and allaying excitement.
Specific implementation mode
To make the object, technical solutions and advantages of the present invention clearer, embodiment of the present invention will be made into one below
Step ground detailed description, embodiments of the present invention are not limited thereto, for not specifically specified technological parameter or condition, can refer to
Routine techniques carries out.
Embodiment 1
A kind of river radix paeoniae rubra hydrosol, preparation method include the following steps：
(1) it pre-processes：Fresh material (river radix paeoniae rubra leaf, aloe) is cleaned up with deionized water, removing wherein go mouldy,
It damages by worms, sick scar part, removal of inclusions obtains pretreated material, wherein the weight ratio of the river radix paeoniae rubra leaf, aloe is
0.1：10；
(2) it crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
(3) it impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly, wherein
Solid-liquid ratio is 1：10, soaking time is 1 hour；
(4) it distills：Distillation still is sealed, 0.1MPa is evacuated to；Then it is heated to deionized water boiling；It opens
30kHz ultrasonications 10 minutes；The condenser of distillation still, and the cooling water that circulates within the condenser are opened, starts to collect distillation
Liquid；
(5) it filters：The distillate of collection is stood 24 hours under 1 DEG C of low temperature, then with 1000 mesh filter-cloth filterings, is obtained
Filtrate, is added hexylene glycol, and the additive amount of hexylene glycol is the 3% of river radix paeoniae rubra hydrosol weight.
Embodiment 2
A kind of river radix paeoniae rubra hydrosol, preparation method include the following steps：
(1) it pre-processes：Fresh material (river radix paeoniae rubra leaf, aloe) is cleaned up with deionized water, removing wherein go mouldy,
It damages by worms, sick scar part, removal of inclusions obtains pretreated material, wherein the weight ratio of the river radix paeoniae rubra leaf, aloe is
10：0.1；
(2) it crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
(3) it impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly, wherein
Solid-liquid ratio is 1：5, soaking time is 2 hours；
(4) it distills：Distillation still is sealed, 0.05MPa is evacuated to；Then it is heated to deionized water boiling；It opens
60kHz ultrasonications 5 minutes；The condenser of distillation still, and the cooling water that circulates within the condenser are opened, starts to collect distillation
Liquid；
(5) it filters：The distillate of collection is stood 12 hours under 5 DEG C of low temperature, then with 2000 mesh filter-cloth filterings, is obtained
Filtrate, is added hexylene glycol, and the additive amount of hexylene glycol is the 3% of river radix paeoniae rubra hydrosol weight.
Embodiment 3
A kind of river radix paeoniae rubra hydrosol, preparation method include the following steps：
(1) it pre-processes：Fresh material (river radix paeoniae rubra leaf, aloe, CORTEX PHELLODENDRI CHINENSE, tingia water lily) is cleaned with deionized water and is done
Only, remove wherein go mouldy, damage by worms, sick scar part, removal of inclusions obtains pretreated material, wherein the river radix paeoniae rubra leaf, reed
Luxuriant growth, CORTEX PHELLODENDRI CHINENSE, tingia water lily weight ratio be 1：1：10:0.1；
(2) it crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
(3) it impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly, wherein
Solid-liquid ratio is 1:4, soaking time is 1.5 hours；
(4) it distills：Distillation still is sealed, 0.06MPa is evacuated to；Then it is heated to deionized water boiling；It opens
40kHz ultrasonications 7 minutes；The condenser of distillation still, and the cooling water that circulates within the condenser are opened, starts to collect distillation
Liquid；
(5) it filters：The distillate of collection is stood 18 hours under 3 DEG C of low temperature, then with 1500 mesh filter-cloth filterings, is obtained
Filtrate, is added hexylene glycol, and the additive amount of hexylene glycol is the 3% of river radix paeoniae rubra hydrosol weight.
Embodiment 4
A kind of river radix paeoniae rubra hydrosol, preparation method include the following steps：
(1) it pre-processes：Fresh material (river radix paeoniae rubra leaf, aloe, CORTEX PHELLODENDRI CHINENSE, tingia water lily) is cleaned with deionized water and is done
Only, remove wherein go mouldy, damage by worms, sick scar part, removal of inclusions obtains pretreated material, wherein the river radix paeoniae rubra leaf, reed
Luxuriant growth, CORTEX PHELLODENDRI CHINENSE, tingia water lily weight ratio be 1：1：0.1:10；
(2) it crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
(3) it impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly, wherein
Solid-liquid ratio is 1:4, soaking time is 1.5 hours；
(4) it distills：Distillation still is sealed, 0.06MPa is evacuated to；Then it is heated to deionized water boiling；It opens
40kHz ultrasonications 7 minutes；The condenser of distillation still, and the cooling water that circulates within the condenser are opened, starts to collect distillation
Liquid；
(5) it filters：The distillate of collection is stood 18 hours under 3 DEG C of low temperature, then with 1500 mesh filter-cloth filterings, is obtained
Filtrate, is added hexylene glycol, and the additive amount of hexylene glycol is the 3% of river radix paeoniae rubra hydrosol weight.
Embodiment 5
Effect detection is carried out to radix paeoniae rubra hydrosol in river of the present invention, is real with the anti-acne essence prepared by embodiment 1-4
Test a group 1-4；In addition setting control group 1-4；
Wherein control group 1 the difference from example 2 is that, be not added with river radix paeoniae rubra leaf；
Wherein control group 2 the difference from example 2 is that, be not added with aloe；
Wherein difference lies in be not added with CORTEX PHELLODENDRI CHINENSE to control group 3 with embodiment 4；
Wherein difference lies in be not added with tingia water lily to control group 4 with embodiment 4；
Experiment 1
Efficacy assessments are carried out to the river radix paeoniae rubra hydrosol of implementation group 1-4 and contrast groups 1-4.The specific test method is as follows：Each reality
It is 20 volunteers to test group, 25-55 Sui, all there are palpitaition, insomnia, palpitation, forgetful and confusing frightened symptoms such as mad；It uses：Often
It each 1 time sooner or later, it is applied to face, is used continuously 14 days；Evaluation criterion：It is effective, effectively, in vain, wherein palpitaition, insomnia, seized with terror
Sad, the forgetful and confusing frightened symptoms such as mad substantially eliminate be judged as it is effective；It partially removes and is judged as effectively；It is other, it is judged as nothing
Effect.Specific test result is shown in Table 1.
1 test recording table of table
As known from Table 1, the effect of comparison implementation group 1-2 and control group 1-2 can obtain：River radix paeoniae rubra leaf, aloe are by specific
Extraction process made from river radix paeoniae rubra hydrosol, can be from the whole synergy that play tranquilizing and allaying excitement；Compare implementation group 3-4 and reality
Apply a group 1-2, the effect of contrast groups 3-4 can obtain：By adding CORTEX PHELLODENDRI CHINENSE on the basis of river radix paeoniae rubra leaf, aloe, tingia sleeps
Lotus can effectively improve the effect of river radix paeoniae rubra hydrosol.
The above described is only a preferred embodiment of the present invention, limitation in any form not is done to the present invention, therefore
All contents without departing from technical solution of the present invention, it is made to the above embodiment according to the technical essence of the invention any simply to repair
Change, equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (8)
1. a kind of preparation method of river radix paeoniae rubra hydrosol, which is characterized in that include the following steps：
(1) it pre-processes：Fresh material (river radix paeoniae rubra leaf, aloe) is cleaned up with deionized water, removing wherein go mouldy, worm
Moth, sick scar part, removal of inclusions obtain pretreated material；
(2) it crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
(3) it impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly；
(4) it distills：Distillation still is sealed, is vacuumized；Then it is heated to deionized water boiling；Open ultrasonication；It beats
The condenser of distillation still is opened, and the cooling water that circulates within the condenser, starts to collect distillate；
(5) it filters：The distillate of collection is stood at low temperature, then uses filter-cloth filtering, filtrate is obtained, appropriate anti-corrosion is added
Agent, you can.
2. preparation method according to claim 1, which is characterized in that the weight of river radix paeoniae rubra leaf, aloe described in step (1)
The ratio between amount is (0.1-10)：(0.1-10).
3. preparation method according to claim 1, which is characterized in that the material described in step (1) further include CORTEX PHELLODENDRI CHINENSE,
Tingia water lily；Preferably, the river radix paeoniae rubra leaf, tingia water lily, CORTEX PHELLODENDRI CHINENSE, aloe weight ratio be (0.1-10)：(0.1-
10)：(0.1-10)：(0.1-10).
4. preparation method according to claim 1, which is characterized in that the feed liquid that the deionization described in step (3) impregnates
Than being (1：5)-(1：10), soaking time is 1-2 hours.
5. preparation method according to claim 1, which is characterized in that be evacuated to pressure in kettle described in step (4)
For 0.05-0.1MPa.
6. preparation method according to claim 1, which is characterized in that the frequency of the ultrasonic wave described in step (4) is 30-
60kHz, duration are 5-10 minutes.
7. preparation method according to claim 1, which is characterized in that the temperature of the standing described in step (5) is 1-5
DEG C, the time is 12-24 hours；The filter cloth mesh number is 1000-2000 mesh.
8. preparation method according to claim 1, which is characterized in that the preservative described in step (5) is hexylene glycol, institute
The additive amount for stating hexylene glycol is the 3% of river radix paeoniae rubra hydrosol weight.
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| CN201810413610.2A CN108553353A (en) | 2018-04-29 | 2018-04-29 | A kind of preparation method of river radix paeoniae rubra hydrosol |
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| CN201810413610.2A CN108553353A (en) | 2018-04-29 | 2018-04-29 | A kind of preparation method of river radix paeoniae rubra hydrosol |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112168762A (en) * | 2020-11-10 | 2021-01-05 | 上海瑜梓堂生物科技有限公司 | Cold compress gel for chest and pleura prepared from cold compress gel |
| CN112336669A (en) * | 2020-11-10 | 2021-02-09 | 上海瑜梓堂生物科技有限公司 | Preparation method and application of cold compress gel for chest |
| CN114028280A (en) * | 2021-11-19 | 2022-02-11 | 陕西蒲城兴农生物科技开发有限公司 | Taxus chinensis hydrolat and preparation method thereof |
-
2018
- 2018-04-29 CN CN201810413610.2A patent/CN108553353A/en not_active Withdrawn
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112168762A (en) * | 2020-11-10 | 2021-01-05 | 上海瑜梓堂生物科技有限公司 | Cold compress gel for chest and pleura prepared from cold compress gel |
| CN112336669A (en) * | 2020-11-10 | 2021-02-09 | 上海瑜梓堂生物科技有限公司 | Preparation method and application of cold compress gel for chest |
| CN114028280A (en) * | 2021-11-19 | 2022-02-11 | 陕西蒲城兴农生物科技开发有限公司 | Taxus chinensis hydrolat and preparation method thereof |
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