CN107048242A - A kind of sea cucumber liquid and preparation method thereof - Google Patents
A kind of sea cucumber liquid and preparation method thereof Download PDFInfo
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- CN107048242A CN107048242A CN201710424006.5A CN201710424006A CN107048242A CN 107048242 A CN107048242 A CN 107048242A CN 201710424006 A CN201710424006 A CN 201710424006A CN 107048242 A CN107048242 A CN 107048242A
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B4/00—General methods for preserving meat, sausages, fish or fish products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/015—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with pressure variation, shock, acceleration or shear stress or cavitation
- A23L3/0155—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with pressure variation, shock, acceleration or shear stress or cavitation using sub- or super-atmospheric pressures, or pressure variations transmitted by a liquid or gas
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to sea cucumber deep process technical field, a kind of sea cucumber liquid and preparation method thereof is especially related to.Sea cucumber liquid of the present invention includes active ingredient, screening agent and water, and the raw material of the active ingredient is sea cucumber；The raw material of the screening agent includes：Hawthorn, Momordica grosvenori, corn.The preparation method of the present invention, step includes enzymolysis, is specially：Complex enzyme and water will be added in sea cucumber after crushing, microwave heating is stirred, and separation obtains enzymolysis liquid；The molecular weight of the enzymolysis liquid is less than 3000.The sea cucumber liquid heavy metal constituent content prepared using the present invention is significantly declined；With fruit taste, no fishy smell is in good taste；Polysaccharide turnover rate is low；It is long without using the preservative holding time.
Description
Technical field
The present invention relates to sea cucumber deep process technical field, a kind of sea cucumber liquid and preparation method thereof is especially related to.
Background technology
《Food book on Chinese herbal medicine》：Sea cucumber has main tonifying primordial Qi, grows the beneficial vital organs of the human body and deficient health-preserving function of dispelling.《The property of medicine is examined》：Sea
Ginseng can fall fire, nourshing kidney, logical intestines moisturize, disease of being dispelled except consumptive disease.《Book on Chinese herbal medicine asks former》：Sea cucumber moisturizing viscera, grow the sharp production of essence, nourishing yin and supplementing blood, it is strong it is positive,
Moisturize, menstruation regulating, nourishing the fetus, diuresis.The Qing Dynasty《The new compilation of materia medica》、《A Supplement to the Compendium of Materia Medica》Sea cucumber is classified as tonic Deng Chinese medicine ancient books and records
Thing.Traditional Chinese Medicine thinks that there is sea cucumber nourishing and strengthening vital, green blood, blood-nourishing, nourishing yin to promote diuresis, main tonifying primordial Qi, benefit to grow the vital organs of the human body and dispel
Deficient function.Western medicine thinks that sea cucumber polysaccharide has powerful reparative regeneration function, can effectively repair what human body was damaged
Cell, recovers and improves organ dysfunction.Sea cucumber is rare low fat, low sugar, the nourishing food without cholesterol, is taken rich in kind more than 50
18 kinds of amino acid including the natural nutrient component of balancing, the essential amino acid that can not be synthesized comprising 8 kinds of human bodies；Abundant
The a variety of macroelements of calcium, iron, zinc, selenium, trace element and mineral matter；A variety of high-efficiency activated nutritional ingredients, such as sea cucumber polysaccharide, sea cucumber
Saponin(e, taurine, SOD, glutathione.
Currently, traditional sea cucumber mainly has instant holothurian, salted sea cucumber, sea cucumber living etc..Traditional processing sea cucumber is, it is necessary to through too high
The process of warm boiling, due to sea cucumber polysaccharide, the characteristic such as sea cucumber soap is sweet, protein is high-temperature denatured or soluble in water, is caused in sea cucumber
The destroyed and a large amount of loss of active material with health value.Sea cucumber living is not only hard but also solid, very flexible, and molecular structure is non-
Often complicated, human body is difficult digestion, and people, the elderly suffered from indiestion is worse.There is substantial amounts of heavy metal and halogen in sea cucumber surface living
Element, without professional technique, cannot be removed, long-term consumption, there is potential safety hazard.
In addition, there is the processing method of other sea cucumber liquid, sea cucumber is ground into liquid, filtering, high-temperature sterilization are caused
Bioactive ingredients are damaged, and are of low nutritive value, and absorption of human body is poor, and sea cucumber liquid causes mouthfeel to be short of without defishying.
And a kind of sea cucumber liquid and preparation method thereof of the invention can effectively solve produced problem in above-mentioned Holothurian machining.
The content of the invention
It is an object of the present invention to provide a kind of preparation method of sea cucumber liquid, the sea cucumber liquid prepared using this method is free of
Heavy metal and halogen, no fishy smell, solve the problem of conventional sea cucumber contains heavy metal fishy smell weight.
To solve above technical problem, the technical solution adopted by the present invention is：
Sea cucumber liquid of the present invention, including active ingredient, screening agent and water,
The raw material of the active ingredient is sea cucumber；
The raw material of the screening agent includes：Hawthorn, Momordica grosvenori, corn.
The preparation method of sea cucumber liquid of the present invention, step includes enzymolysis, is specially：It will be added in sea cucumber after crushing
Complex enzyme and water, microwave heating, are stirred, and separation obtains enzymolysis liquid；
The complex enzyme is the mixing of low-temperature protease and lipase；
The molecular weight of the enzymolysis liquid is less than 3000.
It is preferred that, the complex enzyme is made up of the component of following part by weight：Low-temperature protease: lipase=100: 2；
The part by weight of sea cucumber, complex enzyme and water is：Sea cucumber: complex enzyme: water=10: 1: 100.
It is preferred that, the temperature of the enzymolysis is 50~53 DEG C, and the time is 4.5~5h.
It is preferred that, step also includes ion exchange, is specially：The enzymolysis liquid is removed into weight using ion exchange column methods
Metal, obtains ion exchange sea cucumber liquid.
It is preferred that, step also includes concentration, and the concentration uses inspissator, the ion exchange sea cucumber liquid is concentrated into solid
Shape thing content is 25g/100ml, and separation obtains sea cucumber concentrated liquid.
It is preferred that, step also includes the preparation of screening agent, is specially：Hawthorn, Momordica grosvenori, corn are mixed, crushed, sieving
Afterwards, soak, be heated to boiling, filtering, filtrate adds water, is supplemented to the amount of water before boiling, obtains screening agent.
It is preferred that, step also includes low temperature sterilization, and sterilization pressure is that 700~800MPa, temperature are 70~80 DEG C, and the time is
25~30 minutes.
It is preferred that, the ion exchange resin that the ion exchange is used is chelating ion exchange resin.
It is preferred that, hawthorn, Momordica grosvenori, the weight ratio of corn are：
Hawthorn: Momordica grosvenori: corn=30~50: 20~30: 20~30.
Compared with prior art, the invention has the advantages that：
1. the complex enzyme that enzymolysis step of the present invention is used, at the same using microwave technology reaction temperature is controlled it is more uniform,
Accurately, the enzymolysis liquid molecular weight obtained is moderate, it is easier to which human consumption absorbs, in addition, farthest protecting the battalion of sea cucumber
Form point, the loss late of such as sea cucumber polysaccharide is only 9.6%, and nutritive value is higher；
2. the sea cucumber liquid prepared has fruit taste, no fishy smell is in good taste；
3. it can be preserved 18 months in the case of not adding preservative agent using cold sterilization techniques sterilizing, it is to avoid product addition
Toxic side effect of the preservative to human body；
4. contents of heavy metal elements significantly declines, Cr, As, Ag, Cd, Pb, Hg seriously endanger the heavy metal of health
Element is removed by ion exchange completely, it is to avoid harm of the heavy metal to human body.
Embodiment
The invention will be further described with reference to embodiments.
The description only actually at least one exemplary embodiment is illustrative below, never as to the present invention
And its any limitation applied or used.
It may be not discussed in detail for technology, method and apparatus known to person of ordinary skill in the relevant, but suitable
In the case of, the technology, method and apparatus should be considered as a part for specification.
In shown here and discussion all examples, any occurrence should be construed as merely exemplary, without
It is as limitation.Therefore, other examples of exemplary embodiment can have different values.
Embodiment 1
New sea cucumber deep processing preparation method of the present invention, comprises the following steps：
1. sea cucumber preprocessing
Qualified Weihai stichopus japonicus is selected, is dissected, the silt for removing the internal organs and being wherein mingled with, is cleaned, it is drained and standby.
2. sea cucumber blends
The sea cucumber for treating step 1 under 4 DEG C of low temperature stirs 30 minutes in the case where not adding water inside mixer,
It is set to go completely into liquid condition.
3. enzymolysis
The good 10Kg sea cucumber liquid of low-temperature grinding is put into enzymolysis kettle, 38 DEG C are heated to, constant temperature is kept, low temperature egg is added
White enzyme and lipase complex enzyme 1Kg, while adding 100Kg pure water in reactor, microwave heating, hydrolysis temperature is 50 DEG C,
Enzymolysis time 4.5 hours, is down to room temperature, and centrifuge is separated, and obtains enzymolysis liquid, and the sea cucumber of non-complete hydrolysis returns to enzymolysis kettle
In, together digested with next batch of material；
Wherein the weight ratio of protease and lipase is protease: lipase=100: 2.
4. ion exchange
Enzymolysis liquid is taken, the heavy metal ion in sea cucumber liquid is removed with ion-exchange, obtains ion exchange sea cucumber liquid, ion
The method that exchange process uses ion isolation post, ion isolation post is routine techniques, uses internal diameter for 5~50cm glass column, is selected
Take chelating ion exchange resin, the present embodiment use weight ratio for 1: 1 Eporous MX8C and Eporous K-1 compound trees
Fat；
The selection of glass column dimension is determined according to the enzymolysis liquid measure to be carried out ion exchange.
5. concentration
By step 4) prepare ion exchange sea cucumber liquid concentrated with high-efficiency evaporator, being concentrated into solid content is
25g/100ml, is further separated using centrifuge, obtains sea cucumber concentrated liquid.
6. the preparation of screening agent
From suitable hawthorn, Momordica grosvenori, corn, parts by weight of raw materials is
30 parts of hawthorn；
20 parts of Momordica grosvenori；
20 parts of corn；
Pulverized and sieved, plus 10 times of screening agent raw material gross weight pure water soak 3 hours after heat and boil, 30 minutes
Afterwards, filtered juice is filtered to obtain, pure water is added in filtered juice, the amount of water before boiling is supplemented to, obtains screening agent；
7. finished product
Sea cucumber concentrated liquid, screening agent, water are well mixed and obtain sea cucumber liquid finished product；
Sea cucumber liquid is into including the component of following percetage by weight：
Sea cucumber concentrated liquid 5wt%；
Screening agent 15wt%；
Remaining is water.
8. it is canned
Sea cucumber liquid finished product is carried out to filling, staff's progress quality inspection.
9. low temperature sterilization
By filled sea cucumber liquid finished product being placed in sterilizer uniformly, in right amount, under pressure 700MPa, temperature 70 C
Low temperature sterilization is carried out, is sterilized 25 minutes.
Product is detected, it is as a result as follows：
Table 1
| Element | Raw sample ng/ml | Ng/ml after processing |
| Cr | 22.4500 | 0 |
| As | 126.1400 | 0 |
| Ag | 4.1040 | 0 |
| Cd | 11.2400 | 0 |
| Pb | 4.5789 | 0 |
| Hg | 51.4000 | 0 |
1) using the sea cucumber liquid of the sea cucumber liquid after ion-exchange step heavy-metal ion removal and non-heavy-metal ion removal
Content of beary metal is contrasted, such as table 1, as shown by data, go removing heavy metals step to heavy metal, especially Ag in sea cucumber liquid, Cd, Sb,
Ba, Pb, Hg, Cr, Mn, Ni heavy metals removal are especially pronounced, and inspection does not measure above element in obtained product.
2) sea cucumber liquid prepared by the present invention and the sea cucumber polysaccharide comparative analysis in sea cucumber living, salted sea cucumber, common sea cucumber liquid
It is shown in Table 2.
Table 2
Above-mentioned as shown by data, sea cucumber sea cucumber polysaccharide content living is enriched for 458mg/ only very much, is processed into after salted sea cucumber and subtracts
156mg/ is arrived less only, loss 65.9%；
The sea cucumber liquid sea cucumber polysaccharide content of commonsense method processing only, loses 34.9% for 298mg/；
The sea cucumber liquid sea cucumber polysaccharide content prepared with the present invention is 441mg/, and compared with sea cucumber living, sea cucumber polysaccharide is lost in
Ratio is 9.6%.
3) it can be good at covering the fishy smell of sea cucumber using screening agent manufactured in the present embodiment, and with fruit
Delicate fragrance, it is in good taste.
4) after the low temperature sterilization of the present embodiment, sea cucumber liquid is stored 18 months in the case of without any preservative
Never degenerate, it is to avoid toxic side effect of the preservative to human body.
Therefore, a kind of preparation method for sea cucumber liquid that the present invention is provided is scientific and effective good Holothurian machining mode.
Embodiment 2
Compared with Example 1, the present embodiment difference is, step 3 hydrolysis temperature is 53 DEG C；
After testing, it is essentially identical using the present embodiment method the sea cucumber liquid prepared and indices that embodiment 1 is detected.
Embodiment 3
Compared with embodiment, the difference of the present embodiment is, the preparation formula of step 6 screening agent：
From suitable hawthorn, Momordica grosvenori, corn, parts by weight of raw materials is
50 parts of hawthorn；
20 parts of Momordica grosvenori；
20 parts of corn；
After testing, it is essentially identical using the present embodiment method the sea cucumber liquid prepared and indices that embodiment 1 is detected, but
For from taste, the taste of hawthorn is obvious.
Embodiment 4
Compared with embodiment, the difference of the present embodiment is, the preparation formula of step 6 screening agent：
From suitable hawthorn, Momordica grosvenori, corn, parts by weight of raw materials is
40 parts of hawthorn；
30 parts of Momordica grosvenori；
30 parts of corn；
After testing, it is essentially identical using the present embodiment method the sea cucumber liquid prepared and indices that embodiment 1 is detected.
Embodiment 5
Compared with Example 1, the difference of the present embodiment is, step 7 finished product：
Sea cucumber concentrated liquid, screening agent, water are well mixed and obtain sea cucumber liquid finished product；
Sea cucumber liquid is into including the component of following percetage by weight：
Sea cucumber concentrated liquid 15wt%；
Screening agent 30wt%；
Remaining is water.
It is essentially identical using sea cucumber liquid manufactured in the present embodiment and indices that embodiment 1 is detected, mouthfeel is stronger,
It is sticky.
Embodiment 6
Compared with Example 1, the difference of the present embodiment is, step 7 finished product：
Sea cucumber concentrated liquid, screening agent, water are well mixed and obtain sea cucumber liquid finished product；
Sea cucumber liquid is into including the component of following percetage by weight：
Sea cucumber concentrated liquid 10wt%；
Screening agent 20wt%；
Remaining is water.
Essentially identical using sea cucumber liquid manufactured in the present embodiment and indices that embodiment 1 is detected, mouthfeel is moderate.
Embodiment 7
Compared with Example 1, the difference of the present embodiment is, step 9 low temperature sterilization：
By filled sea cucumber liquid finished product being placed in sterilizer uniformly, in right amount, at pressure 800MPa, 80 DEG C of temperature
Low temperature sterilization is carried out, is sterilized 30 minutes.
It is essentially identical using sea cucumber liquid manufactured in the present embodiment and indices that embodiment 1 is detected.
Although some specific embodiments of the present invention are described in detail by example, the skill of this area
Art personnel are it should be understood that example above is merely to illustrate, the scope being not intended to be limiting of the invention.The skill of this area
Art personnel to above example it should be understood that can modify without departing from the scope and spirit of the present invention.This hair
Bright scope is defined by the following claims.
Claims (10)
1. a kind of sea cucumber liquid, it is characterised in that including active ingredient, screening agent and water,
The raw material of the active ingredient is sea cucumber；
The raw material of the screening agent includes：Hawthorn, Momordica grosvenori, corn.
2. a kind of preparation method of sea cucumber liquid, it is characterised in that step includes enzymolysis, is specially：It will add in sea cucumber after crushing
Enter complex enzyme and water, microwave heating is stirred, and separation obtains enzymolysis liquid；
The complex enzyme is the mixing of low-temperature protease and lipase；
The molecular weight of the enzymolysis liquid is less than 3000.
3. the preparation method of sea cucumber liquid according to claim 2, it is characterised in that
The complex enzyme is made up of the component of following part by weight：Low-temperature protease: lipase=100: 2；
The part by weight of sea cucumber, complex enzyme and water is：Sea cucumber: complex enzyme: water=10: 1: 100.
4. the preparation method of sea cucumber liquid according to claim 2, it is characterised in that
The temperature of the enzymolysis is 50~53 DEG C, and the time is 4.5~5h.
5. the preparation method of sea cucumber liquid according to claim 2, it is characterised in that step also includes ion exchange, specifically
For：The enzymolysis liquid is removed into removing heavy metals using ion exchange column methods, ion exchange sea cucumber liquid is obtained.
6. the preparation method of sea cucumber liquid according to claim 5, it is characterised in that step also includes concentration, the concentration
Using inspissator, the ion exchange sea cucumber liquid is concentrated into solid content for 25g/100ml, separation obtains the concentration of sea cucumber water
Liquid.
7. the preparation method of sea cucumber liquid according to claim 2, it is characterised in that step also includes the preparation of screening agent,
Specially：Hawthorn, Momordica grosvenori, corn are mixed, crushes, after sieving, soaks, boiling is heated to, filtering, filtrate adds water, and mends
The amount of water before boiling is charged to, screening agent is obtained.
8. the preparation method of sea cucumber liquid according to claim 2, it is characterised in that step also includes low temperature sterilization, sterilizing
Pressure is that 700~800MPa, temperature are 70~80 DEG C, and the time is 25~30 minutes.
9. the preparation method of sea cucumber liquid according to claim 5, it is characterised in that the ion that the ion exchange is used is handed over
Resin is changed for chelating ion exchange resin.
10. the preparation method of sea cucumber liquid according to claim 7, it is characterised in that hawthorn, Momordica grosvenori, the weight of corn
Than for：
Hawthorn: Momordica grosvenori: corn=30~50: 20~30: 20~30.
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102940245A (en) * | 2012-10-26 | 2013-02-27 | 青岛佳日隆海洋食品有限公司 | Sea cucumber oral liquid and preparation process thereof |
| CN104719970A (en) * | 2015-02-27 | 2015-06-24 | 蓬莱市海洋生物有限公司 | Production process of sea cucumber oral liquid |
-
2017
- 2017-06-07 CN CN201710424006.5A patent/CN107048242A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102940245A (en) * | 2012-10-26 | 2013-02-27 | 青岛佳日隆海洋食品有限公司 | Sea cucumber oral liquid and preparation process thereof |
| CN104719970A (en) * | 2015-02-27 | 2015-06-24 | 蓬莱市海洋生物有限公司 | Production process of sea cucumber oral liquid |
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| 丁忠浩: "《废水资源化综合利用技术》", 31 January 2007, 国防工业出版社 * |
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Application publication date: 20170818 |