CN108478446A - A kind of capsule face cream and the method for manufacturing the capsule face cream - Google Patents
A kind of capsule face cream and the method for manufacturing the capsule face cream Download PDFInfo
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- CN108478446A CN108478446A CN201810447142.0A CN201810447142A CN108478446A CN 108478446 A CN108478446 A CN 108478446A CN 201810447142 A CN201810447142 A CN 201810447142A CN 108478446 A CN108478446 A CN 108478446A
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- capsule
- layer
- gel
- dropper
- extract
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The invention discloses a kind of capsule face creams, including the double-deck capsule, the bilayer capsule includes the lipid layer being made of liposoluble constituent, the lipid layer is wrapped with the water quality layer being made of water soluble ingredient, the liposoluble constituent includes at least one surfactant before being contacted with the water soluble ingredient, the lipid layer and the water quality layer collectively constitute capsule core, the capsule core be wrapped with liquid polyelectrolyte reacted with gel-based solution made of gel shell, its advantage is that the surfactant with low concentration, to reduce the risk that skin sensitivity occurs for user;The invention also discloses a kind of methods of manufacture capsule face cream, this method is allowed to drippage and generates gel shell in gel-based solution after being squeezed out capsule core by the way of co-extrusion, it is simple and efficient its advantage is that this method implements, the double-deck capsule produced can effectively keep apart liposoluble constituent and water soluble ingredient, and generate the shell being wrapped in outside capsule core.
Description
Technical field
The present invention relates to a kind of capsule face creams and the method for manufacturing the capsule face cream, the face cream can be specifically used as skin
Nursing.
Background technology
Face cream is a kind of common skin-protection product, is mainly used for the nursing to face skin.Since the ingredient of face cream includes
Liposoluble constituent and water soluble ingredient, therefore usually require addition weight percent and ensure between the surfactant of 2%-5%
Liposoluble constituent and water soluble ingredient are fully merged.
But weight percent, between the addition of the surfactant of 2%-5%, be easy to cause user has this in use
Skin sensitivity is easy to happen when the skin care item of the surfactant of concentration, to influence usage experience.
Invention content
The object of the present invention is to provide a kind of capsule face creams, its advantage is that the surfactant with low concentration, to
Reduce the risk that skin sensitivity occurs for user.
The present invention above-mentioned technical purpose technical scheme is that:A kind of capsule face cream, including it is double
Layer capsule, for the diameter of the bilayer capsule between 2mm-5mm, the bilayer capsule includes gel shell, water quality layer and lipid
Layer;
The gel shell for wrapping up water quality layer and lipid layer, in the water quality layer containing be useful for skin care it is water-soluble at
Point, containing the liquid polyelectrolyte that can be reacted with multivalent ion in the water soluble ingredient, the gel shell is by the poly- electrolysis of liquid
Matter is reacted with gel-based solution to be made, and the gel-based solution contains multivalent ion,
The water quality layer is wrapped in the gel shell, and the lipid layer is wrapped in the water quality layer, is contained in the lipid layer
It is useful for nourishing the liposoluble constituent of skin, the liposoluble constituent includes at least one before contacting with the water soluble ingredient
Kind nonionic surfactant, the surfactant account for the weight percent of liposoluble constituent between 0.05%-0.3%.
Wherein, liposoluble constituent can be in a liquid state, can also journey gel state or emulsion form, but its viscosity should be less than
1800mPa.s;Water soluble ingredient can be in a liquid state, can also journey gel state or suspending agent form, but its viscosity should be less than
1600mPa.s。
Nonionic surfactant can be selected from fatty alcohol, alkyl glucoside, polysorbate or coconut oleoyl amine and surface
The molecular weight of activating agent is between 200g/mol-10000g/mol, and preferably, the molecular weight of surfactant between
Between 500g/mol-1000g/mol.
In all these applications, the gel shell of the double-deck capsule is usually made of the material compatible with human-body biological.For this purpose,
Biocompatible, biodegradable and in most cases nontoxic polymer can be used(Such as polysaccharide)To form shell.Favorably
Ground, the polymer can become particularly sticky state from the liquid of solution shape, ensure to institute in the double-deck capsule to be formed
Accommodate the gelinite that the machinery of liquid is kept.Under gel state, the individual chain of polyelectrolyte forms guarantor together with multivalent ion
The strict three dimensional network held liquid core and it is prevented to flow.Individual chain is mutually kept, and cannot freely be flowed each other.In the shape
Under state, it is infinity to be formed by gel viscosity.In addition, gel has the wealthy value of flow stress.The stress threshold values is more than 0.08Pa.
Elasticity modulus of the gel also with non-zero and more than 50kPa.
Therefore, alginates, pectin or gellan gum may be selected as polyelectrolyte.
So, the lipid layer that liposoluble constituent is formed is wrapped in interior, water quality by the water quality layer that water soluble ingredient is formed
Layer is wrapped with gel shell, and gel shell can make water quality layer and lipid layer and air insulated, to make in lipid layer and water quality layer
Active ingredient be not easy to contact and aoxidize with air.Further, since the addition of a small amount of surfactant, can effectively by
Water quality layer and lipid layer are kept apart, and the active ingredient in lipid layer and water quality layer is made to be not susceptible to react.But since surface is lived
Property agent account for the weight percent of liposoluble constituent between 0.05%-0.3%, far less than the concentration of most of face creams in the market
Ratio(The surfactant of higher concentration is easy to cause user and skin sensitivity occurs), and in contrast, non-ionic surface is lived
Property agent sensitization risk be less than cationic surfactant and anion surfactant, therefore can effectively reduce user hair
The risk of myogenic skin sensitivity, therefore the risk that skin sensitivity occurs for user can be effectively reduced.
The present invention is further arranged to:The liposoluble constituent includes Butyrospermum parkii fruit fat, isononyl isononanoate, cocounut oil
Alcohol-caprylate/decylate, thorn A Gan trees benevolence oil, tocopherol, the malt dregs of rice wax that gives up, horse fat, retinyl palmitate, lecithin and
Oleic acid.
Wherein, Butyrospermum parkii fruit fat is extracted from the fruit of Butyrospermum parkii, containing abundant unsaturated fatty acid,
The moisture-retaining capacity that can reinforce skin, the skin being damaged to dry skin, that is, cutin can be moistened.Product can be adjusted simultaneously
Mobility, improve viscosity, improve product organoleptic quality and use skin sense.Horse fat makes in cosmetics as skin conditioning agent
With.Horse fat is refined with the fat under horse-hair hair or at neck, and Japan is the first house oil application safety by refinement
The country of certification.Contain a large amount of linoleic acid in house oil, penetration is very strong.The component ratio of the ingredient and horse sweat of people's sweat
It is similar in the extreme, in addition to a small amount of " saturated fatty acids " forms layer protecting film, a large amount of unsaturated ingredient quilt in skin surface
Skin absorbs, especially must aliphatic acid effectively participate in the metabolic function of human skin tissue, the reparation to skin damage cell
Play the role of very important.Alpha-linolenic acid containing unsaturated fatty acid is no more than 1% in the general depot fat of animal, but
It is up to 15% or more containing alpha-linolenic acid and linoleic acid amount in horse fat, is rich in unsaturated fatty acid, stretchability is good, has lubrication to feel, energy
Promote the vitro tissues such as scalp, nail activity, there is good infiltration and nutritve function to skin and hair, belongs to trophism oil
Fat.
The present invention is further arranged to:In the liposoluble constituent percentage of capsule face cream total weight shared by each ingredient according to
It is secondary to be:Butyrospermum parkii fruit fat 3.3%-3.6%, isononyl isononanoate 3.1%-3.7%, lauric alcohol-caprylate/decylate 3.2%-
3.6%, thorn A Gan tree benevolence oil 1.1%-1.5%, tocopherol 1.2%-1.6%, the malt dregs of rice wax 1.3%-1.6% that gives up, horse fat 1.0%-1.5%,
Retinyl palmitate 1.1%-1.6%, lecithin 0.6%-1.2% and oleic acid 0.3%-1.7%.
The present invention is further arranged to:The water soluble ingredient includes isoprene, glycerine, C9-12 alkane, poly dimethyl
Siloxanes, niacinamide, collagen, biological carbohydrate gum -1, hydroxy decyl ubiquinone, saccharomycete lysis object, resists Butyrospermum parkii fruit fat extract
Bad hematic acid sodium phosphate, hydrolysis Sodium Hyaluronate, Radix Malvae sylvestris extract, leaf of Mentha piperita extract, cowslip extract, plumage
Clothing grass extract, veronica officinalis extract, sweet mary leaf extract, common milfoil extract, palmityl tripeptides -5, palmityl are few
Peptide, palmityl tetrapeptide -7, butanediol, tocopherol(Vitamin E), valine, threonine, glycine, glutamic acid, allantoin, mountain
Pears(Sugar)Alcohol and parahydroxyacet-ophenone.
The present invention is further arranged to:In the water soluble ingredient percentage of capsule face cream total weight shared by each ingredient according to
It is secondary to be:Isoprene 3.2%-3.6%, glycerine 3.1%-3.7%, C9-12 alkane 3.3%-3.6%, dimethyl silicone polymer 3.0%-
3.7%, Butyrospermum parkii fruit fat extract 3.3%-3.5%, niacinamide 1.4%-1.6%, collagen 1.2%-1.6%, biological carbohydrate gum -1
1.3%-1.6%, hydroxy decyl ubiquinone 1.2%-1.6%, saccharomycete lysis object 1.1%-1.6%, Sodium Ascorbyl Phosphate 1.4%-
1.7%, hydrolysis Sodium Hyaluronate 1.4%-1.8%, Radix Malvae sylvestris extract 1.2%-1.7%, leaf of Mentha piperita extract 1.1%-1.6%, Huang
Spend nine wheel grass extract 1.5%-1.7%, garment or robe made of feathers grass extract 1.1%-1.8%, veronica officinalis extract 1.0%-1.9%, fragrant bee
Floral leaf extract 1.0%-1.8%, common milfoil extract 1.1%-1.9%, -5 1.2%-1.6% of palmityl tripeptides, palmitoyl oligopeptide
1.3%-1.7%, -7 1.1%-1.7% of palmityl tetrapeptide, butanediol 1.2%-1.6%, tocopherol 1.2%-1.5%, valine 0.6%-
1.4%, threonine 0.3%-1.1%, glycine 0.4%-0.7%, glutamic acid 0.5%-1.6%, allantoin 0.4%-0.9%, sorb(Sugar)
Alcohol 0.7%-1.3% and parahydroxyacet-ophenone 0.5%-1.2%.
The purpose of the present invention is also providing a kind of method of manufacture capsule face cream, its advantage is that this method implements simple
Efficiently, the double-deck capsule produced can effectively keep apart liposoluble constituent and water soluble ingredient, and generate and be wrapped in
Shell outside capsule core.
The present invention above-mentioned technical purpose technical scheme is that:A kind of side of manufacture capsule face cream
Method includes the following steps:
A) liposoluble constituent is contained in the first syringe, water soluble ingredient is contained in the second syringe, described first
Syringe and the second syringe are connected with the downward opening double-deck dropper, and the bilayer dropper includes internal layer dropper and outer layer drop
Pipe, first syringe are connected with internal layer dropper, and second syringe is connected with outer layer dropper,
It is equipped with container below the bilayer dropper, gel-based solution is loaded in the container, is contained in the gel-based solution
The reactant of gelation reaction can occur with the polyelectrolyte in water soluble ingredient,
Surfactant is added into the liposoluble constituent;
B) liposoluble constituent is injected in internal layer dropper using first syringe, and in the outlet of the internal layer dropper
Place forms lipid layer drop, is injected the water soluble ingredient in outer layer dropper using second syringe, in the liposoluble
Property ingredient under the action of surfactant, the water soluble ingredient forms in the exit of the outer layer dropper and is wrapped in lipid
Water quality layer outside layer drop, the lipid layer and the water quality layer form capsule core;
C) capsule core being coextruded from the double-deck dropper is dripped in container due to the effect of gravity, and then described in immersing
In gel-based solution, keep the polyelectrolyte in the water quality layer and the reactant generation gelation in the gel-based solution anti-
It answers, to form the gel shell of package water quality layer outside water quality layer, the thickness of the gel shell is between the double-deck capsule diameter
Between 0.7% to 1.3%;
D) the made double-deck capsule of recycling.
Advantageously, the diameter of internal layer dropper is more than 0.8mm and substantially between 0.8mm and 1.6mm;Outer layer dropper
Diameter is at least bigger 0.3mm than internal layer dropper, advantageously big at least 0.5mm.The maximum gauge of outer layer dropper is less than 3mm.First note
The injection flow of emitter should control between 60ml/h and 80ml/h, and the injection flow of the second syringe should be controlled in the first injection
Device is injected between 0.05 to 0.15 times of flow.
The present invention is further arranged to:Weight percent of the polyelectrolyte in the face cream is between 0.7% and 1.6%
Between.
Advantageously, the individual chain of polyelectrolyte in the liquid state, which has, is more than 66000 grams/mol(g/mol)Mole matter
It measures, the three dimensional gel of contained polyelectrolyte locks moisture and surfactant in gel shell.
Advantageously, the clean property agent of anion, nonionic surfactant, cationic surfactant may be selected in surfactant
Or mixtures thereof, the molecular weight of surfactant between 200g/mol and l500g/mol, advantageously between 300g/mol and
Between 1000g/mol.Wherein, mass content of the surfactant in gel shell is more than 0.001 % and be advantageously greater than 0.1%.
The present invention is further arranged to:The gel-based solution contains multivalent ion, and the polyelectrolyte is energy and multivalence
Ionic reaction forms the polysaccharide of gel shell.
The present invention is further arranged to:The polysaccharide is gellan gum.
The present invention is further arranged to:The surfactant is nonionic surfactant.Wherein, non-ionic surface is lived
Property agent can be the polyoxyethylene deriv and/or polyoxypropylene derivatives for example expected selected from fatty alcohol, aliphatic acid or a heatable brick bed base,
Or selected from fragrant phenol, a heatable brick bed base glucose former times, poly- sorb vinegar or coconut oleoyl amine.
In conclusion the invention has the advantages that:
1, surfactant concentration is relatively low, and user is not susceptible to skin sensitivity;
2, it implements and is simple and efficient, effectively liposoluble constituent and water soluble ingredient can be isolated for the double-deck capsule produced
It comes, and generates the shell being wrapped in outside capsule core.
Description of the drawings
Fig. 1 is the process schematic for manufacturing capsule face cream;
Fig. 2 is the double-deck capsule structure schematic diagram in Fig. 1;
In figure, 1, the double-deck capsule;11, lipid layer;12, liposoluble constituent;13, water quality layer;14, water soluble ingredient;15, gel
Shell;16, capsule core;2, the first syringe;3, the second syringe;4, the double-deck dropper;41, internal layer dropper;42, outer layer dropper;5、
Container;51, gel-based solution.
Specific implementation mode
In order to which the present invention is further explained and its advantage, following specific examples is provided, it should be understood that they are used only as
Example is by no means limitative.In the next embodiment, unless otherwise specified, all parts and percentages are by weight
Amount provides.
Embodiment:A kind of capsule face cream, as depicted in figs. 1 and 2, the formula provided according to table 1 prepares of the present invention
Capsule face cream:
Table 1
Processing:
(1)By weighed water, isoprene, glycerine, C9-12 alkane, dimethyl silicone polymer, Butyrospermum parkii fruit fat extract,
Niacinamide, collagen, biological carbohydrate gum -1, hydroxy decyl ubiquinone, saccharomycete lysis object, Sodium Ascorbyl Phosphate, hydrolysis hyaluronic acid
Sodium, Radix Malvae sylvestris extract, leaf of Mentha piperita extract, cowslip extract, garment or robe made of feathers grass extract, veronica officinalis extraction
Object, sweet mary leaf extract, common milfoil extract, palmityl tripeptides -5, palmitoyl oligopeptide, palmityl tetrapeptide -7, butanediol, life
Educate phenol(Vitamin E), valine, threonine, glycine, glutamic acid, allantoin, sorb(Sugar)Alcohol, parahydroxyacet-ophenone are mounted in
100 milliliters of beakers(Container 5A)In;
(2)By container 5A with high-rate of shear(1000-1200rpm)Continuous homogenization 5-7 minutes;
(3)14 solution of water soluble ingredient made of recycling;
(4)By weighed Butyrospermum parkii fruit fat, isononyl isononanoate, lauric alcohol-caprylate/decylate, thorn A Gan trees benevolence it is oily,
Tocopherol(Vitamin E), useless malt dregs of rice wax, horse fat, retinyl palmitate, lecithin, oleic acid be mounted in 100 milliliters of beakers(Hold
Device 5B)In;
(5)By container 5B with high-rate of shear(1000-1200rpm)Continuous homogenization 10-15 minutes;
(6)12 solution of liposoluble constituent made of recycling.
A method of manufacture capsule face cream includes the following steps as depicted in figs. 1 and 2:
A) liposoluble constituent 12 is contained in the first syringe 2, water soluble ingredient 14 is contained in the second syringe 3, the
One syringe 2 and the second syringe 3 are connected with the downward opening double-deck dropper 4, and the double-deck dropper 4 includes internal layer dropper 41 and outer layer
Dropper 42, the first syringe 2 are connected with internal layer dropper 41, and the second syringe 3 is connected with outer layer dropper 42,
4 lower section of the double-deck dropper is equipped with container 5, and gel-based solution 51 is loaded in container 5, contains energy and water in gel-based solution 51
The reactant of gelation reaction occurs for the polyelectrolyte in soluble components 14,
Surfactant is added into liposoluble constituent 12;
B) the first syringe 2 is used to inject liposoluble constituent 12 in internal layer dropper 41, and in the exit shape of internal layer dropper 41
At 11 drop of lipid layer, water soluble ingredient 14 is injected in outer layer dropper 42 using the second syringe 3, in liposoluble constituent 12
Under the action of surfactant, water soluble ingredient 14 is formed in the exit of outer layer dropper 42 and is wrapped in outside 11 drop of lipid layer
Water quality layer 13, lipid layer 11 and water quality layer 13 form capsule core 16;
C) from the capsule core 16 being coextruded in the double-deck dropper 4 since the effect of gravity is dripped in container 5, and then immersion precipitation
Change in solution 51, makes the polyelectrolyte in water quality layer 13 that gelation reaction occur with the reactant in gel-based solution 51, to
The gel shell 15 of package water quality layer 13 is formed outside water quality layer 13, the thickness of gel shell 15 is between 1 diameter of the double-deck capsule
Between 0.7% to 1.3%;
D) the made double-deck capsule 1 of recycling.
Advantageously, the diameter of internal layer dropper 41 is more than 0.8mm and substantially between 0.8mm and 1.6mm;Outer layer dropper
42 diameter is at least bigger 0.3mm than internal layer dropper 41, advantageously big at least 0.5mm.The maximum gauge of outer layer dropper 42 is less than
3mm.The injection flow of first syringe 2 should control between 60ml/h and 80ml/h, and the injection flow of the second syringe 3 should be controlled
It makes between 0.05 to 0.15 times that the first syringe 2 injects flow.
The present invention is further arranged to:Weight percent of the polyelectrolyte in Essence is between 0.7% and 1.6%.
Advantageously, the individual chain of polyelectrolyte in the liquid state, which has, is more than 66000 grams/mol(g/mol)Mole matter
It measures, the three dimensional gel of contained polyelectrolyte locks moisture and surfactant in gel shell 15.
Advantageously, the clean property agent of anion, nonionic surfactant, cationic surfactant may be selected in surfactant
Or mixtures thereof, the molecular weight of surfactant is between 200g/mol and l500g/mol, advantageously between 300g/mol
Between 1000g/mol.Wherein, mass content of the surfactant in gel shell 15 be more than 0.001 % and be advantageously greater than
0.1%。
The present invention is further arranged to:Gel-based solution 51 contains multivalent ion, and polyelectrolyte is can be anti-with multivalent ion
The polysaccharide of gel shell 15 should be formed.
The present invention is further arranged to:Polysaccharide is gellan gum.
The present invention is further arranged to:Surfactant is nonionic surfactant.Wherein, nonionic surfactant
It can be the polyoxyethylene deriv and/or polyoxypropylene derivatives for example expected selected from fatty alcohol, aliphatic acid or a heatable brick bed base, or choosing
From fragrant phenol, a heatable brick bed base glucose former times, poly- sorb vinegar or coconut oleoyl amine.
This specific embodiment is only explanation of the invention, is not limitation of the present invention, people in the art
Member can as needed make the present embodiment the modification of not creative contribution after reading this specification, but as long as at this
It is all protected by Patent Law in the right of invention.
Claims (10)
1. a kind of capsule face cream, it is characterized in that:Including the double-deck capsule (1), the diameter of the bilayer capsule (1) is between 2mm-5mm
Between, the bilayer capsule (1) includes gel shell (15), water quality layer (13) and lipid layer (11);
The gel shell (15) contains in the water quality layer (13) for wrapping up water quality layer (13) and lipid layer (11) and is useful for skin
The water soluble ingredient (14) of nursing, the polyelectrolyte containing liquid in the water soluble ingredient (14), the gel shell (15) by
Liquid polyelectrolyte is reacted with gel-based solution (51) to be made,
The water quality layer (13) is wrapped in the gel shell (15), and the lipid layer (11) is wrapped in the water quality layer (13)
It is interior, in the lipid layer (11) containing be useful for nourish skin liposoluble constituent (12), the liposoluble constituent (12) with institute
Before stating water soluble ingredient (14) contact the weight of liposoluble constituent is accounted for comprising at least one surfactant, the surfactant
Percentage is measured between 0.05%-0.3%.
2. a kind of capsule face cream according to claim 1, it is characterized in that:The liposoluble constituent (12) includes Butyrospermum parkii
Fruit fat, lauric alcohol-caprylate/decylate, thorn A Gan trees benevolence oil, tocopherol, useless malt dregs of rice wax, horse fat, regards isononyl isononanoate
Flavol palmitate, lecithin and oleic acid.
3. a kind of capsule face cream according to claim 2, it is characterized in that:In the liposoluble constituent (12) shared by each ingredient
The percentage of capsule face cream total weight is followed successively by:Butyrospermum parkii fruit fat 3.3%-3.6%, isononyl isononanoate 3.1%-3.7%, cocounut oil
Alcohol-caprylate/decylate 3.2%-3.6%, thorn A Gan tree benevolence oil 1.1%-1.5%, tocopherol 1.2%-1.6%, useless malt dregs of rice wax
1.3%-1.6%, horse fat 1.0%-1.5%, retinyl palmitate 1.1%-1.6%, lecithin 0.6%-1.2% and oleic acid 0.3%-
1.7%。
4. a kind of capsule face cream according to claim 1, it is characterized in that:The water soluble ingredient (14) includes isoamyl two
Alcohol, glycerine, C9-12 alkane, dimethyl silicone polymer, Butyrospermum parkii fruit fat extract, niacinamide, collagen, biological carbohydrate gum -1, hydroxyl
Decyl ubiquinone, saccharomycete lysis object, Sodium Ascorbyl Phosphate, hydrolysis Sodium Hyaluronate, Radix Malvae sylvestris extract, leaf of Mentha piperita carry
Take object, cowslip extract, garment or robe made of feathers grass extract, veronica officinalis extract, sweet mary leaf extract, common milfoil extraction
Object, palmityl tripeptides -5, palmitoyl oligopeptide, palmityl tetrapeptide -7, butanediol, tocopherol(Vitamin E), valine, threonine,
Glycine, glutamic acid, allantoin, sorb(Sugar)Alcohol and parahydroxyacet-ophenone.
5. a kind of capsule face cream according to claim 4, it is characterized in that:In the water soluble ingredient (14) shared by each ingredient
The percentage of capsule face cream total weight is followed successively by:Isoprene 3.2%-3.6%, glycerine 3.1%-3.7%, C9-12 alkane 3.3%-
3.6%, dimethyl silicone polymer 3.0%-3.7%, Butyrospermum parkii fruit fat extract 3.3%-3.5%, niacinamide 1.4%-1.6%, collagen
Albumen 1.2%-1.6%, biological -1 1.3%-1.6% of carbohydrate gum, hydroxy decyl ubiquinone 1.2%-1.6%, saccharomycete lysis object 1.1%-1.6%,
It is Sodium Ascorbyl Phosphate 1.4%-1.7%, hydrolysis Sodium Hyaluronate 1.4%-1.8%, Radix Malvae sylvestris extract 1.2%-1.7%, peppery thin
Lotus Leafextract 1.1%-1.6%, cowslip extract 1.5%-1.7%, garment or robe made of feathers grass extract 1.1%-1.8%, medicinal grandmother
Receive extract 1.0%-1.9%, sweet mary leaf extract 1.0%-1.8%, common milfoil extract 1.1%-1.9%, palmityl tripeptides -5
1.2%-1.6%, palmitoyl oligopeptide 1.3%-1.7%, -7 1.1%-1.7% of palmityl tetrapeptide, butanediol 1.2%-1.6%, tocopherol
1.2%-1.5%, valine 0.6%-1.4%, threonine 0.3%-1.1%, glycine 0.4%-0.7%, glutamic acid 0.5%-1.6%, urine
Bursin 0.4%-0.9%, sorb(Sugar)Alcohol 0.7%-1.3% and parahydroxyacet-ophenone 0.5%-1.2%.
6. a kind of method of manufacture capsule face cream, includes the following steps:
A) liposoluble constituent (12) is contained in the first syringe (2), water soluble ingredient (14) is contained in the second syringe
(3) in, first syringe (2) and the second syringe (3) are connected with the downward opening double-deck dropper (4), the double-deck drop
It includes internal layer dropper (41) and outer layer dropper (42) to manage (4), and first syringe (2) is connected with internal layer dropper (41), institute
The second syringe (3) is stated with outer layer dropper (42) to be connected,
It is equipped with container (5) below the bilayer dropper (4), gel-based solution (51), the gel are loaded in the container (5)
Change the reactant for containing in solution (51) and gelation reaction capable of occurring with the polyelectrolyte in water soluble ingredient (14),
To addition surfactant in the liposoluble constituent (12);
B) liposoluble constituent (12) is injected in internal layer dropper (41) using first syringe (2), and described interior
The exit of layer dropper (41) forms lipid layer (11) drop, using second syringe (3) by the water soluble ingredient
(14) in injection outer layer dropper (42), in the liposoluble constituent (12) under the action of surfactant, it is described it is water-soluble at
(14) are divided to form the water quality layer (13) being wrapped in outside lipid layer (11) drop in the exit of the outer layer dropper (42), it is described
Lipid layer (11) and the water quality layer (13) composition capsule core (16);
C) from the double-deck middle capsule core (16) being coextruded of dropper (4) since the effect of gravity is dripped in container (5), into
And immerse in the gel-based solution (51), make in polyelectrolyte and the gel-based solution (51) in the water quality layer (13)
Reactant gelation reaction occurs, to form the gel shell (15) of package water quality layer (13), institute outside the water quality layer (13)
The thickness of gel shell (15) is stated between the 0.7% to 1.3% of the double-deck capsule (1) diameter;
D) the made double-deck capsule (1) of recycling.
7. a kind of method of manufacture capsule face cream according to claim 6, it is characterized in that:The polyelectrolyte is in the face
Weight percent in frost is between 0.7% and 1.6%.
8. a kind of method of manufacture capsule face cream according to claim 7, it is characterized in that:The gel-based solution (51) contains
It is that the polysaccharide to form gel shell (15) can be reacted with multivalent ion to have multivalent ion, the polyelectrolyte.
9. a kind of method of manufacture capsule face cream according to claim 8, it is characterized in that:The polysaccharide is gellan gum.
10. according to a kind of method of any manufacture capsule face creams of claim 6-9, it is characterized in that:The surface-active
Agent is nonionic surfactant.
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Cited By (1)
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CN110876712A (en) * | 2019-11-15 | 2020-03-13 | 金迪 | Preparation method of ointment for moistening skin and resisting tinea pedis |
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CN102300564A (en) * | 2008-12-01 | 2011-12-28 | 卡普苏姆公司 | Method for manufacturing capsule series, and related capsule series |
FR2964017A1 (en) * | 2010-09-01 | 2012-03-02 | Capsum | Fabricating a series of capsules comprises conveying in double casing of first and second liquid solution, forming a series of drops, falling each drop in a gas volume of gas at outlet of the casing and immersing drop in a gelling solution |
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CN102300564A (en) * | 2008-12-01 | 2011-12-28 | 卡普苏姆公司 | Method for manufacturing capsule series, and related capsule series |
US20120003285A1 (en) * | 2008-12-01 | 2012-01-05 | Capsum | Method for manufacturing capsule series, and related capsule series |
FR2964017A1 (en) * | 2010-09-01 | 2012-03-02 | Capsum | Fabricating a series of capsules comprises conveying in double casing of first and second liquid solution, forming a series of drops, falling each drop in a gas volume of gas at outlet of the casing and immersing drop in a gelling solution |
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