CN108272708A - A kind of Indian beech hydrosol with effects of tranquilizing and allaying excitement - Google Patents
A kind of Indian beech hydrosol with effects of tranquilizing and allaying excitement Download PDFInfo
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- CN108272708A CN108272708A CN201810380706.3A CN201810380706A CN108272708A CN 108272708 A CN108272708 A CN 108272708A CN 201810380706 A CN201810380706 A CN 201810380706A CN 108272708 A CN108272708 A CN 108272708A
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- Prior art keywords
- indian beech
- hydrosol
- preparation
- indian
- beech
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Botany (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of preparation methods of Indian beech hydrosol, its processing procedure has merged immersion, ultrasound, distillation, has stood a variety of processing means such as filtering, Cord blood and filter at low temperature, simultaneously Indian beech hydrosol is prepared using the treatment conditions of special parameter, obtained Indian beech hydrosol contains water-soluble active ingredient, stable quality, it is not easy that sediment, appearance transparent clarification is precipitated, while also having effects that replenishing water and preserving moisture, tranquilizing and allaying excitement.
Description
Technical field
The present invention relates to cosmetic fields, are specifically related to a kind of Indian beech hydrosol with effects of tranquilizing and allaying excitement.
Background technology
With the rapid development of society, people’s lives rhythm is also getting faster, accordingly the pressure caused by human body
Steeply rise, primary insomnia, examination catatonic syndrome, vegetative nerve functional disturbance, endocrine disorder, sleep rhythm obstacle,
Climacteric syndrome, neurasthenia, depression etc. annoying always people, seriously affect normal daily life, calmness peace
The product of god becomes the new demand of people.
Indian beechPongamia pinnata (Linn.) PierreFor a kind of unique plant of pulse family Pongamia, stem
Portion's Glabrous is distributed widely in river levee and the coastal area of country in Southeast Asia, with being found in the tide of India forest earliest, not
Name India trifoliate jewelvine is a kind of extremely xylophyta with medical value.In traditional medication, the seed oil of Indian beech can be used
In treatment itch, running sore and other skin diseases；Flower is used for treating diabetes；Root is for treating hemorrhagic hemorrhoid, tinea pedis
Disease, diabetes and antibacterial；And the research of tranquilizing and allaying excitement is had not been reported.
Invention content
The technical problem to be solved in the present invention is to provide a kind of Indian beech hydrosols with effects of tranquilizing and allaying excitement.
The technical solution to solve the above problems is as follows：
A kind of Indian beech hydrosol, preparation method include the following steps：
（1）Pretreatment：By fresh material（Indian beech leaf, lavender）Cleaned up with deionized water, removing wherein go mouldy, worm
Moth, sick scar part, removal of inclusions obtain pretreated material；
（2）It crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
（3）It impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly；
（4）Distillation：Distillation still is sealed, is vacuumized；Then it is heated to deionized water boiling；Open ultrasonication；It beats
The condenser of distillation still is opened, and the cooling water that circulates within the condenser, starts to collect distillate；
（5）Filtering：The distillate of collection is stood at low temperature, then uses filter-cloth filtering, filtrate is obtained, appropriate anti-corrosion is added
Agent, you can.
In wherein some embodiments, step（1）Described in Indian beech leaf, spina date seed weight ratio be（0.1-
10）：（0.1-10）.
In wherein some embodiments, step（1）Described in material further include Schisandra chinensis, spina date seed；Preferably, described
Indian beech leaf, spina date seed, Schisandra chinensis, lavender weight ratio be（0.1-10）：（0.1-10）：（0.1-10）：（0.1-
10）.
In wherein some embodiments, step（3）Described in deionization impregnate solid-liquid ratio be（1：5）-（1：10）, leaching
It is 1-2 hours to steep the time；
In wherein some embodiments, step（4）Described in the pressure that is evacuated in kettle be 0.05-0.1MPa；
In wherein some embodiments, step（4）Described in the frequency of ultrasonic wave be 30-60kHz, the duration is 5-10 point
Clock；
In wherein some embodiments, step（5）Described in standing temperature be 1-5 DEG C, the time be 12-24 hours；It is described
Filter cloth mesh number be 1000-2000 mesh.
In wherein some embodiments, step（5）Described in preservative be hexylene glycol, the additive amount of hexylene glycol is that water is yellow
The 3% of skin hydrosol weight.
Second aspect of the present invention provides Indian beech hydrosol made from a kind of preparation method by mentioned earlier.
The advantageous effect that technical solution provided in an embodiment of the present invention is brought is：The present invention is initiative by Indian beech application
In skin care item, the application for being Indian beech in skin care item provides a kind of effective way.The preparation method of the present invention, is distilling
It is preceding to be handled using ultrasonic wave, it has been greatly facilitated extraction efficiency, has increased the dissolution rate of Indian beech and lavender active constituent.It is super
The cavitation effect that sonicated is brought can make Indian beech leaf and lavender cell burst because instantaneously generating running quickly for cavitation bubble in aqueous solution
And rupture, so that aqueous solution is penetrated into cell interior, improves the recovery rate of active material.In addition, the present invention also carries out distillate
Stand at low temperature and freezing and filtering make under low temperature the macromolecular substances in distillate accelerate Precipitation, will be analysed finally by filter cloth
The microscopic precipitate gone out filters out.The Indian beech hydrosol crossed through this process does not have showing for visible foreign precipitation within the shelf-life
As.A variety of macromolecular substances such as distillate its complicated component, including vegetable protein, tannin, plant polyose because of collection.If no
The Indian beech hydrosol of collection is handled, after placing a period of time, macromolecular substances will gradually be precipitated to form precipitation, serious shadow
Consumer is rung to use.In traditional hydrosol preparation process, often without filter operation, or room temperature mistake only is carried out to distillate
Filter, hydrosol obtained in this way, often appearing in just has the phenomenon that visible foreign precipitation in the shelf-life.Its processing of preparation method of the present invention
Process fusion impregnates, ultrasound, distillation, stands a variety of processing means such as filtering, Cord blood and filter at low temperature, while using special
The treatment conditions of parameter are determined to prepare Indian beech hydrosol, and obtained Indian beech hydrosol contains water-soluble active ingredient, and quality is steady
It is fixed, it is not easy that sediment, appearance transparent clarification is precipitated, while also having effects that replenishing water and preserving moisture, tranquilizing and allaying excitement.
Specific implementation mode
To make the object, technical solutions and advantages of the present invention clearer, embodiment of the present invention will be made into one below
Step ground detailed description, embodiments of the present invention are not limited thereto, for not specifically specified technological parameter or condition, can refer to
Routine techniques carries out.
Embodiment 1
A kind of Indian beech hydrosol, preparation method include the following steps：
（1）Pretreatment：By fresh material（Indian beech leaf, lavender）Cleaned up with deionized water, removing wherein go mouldy, worm
Moth, sick scar part, removal of inclusions obtains pretreated material, wherein the weight ratio of the Indian beech leaf, lavender is
0.1：10；
（2）It crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
（3）It impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly, wherein feed liquid
Than being 1：10, soaking time is 1 hour；
（4）Distillation：Distillation still is sealed, 0.1MPa is evacuated to；Then it is heated to deionized water boiling；Open 30kHz
Ultrasonication 10 minutes；The condenser of distillation still, and the cooling water that circulates within the condenser are opened, starts to collect distillate；
（5）Filtering：The distillate of collection is stood 24 hours under 1 DEG C of low temperature, then with 1000 mesh filter-cloth filterings, is filtered
Liquid, is added hexylene glycol, and the additive amount of hexylene glycol is the 3% of Indian beech hydrosol weight.
Embodiment 2
A kind of Indian beech hydrosol, preparation method include the following steps：
（1）Pretreatment：By fresh material（Indian beech leaf, lavender）Cleaned up with deionized water, removing wherein go mouldy, worm
Moth, sick scar part, removal of inclusions obtains pretreated material, wherein the weight ratio of the Indian beech leaf, lavender is
10：0.1；
（2）It crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
（3）It impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly, wherein feed liquid
Than being 1：5, soaking time is 2 hours；
（4）Distillation：Distillation still is sealed, 0.05MPa is evacuated to；Then it is heated to deionized water boiling；Open 60kHz
Ultrasonication 5 minutes；The condenser of distillation still, and the cooling water that circulates within the condenser are opened, starts to collect distillate；
（5）Filtering：The distillate of collection is stood 12 hours under 5 DEG C of low temperature, then with 2000 mesh filter-cloth filterings, is filtered
Liquid, is added hexylene glycol, and the additive amount of hexylene glycol is the 3% of Indian beech hydrosol weight.
Embodiment 3
A kind of Indian beech hydrosol, preparation method include the following steps：
（1）Pretreatment：By fresh material（Indian beech leaf, lavender, Schisandra chinensis, spina date seed）It is cleaned up with deionized water,
Removing wherein goes mouldy, damages by worms, sick scar part, and removal of inclusions obtains pretreated material, wherein the Indian beech leaf, smoking clothing
Grass, Schisandra chinensis, spina date seed weight ratio be 1：1：10:0.1；
（2）It crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
（3）It impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly, wherein feed liquid
Than being 1:4, soaking time is 1.5 hours；
（4）Distillation：Distillation still is sealed, 0.06MPa is evacuated to；Then it is heated to deionized water boiling；Open 40kHz
Ultrasonication 7 minutes；The condenser of distillation still, and the cooling water that circulates within the condenser are opened, starts to collect distillate；
（5）Filtering：The distillate of collection is stood 18 hours under 3 DEG C of low temperature, then with 1500 mesh filter-cloth filterings, is filtered
Liquid, is added hexylene glycol, and the additive amount of hexylene glycol is the 3% of Indian beech hydrosol weight.
Embodiment 4
A kind of Indian beech hydrosol, preparation method include the following steps：
（1）Pretreatment：By fresh material（Indian beech leaf, lavender, Schisandra chinensis, spina date seed）It is cleaned up with deionized water,
Removing wherein goes mouldy, damages by worms, sick scar part, and removal of inclusions obtains pretreated material, wherein the Indian beech leaf, smoking clothing
Grass, Schisandra chinensis, spina date seed weight ratio be 1：1：0.1:10；
（2）It crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
（3）It impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly, wherein feed liquid
Than being 1:4, soaking time is 1.5 hours；
（4）Distillation：Distillation still is sealed, 0.06MPa is evacuated to；Then it is heated to deionized water boiling；Open 40kHz
Ultrasonication 7 minutes；The condenser of distillation still, and the cooling water that circulates within the condenser are opened, starts to collect distillate；
（5）Filtering：The distillate of collection is stood 18 hours under 3 DEG C of low temperature, then with 1500 mesh filter-cloth filterings, is filtered
Liquid, is added hexylene glycol, and the additive amount of hexylene glycol is the 3% of Indian beech hydrosol weight.
Embodiment 5
Effect detection is carried out to Indian beech hydrosol of the present invention, using the anti-acne essence prepared by embodiment 1-4 as experimental group
1-4；In addition setting control group 1-4；
Wherein control group 1 the difference from example 2 is that, be not added with Indian beech leaf；
Wherein control group 2 the difference from example 2 is that, be not added with lavender；
Wherein difference lies in be not added with Schisandra chinensis to control group 3 with embodiment 4；
Wherein difference lies in be not added with spina date seed to control group 4 with embodiment 4；
Experiment 1
Efficacy assessments are carried out to the Indian beech hydrosol of implementation group 1-4 and contrast groups 1-4.The specific test method is as follows：Each experimental group
It is 20 volunteers, 25-55 Sui, all there are palpitaition, insomnia, palpitation, forgetful and confusing frightened symptoms such as mad；It uses：It is early daily
In each 1 time of evening, it is applied to face, is used continuously 14 days；Evaluation criterion：It is effective, effectively, in vain, wherein palpitaition, insomnia, palpitation, strong
Forget and the confusing frightened symptoms such as mad substantially eliminate be judged as it is effective；It partially removes and is judged as effectively；Other, it is invalid to be judged as.Specifically
Test result is shown in Table 1.
1 test recording table of table
As known from Table 1, the effect of comparison implementation group 1-2 and control group 1-2 can obtain：Indian beech leaf, lavender are by specific
Indian beech hydrosol made from extraction process, can be from the whole synergy for playing tranquilizing and allaying excitement；Compare implementation group 3-4 and implementation
Organize 1-2, the effect of contrast groups 3-4 can obtain：By adding Schisandra chinensis, spina date seed on the basis of Indian beech leaf, lavender
The effect of Indian beech hydrosol can be effectively improved.
The above described is only a preferred embodiment of the present invention, limitation in any form not is done to the present invention, therefore
All contents without departing from technical solution of the present invention, it is made to the above embodiment according to the technical essence of the invention any simply to repair
Change, equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (8)
1. a kind of Indian beech hydrosol, which is characterized in that preparation method includes the following steps：
（1）Pretreatment：By fresh material（Indian beech leaf, lavender）Cleaned up with deionized water, removing wherein go mouldy, worm
Moth, sick scar part, removal of inclusions obtain pretreated material；
（2）It crushes：It will be blended in above-mentioned pretreated material input pulverizer, obtain crushed mixture；
（3）It impregnates：Crushed mixture is put into distillation still；Deionized water is added to impregnate, and opens and mixes slowly；
（4）Distillation：Distillation still is sealed, is vacuumized；Then it is heated to deionized water boiling；Open ultrasonication；It beats
The condenser of distillation still is opened, and the cooling water that circulates within the condenser, starts to collect distillate；
（5）Filtering：The distillate of collection is stood at low temperature, then uses filter-cloth filtering, filtrate is obtained, appropriate anti-corrosion is added
Agent, you can.
2. the preparation method of Indian beech hydrosol according to claim 1, which is characterized in that step（1）Described in water it is yellow
Pi Ye, spina date seed weight ratio be（0.1-10）：（0.1-10）.
3. the preparation method of Indian beech hydrosol according to claim 1, which is characterized in that step（1）Described in material
Further include Schisandra chinensis, spina date seed；Preferably, the Indian beech leaf, spina date seed, Schisandra chinensis, lavender weight ratio be
（0.1-10）：（0.1-10）：（0.1-10）：（0.1-10）.
4. the preparation method of Indian beech hydrosol according to claim 1, which is characterized in that step（3）Described in go from
Son impregnate solid-liquid ratio be（1：5）-（1：10）, soaking time is 1-2 hours.
5. the preparation method of Indian beech hydrosol according to claim 1, which is characterized in that step（4）Described in pumping it is true
Pressure is 0.05-0.1Mpa in sky to kettle.
6. the preparation method of Indian beech hydrosol according to claim 1, which is characterized in that step（4）Described in ultrasound
The frequency of wave is 30-60kHz, and the duration is 5-10 minutes.
7. the preparation method of Indian beech hydrosol according to claim 1, which is characterized in that step（5）Described in standing
Temperature be 1-5 DEG C, the time be 12-24 hours；The filter cloth mesh number is 1000-2000 mesh.
8. the preparation method of Indian beech hydrosol according to claim 1, which is characterized in that step（5）Described in anti-corrosion
Agent is hexylene glycol, and the additive amount of hexylene glycol is the 3% of Indian beech hydrosol weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810380706.3A CN108272708A (en) | 2018-04-25 | 2018-04-25 | A kind of Indian beech hydrosol with effects of tranquilizing and allaying excitement |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810380706.3A CN108272708A (en) | 2018-04-25 | 2018-04-25 | A kind of Indian beech hydrosol with effects of tranquilizing and allaying excitement |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108272708A true CN108272708A (en) | 2018-07-13 |
Family
ID=62812103
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810380706.3A Withdrawn CN108272708A (en) | 2018-04-25 | 2018-04-25 | A kind of Indian beech hydrosol with effects of tranquilizing and allaying excitement |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108272708A (en) |
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2018
- 2018-04-25 CN CN201810380706.3A patent/CN108272708A/en not_active Withdrawn
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Application publication date: 20180713 |