CN108552224A - A kind of composition pesticide containing Dipel and Celastrus angulatus - Google Patents

A kind of composition pesticide containing Dipel and Celastrus angulatus Download PDF

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Publication number
CN108552224A
CN108552224A CN201810610576.8A CN201810610576A CN108552224A CN 108552224 A CN108552224 A CN 108552224A CN 201810610576 A CN201810610576 A CN 201810610576A CN 108552224 A CN108552224 A CN 108552224A
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dipel
celastrus angulatus
composition pesticide
celastrus
pesticide containing
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王育鹏
张震
陈海燕
章力干
沈章军
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Anhui Agricultural University AHAU
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Anhui Agricultural University AHAU
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/06Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
    • A01N43/12Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Environmental Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Wood Science & Technology (AREA)
  • Microbiology (AREA)
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  • Biotechnology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention belongs to technical field of pesticide, and in particular to a kind of composition pesticide containing Dipel and Celastrus angulatus.A kind of composition pesticide containing Dipel and Celastrus angulatus, active constituent are made of Dipel and Celastrus angulatus, and the mass ratio of the Dipel and Celastrus angulatus is 1: 5~5: 1.The active insecticidal components of the present invention are Dipel and Celastrus angulatus, and two active constituents are different to the mechanism of action of pest, and there is the two compounding certain complementation and synergistic effect, preventive effect to be apparently higher than single dose;Formulation rate is reduced simultaneously, alleviates pesticide medication burden and the pollution to environment;The present invention can have special efficacy for cabbage caterpillar and diamondback moth;Pests are not easy to produce resistance.

Description

A kind of composition pesticide containing Dipel and Celastrus angulatus
Technical field
The invention belongs to technical field of pesticide, and in particular to a kind of pesticide combination containing Dipel and Celastrus angulatus Object.
Background technology
Dipel (Bacillus thuringiensis, abbreviation Bt) is a kind of production crystal including many mutation Bacillus can be cooked microbial source low toxic pesticide, based on stomach poison function.The bacterium can generate two major classes toxin, i.e. endotoxin (parasporal crystal) and exotoxin make pest stop feeding, and last pest is because hungry and dead, and exotoxin effect is slow, is sloughing off Effect is apparent when skin and metamorphosis, the two periods are the peak periods of RNA synthesis, and exotoxin can inhibit the RNA polymerizations dependent on DNA Enzyme.Medicine effect is slow, can just take effect within 2 days or so after pests, about 1 day lasting period, therefore should compare conventional chemical when use Medicament shifts to an earlier date 2~3 days, and preferable in pest low age phase using effect.Therefore the bacillus can be cooked microbial source low toxic pesticide, be used In prevention Orthoptera, the various pests of coleoptera, Diptera, Hymenoptera, especially Lepidoptera.
The active insecticidal components of Celastrus angulatus have anesthesia, food refusal and stomach toxicity, action of contace poison to pest, and do not generate anti-medicine Property does not kill the features such as natural enemy, stable in physicochemical property, especially to having stomach to insects such as black cutworn, lopper worm, anomis flavas Malicious toxic action.According to recent studies have shown that, Celastrus angulatus to beet armyworm, prodenia litura special efficacy, to rice leaf roller, pink rice borer, Striped rice borer, yellow rice borer are efficient, and the lasting period is up to 30 days, because being botanical pesticide, pest not will produce resistance.
Lepidoptera pest distribution is extremely wide, the abundantest with tropical type.The larva of most types is caused harm all kinds of Cultivated plant, the often feeding of the bodily form the greater blade or brill moth limb to the greatest extent;Bodily form smaller often leaf roll, sew leaf, knot sheath, spinning netting Or it pierces plant tissue feeding and causes harm.
It is the small green worm of diamondback moth alias, pointed at both ends, be the worldwide pest that migrates, wild cabbage of mainly causing harm, violet cabbage, broccoli, The crucifers such as a kind of sedge dish, leaf mustard, cauliflower, Chinese cabbage, rape, radish.Harm characteristics:First instar larvae only feeding mesophyll, leaves Epidermis forms spot transparent one by one in dish leaf, and dish leaf can be eaten into hole and incised by 3~4 instar larvaes, full leaf quilt when serious It eats and reticulates.Often lobus cardiacus is concentrated to cause harm in seedling stage, influences packet.It is reserving seed for planting in strain, is endangering tender stem, young pod and seed.
Cabbage caterpillar larva bites host's blade, and when cabbage caterpillar feeding, fecal pollution is discharged in feeding.Larvae underwent 5 instars, 2 Mesophyll was only gnawed before age, is left layer of transparent epidermis, was mostly caused harm in blade back before 3 ages;Blade face is gone to after 3 ages to nibble, and nibbles blade Hole is incised, and blade is all eaten up when serious, only remains thick vein and petiole, is caused to have no harvest, is easily caused soft rot of cabbage Prevalence;The food ingestion of 4-5 instar larvaes accounts for the 97% of entire larval phase food ingestion.
Since people depend on the insecticide using single type, pest to easy to produce drug resistance, cause insecticide for a long time Chemical dosage sharply increase, not only aggravated agriculture name financial burden, pollution environment.
Therefore, new efficient, less toxic, safe compounded pesticides prevention lepidoptera pest is developed to have great importance.
Invention content
The present invention in order to solve the above technical problems, provides a kind of pesticide combination containing Dipel and Celastrus angulatus Object, the composition pesticide overcome the deficiency of the insecticide containing single-activity component, there is outstanding prevention to imitate lepidoptera pest Fruit, while reducing formulation rate.
Technical solution is used by the present invention solves above-mentioned technical problem:
A kind of composition pesticide containing Dipel and Celastrus angulatus, active constituent is by Dipel and Celastrus angulatus The mass ratio of composition, the Dipel and Celastrus angulatus is 1: 5~5: 1.
Further, the mass ratio of the Dipel and Celastrus angulatus is 1: 4~5: 1.
Further, the mass ratio of the Dipel and Celastrus angulatus is 1: 3~5: 1.
Further, the mass ratio of the Dipel and Celastrus angulatus is 1: 2~5: 1
Further, the mass ratio of the Dipel and Celastrus angulatus is 1: 1~5: 1.、
Further, also containing pesticidal preparations auxiliary element the agent for being suitble to agriculturally use is made in the composition pesticide Type.
Further, the dosage form is any one of wettable powder, water dispersible granules, dispersible oil-suspending agent.
Further, the pesticidal preparations auxiliary element is auxiliary agent or/and filler.
Further, the weight percent of the Dipel and Celastrus angulatus weight summation in the composition pesticide For 0.6%-10%.
Further, the weight percent of the Dipel and Celastrus angulatus weight summation in the composition pesticide For 0.6%-2.5%.
The present invention compared with the existing technology has the following advantages and effect:
1, active insecticidal components of the invention are Dipel and Celastrus angulatus, effect of two active constituents to pest Mechanism is different, and there is the two compounding certain complementation and synergistic effect, preventive effect to be apparently higher than single dose;Reduce dispenser simultaneously Amount alleviates pesticide medication burden and the pollution to environment;
2, the present invention can have special efficacy for cabbage caterpillar and diamondback moth;Pests are not easy to produce resistance;
3, aqueous suspension agent is to prevent product from decomposing, precipitate, lump, freezing, and needs to add stabilizer, antifreezing agent etc., this hair The bright wettable powder that can be made into, water dispersible granules are in solid-state, have the advantages that convenience in transport compared with aqueous suspension agent;It is dispersible Oil-suspending agent has more preferably insecticidal effect compared with aqueous suspension agent.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, present invention following specific examples It illustrates, but the present invention is by no means limited to these examples.It is as described below to be used only for explaining the present invention, it can not therefore manage Solution is the limitation to the scope of the claims of the present invention.It should be pointed out that is done all within the spirits and principles of the present invention is any Modification, equivalent substitute and improvement etc., should be included within the scope of the present invention.
Pesticidal preparations are made in the combination of active principles of different pesticides, are that current one kind for developing and developing novel pesticide is quick Effective method.After different types of pesticide active ingredient mixing, it is usually expressed as three kinds of type of action:Summation action, synergy Effect and antagonism.But after different types of pesticide active ingredient mixing, it is unpredictable for specifically will produce which kind of effect; And pesticide active ingredient is not simply to mix, it is also necessary to the auxiliary ingredient of pesticidal preparations is added, pesticidal preparations auxiliary element The difference of type and amount will have a direct impact on the performance of pesticide active ingredient, so knot can just be obtained by only passing through many experiments Fruit.
Pesticidal preparations auxiliary element is auxiliary agent and filler, and different auxiliary agents is selected in the different formulations of pesticide and/or is filled out Material.Auxiliary agent has solvent, cosolvent, emulsifier, dispersant, wetting agent, disintegrant, binder, antifoaming agent, antifreeze, thickener. The one kind or more of solvent in dimethylbenzene, No. 100 solvent naphthas, No. 150 solvent naphthas, No. 200 solvent naphthas, formaldehyde in the present invention Kind;The one kind or more of cosolvent in methanol, ethyl alcohol, ethyl acetate, cyclohexanone, toluene, acetone, N-Methyl pyrrolidone Kind;Emulsifier is selected from fatty diglycollic amide, calcium dodecyl benzene sulfonate, fatty alcohol polyoxyethylene ether, alkyl phenol polyoxy second It is one or more in alkene ether, agriculture breast 500, Nongru-700 number, alkyl glycosides, α-sodium olefin sulfonate;Dispersant is selected from lignin Sodium sulfonate, calcium lignosulfonate, naphthalenesulfonic acid-formaldehyde condensate, sodium methylene bis-naphthalene sulfonate, formaldehyde condensation products sulfate, poly- carboxylic It is one or more in hydrochlorate, alkylphenol polyoxyethylene phosphate, alkyl phenol polyoxyethylene ether, polyoxyethylene carboxylate; Wetting agent is selected from lauryl sodium sulfate, Nekal BX, spaonin powder, neopelex, silkworm excrement, spaonin powder, tea seed cake It is one or more in powder;Disintegrant is selected from:One kind in bentonite, ammonium sulfate, aluminium chloride, urea, magnesium chloride, glucose or It is a variety of;Binder is selected from:It is one or more in starch, diatomite, cyclodextrin, PVA, rosin, carboxymethyl (ethyl) cellulose; Antifoaming agent is selected from:C8-210 aliphatic alcohols compound, epoxidized soybean oil, ethyl alcohol, silicone compound, organic silicone oil, C10-C20 It is one or more in saturated fat acids compound;Antifreeze is selected from:Sorbierite, ethylene glycol, polyethylene glycol, propylene glycol, third It is one or more in triol, urea, sodium chloride;Thickener in gelatin, xanthans, polyethylene glycol, polyvinyl alcohol one Kind is a variety of.Filler in the present invention is selected from precipitated calcium carbonate, diatomite, bentonite, attapulgite, white carbon, lightweight carbonic acid It is one or more in calcium.
A kind of Pesticidal combination proposed by the present invention is described in detail below in conjunction with case, it is used in experiment 3.2% Dipel wettable powder, 1.0% Celastrus angulatus missible oil are commercially available from market, Dipel quality point Number refers both to bacillus thuringiensis toxin protein mass fraction in this embodiment.
Embodiment 1:
1.5% Dipel Celastrus angulatus suspending agents
Dipel 0.5%, Celastrus angulatus 1.0%, spaonin powder 3%, calcium lignosulfonate 4%, sodium chloride 0.5%, Propylene glycol 2%, sodium carboxymethylcellulose 4%, deionized water supply 100%.The above raw material is routinely prepared to the side of suspending agent Method is mixed to prepare 1.5% Dipel Celastrus angulatus suspending agents.
Embodiment 2;
2% Dipel Celastrus angulatus suspending agents
Dipel 1.5%, Celastrus angulatus 0.5%, neopelex 5%, calcium lignosulfonate 3%, second Glycol 3%, xanthans 0.3%, deionized water supply 100%.The method that the above raw material routinely prepares suspending agent is mixed into system Obtain 2% Dipel Celastrus angulatus suspending agents.
Embodiment 3:
The 1.0% dispersible oil-suspending agent of Dipel Celastrus angulatus
Dipel 0.2%, Celastrus angulatus 0.8%, alkyl phenol polyoxyethylene ether 5%, alkylphenol-polyethenoxy base phosphorus Acid esters 10%, organoclay 1%, methyl oleate supply 100%.The method that the above raw material routinely prepares suspending agent is mixed to prepare 1.0% Dipel Celastrus angulatus suspending agents.
Embodiment 4:
1.5% Dipel Celastrus angulatus disperses oil-suspending agent
Dipel 0.75%, Celastrus angulatus 0.75%, alkyl phenol polyoxyethylene ether 7%, alkylphenol-polyethenoxy base Phosphate 8%, organoclay 0.5%, methyl oleate supply 100% and the method that the above raw material routinely prepares suspending agent are mixed system Obtain 1.5% Dipel Celastrus angulatus suspending agents.
Embodiment 5:
2.4% Dipel Celastrus angulatus wettable powders
Dipel 2.0%, Celastrus angulatus 0.4%, tea seed cake powder 5%, ethyl alcohol 2%, sodium lignin sulfonate 5%, diatom Soil supplies 100%.The above raw material is mixed according to the method that wettable powder is formulated conventionally, is crushed to certain fineness, using It is mixed into product, obtains 2.4% Dipel Celastrus angulatus wettable powders.
Embodiment 6:
0.6% Dipel Celastrus angulatus wettable powders
Dipel 0.1%, Celastrus angulatus 0.5%, tea seed cake powder 4%, ethyl alcohol 1.5%, sodium lignin sulfonate 4%, silicon Diatomaceous earth supplies 100%.The above raw material is mixed according to the method that wettable powder is formulated conventionally, is crushed to certain fineness, then pass through It crosses and is mixed into product, obtain 0.6% Dipel Celastrus angulatus wettable powders.
Embodiment 7:
1.2% Dipel Celastrus angulatus water dispersible granules
Dipel 0.8%, Celastrus angulatus 0.4%, sodium lignin sulfonate 5%, ammonium sulfate 2%, polycarboxylate 3%, Starch 2%, precipitated calcium carbonate supply 100%.The above raw material is mixed to prepare according to the method that water dispersible granules are formulated conventionally 1.2% Dipel Celastrus angulatus water dispersible granules.
Embodiment 8:
0.8% Dipel Celastrus angulatus water dispersible granules
Dipel 0.2%, Celastrus angulatus 0.6%, sodium lignin sulfonate 4%, ammonium sulfate 2%, polycarboxylate 2.5%, starch 2.5%, precipitated calcium carbonate supply 100%.The above raw material is mixed according to the method that water dispersible granules are formulated conventionally Close the Dipel Celastrus angulatus water dispersible granules being made to 0.8%.
Embodiment 9:
2.0% Dipel Celastrus angulatus missible oil
Dipel 1.6%, Celastrus angulatus 0.4%, agriculture breast No. 500 3%, Nongru-700 number 4%, dimethylbenzene 8%, first 3%, No. 200 solvent naphtha of alcohol supplies 100%.The method that the above raw material routinely prepares missible oil is mixed to prepare 15% rosickyite bacterium Azoles matrine missible oil.
Embodiment 10:
7.5% Dipel Celastrus angulatus missible oil
Dipel 5%, Celastrus angulatus 2.5%, agriculture breast No. 500 2.5%, Nongru-700 number 5%, dimethylbenzene 10%, first 2%, No. 200 solvent naphtha of alcohol supplies 100%.
Embodiment 11:
5.0% Dipel Celastrus angulatus wettable powder
Dipel 4.0%, Celastrus angulatus 1.0%, tea seed cake powder 3%, ethyl alcohol 1.2%, sodium lignin sulfonate 3.5%, Diatomite supplies 100%.The above raw material is mixed according to the method that wettable powder is formulated conventionally, is crushed to certain fineness, then By being mixed into product, 5.0% Dipel Celastrus angulatus wettable powder is obtained.
Embodiment 12;
2.5% Dipel Celastrus angulatus suspending agent
Dipel 2.0%, Celastrus angulatus 0.5%, neopelex 4%, calcium lignosulfonate 4%, second Glycol 4%, xanthans 0.2%, deionized water supply 100%.The method that the above raw material routinely prepares suspending agent is mixed into system Obtain 2.5% Dipel Celastrus angulatus suspending agent.
Embodiment 13:
The 1.0% dispersible oil-suspending agent of Dipel Celastrus angulatus
Dipel 0.5%, Celastrus angulatus 0.5%, alkyl phenol polyoxyethylene ether 4%, alkylphenol-polyethenoxy base phosphorus Acid esters 3%, organoclay 0.5%, methyl oleate supply 100%.The method that the above raw material routinely prepares suspending agent is mixed into system Obtain 1.0% Dipel Celastrus angulatus suspending agent.
Embodiment 14:
0.5% Dipel Celastrus angulatus water dispersible granules
Dipel 0.1%, Celastrus angulatus 0.4%, sodium lignin sulfonate 4%, ammonium sulfate 1%, polycarboxylate 4%, Starch 1.5%, precipitated calcium carbonate supply 100%.The above raw material is mixed to prepare according to the method that water dispersible granules are formulated conventionally To 0.5% Dipel Celastrus angulatus water dispersible granules.
The present invention is to combine confrontation diamondback moth, cabbage caterpillar with apparent synergy work between Dipel, Celastrus angulatus With, and it is not only the simple addition of two kinds of pesticide activity component insecticidal effects, specifically it is illustrated with following embodiment.
Embodiment 15:The Toxicity Determination of Dipel and Celastrus angulatus compounding
1, Dipel and the test of Celastrus angulatus different ratio co-toxicity
1.1 reagent agent
50000IU/ milligrams of Bacillus thuringiensis, 6% Celastrus angulatus mother liquor, Dipel and Celastrus angulatus be not year-on-year Example mixture preparation
1.2 selected insect source
Diamondback moth, cabbage caterpillar
1.3 single dose assay methods
Spray-on process is used to cabbage caterpillar and diamondback moth, culture dish is placed in Potter spray towers tries to get to the heart of a matter and carry out metered dose, Spray value is 1ml, takes out test worm after liquid sedimentation 1min and is raised.No less than 4 repetitions are not handled, and set blank control. Processing checks test worm death condition after 96 hours.Death rate Abbott formula corrections, further according to logarithm-death rate niqueMin point Analysis method finds out virulence regression equation and lethal.
1.4 the joint toxicity measuring method of different ratio
According to the toxicity test of single dose as a result, with the Dipel of different ratio and Celastrus angulatus using above-mentioned 1.3 Method is measured, and calculates LC50, and calculate co-toxicity coefficient (CTC) by Sun Yunpei's Method, and be calculated according to the following formula:
ATI=(S/M) * 100
In formula:
ATI --- mixture surveys toxicity index;
S --- the LC50 of standard pesticide agent, unit mg/l;
The LC50 of M --- mixture, unit mg/l.
TTI=TIA*PA+TIB*PB
In formula:
TTI --- mixtures theoretical toxicity index;
TIA --- A medicament theoretical toxicity index;
PA --- percentage composition of the A medicaments in mixture, unit are percentage;
TIB --- B medicament theoretical toxicity index;
PB --- percentage composition of the B medicaments in mixture, unit are percentage;
CTC=(ATI/TTI) * 100
In formula:
CTC --- co-toxicity coefficient;
ATI --- mixture surveys toxicity index:
TTI --- mixtures theoretical toxicity index.
Co-toxicity coefficient (CTC) >=120 shows as synergistic effect;CTC≤80 show as antagonism;80 < CTC <, 120 tables It is now summation action, the results are shown in Table one, table two.
Table 1:Dipel and Celastrus angulatus different ratio are to diamondback moth toxicity test result
Medicament LC50(mg/L) TTI ATI CTC
Dipel 3.67 - 100.0 -
Celastrus angulatus 2.14 - 171.5 -
Dipel: Celastrus angulatus=1: 5 1.70 159.6 215.4 135
Dipel: Celastrus angulatus=1: 4 1.84 157.2 199.6 127
Dipel: Celastrus angulatus=1: 3 1.91 153.6 192.0 125
Dipel: Celastrus angulatus=1: 2 1.79 147.7 205.3 139
Dipel: Celastrus angulatus=1: 1 1.90 135.8 192.8 142
Dipel: Celastrus angulatus=2: 1 2.22 123.8 164.7 133
Dipel: Celastrus angulatus=3: 1 2.43 117.9 150.9 128
Dipel: Celastrus angulatus=4: 1 2.28 114.3 161.2 141
Dipel: Celastrus angulatus=5: 1 2.41 111.9 152.2 136
Each ratio its co-toxicity coefficient of Dipel and Celastrus angulatus compounding is above 120 as can be seen from Table 1, says There is apparent synergistic effect after bright two kinds of ingredient compoundings, it can be seen that, the two compounding has very strong reasonability.
Table 2:Dipel and Celastrus angulatus different ratio are to cabbage caterpillar toxicity test result
Medicament LC50(mg/L) TTI ATI CTC
Dipel 2.89 - 100.0 -
Celastrus angulatus 1.93 - 149.7 -
Dipel: Celastrus angulatus=1: 5 1.62 178.2 141.4 126
Dipel: Celastrus angulatus=1: 4 1.59 181.7 139.8 130
Dipel: Celastrus angulatus=1: 3 1.64 175.7 137.3 128
Dipel: Celastrus angulatus=1: 2 1.56 185.1 133.1 139
Dipel: Celastrus angulatus=1: 1 1.62 178.5 124.9 143
Dipel: Celastrus angulatus=2: 1 1.84 157.4 116.6 135
Dipel: Celastrus angulatus=3: 1 2.07 139.4 112.4 124
Dipel: Celastrus angulatus=4: 1 1.98 146.2 109.9 133
Dipel: Celastrus angulatus=5: 1 1.89 152.7 108.3 141
Each ratio its co-toxicity coefficient of Dipel and Celastrus angulatus compounding is above 120 as can be seen from Table 2, says There is apparent synergistic effect after bright two kinds of ingredient compoundings, it can be seen that, the two compounding has very strong reasonability.
Embodiment 16:
The test of pesticide effectiveness of Dipel and Celastrus angulatus compounding
With the complex preparation of embodiment 1 to 8 gained of embodiment field medicine effect test is carried out with each component single dose.It selects calm The weather of no rain is tested, investigation all stage without rainfall, using diamondback moth and cabbage caterpillar as subjects, each dispenser Interval is 7d, altogether dispenser 3 times, and with 3d after last dispenser, 7d, 21d investigate diamondback moth and cabbage caterpillar respectively, and calculate preventive effect. Preventive effect is calculated as follows:
Control effect (%)=(1-TaCb/TbCa) × 100%
In formula:Ta is the individual amount survived after treatment region is prevented;Tb is the individual amount of survival before treatment region prevention;Ca The individual amount survived after being prevented for check plot;Ca is the individual amount of survival before the prevention of check plot.
Test result is as follows:
1, Dipel Celastrus angulatus composition is to diamondback moth field trial
Table 3:Control effect of the Dipel Celastrus angulatus composition to diamondback moth
As can be seen from Table 3, diamondback moth can be effectively prevented after Dipel and Celastrus angulatus compounding, control effect is excellent In comparison medicament, the lasting period is long, and 21d preventive effects are up to 89.4% or more after last dispenser, and are testing in scope of medication, to target Crop does not have poisoning.
2, Dipel Celastrus angulatus composition is to cabbage caterpillar field trial
Table 4:Control effect of the Dipel Celastrus angulatus composition to cabbage caterpillar
As can be seen from Table 4, cabbage caterpillar can be effectively prevented after Dipel and Celastrus angulatus compounding, control effect is excellent In comparison medicament, the lasting period is long, and 21d preventive effects are up to 88.2% or more after last dispenser, and are testing in scope of medication, to target Crop does not have poisoning.
In summary test result can be seen that after Dipel and Celastrus angulatus compound by different proportion, to agricultural The control effect of insect pest significantly improves, identical in control effect, greatly reduces the usage amount of active ingredient, to It reduces the harm to environment and has delayed the resistance of pest.

Claims (10)

1. a kind of composition pesticide containing Dipel and Celastrus angulatus, it is characterised in that:Active constituent is by Dipel It is formed with Celastrus angulatus, the mass ratio of the Dipel and Celastrus angulatus is 1: 5~5: 1.
2. a kind of composition pesticide containing Dipel and Celastrus angulatus according to claim 1, it is characterised in that:Institute The mass ratio for stating Dipel and Celastrus angulatus is 1: 4~5: 1.
3. a kind of composition pesticide containing Dipel and Celastrus angulatus according to claim 1, it is characterised in that:Institute The mass ratio for stating Dipel and Celastrus angulatus is 1: 3~5: 1.
4. a kind of composition pesticide containing Dipel and Celastrus angulatus according to claim 1, it is characterised in that:Institute The mass ratio for stating Dipel and Celastrus angulatus is 1: 2~5: 1.
5. a kind of composition pesticide containing Dipel and Celastrus angulatus according to claim 1, it is characterised in that:Institute The mass ratio for stating Dipel and Celastrus angulatus is 1: 1~5: 1.
6. a kind of composition pesticide containing Dipel and Celastrus angulatus according to claim 1, it is characterised in that:It should Also containing pesticidal preparations auxiliary element the dosage form for being suitble to agriculturally use is made in composition pesticide.
7. a kind of composition pesticide containing Dipel and Celastrus angulatus according to claim 6, it is characterised in that:Institute It is any one of wettable powder, water dispersible granules, dispersible oil-suspending agent to state dosage form.
8. a kind of composition pesticide containing Dipel and Celastrus angulatus according to claim 6, it is characterised in that:Institute It is auxiliary agent or/and filler to state pesticidal preparations auxiliary element.
9. a kind of composition pesticide containing Dipel and Celastrus angulatus according to claim 1, it is characterised in that:Institute It is 0.6%-10% to state the weight percent of Dipel and Celastrus angulatus weight summation in the composition pesticide.
10. a kind of composition pesticide containing Dipel and Celastrus angulatus according to claim 1, it is characterised in that: The weight percent of the Dipel and Celastrus angulatus weight summation in the composition pesticide is 0.6%-2.5%.
CN201810610576.8A 2018-06-12 2018-06-12 A kind of composition pesticide containing Dipel and Celastrus angulatus Pending CN108552224A (en)

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CN109430294A (en) * 2018-11-27 2019-03-08 中国农业科学院植物保护研究所 A method of prevention and treatment corn field mythimna separata

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* Cited by examiner, † Cited by third party
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CN1359622A (en) * 2002-01-21 2002-07-24 河北省食品企业发展公司 Composite biological agricultural chemical

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1359622A (en) * 2002-01-21 2002-07-24 河北省食品企业发展公司 Composite biological agricultural chemical

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109430294A (en) * 2018-11-27 2019-03-08 中国农业科学院植物保护研究所 A method of prevention and treatment corn field mythimna separata

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