CN108451816A - A kind of inhibiting bacteria and diminishing inflammation acne-removing composition - Google Patents
A kind of inhibiting bacteria and diminishing inflammation acne-removing composition Download PDFInfo
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- CN108451816A CN108451816A CN201810353333.0A CN201810353333A CN108451816A CN 108451816 A CN108451816 A CN 108451816A CN 201810353333 A CN201810353333 A CN 201810353333A CN 108451816 A CN108451816 A CN 108451816A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses a kind of inhibiting bacteria and diminishing inflammation acne-removing compositions, include the ingredient of following mass percent：Radix Wikstroemae extract 0.5 10%, cotton rose leaf extract 0.1 6%, maniod ebish flower extract 0.1 6%.The present composition adds plant component brother king extract, cotton rose leaf extract, maniod ebish flower extract synergy, effectively plays bacteriostasis, to effectively inhibit inflammatory reaction, effective anti-inflammatory, and realizes the purpose of anti-acne.
Description
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of inhibiting bacteria and diminishing inflammation acne-removing composition.
Background technology
Acne is being commonly called as acne, is called " whelk ", " dark sore " or " acne ", is that one kind of pilosebaceous unit is chronic
Inflammatory dermatoses, the performance of small pox are sent out from gently to being hoary hair's blackhead, inflamed papules and warts, tumour and tubercle again
Small pox that is red and suppurating is that have existing for bacterium infection.
Sebum secretion is vigorous easily to put aside dirt, especially fat-soluble organic substance and perhaps multiple-microorganism, and induces scorching
Disease and infection.Pore is coarse, is easy to cause bacterium, fungi, virus etc. that can drive straight in, and causes infection, so as to cause inflammation
Reaction, small pox generate.
Invention content
The technical problem to be solved in the present invention is to provide a kind of inhibiting bacteria and diminishing inflammation acne-removing compositions.Present composition addition is planted
Object ingredient brother king extract, cotton rose leaf extract, maniod ebish flower extract are synergistic, effectively play bacteriostasis, to
Effectively inhibit inflammatory reaction, effective anti-inflammatory, and realizes the purpose of anti-acne.
To achieve the above object, the present invention provides following scheme：
A kind of inhibiting bacteria and diminishing inflammation acne-removing composition, includes the ingredient of following mass percent：Radix Wikstroemae extract 0.5-10%,
Cotton rose leaf extract 0.1-6%, maniod ebish flower extract 0.1-6%.
Further, the composition includes the ingredient of following mass percent：Radix Wikstroemae extract 0.8-8%, wood
Folium Hibisci Mutabilis extract 0.5-5%, maniod ebish flower extract 0.5-5%.
Further, the composition, which is characterized in that include the ingredient of following mass percent：Wikstroemia indica carries
Take object 4.5%, cotton rose leaf extract 3%, maniod ebish flower extract 3%.
A kind of inhibiting bacteria and diminishing inflammation acne-removing composition, the preparation method of the Radix Wikstroemae extract：By Wikstroemia indica clean dry, powder
It is broken to cross 20-40 mesh sieve, according to solid-liquid ratio 1：Petroleum ether is added in 5-10, and water-bath refluxing extraction 2-3h is discarded until petroleum ether is in colourless
Petroleum ether layer；After volatilizing petroleum ether, then press solid-liquid ratio 1:Ethyl acetate water-bath refluxing extraction is added to colourless, merging extraction in 5-10
Ethyl acetate extract is concentrated to dryness by liquid, is set in vacuum drying chamber and is dried to constant weight.
A kind of inhibiting bacteria and diminishing inflammation acne-removing composition, the preparation method of the cotton rose leaf extract：Preparation method：By cotton rose
Leaf clean dry crushed 20-40 mesh sieve, according to solid-liquid ratio 1：Refluxing extraction 3 times after 5-15 addition 70-90% ethyl alcohol, every time
1-3h, merging filtrate is through reduced pressure and vacuum drying.
A kind of inhibiting bacteria and diminishing inflammation acne-removing composition, the preparation method of the maniod ebish flower extract：Preparation method is：By yellow another name for Sichuan Province
Sunflower is dried and crushed into powder, according to solid-liquid ratio 1：10-20 is added 60-85% alcohol refluxs and extracts 3 times, each 0.5-1h, merges
It is concentrated through Rotary Evaporators after filtrate, vacuum freeze drying.
The present invention also provides the compositions can be used for cosmetics, wherein the composition can be used as additive use
In the preparation of inhibiting bacteria and diminishing inflammation anti-acne facial cleanser.
The present invention also provides a kind of inhibiting bacteria and diminishing inflammation anti-acne facial cleansers, further include the ingredient of following mass percent：Spiny dogfish
Alkane 1-5%, cetostearyl alcohol 1.8-2.2%, dimethyl silicone polymer 2-6%, sodium lauryl sulfate 1-3%, alkyl sulfate
2-6%, myristic acid 1-3%, PEG-20 methyl sesquistearate 1.5-3%, carbomer 0.2-0.8%, xanthans
0.02-0.06%, Phenoxyethanol 0.01-0.02%, methyl hydroxybenzoate 0.01-0.02%, Nipasol 0.01-0.02%, glycerine
5-20%, potassium hydroxide 0.02-0.3%, stearic acid 1-3%, deionized water surplus.
Compared with prior art, the invention has the advantages that：
(1) of the invention by three kinds of Radix Wikstroemae extract, cotton rose leaf extract, maniod ebish flower extract natural plant compositions
Reasonable compatibility is carried out, scientific matching makes different effective active compositions generate synergistic function, substantially increases active constituent
Utilization rate.(2) present invention has the bacteriostasis efficacy of wide spectrum, while can effectively inhibit inflammation related substances, and it is logical to reduce blood vessel
Permeability prevents inflammation from spreading, and protecting cell surface not leads to inflammation caused by a large amount of residuals because of a large amount of microbial reproductions
Disease, to achieve the purpose that anti-acne.(3) present composition is green safe, mildly non-stimulated to human skin, and preparation process
Simply, industrialized production is adapted to.
Specific implementation mode
To make the object, technical solutions and advantages of the present invention clearer, embodiment of the present invention will be made into one below
Step ground detailed description, embodiments of the present invention are not limited thereto, for not specifically specified technological parameter or condition, can refer to
Routine techniques carries out.
Involved each ingredient is described as follows in composition of the present invention：
Wikstroemia indica is that Thymelaeceae tabernaemontanus bulrush flower belongs to the dry root that Nanling small cup spends Wikstroemia indices (L.) C.A.Mey.
Skin, taste bitter and cold, micro-pungent cure mainly traumatic injury, relieve fatigue and ease pain；It is distributed in Jiangxi, Zhejiang, Hunan, Guangdong, the Guangxi rivers Deng Di,
For civil common Chinese herbal medicine.Modern pharmacology and clinical research show that Wikstroemia indica has anti-inflammatory, removing toxic substances, analgesia and other effects, for controlling
Treat the diseases such as bronchitis, pneumonia, tonsillitis, mastitis, cellulitis.Extracorporeal bacteria inhibitor test shows Wikstroemia indica piece to B-mode
Hemolytic streptococcus, Diplococcus pneumopniae, staphylococcus aureus, Pseudomonas aeruginosa and Escherichia coli have stronger bacteriostasis,
Bacteriostasis efficacy with wide spectrum.In addition, Wikstroemia indica has apparent resist inflammation on repercussive function to general acute inflammation, to chemical factor
It is pain caused to have analgesic activity.
Cottonrose hibiscus leaf is the leaf of malvaceae plant cotton rose.Acrid flavour is flat, nontoxic, cool blood, removing toxic substances, analgesic.Containing glycosides displayed, phenol
The ingredients such as class, amino acid, tannin, reduced sugar, main chemical compositions are glycosides displayed, including dry measure used in former times skin glucoside, different dry measure used in former times skin glucoside, Hypericum Chinense
Glucoside and spiraeoside and anthocyanin etc..These flavonoid glycoside substances cross multipotency in physical peroxide and are converted into antioxidant, to
It can be eliminated with peroxide reactions.Meanwhile cotton rose flavones can inhibit inflammation related substances, reducing vasopermeability prevents inflammation
Diffusion, while cell surface being protected not lead to inflammation caused by a large amount of residuals because of a large amount of microbial reproductions, while energy
Enhance immune system, reduce the generation of inflammation, inhibits acne to achieve the purpose that reduce.
Sunset abelmoschus root is Malvaceae Abelmoschus 1 year to herbaceos perennial, written by Song Dynasty palm Yu's tin《Jia Youben
Grass》, history tree is on the books thereafter, and records in each version《Pharmacopoeia of People's Republic of China》.Main chemical compositions are flavones
The compounds such as class, organic acid, tannins and long-chain hydro carbons.Have the function of clearing heat and promoting diuresis, subdhing swelling and detoxicating, blood activating and promoting tissue regeneration etc..It is yellow
Hollyhock flavones can effectively enhance activities of antioxidant enzymes, and related to concentration, there is certain degree of controllability, can stability contorting region of interest oxygen
Change reduction balance.Meanwhile for local inflammation factor content excessively to generate the case where inflammation shows variola, sunset abelmoschus root is yellow
Ketone effectively can inhibit inflammatory factor to increase, and gradually reduce abnormal immune response intensity, to solve the problems, such as local variola.
Embodiment 1
A kind of inhibiting bacteria and diminishing inflammation anti-acne facial cleanser, includes the ingredient of following mass percent：Radix Wikstroemae extract 0.8%, wood
Folium Hibisci Mutabilis extract 0.5%, maniod ebish flower extract 0.5%, saualane 2%, cetostearyl alcohol 1.8%, polydimethylsiloxanes
Alkane 3%, sodium lauryl sulfate 1.5%, alkyl sulfate 3%, myristic acid 1.5%, PEG-20 methyl sesquialter stearic acid
Ester 2%, carbomer 0.4%, xanthans 0.03%, Phenoxyethanol 0.01%, methyl hydroxybenzoate 0.01%, Nipasol 0.01%,
Glycerine 8%, potassium hydroxide 0.15%, stearic acid 1.5%, deionized water surplus.
Embodiment 2
A kind of inhibiting bacteria and diminishing inflammation anti-acne facial cleanser, includes the ingredient of following mass percent：Radix Wikstroemae extract 8%, the wooden cottonrose hibiscus
Rong's leaf extract 5%, maniod ebish flower extract 5%, saualane 4%, cetostearyl alcohol 2%, dimethyl silicone polymer 5%, sulphur
Sour sodium laurate 2.5%, alkyl sulfate 5%, myristic acid 2.5%, PEG-20 methyls sesquistearate 2.5%,
Carbomer 0.7%, xanthans 0.05%, Phenoxyethanol 0.02%, methyl hydroxybenzoate 0.02%, Nipasol 0.02%, glycerine
18%, potassium hydroxide 0.25%, stearic acid 2.5%, deionized water surplus.
Embodiment 3
A kind of inhibiting bacteria and diminishing inflammation anti-acne facial cleanser, includes the ingredient of following mass percent：Radix Wikstroemae extract 4.5%, wood
Folium Hibisci Mutabilis extract 3%, maniod ebish flower extract 3%, saualane 3%, cetostearyl alcohol 2%, dimethyl silicone polymer 4%,
Sodium lauryl sulfate 2%, alkyl sulfate 4%, myristic acid 2%, PEG-20 methyls sesquistearate 2.5%, card
Wave nurse 0.5%, xanthans 0.04%, Phenoxyethanol 0.01%, methyl hydroxybenzoate 0.01%, Nipasol 0.01%, glycerine 12%,
Potassium hydroxide 0.2%, stearic acid 2%, deionized water surplus.
Embodiment 4
A kind of inhibiting bacteria and diminishing inflammation anti-acne facial cleanser, includes the ingredient of following mass percent：Radix Wikstroemae extract 10%, the wooden cottonrose hibiscus
Rong's leaf extract 6%, maniod ebish flower extract 6%, saualane 5%, cetostearyl alcohol 2.2%, dimethyl silicone polymer 6%,
Sodium lauryl sulfate 3%, alkyl sulfate 6%, myristic acid 3%, PEG-20 methyls sesquistearate 3%, card wave
Nurse 0.8%, xanthans 0.06%, Phenoxyethanol 0.02%, methyl hydroxybenzoate 0.02%, Nipasol 0.02%, glycerine 20%, hydrogen
Potassium oxide 0.3%, stearic acid 3%, deionized water surplus.
Embodiment 5
A kind of inhibiting bacteria and diminishing inflammation anti-acne facial cleanser, includes the ingredient of following mass percent：Radix Wikstroemae extract 0.5%, wood
Folium Hibisci Mutabilis extract 0.1%, maniod ebish flower extract 0.1%, saualane 1%, cetostearyl alcohol 1.8%, polydimethylsiloxanes
Alkane 2%, sodium lauryl sulfate 1%, alkyl sulfate 2%, myristic acid 1%, PEG-20 methyl sesquistearates
1.5%, carbomer 0.2%, xanthans 0.02%, Phenoxyethanol 0.01%, methyl hydroxybenzoate 0.01%, Nipasol 0.01%,
Glycerine 5%, potassium hydroxide 0.02%, stearic acid 1%, deionized water surplus.
A kind of preparation method of inhibiting bacteria and diminishing inflammation anti-acne facial cleanser is in embodiment 1-5：(1) by saualane, cetostearyl alcohol,
Dimethyl silicone polymer, myristic acid, sodium lauryl sulfate, alkyl sulfate, PEG-20 methyl sesquistearates are mixed
Conjunction is heated to 80 DEG C, and A phases are made；(2) by carbomer, xanthans, methyl hydroxybenzoate, Nipasol, glycerine, stearic acid, deionization
Water is mixed and heated to 80 DEG C, and B phases are made；(3) A is added to B phases, C phases are made in emulsifying homogeneous 5min, insulated and stirred 20min；
(4) C phases are cooled to 45 DEG C, Radix Wikstroemae extract, cotton rose leaf extract, maniod ebish flower extract, Phenoxyethanol, hydrogen is added
Potassium oxide stirs evenly, discharging.
Comparative example 1
Difference lies in Radix Wikstroemae extract is not added with embodiment 1.
Comparative example 2
Difference lies in cotton rose leaf extract is not added with embodiment 1.
Comparative example 3
Difference lies in maniod ebish flower extract is not added with embodiment 1.
Comparative example 4
Difference lies in the composition includes the ingredient of following mass percent with embodiment 1：Radix Wikstroemae extract
10.1%, cotton rose leaf extract 6.1%, maniod ebish flower extract 6.1%.
Efficacy validation
Bacterium bacteriostasis efficacy is verified
For trying strain：Staphylococcus aureus, Escherichia coli, propionibacterium acnes
Culture medium and condition of culture：Nutrient agar (36 ± 1 DEG C of incubator 48 ± 2h of culture, for golden yellow grape
Coccus, Escherichia coli culture), cooked meat medium (be used for propionibacterium acnes culture).
Table 1：Each embodiment, comparative example, blank sample to the antibacterial circle diameter of bacterium ( N=6)
Composition Radix Wikstroemae extract, cotton rose leaf extract, the maniod ebish flower extract of the present invention known to 1 data of table
Compounding significantly inhibits bacterium, and inhibition zone is apparent.
Fungi inhibits efficacy validation
For trying strain：Aspergillus niger, aspergillus flavus, Trichoderma viride
Culture medium and condition of culture：Nutrient agar (27 ± 1 DEG C of 48 ± 2h of insulating box culture).
Test method：With reference to National Standard of the People's Republic of China GB15797-2002, " Disposable Sanitary Accessory is defended
Appendix C 4 " stripping property resists (suppression) bacterium product bacteriostasis property test method " in raw standard ".
Formula：X=(A-B)/A × 100%
In formula:X --- bacteriostasis rate, %
A --- control sample averagely recycles bacterium colony；
B --- test specimen averagely recycles bacterium colony.
Table 2：Each embodiment, comparative example to the inhibiting rate of fungi (N=3)
Composition Radix Wikstroemae extract, cotton rose leaf extract, the maniod ebish flower extract of the present invention known to 2 data of table
Compounding significantly inhibits fungi, and bacteriostasis rate is higher.
The composition Radix Wikstroemae extract, cotton rose leaf extract of the present invention, sunset abelmoschus root known to table 1,2 data analysis of table
Flower extract compounding has synergistic function, can play significant fungistatic effect.
Efficacy assessments
600 volunteers are selected, per each 50 triers of test group.The suppression prepared using embodiment 1-5, comparative example 1-4
Bacterium anti-inflammatory anti-acne facial cleanser, the daily morning and evening face cleaning of participant are used 1 time, are persistently used 1 month.It must not be used in experimentation
Its any skin-protection product, and subject has been fully completed verification process, and experimental result is shown in Table 3, and effect divides three grades：
Anti-inflammatory anti-acne effect is apparent：Anti-inflammatory anti-acne effect is apparent, and improvement skin inflammatory reaction is with obvious effects, not red and swollen, nothing
Feeling of pain, small pox removal；
Anti-inflammatory anti-acne effect is general：Anti-inflammatory anti-acne effect is general, and improvement skin inflammatory reaction effect is general, and skin inflammation is anti-
There should be mitigation, a little red and swollen, feeling of pain, small pox disappears small；
Anti-inflammatory anti-acne effect unobvious：Scytitis reaction, small pox without improvement, scytitis, long acne situation with it is poor before
Not less, feel without apparent after.
3 each embodiment of table, comparative example using effect
The inhibiting bacteria and diminishing inflammation anti-acne that the embodiment of the present invention is provided is can be seen that from the result of the self-assessment of trier to wash one's face
Milk has the effect of most trier's skin preferably to improve skin inflammatory reaction, anti-acne, realizes the mesh of inhibiting bacteria and diminishing inflammation anti-acne
's.
The present invention is described by way of example above, but the present invention is not limited to above-mentioned specific embodiment, all to be based on
Any changes or modifications that the present invention is done belong to the scope of protection of present invention.
Claims (9)
1. a kind of inhibiting bacteria and diminishing inflammation acne-removing composition, which is characterized in that include the ingredient of following mass percent：Radix Wikstroemae extract
0.5-10%, cotton rose leaf extract 0.1-6%, maniod ebish flower extract 0.1-6%.
2. composition as described in claim 1, which is characterized in that include the ingredient of following mass percent：Wikstroemia indica extracts
Object 0.8-8%, cotton rose leaf extract 0.5-5%, maniod ebish flower extract 0.5-5%.
3. composition as described in claim 1, which is characterized in that include the ingredient of following mass percent：Wikstroemia indica extracts
Object 4.5%, cotton rose leaf extract 3%, maniod ebish flower extract 3%.
4. composition as described in any one of claims 1-3, which is characterized in that the preparation method of the Radix Wikstroemae extract：
By Wikstroemia indica clean dry, 20-40 mesh sieve is crushed, according to solid-liquid ratio 1：5-10 addition petroleum ethers, water-bath refluxing extraction 2-3h,
It is in colourless to petroleum ether, discards petroleum ether layer；After volatilizing petroleum ether, then press solid-liquid ratio 1:Ethyl acetate water-bath reflux is added in 5-10
Extraction merges extracting solution, ethyl acetate extract is concentrated to dryness to colourless, sets in vacuum drying chamber and dries to constant weight.
5. composition as described in any one of claims 1-3, which is characterized in that the preparation side of the cotton rose leaf extract
Method：Preparation method：By cottonrose hibiscus leaf clean dry, 20-40 mesh sieve is crushed, according to solid-liquid ratio 1：70-90% second is added in 5-15
Refluxing extraction 3 times after alcohol, each 1-3h, merging filtrate is through reduced pressure and vacuum drying.
6. composition as described in any one of claims 1-3, which is characterized in that the preparation side of the maniod ebish flower extract
Method：Preparation method is：Sunset abelmoschus flower is dried and crushed into powder, according to solid-liquid ratio 1：The extraction of 60-85% alcohol refluxs is added in 10-20
It 3 times, each 0.5-1h, is concentrated through Rotary Evaporators after merging filtrate, vacuum freeze drying.
7. composition as claimed in any one of claims 1 to 6, which is characterized in that the composition can be used for the system of cosmetics
It is standby.
8. composition as claimed in claim 7, which is characterized in that the composition can be used as additive and dispel for inhibiting bacteria and diminishing inflammation
The preparation of acne facial cleanser.
9. a kind of inhibiting bacteria and diminishing inflammation anti-acne facial cleanser, which is characterized in that further include the ingredient of following mass percent：Saualane 1-
5%, cetostearyl alcohol 1.8-2.2%, dimethyl silicone polymer 2-6%, sodium lauryl sulfate 1-3%, alkyl sulfate 2-
6%, myristic acid 1-3%, PEG-20 methyls sesquistearate 1.5-3%, carbomer 0.2-0.8%, xanthans
0.02-0.06%, Phenoxyethanol 0.01-0.02%, methyl hydroxybenzoate 0.01-0.02%, Nipasol 0.01-0.02%, glycerine
5-20%, potassium hydroxide 0.02-0.3%, stearic acid 1-3%, deionized water surplus.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810353333.0A CN108451816A (en) | 2018-04-18 | 2018-04-18 | A kind of inhibiting bacteria and diminishing inflammation acne-removing composition |
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| CN201810353333.0A CN108451816A (en) | 2018-04-18 | 2018-04-18 | A kind of inhibiting bacteria and diminishing inflammation acne-removing composition |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110812308A (en) * | 2019-09-09 | 2020-02-21 | 浙江工业大学 | Traditional Chinese medicine composition and application thereof in preparation of skin care products |
| CN114642621A (en) * | 2022-05-06 | 2022-06-21 | 贵州阿依阿果食品有限公司 | Abelmoschus manihot flower facial mask, preparation method and application thereof |
-
2018
- 2018-04-18 CN CN201810353333.0A patent/CN108451816A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110812308A (en) * | 2019-09-09 | 2020-02-21 | 浙江工业大学 | Traditional Chinese medicine composition and application thereof in preparation of skin care products |
| CN114642621A (en) * | 2022-05-06 | 2022-06-21 | 贵州阿依阿果食品有限公司 | Abelmoschus manihot flower facial mask, preparation method and application thereof |
| CN114642621B (en) * | 2022-05-06 | 2024-06-07 | 广州合颜和美生物工程有限公司 | Abelmoschus manihot flower mask, preparation method and application thereof |
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Application publication date: 20180828 |