CN108440093A - A kind of biological particles charcoal base manure material and preparation method thereof - Google Patents
A kind of biological particles charcoal base manure material and preparation method thereof Download PDFInfo
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- CN108440093A CN108440093A CN201810344154.0A CN201810344154A CN108440093A CN 108440093 A CN108440093 A CN 108440093A CN 201810344154 A CN201810344154 A CN 201810344154A CN 108440093 A CN108440093 A CN 108440093A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/02—Biological treatment
- C02F11/04—Anaerobic treatment; Production of methane by such processes
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D3/00—Calcareous fertilisers
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
- C10B53/00—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
- C10B53/02—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form of cellulose-containing material
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
- C10B57/00—Other carbonising or coking processes; Features of destructive distillation processes in general
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Inorganic Chemistry (AREA)
- Treatment Of Sludge (AREA)
- Fertilizers (AREA)
Abstract
The present invention discloses a kind of biological particles charcoal base manure material and preparation method thereof, including following parts by weight of component：20 30 parts of excrement slag, 35 40 parts of stalk mixture, 12 16 parts of Castor seed Meal, 15 23 parts of furfural dregs, 79 parts of lignosulfonate vinyl acetate, 68 parts of arbuscular mycorrhiza, 21 25 parts of moderate-element, 45 parts of trace element；The preparation method first under nitrogen protection, carries out charcoal thermal decomposition, then control strictly anaerobic condition to stalk; liquefaction, biogas fermentation excrement slag and furfural dregs; and biological particles charcoal base manure material is made after finally that all materials are homogeneous, granulation, drying in lye preimpregnation, steam puffing castor-bean dregs.The present invention isolates the fuel such as methane, hydrogen and carbon monoxide, ethyl alcohol, butanol by the way of charcoal thermal decomposition and biogas fermentation, improve biomass material surcharge, and it is balanced comprehensively to produce charcoal base manure material nutrient element, can long duration discharge fertility, be easy to crops and be absorbed and utilized.
Description
Technical field
The present invention relates to biomass solid waste processing technology fields, and in particular to a kind of biological particles charcoal base manure material and its
Preparation method.
Background technology
Biomass carbon refers to utilizing Pintsch process timber, grass, maize straw or other biologies under anaerobic or hypoxia condition
Matter raw material, which carbonizes, to be formed, and in pyrolytic process, also generates wood tar, wood vinegar, fuel gas etc..Biomass carbon it is main at
Point it is carbon simple substance, is unlikely to deteriorate oxidation, can improve soil, long-term preservation of fertility, but to assemble cause of disease micro- for its microcellular structure
Biology and harmful substance, change soil physico-chemical property, and the prior art production biomass carbon base material mainly supplement nitrogen, phosphorus,
The a great number of elements such as potassium, and the moderate-element needed for plant growth and trace element are had ignored, the disorder of plant physiology function is caused,
Developmental arrest.
Application No. is the patent of CN201310618380.0, disclose a kind of corn dedicated biomass charcoal based compound fertilizer and its
Charcoal based compound fertilizer, tool is made by mixing the inorganic fertilizers such as rape stalk powdered carbon and agramon, urea phosphate in preparation method
Have stronger water conservation, fertilizer conservation performance, can long-term sustained release fertility, but be a lack of trace element, easily lead to plant and occur to lack
Swaged lesion, and powdered carbon enrichment pathogenic microorganism and harmful substance can not be inhibited.Application No. is the special of CN201710594251.0
Profit, discloses a kind of salix monogolica straw biomass charcoal base manure and preparation method thereof, which is salix monogolica stalk
Biomass carbon, fertilizer, soil conditioner, bentonite can delay fertilizer to discharge, and improve utilization rate of fertilizer, but also do not solve life
Substance charcoal micro-porous adsorption pathogenic microorganism causes the problem of plant regionality morbidity.
Invention content
In view of the deficiencies of the prior art, the purpose of the present invention is to provide a kind of biological particles charcoal base manure material and its
Preparation method.
Technical scheme of the present invention is summarized as follows：
A kind of biological particles charcoal base manure material, including following parts by weight of component：20-30 parts of excrement slag, stalk mixture 35-40
Part, 12-16 parts of Castor seed Meal, 15-23 parts of furfural dregs, lignosulfonate -7-9 parts of vinyl acetate, 6-8 parts of arbuscular mycorrhiza, middle amount member
21-25 parts plain, 4-5 parts of trace element.
Preferably, it is 1 that the excrement cinder ladle, which includes sheep manure, cow dung, chicken manure and each component weight ratio,：(0.6-0.8)：(1.2-
1.6)。
Preferably, the stalk mixture include maize straw, two kinds of wheat stalk, cotton stalk, peanut straw
Or it is two or more.
Preferably, it is 2.5 that the moderate-element, which includes calcium, magnesium, sulphur and each element weight ratio,：1：1.
Preferably, the trace element includes that boron, copper, iron, manganese, molybdenum, zinc and each element content are not less than 0.35%.
The present invention also provides a kind of above-mentioned preparation methods of biological particles charcoal base manure material, include the following steps：
Step 1：Stalk compound powder is broken to 60-80 mesh, water content is dried to and is less than 20%, in 60-80KPa nitrogen
Under the conditions of, it is warming up to 500-600 DEG C, charing pyrolysis 6h with 8-12 DEG C/min, and isolate biological fuel gas, straw charcoal is made；
Step 2：Under strict anaerobic conditions, liquid stools slag and furfural dregs 2-3d, then biogas fermentation 10-12d, and detach
Go out methane, ethyl alcohol, butanol, organic base fertilizer is made；
Step 3：Castor seed Meal is crushed, 20 mesh sieve is crossed, is placed in the potassium hydroxide solution of 0.1-0.2mol/L and impregnates 30min
Afterwards, with swollen quick-fried 8 times of 0.6-1.8MPa, 135-140 DEG C of water vapour, swollen quick-fried total time is 10-15min, adjusts PH to neutrality, obtains
To detoxified castor meal；
Step 4：Mixed straw charcoal, organic base fertilizer, detoxified castor meal, lignosulfonate-vinyl acetate, arbuscular mycorrhiza, and
Moderate-element and trace element is added, after the homogeneous 15min of 6000-10000r/min rotating speeds, then is granulated, dries, is made described
Biological particles charcoal base manure material.
Preferably, the biological fuel gas is the gaseous mixture of methane, hydrogen and carbon monoxide, can be applied to cleaning energy
Source.
Preferably, the condensing temperature is 25-30 DEG C.
Preferably, the biogas fermentation temperature is 35-55 DEG C.
Preferably, the methane, ethyl alcohol, butanol can be applied to bio-fuel.
Beneficial effects of the present invention：
(1) present invention obtains biological fuel gas and straw charcoal by high temperature pyrolysis, and biological fuel gas is for civilian or industrial
Clean energy resource improves straw biomass surcharge, isolates and also contains a small amount of wood tar and pyroligneous acid, wood tar in straw charcoal
It is natural antibiotic with pyroligneous acid, the organic acids such as 4- methylvaleric acids, acetic acid can inhibit the growth of pathogenic microorganism in ingredient
And breeding, 2,6- syringol, 2,6-di-tert-butyl p-cresol, 2- cyclopentene-1-ones can be used as anti-oxidant in ingredient
Agent prevents fertilizer oxidation deactivation, makes to discharge fertility steadily in the long term；
(2) liquefaction, biogas fermentation handle excrement slag and furfural dregs to the present invention successively, isolate methane, ethyl alcohol, butanol, can make
For bio-fuel, improve excrement slag and furfural dregs biomass surcharge, in fermentation process, generate a large amount of enzyme systems, promote excrement slag and
Furfural dregs conversion, degradation, build up fertility, and it is decomposed after organic fertilizer do not easily cause burn seedlings phenomenon；
(3) arbuscular mycorrhiza is covered in stalk carbon surface in the present invention, hinders straw charcoal to pathogenic microorganism and harmful substance
Aggtegation, and the spore secreted out of can depend on root system of plant, form new homobium, will be absorbed from soil nutrient,
Water Transportation improves plant and resists the ability of poor environment, and synthesize synthesis of biologically active substance to plant, such as gibberellin, carefully
Born of the same parents' mitogen, auxin, antibiotic promote plant growth；
(4) present invention combines plant growth characteristics and regulation of fertilizer requirement determines the best addition model of moderate-element and trace element
It encloses, the nutrient of general equilibrium is provided for plant growth, avoid the generation of early ageing and defective disease.
Specific implementation mode
With reference to embodiment, the present invention is described in further detail, to enable those skilled in the art with reference to specification
Word can be implemented according to this.
Embodiment 1
A kind of biological particles charcoal base manure material, including following parts by weight of component：20 parts of excrement slag, 35 parts of stalk mixture, castor
12 parts of the numb dregs of rice, 15 parts of furfural dregs, 7 parts of lignosulfonate-vinyl acetate, 6 parts of arbuscular mycorrhiza, 21 parts of moderate-element, trace element 4
Part.
In the present embodiment, a kind of above-mentioned preparation method of biological particles charcoal base manure material includes the following steps：
Step 1：Maize straw and wheat stalk are mixed, stalk mixture is obtained, and be crushed to 60 mesh, is dried to aqueous
Amount is less than 20%, under 60KPa condition of nitrogen gas, is warming up to 500 DEG C, charing pyrolysis 6h with 8 DEG C/min, and detach main component and be
The biological fuel gas of methane, hydrogen and carbon monoxide, can be applied to clean energy resource, and straw charcoal is made；
Step 2：According to 1：0.6：1.2 weight ratio mixing sheep manure, cow dung, chicken manure, under strict anaerobic conditions, 25 DEG C
Liquid stools slag and furfural dregs 2d, then 35 DEG C are controlled, biogas fermentation 10d is carried out, and isolate methane, ethyl alcohol, butanol, can be applied to
Organic base fertilizer is made in bio-fuel；
Step 3：Castor seed Meal is crushed, 20 mesh sieve is crossed, is placed in the potassium hydroxide solution of 0.1mol/L after impregnating 30min, with
Swollen quick-fried 8 times of 0.6MPa, 135 DEG C of water vapour, swollen quick-fried total time are 10min, adjust PH to neutrality, obtain detoxified castor meal；
Step 4：Mixed straw charcoal, organic base fertilizer, detoxified castor meal, lignosulfonate-vinyl acetate, arbuscular mycorrhiza, and
Moderate-element and trace element is added, which includes that calcium, magnesium, sulphur and each element weight ratio are 2.5：1：1, the micro member
Element includes that boron, copper, iron, manganese, molybdenum, zinc and each element content are not less than 0.35%, after the homogeneous 15min of 6000r/min rotating speeds, then
It is granulated, drying, the biological particles charcoal base manure material is made.
Embodiment 2
25 parts of excrement slag, 38 parts of stalk mixture, 14 parts of Castor seed Meal, 19 parts of furfural dregs, 8 parts of lignosulfonate-vinyl acetate,
7 parts of arbuscular mycorrhiza, 23 parts of moderate-element, 4.5 parts of trace element.
The preparation method is the same as that of Example 1, difference lies in：
Step 1：Stalk mixture includes maize straw, wheat stalk, cotton stalk, and smashing fineness is 70 mesh, nitrogen pressure
It is 70KPa by force, heating rate is 10 DEG C/min, and maximum temperature is 550 DEG C；
Step 2：Excrement slag each component weight ratio is 1：0.7：1.4, condensing temperature and number of days are 25-30 DEG C, 2-3d, biogas
Fermentation temperature and number of days are 45 DEG C, 11d；
Step 3：Concentration of potassium hydroxide is 0.15mol/L, the swollen detonation pressure of water vapour is strong, temperature 0.6-1.8MPa, 138 DEG C,
Swollen quick-fried total time is 13min；
Step 4：Homogeneous rotating speed is 8000r/min.
Embodiment 3
30 parts of excrement slag, 40 parts of stalk mixture, 16 parts of Castor seed Meal, 23 parts of furfural dregs, 9 parts of lignosulfonate-vinyl acetate,
8 parts of arbuscular mycorrhiza, 25 parts of moderate-element, 5 parts of trace element.
The preparation method is the same as that of Example 1, difference lies in：
Step 1：Stalk mixture includes maize straw, wheat stalk, cotton stalk, peanut straw, smashing fineness 80
Mesh, nitrogen pressure 80KPa, heating rate are 12 DEG C/min, and maximum temperature is 600 DEG C；
Step 2：Excrement slag each component weight ratio is 1：0.8：1.6, condensing temperature and number of days are 30 DEG C, 3d, biogas fermentation temperature
Degree and number of days are 55 DEG C, 12d；
Step 3：Concentration of potassium hydroxide is 0.2mol/L, the swollen detonation pressure of water vapour is strong, temperature 1.8MPa, 140 DEG C, it is swollen quick-fried
Total time is 15min；
Step 4：Homogeneous rotating speed is 10000r/min.
Comparative example 1
The preparation method is the same as that of Example 1, difference lies in, in step 1 using anaerobic fermentation handle stalk mixture, without into
Row pyrolysis charring.
Comparative example 2
For preparation method with embodiment 2, difference lies in do not add arbuscular mycorrhiza in step 4.
Comparative example 3
For preparation method with embodiment 3, difference lies in do not add moderate-element and trace element in step 4.
Following table is the ingredient and character analysis of each embodiment and each comparative example：
As seen from the above table, the present invention produces the equilibrium of biological particles charcoal base manure material nutrient comprehensively, and retain water and nutrients performance is strong,
Energy long duration discharges fertility, is easy to crops and is absorbed and utilized, and enhances the disease resistance and resistance of crops.
Although the embodiments of the present invention have been disclosed as above, but its is not only in the description and the implementation listed
With it can be fully applied to various fields suitable for the present invention, for those skilled in the art, can be easily
Realize other modification, therefore without departing from the general concept defined in the claims and the equivalent scope, the present invention is simultaneously unlimited
In specific details.
Claims (10)
1. a kind of biological particles charcoal base manure material, which is characterized in that including following parts by weight of component：20-30 parts of excrement slag, stalk are mixed
Close 35-40 parts of material, 12-16 parts of Castor seed Meal, 15-23 parts of furfural dregs, lignosulfonate -7-9 parts of vinyl acetate, arbuscular mycorrhiza 6-8
Part, 21-25 parts of moderate-element, 4-5 parts of trace element.
2. a kind of biological particles charcoal base manure material according to claim 1, which is characterized in that the excrement cinder ladle includes sheep manure, ox
Excrement, chicken manure and each component weight ratio are 1：(0.6-0.8)：(1.2-1.6).
3. a kind of biological particles charcoal base manure material according to claim 1, which is characterized in that the stalk mixture includes jade
Rice stalk, wheat stalk, cotton stalk, peanut straw two or more.
4. a kind of biological particles charcoal base manure material according to claim 1, which is characterized in that the moderate-element include calcium,
Magnesium, sulphur and each element weight ratio are 2.5：1：1.
5. a kind of biological particles charcoal base manure material according to claim 1, which is characterized in that it is described trace element include boron,
Copper, iron, manganese, molybdenum, zinc and each element content are not less than 0.35%.
6. a kind of preparation method of biological particles charcoal base manure material as described in claim 1-5 any one, which is characterized in that packet
Include following steps：
Step 1：Stalk compound powder is broken to 60-80 mesh, water content is dried to and is less than 20%, in 60-80KPa condition of nitrogen gas
Under, it is warming up to 500-600 DEG C, charing pyrolysis 6h with 8-12 DEG C/min, and isolate biological fuel gas, straw charcoal is made；
Step 2：Under strict anaerobic conditions, liquid stools slag and furfural dregs 2-3d, then biogas fermentation 10-12d, and isolate first
Organic base fertilizer is made in alkane, ethyl alcohol, butanol；
Step 3：Castor seed Meal is crushed, 20 mesh sieve is crossed, is placed in the potassium hydroxide solution of 0.1-0.2mol/L after impregnating 30min, with
Swollen quick-fried 8 times of 0.6-1.8MPa, 135-140 DEG C of water vapour, swollen quick-fried total time are 10-15min, adjust PH to neutrality, are taken off
Malicious Castor seed Meal；
Step 4：Mixed straw charcoal, organic base fertilizer, detoxified castor meal, lignosulfonate-vinyl acetate, arbuscular mycorrhiza, and be added
Moderate-element and trace element are granulated after the homogeneous 15min of 6000-10000r/min rotating speeds, and the biological particles charcoal is made
Base manure material.
7. a kind of preparation method of biological particles charcoal base manure material according to claim 6, which is characterized in that the biomass
Combustion gas is the gaseous mixture of methane, hydrogen and carbon monoxide, can be applied to clean energy resource.
8. a kind of preparation method of biological particles charcoal base manure material according to claim 6, which is characterized in that the liquefaction temperature
Degree is 25-30 DEG C.
9. a kind of preparation method of biological particles charcoal base manure material according to claim 6, which is characterized in that the biogas hair
Ferment temperature is 35-55 DEG C.
10. a kind of preparation method of biological particles charcoal base manure material according to claim 6, which is characterized in that the methane,
Ethyl alcohol, butanol can be applied to bio-fuel.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109650954A (en) * | 2018-12-27 | 2019-04-19 | 北京嘉博文生物科技有限公司 | A method of using biomass carbonated+two-part fementative composition process afforestation solid organic castoff |
| CN111943765A (en) * | 2020-08-26 | 2020-11-17 | 云南威鑫农业科技股份有限公司 | Preparation method of environment-friendly biochar-based fertilizer capable of being continuously produced |
| CN111943754A (en) * | 2020-08-18 | 2020-11-17 | 山东农业大学 | Crop straw biochar composite microbial organic fertilizer and preparation method and application thereof |
| CN113024328A (en) * | 2020-09-17 | 2021-06-25 | 沈阳中科新型肥料有限公司 | Application of compound containing 2-cyclopentenone as synergist of nitrogen-containing fertilizer |
| US11124461B2 (en) | 2019-07-04 | 2021-09-21 | Incitec Pivot Limited | Fertilizer |
| CN115259962A (en) * | 2021-12-22 | 2022-11-01 | 淮阴师范学院 | Preparation method of livestock and poultry manure biochar-based slow-release phosphorus-potassium fertilizer |
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| CN107721640A (en) * | 2017-11-20 | 2018-02-23 | 芜湖继伟农业有限公司 | A kind of preparation method of the charcoal base microbe slow release fertilizer of EM bacterium fermented stalk |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109650954A (en) * | 2018-12-27 | 2019-04-19 | 北京嘉博文生物科技有限公司 | A method of using biomass carbonated+two-part fementative composition process afforestation solid organic castoff |
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| CN111943765A (en) * | 2020-08-26 | 2020-11-17 | 云南威鑫农业科技股份有限公司 | Preparation method of environment-friendly biochar-based fertilizer capable of being continuously produced |
| CN113024328A (en) * | 2020-09-17 | 2021-06-25 | 沈阳中科新型肥料有限公司 | Application of compound containing 2-cyclopentenone as synergist of nitrogen-containing fertilizer |
| CN115259962A (en) * | 2021-12-22 | 2022-11-01 | 淮阴师范学院 | Preparation method of livestock and poultry manure biochar-based slow-release phosphorus-potassium fertilizer |
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Application publication date: 20180824 |
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