CN108324636A - A kind of skin care compositions and with careful pore effect cosmetic, preparation method - Google Patents
A kind of skin care compositions and with careful pore effect cosmetic, preparation method Download PDFInfo
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- CN108324636A CN108324636A CN201810245122.5A CN201810245122A CN108324636A CN 108324636 A CN108324636 A CN 108324636A CN 201810245122 A CN201810245122 A CN 201810245122A CN 108324636 A CN108324636 A CN 108324636A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The present invention discloses a kind of skin care compositions and with careful pore effect cosmetic, preparation method, belong to cosmetic technical field, including Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae, the Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae weight ratio be (1~5):(1~5):(1~5):(1~3):(1~5).The skin care compositions of the present invention, fragrant, skin sense is preferable, it is added in the cosmetics such as condensation, cream, lotion, facial cleanser, cleansing cream, shampoo, toner or firming lotion, facial mask, bath agent, by controlling rational additive amount and process conditions appropriate, the institutional framework of cosmetics will not be damaged, detrimental effect will not be brought to the stability of cosmetics, discoloration, layering and other issues will not be caused.
Description
Technical field
The present invention relates to a kind of skin care compositions and with careful pore effect cosmetic, preparation method, belong to makeup
Product technical field.
Background technology
With the development of society, the progress of medicine, the improvement of quality of life, people start to pursue the life for having quality, right
The careful attention degree of facial skin especially pore also significantly improves especially skin problem, and pore is coarse always to be puzzlement
One of the case where people, the people for liking to be beautiful will also attend to anything else in addition to facing social the increasing pressure to take face into account
Beauty brings many inconvenience to people's life really.
It is a kind of common at present skin symptom that pore is coarse, when the old cutin accumulation of skin is more, skin can be made to thicken,
Roughening, pore becomes coarse, and skin also absorbs moisture and maintenance ingredient because can not be successfully, and becomes obscure, dry, accelerates stimulation
Fat secretion amount, pore can become larger once again.In addition, with advancing age, skin gradually loses elasticity, perifollicolar lacks branch
Structure is held, is also easy to that pore is made to seem bigger;The skin environment done in outer oil, can also be such that pore becomes thick.
The coarse harm of pore is very more, and appearance, which to the direct feel of people is skin, first seems coarse lackluster;
Also, it because coarse pore, convenience is opened to bacterium, becomes easily infected by bacterium and leads to infection and allergic reaction;Separately
Outside, coarse pore is easy lost moisture, causes dry skin, coarse, premature senile symptom occur.
A kind of existing Chinese patent " cosmetics and preparation method thereof with careful pore effect " (application number
201610595371.8) a kind of cosmetics with careful pore effect are disclosed, it is composed of the following components:Witch hazel is extracted
Object 10%~20%, N- methyl-Beta-alanine 0.5%~2%, Hydrolyzed Collagen 3%~10%, lecithin 10%~
50%, cholesterol 5%~20%, Tween 80 5%~20%, preservative 0.01%~0.03%, PBS buffer solution 10%~
50%, the sum of above constituent mass percentage is 100%.The invention also discloses the preparation methods of above-mentioned cosmetics, by former material
Material is mixed to form W/O lotions, then successively through revolving, hydration, cross film and freeze thawing treatment after to get.The sense of touch of above-mentioned cosmetics
Poor, using effect is bad, contains more chemical composition simultaneously, cannot meet the needs of natural people, environmental protection.
In addition, existing Chinese patent " a kind of whitening and softening skin and can careful pore cosmetics and preparation method thereof " (application
Number:201410215261.5), be related to a kind of whitening and softening skin and can careful pore cosmetics and preparation method thereof.Including as follows
Step:VC ethylethers, Trenaxmine, ursin and mulberry fruit extract liquor are added to the water, are heated to 70 DEG C by water phase liquid preparation process
Dissolving forms water phase liquid;Oil phase liquid preparation process, by licoflavone, Symwhite-337, propylene glycol and glycerine Hybrid Heating
It is dissolved to 85 DEG C, forms oil phase liquid;The water phase liquid and oil phase liquid are mixed evenly, are put into fermentation by base fluid preparation process
Tank, is added kojic acid, glucose, and base fluid is made in 3 days in 30 DEG C of fermentations;Medicinal powder preparation process, by uva ursi, Radix Glycyrrhizae, ginseng and snow
Lotus flower is respectively dried, be ground into powder after, endothelin antagonist is added, is sufficiently mixed and medicinal powder is made;Finished product step is mixed, it will
The base fluid is put into blender, and medicinal powder is uniformly sprinkled into the base fluid while stirring, and continues 30 to 40 minutes, takes out dress
Enter container, obtains the cosmetics.Above-mentioned cosmetics it is more use chemical composition, it is natural, environmental protection that people cannot be met
Demand;And preparation process is cumbersome, complex process.
Currently, a preferable cosmetics not yet, can have both careful pore effect, while again can sufficient people are natural, ring
The beauty demand of guarantor.
Invention content
In view of the above existing problems in the prior art, the present invention provides a kind of skin care compositions and there is careful pore effect
Cosmetics, preparation method are effectively improved the coarse equal skin problem of skin pore.
To achieve the goals above, a kind of skin care compositions that the present invention uses, including Swertia patens, bitter white hoof, the stem of noble dendrobium, pool
Rush down, Radix Glycyrrhizae, the Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae weight ratio be (1~5):(1~5):(1~5):(1~
3):(1~5).
Further, the Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae preferably use Herba Swertiae bimaculatae extract, hardship white respectively
Hoof extract, Herba Dendrobii extract, Alisma extract, licorice are made by following steps respectively:
Chinese herbal medicine Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae are crushed respectively, according to feed liquid weight ratio 1:(30~50)
The ethyl alcohol of 90% or more volumetric concentration is added, after extracting 0.5~4 hour, recycles ethyl alcohol, i.e., obtains each extraction of medicinal extract form respectively
Object.
As an improvement, the Chinese herbal medicine Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae smash it through 60 mesh sieve.
As a further improvement, the Herba Swertiae bimaculatae extract, laricifomes officinalis, Herba Dendrobii extract, Alisma extract,
Licorice is made especially by following steps respectively:
1) it uses grinder that each Chinese herbal medicine is ground into powdery fine crushing respectively, crosses 60 mesh sieve, screened mesh Chinese medicine fine crushing;
2) it is 1 according to the feed liquid weight ratio of Chinese herbal medicine and ethyl alcohol:(30~50) weigh ethanol in proper amount reagent, during immersion is each
Herbal medicine 0.5~2 hour places electric jacket heating, and heating temperature opens cool circulation water and carry out circumfluence distillation 1~3 to 78 DEG C
Hour, obtain alcohol extract;
3) alcohol extract is moved into Rotary Evaporators, vacuumized, 60 DEG C of progress heating recovery ethyl alcohol of water-bath, 30min~
To get each extract of medicinal extract form after 60min.
In addition, a kind of having careful pore effect cosmetic, contain skin care group described in any one of the above embodiments in the cosmetics
Close object.
As an improvement, the cosmetics are lotion, by weight percentage, which includes:
AMPHISOL K of 0.4%-0.8%, the butanediol of 4%-8%, 0.04%-0.1% Sensiva SC50,
The pentanediol of 1%-3%, the trehalose of 2%-6%, 0.02%-0.08% EDTA-2Na, 0.05%-5% skincare composition
Object, the hexylene glycol of 0.4%-0.8%, 0.4%-0.8% CARBOMER-TR, 0.4%-0.8% EMULIM 22,4%-
The TEA of 8% saualane, the VE acetates of DM10,1%-5% of 1%-5%, the butter fruit of 1%-5%, 0.4%-0.8%,
The deionized water of surplus;
The specific preparation process of above-mentioned emulsion is:
1) it in deionized water by the CARBOMER-TR of formula ratio dissolvings, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), AMPHISOL K of formula ratio, butanediol, Sensiva SC50, penta are separately added into
Glycol, trehalose, EDTA-2Na, skin care compositions, hexylene glycol obtain water phase material to being completely dissolved;
3) EMULIM 22, saualane, DM10, VE acetate, butter fruit are completely dissolved respectively, obtain oil phase material;
4) oil phase material that step 3) obtains is poured into the water phase material of step 2), continue heating stirring to completely it is molten
Solution;
5) after the dissolving completely of above-mentioned all materials, continue stirring and be cooled to 45 DEG C hereinafter, adding TEA to get the breast
Liquid.
As an improvement, the cosmetics are condensation, by weight percentage, which includes:
EDTA-2Na, 0.4%- of the butanediol of 4%-8%, the hyaluronic acid of 0.1%-0.5%, 0.02%-0.08%
0.8% card wave 940, the penta of the skin care compositions of 0.05%-5%, the Sensiva SC50 of 0.1%-0.5%, 1%-5%
The arginine of glycol, 0.1%-0.5%, the deionized water of surplus;
The specific preparation process of above-mentioned condensation is:
1) it in deionized water by the dissolving of the card wave 940 of formula ratio, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), it is separately added into butanediol, hyaluronic acid, EDTA-2Na, until being completely dissolved;
3) after step 2) dissolving completely, the skin care compositions, Sensiva SC50, pentanediol of formula ratio is added, waits for molten
Xie Hou continues stirring and is simultaneously stopped heating;
4) it waits for that the solution of step 3) is cooled to 45 DEG C hereinafter, weigh the arginine of formula ratio, is added to the solution of step 3)
In, to get the condensation after stirring evenly.
As an improvement, the cosmetics are cream, by weight percentage, which includes:
The hexylene glycol of 0.4%-0.8%, the skin care compositions of 0.05%-5%, 0.1%-0.5% hyaluronic acid,
The fragrant fresh ketone of 0.4%-0.8%, the PEG-100 stearates of card wave TR-1,1%-5% of 0.4%-0.8%, 5%-10%
5 viscosity silicone oils, the 1%-3% of saualane, the cetanol of 1%-5%, the butter fruit of VE, 1%-5% of 1%-5%, 1%-5%
DRY-FLO PURE of DC1403,1%-5%, 0.4%-0.8% 10%NaOH, the deionized water of surplus;
The specific preparation process of above-mentioned cream is:
1) it in deionized water by card wave TR-1 dissolvings, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), be separately added into hexylene glycol, skin care compositions, hyaluronic acid, fragrant fresh ketone to completely it is molten
Solution, obtains water phase material;
3) the PEG-100 stearates of formula ratio, saualane, cetanol, VE, butter fruit are completely dissolved respectively, are obtained oily
Phase materials;
4) oil phase material that step 3) obtains is added in the water phase material of step 2), continue heating stirring to completely it is molten
Solution;
5) after the water phase of step 4) and oil phase dissolving completely, 5 viscosity silicone oils, DC1403, DRY-FLO are separately added into
PURE, until being completely dissolved;
6) after above-mentioned all materials dissolving completely, continue stirring and be cooled to 45 DEG C hereinafter, adding 10%NaOH to get cream
Frost.
As an improvement, the cosmetics are the nutrient solution in patch facial mask, and by weight percentage, the patch facial mask nutrition
Liquid includes:
EDTA-2Na, 0.4%-0.8% of the butanediol of 4%-8%, the niacinamide of 1%-8%, 0.02%-0.08%
Card wave 940, the xanthans of 0.1%-0.5%, the skin care compositions of 0.05%-5%, 0.1%-0.3% allantoin,
The TEA of the Sensiva SC50 of 0.1%-0.5%, the pentanediol of 1%-5%, 0.4%-0.8%, the deionized water of surplus;
The specific preparation process of above-mentioned patch facial mask nutrient solution is:
1) it in deionized water by the dissolving of card wave 940, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), butanediol, niacinamide, EDTA-2Na, xanthans, stirring and dissolving are separately added into;
3) after the solution of step 2) is completely dissolved, skin care compositions, allantoin, Sensiva SC50, pentanediol is added,
After to be dissolved, continue stirring and be simultaneously stopped heating;
4) wait for that solution is cooled to 45 DEG C hereinafter, addition TEA, stirs evenly up to the patch facial mask nutrient solution.
The beneficial effects of the invention are as follows:
1) skin care compositions of the invention, composition are mainly the natural component extracted in Chinese herbal medicine, each extract
Component interacts, and has synergistic effect especially in terms of careful pore, the skin that compacts.The skin care compositions of the present invention can answer
For in skin type or cleaning class cosmetics, such as being used in condensation, aqua and face pack prescription, assign the careful pore of cosmetics and
It compacts skin effect.When each Chinese herbal medicine medicinal extract of the present invention is applied to cosmetics, for ease of being added in cosmetics, it can incite somebody to action
Medicinal extract is dissolved in cosmetics in polyalcohol such as butanediol and/or glycerine, effectively medicinal extract can be avoided to directly apply to cosmetics
Especially type of latex type cosmetics when, caused precipitated and separated phenomenon.Specific embodiment according to the present invention, the medicinal extract form
Extract and polyalcohol weight ratio be 1:(5~30), polyalcohol dosage, which is usually subject to, preferably dissolves the medicinal extract, more
Specific dosage can suitably be adjusted according to content of the polyalcohol in cosmetics.
2) application the present invention also provides the skin care compositions in preparing the cosmetics with careful pore effect.
Specifically, the cosmetics can be skin-care cosmetics (such as condensation, face cream, facial treatment milk, toner, facial mask battalion
Nutrient solution etc.) or cleaning class cosmetics (such as mildy wash etc.).Specifically, the skin care compositions is to be converted to raw material river deer tooth
Dish, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae overall dry weight, be that 0.05%~5% to account for cosmetics total weight is applied to these
In cosmetics.
3) skin care compositions of the present invention with careful pore effect can mutually be added to describedization as addition
(each extract in the composition of the present invention can be added respectively when concrete application, being added to after being also pre-mixed in cosmetic
In cosmetic, addition use after being preferably pre-mixed each extract uniformly in proportion).Specific embodiment party according to the present invention
Case, cosmetics of the invention are in addition to including the skincare composition beyond the region of objective existence with careful pore effect, the selection of other components
It can be carried out according to the routine operation in this field, such as may include some conventional oil phases and water phase, or further comprised
Other common addition phases in fields.In some emulsified make-ups, emulsifier, excipient (thickening) agent are generally included,
It can also add the basic material and necessary additive that cosmetics usually contain, such as emollient (such as it is vegetable oil, white oil, dynamic
Object grease and its derivative etc.), it is moisturizer (such as glycerine, propylene glycol, 1,3 butylene glycol etc.), essence, deionized water, anti-oxidant
Agent, preservative etc. can also add some nutritional ingredients, and the application of these specific ingredients and dosage can be according to the tools of the cosmetics
Body type and selected, or added according to convention amount, this is easy to grasp for a person skilled in the art.
4) skin care compositions of the invention, fragrant, skin sense is preferable, is added to condensation, cream, lotion, facial cleanser, washes
In the cosmetics such as face cream, shampoo, toner or firming lotion, facial mask, bath agent, by controlling rational additive amount and appropriate
Process conditions, will not damage the institutional framework of cosmetics, will not bring detrimental effect to the stability of cosmetics, no
It can cause discoloration, layering and other issues.
Description of the drawings
Fig. 1 is the ITA value test charts that subject smears lotion;
Fig. 2 is the ITA value test charts that subject smears condensation;
Fig. 3 is the ITA value test charts that subject smears cream;
Fig. 4 is the VISIA images of subject one in the present invention;
Fig. 5 is the VISIA images of subject two in the present invention;
Fig. 6 is the VISIA images of subject three in the present invention.
Specific implementation mode
In order to make the objectives, technical solutions and advantages of the present invention clearer, below by accompanying drawings and embodiments, to this
Invention is further elaborated.However, it should be understood that the specific embodiments described herein are merely illustrative of the present invention,
The range being not intended to restrict the invention.
Unless otherwise defined, all technical terms and scientific terms used herein are led with the technology for belonging to the present invention
The normally understood meaning of technical staff in domain is identical, and used term is intended merely to retouch in the description of the invention herein
State the purpose of specific embodiment, it is not intended that in the limitation present invention.
A kind of skin care compositions, including Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae, the Swertia patens, bitter white hoof, stone
Dry measure used in former times, rhizoma alismatis, Radix Glycyrrhizae weight ratio be (1~5):(1~5):(1~5):(1~3):(1~5).The skin care compositions of the present invention,
It forms the predominantly natural component that is extracted from plant, each extract components interaction, especially careful pore,
Skin aspect of compacting has synergistic effect.Skin can fundamentally be solved to be easy allergic problem, be easy the symptoms such as long acne, simultaneously
Water lock effect is good, skin-tightening and it is glossy, while having good effect to replenishing water and preserving moisture, crease-resistant, anti-aging.The skin care group
It closes in object, based on Swertia patens, rhizoma alismatis, coordinates plurality of Chinese plant, scientific compatibility, synergy of mutually promoting, there have to be apparent careful
Pore effect.
As an improvement, the Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae preferably use Herba Swertiae bimaculatae extract, hardship respectively
White hoof extract, Herba Dendrobii extract, Alisma extract, licorice, are made by following steps respectively:
Chinese herbal medicine Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae are crushed respectively, according to feed liquid weight ratio 1:(30~50)
The ethyl alcohol of 90% or more volumetric concentration is added, after extracting 0.5~4 hour, recycles ethyl alcohol, i.e., obtains each extraction of medicinal extract form respectively
Object.Preferred embodiment according to the present invention, Herba Swertiae bimaculatae extract, laricifomes officinalis, Herba Dendrobii extract, rhizoma alismatis extraction
Object, licorice can individually extract acquisition respectively with Chinese herbal medicine Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae, also may be used
To be that will extract to obtain after two or more mixing therein.
As an improvement, the Chinese herbal medicine Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae smash it through 60 mesh sieve.
As a further improvement, the Herba Swertiae bimaculatae extract, laricifomes officinalis, Herba Dendrobii extract, Alisma extract,
Licorice is made especially by following steps respectively:
1) it uses grinder that each Chinese herbal medicine is ground into powdery fine crushing respectively, crosses 60 mesh sieve, screened mesh Chinese medicine fine crushing;
2) it is 1 according to the feed liquid weight ratio of Chinese herbal medicine and ethyl alcohol:(30~50) weigh ethanol in proper amount reagent, during immersion is each
Herbal medicine 0.5~2 hour places electric jacket heating, and heating temperature opens cool circulation water and carry out circumfluence distillation 1~3 to 78 DEG C
Hour, obtain alcohol extract;
3) alcohol extract is moved into Rotary Evaporators, vacuumized, 60 DEG C of progress heating recovery ethyl alcohol of water-bath, 30min~
To get each extract of medicinal extract form after 60min.
The present invention also provides a kind of cosmetics, wherein containing the skin care group of the present invention with careful pore effect
Close object.The cosmetics can be skin-care cosmetics (such as condensation, face cream, facial treatment milk, toner, facial mask etc.) or
It is cleaning class cosmetics (such as mildy wash etc.), preferably face cream or facial treatment milk, facial mask.Specifically, the skincare composition
Object be converted to raw material Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae overall dry weight, the additive amount in cosmetics is makeup
The 0.05%-5% of product total weight can have different content according to the specific type difference of cosmetics.
As an improvement, the cosmetics are lotion, by weight percentage, which includes:
AMPHISOL K (Phosphoric acid monohexadecyl ester potassium), the butanediol of 4%-8%, the 0.04%-0.1% of 0.4%-0.8%
Sensiva SC50, the pentanediol of 1%-3%, the trehalose of 2%-6%, 0.02%-0.08% EDTA-2Na,
0.05%-5% (be converted to raw material Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae overall dry weight, it is same as below) skin care
The EMULIM of composition, the hexylene glycol of 0.4%-0.8%, the CARBOMER-TR (card wave) of 0.4%-0.8%, 0.4%-0.8%
DM10 (dimethyl silicone polymer), the 1%-5% of 22 (tribehenin essence PEG-20 esters), the saualane of 4%-8%, 1%-5%
VE acetates, the butter fruit of 1%-5%, 0.4%-0.8% TEA (triethanolamine), the deionized water of surplus;
The specific preparation process of above-mentioned emulsion is:
1) it in deionized water by the CARBOMER-TR of formula ratio dissolvings, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), AMPHISOL K of formula ratio, butanediol, Sensiva SC50, penta are separately added into
Glycol, trehalose, EDTA-2Na, skin care compositions, hexylene glycol obtain water phase material to being completely dissolved;
3) EMULIM 22, saualane, DM10, VE acetate, butter fruit are completely dissolved respectively, obtain oil phase material;
4) oil phase material that step 3) obtains is poured into the water phase material of step 2), continue heating stirring to completely it is molten
Solution;
5) after the dissolving completely of above-mentioned all materials, continue stirring and be cooled to 45 DEG C hereinafter, adding TEA to get the breast
Liquid.
As an improvement, the cosmetics are condensation, by weight percentage, which includes:
EDTA-2Na, 0.4%- of the butanediol of 4%-8%, the hyaluronic acid of 0.1%-0.5%, 0.02%-0.08%
0.8% card wave 940, the penta of the skin care compositions of 0.05%-5%, the Sensiva SC50 of 0.1%-0.5%, 1%-5%
The arginine of glycol, 0.1%-0.5%, the deionized water of surplus;
The specific preparation process of above-mentioned condensation is:
1) it in deionized water by the dissolving of the card wave 940 of formula ratio, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), it is separately added into butanediol, hyaluronic acid, EDTA-2Na, until being completely dissolved;
3) after step 2) dissolving completely, the skin care compositions, Sensiva SC50, pentanediol of formula ratio is added, waits for molten
Xie Hou continues stirring and is simultaneously stopped heating;
4) it waits for that the solution of step 3) is cooled to 45 DEG C hereinafter, weigh the arginine of formula ratio, is added to the solution of step 3)
In, to get the condensation after stirring evenly.
As an improvement, the cosmetics are cream, by weight percentage, which includes:
The hexylene glycol of 0.4%-0.8%, the skin care compositions of 0.05%-5%, 0.1%-0.5% hyaluronic acid,
PEG-100 stearates, the 5%- of the fragrant fresh ketone of 0.4%-0.8%, the card wave TR-1 (card wave) of 0.4%-0.8%, 1%-5%
The 5 of 10% saualane, the cetanol of 1%-5%, the VE (vitamin E) of 1%-5%, the butter fruit of 1%-5%, 1%-5%
Viscosity silicone oil, the DC1403 (silicone oil) of 1%-3%, the DRY-FLO PURE (modified starch) of 1%-5%, 0.4%-0.8%
10%NaOH, the deionized water of surplus;
The specific preparation process of above-mentioned cream is:
1) it in deionized water by card wave TR-1 dissolvings, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), be separately added into hexylene glycol, skin care compositions, hyaluronic acid, fragrant fresh ketone to completely it is molten
Solution, obtains water phase material;
3) the PEG-100 stearates of formula ratio, saualane, cetanol, VE, butter fruit are completely dissolved respectively, are obtained oily
Phase materials;
4) oil phase material that step 3) obtains is added in the water phase material of step 2), continue heating stirring to completely it is molten
Solution;
5) after the water phase of step 4) and oil phase dissolving completely, 5 viscosity silicone oils, DC1403, DRY-FLO are separately added into
PURE, until being completely dissolved;
6) after above-mentioned all materials dissolving completely, continue stirring and be cooled to 45 DEG C hereinafter, adding 10%NaOH to get cream
Frost.
As an improvement, the cosmetics are the nutrient solution in patch facial mask, and by weight percentage, the patch facial mask nutrition
Liquid includes:
EDTA-2Na, 0.4%-0.8% of the butanediol of 4%-8%, the niacinamide of 1%-8%, 0.02%-0.08%
Card wave 940, the xanthans of 0.1%-0.5%, the skin care compositions of 0.05%-5%, 0.1%-0.3% allantoin,
The TEA (triethanolamine) of the Sensiva SC50 of 0.1%-0.5%, the pentanediol of 1%-5%, 0.4%-0.8%, surplus are gone
Ionized water;
The specific preparation process of above-mentioned patch facial mask nutrient solution is:
1) it in deionized water by the dissolving of card wave 940, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), butanediol, niacinamide, EDTA-2Na, xanthans, stirring and dissolving are separately added into;
3) after the solution of step 2) is completely dissolved, skin care compositions, allantoin, Sensiva SC50, pentanediol is added,
After to be dissolved, continue stirring and be simultaneously stopped heating;
4) wait for that solution is cooled to 45 DEG C hereinafter, addition TEA, stirs evenly up to the patch facial mask nutrient solution.
In above-mentioned formula, suitable preservative, essence etc. can be also added, the application of these specific ingredients and dosage can be according to
The routine techniques of existing cosmetics carries out.
Careful pore effect skin care compositions of the present invention, fragrant, skin sense is preferable, is added to condensation, cream, breast
In the cosmetics such as liquid, facial cleanser, cleansing cream, shampoo, toner or firming lotion, facial mask, bath agent, by controlling rational addition
Amount and process conditions appropriate, will not damage the institutional framework of cosmetics, will not be brought to the stability of cosmetics
Detrimental effect will not cause discoloration, layering and other issues.
The present invention provides a kind of skin care compositions with careful pore effect, are applied to the production of cosmetics,
Regulation and control skin oil and fat, careful pore and compact and play synergistic effect in terms of skin, and natural extract it is mild to skin, substantially without
Irritation, their addition can preferably improve the beauty of skin.In addition, the present invention produce cosmetic product appearance,
Inherent quality can maintain a long-term stability.
Embodiment 1
Herba Swertiae bimaculatae extract, laricifomes officinalis, Herba Dendrobii extract, Alisma extract, the preparation of licorice and shield
The preparation of skin composition.
The Chinese herbal medicines such as Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae are taken, the mixed of a variety of Chinese herbal medicines is made in accordance with the following methods
Close extract:
1) each Chinese medicine is ground into powdery fine crushing and crosses 60 mesh sieve by grinder, was screened mesh Chinese medicine fine crushing and is used, sieving
The herb powder of net is uniformly mixed;
2) the feed liquid ratio 1 of the ethyl alcohol extraction determined according to orthogonal experiment:30, weigh appropriate 95% ethanol reagent leaching
It steeps Chinese medicine 1 hour, places electric jacket heating, heating temperature opens cool circulation water and carry out circumfluence distillation 2 hours to 78 DEG C;
3) alcohol extract is moved into Rotary Evaporators, adjusts 60 rpms of suitable rotational speed, vacuumizes, 60 DEG C of progress of water-bath
Heating recovery ethyl alcohol, medicinal extract is steamed to obtain after 45min, and the mixing of as Swertia patens of the invention, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae carries
Take object medicinal extract.
It, can be by medicinal extract according to 1 for ease of being added in cosmetics when the medicinal extract is applied to cosmetics:20 ratios are molten
With in polyalcohol such as butanediol or glycerine in cosmetics, cosmetics especially type of latex type is directly applied to avoid medicinal extract
Caused precipitated and separated phenomenon when cosmetic.
The Chinese herbal medicines such as Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae can also be taken respectively, be made respectively according to the method described above
Swertia patens medicinal extract extract, bitter white hoof medicinal extract extract, stem of noble dendrobium medicinal extract extract, rhizoma alismatis medicinal extract extract, extract of licorice root extraction
Each medicinal extract extract is mixed, is dissolved in polyalcohol used for cosmetic and preserving by object in proportion again later.
In addition, in actual production, for ease of being added in cosmetics, also each medicinal extract extract can suitably be adjusted to predetermined
Normal concentration.
Embodiment 2
Different prescription fungistatic effect contrast experiments.
Experimental principle:
Each Chinese herbal medicine medicinal extract extract is prepared according to the method for embodiment 1, and each extract is configured to composite extract
Sample prescription, as shown in table 1, wherein each extract proportioning is 1 in No. 1 sample and No. 2 sample prescriptions:1:1:1 (to be converted to
It is the dry weight meter of each herbal raw material, same as below), No. 3 samples be 1:1:1:1:1.
1 composite extract sample prescription of table
No. 1 sample prescription | Bitter white hoof, the stem of noble dendrobium, Radix Glycyrrhizae |
No. 2 sample prescriptions | Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis |
No. 3 sample prescriptions | Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae |
Experimental method:
Actication of culture:The propionibacterium acnes that -80 DEG C are stored are seeded in fluid nutrient medium, Anaerobic culturel box is put into
In.After 37 DEG C are cultivated 7 days, scribing line separation is carried out on solid medium, streak plate is activated 7 days in 37 DEG C of incubators, obtained
Single bacterium colony.Single bacterium colony is seeded to aseptic liquid nutrient medium, 37 DEG C activate 7 days.
Odontothrips loti step:The bacteria suspension of activation is centrifuged, precipitation is resuspended to bacteria concentration about with sterile saline
107CFU/mL;100 μ L bacteria suspensions are taken to be coated on solid plate culture medium, gripping sterile Oxford cup with tweezers puts to culture medium
Surface, pressing lightly on makes Oxford cup completely attach to (each tablet places 3 Oxford cups) with culture medium, is added into Oxford cup
200 μ L prepare liquids.Tablet is put into Anaerobic culturel box, culture observes inhibition zone size after 14 days, measures antibacterial circle diameter.It is real
It tests and makees positive control with sterile water work feminine gender and blank control, 0.02% methyl hydroxybenzoate.
Various concentration sample is shown in Table 2 to the antibacterial circle diameter of propionibacterium acnes.
Biocidal property (D of the 2 various concentration sample of table to propionibacterium acnes:mm)
Analytical table 2 is it is found that three kinds of Chinese prescription raw materials play the role of certain inhibition propionibacterium acnes, wherein sample
3 is especially prominent, and sample 2 and No. 3 contrast differences of sample are little, shows that wherein being added with for medicine acts on but be not decisive shadow simply
It rings;See that sample 1 and 3 contrast difference of sample are bigger simultaneously, it can be seen that wherein play main influence is Swertia patens and pool
It rushes down.
Embodiment 3
Skin shine Contrast on effect tests (lotion).
Experimental principle:
Prepare the medicinal extract extract of each Chinese herbal medicine according to the method for embodiment 1, and according to being converted to raw material dry weight meter river deer tooth
2 parts of dish, bitter white 1 part of hoof, 1 part of the stem of noble dendrobium, 1 part of rhizoma alismatis, 1 part of Radix Glycyrrhizae ratio mix to obtain extract formula, be further prepared into and contain
The cosmetic emulsion sample of extract formula.
Volunteer smears the samples of latex containing extract formula of the present invention in left and right forehead respectively and without containing the present invention
The blank emulsion sample of extract formula continues 8 weeks to 10 subject's tests, right using the 3rd, 5,8 week in subject respectively
Subject's ITA values are tested.Specific test result is as follows table 3-5;Wherein to containing powerful substance emulsion formulations, blank sample
The emulsion formulations of product, the average rate of change of two kinds of samples is referring to Fig. 1.
The ITA values test in the 3rd week of table 3
The ITA values test in the 5th week of table 4
The ITA values test in the 8th week of table 5
It is found that subject is after lasting use sample 3 weeks, skin shine is significantly improved analytical table 3-5 and Fig. 1, and
Usage time is longer, and effect is more apparent, and carrying out skin I TA values the 3rd week, the 5th week, the 8th week respectively tests the (improvement of ITA values
It is a careful important embodiment of skin pore), test result comparison is apparent, is added with the lotion sample of prescription element of the present invention
Product improve the samples of latex that be significantly better than without adding Chinese prescription to subjects skin's glossiness.
Embodiment 4
Skin shine Contrast on effect tests (condensation).
Experimental principle:
Prepare the medicinal extract extract of each Chinese herbal medicine according to the method for embodiment 1, and according to being converted to raw material dry weight meter river deer tooth
3 parts of dish, bitter white 2 parts of hoof, 1.5 parts of the stem of noble dendrobium, 2 parts of rhizoma alismatis, 2 parts of Radix Glycyrrhizae ratio mix to obtain extract formula, be further prepared into
Cosmetics condensation sample containing extract formula.
Volunteer smears the condensation sample containing extract formula of the present invention in left and right forehead respectively and without containing the present invention
The blank condensation sample of extract formula continues 8 weeks to 5 subjects test, respectively subject use the 3rd, 5,8 week to by
Examination person's ITA values are tested.Specific test result is as follows table 6-8;Wherein to containing powerful substance condensation formula, blank sample
Condensation formula, the average rate of change of two kinds of samples is referring to Fig. 2.
The ITA values test in the 3rd week of table 6
The ITA values test in the 5th week of table 7
The ITA values test in the 8th week of table 8
Analytical table 6-8 and Fig. 2 it is found that subject it is lasting using sample 3 weeks after, hence it is evident that have the effect that skin shine improves
Fruit, and the time is longer, improvement effect is more apparent, and carrying out skin I TA values the 3rd week, the 5th week, the 8th week respectively tests (ITA values
Improvement be a careful important embodiment of skin pore), test result comparison is apparent, is added with the condensation sample of prescription element
The condensation sample that be significantly better than without adding Chinese prescription is improved to subjects skin's glossiness, while showing sample in water
Effect is equally apparent in agent product.
Embodiment 5
Skin shine Contrast on effect tests (cream).
Prepare the medicinal extract extract of each Chinese herbal medicine according to the method for embodiment 1, and according to being converted to raw material dry weight meter river deer tooth
1 part of dish, bitter white 2 parts of hoof, 3 parts of the stem of noble dendrobium, 3 parts of rhizoma alismatis, 2 parts of Radix Glycyrrhizae ratio mix to obtain extract formula, be further prepared into and contain
The cosmetics cream sample of extract formula.
Volunteer smears the cream sample containing extract formula of the present invention in left and right forehead respectively and without containing the present invention
The blank cream sample of extract formula continues 8 weeks to 5 subjects test, respectively subject use the 3rd, 5,8 week to by
Examination person's ITA values are tested.Specific test result is as follows table 9-11;Wherein to containing powerful substance cream formula, blank sample
Cream formula, the average rate of change of two kinds of samples is referring to Fig. 3.
The ITA values test in the 3rd week of table 9
The ITA values test in the 5th week of table 10
The ITA values test in the 8th week of table 11
Analytical table 9-11 and Fig. 3 it is found that subject it is lasting using sample 3 weeks after, hence it is evident that there is skin shine to improve
Effect, and time longer improvement effect is more apparent, carrying out skin I TA values the 3rd week, the 5th week, the 8th week respectively tests (ITA values
Improvement be a careful important embodiment of skin pore), test result comparison is apparent, is added with the cream sample of prescription element
The cream sample that be significantly better than without adding Chinese prescription is improved to subjects skin's glossiness, while can be seen that in oil
In mutually relatively high formula system, Chinese prescription can equally play a role.
Embodiment 6
Image (VISIA faces imager), the analysis experiment of IPP softwares.
Experimental method:Tester test before first clean test position with clear water, after the 20min that sits quietly, progress VISIA take pictures,
Each test index values of 0W (T0) before recipient site sample is smeared are tested, then smear tested material according to regulation dosage, and in smearing
Tested material 2W (T1), 4W (T2), 6W (T3), 8W (T4) carry out VISIA and take pictures, test recipient site skin.During experiment, by
Position exposure is tried, is placed in test mode, keeps loosening.
Test result is as shown in table 12 and Fig. 4-6.
12 sample of table smears test result
The result of analytical table 12 and Fig. 4-6 it is found that several subjects persistently use sample 8 weeks, respectively the 2nd week, the 4th
It carries out full face VISIA in week, the 6th week, the 8th week to take pictures, most subjects start to change after using 4 weeks, begin within the 8th week bright
Aobvious variation;Changing value reaches as high as -6.65 in subject, it can be seen that effect is than more significant from data;Fig. 4-6 is to choose at random
The VISIA photo artworks of 3 subjects, the visible subject's pore of naked eyes is selected to become smaller, linked up with subject and although it is understood that subject
Feel that skin is fine and smooth, smooth many, it can be seen that this Chinese prescription have apparent careful pore, improve pachylosis,
Improve the effect of skin smoothness.
Embodiment 7
Skin care compositions is with the application in careful pore effect cosmetic.
The cosmetics are lotion, and by weight percentage, which includes:AMPHISOL K (0.4%), butanediol
(4%), 3 in Sensiva SC50 (0.1%), pentanediol (1%), trehalose (5%), EDTA-2Na (0.02%), embodiment 2
Number sample prescription (5%), hexylene glycol (0.5%), CARBOMER-TR (0.5%), EMULIM 22 (0.5%), saualane
(5%), DM10 (5%), VE acetates (5%), butter fruit (5%), TEA (0.5%), deionized water complement to 100%;
The specific preparation process of above-mentioned emulsion is:
1) it in deionized water by the CARBOMER-TR of formula ratio dissolvings, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), AMPHISOL K of formula ratio, butanediol, Sensiva SC50, penta are separately added into
Glycol, trehalose, EDTA-2Na, skin care compositions (No. 3 sample prescriptions in embodiment 2), hexylene glycol obtain water phase to being completely dissolved
Material;
3) EMULIM 22, saualane, DM10, VE acetate, butter fruit are completely dissolved respectively, obtain oil phase material;
4) oil phase material that step 3) obtains is poured into the water phase material of step 2), continue heating stirring to completely it is molten
Solution;
5) after the dissolving completely of above-mentioned all materials, continue stirring and be cooled to 45 DEG C hereinafter, adding TEA to get the breast
Liquid.
Embodiment 8
Skin care compositions is with the application in careful pore effect cosmetic.
The cosmetics are condensation, and by weight percentage, which includes:
Butanediol (5%), hyaluronic acid (0.2%), EDTA-2Na (0.02%), card wave 940 (0.4%), 4 sample of embodiment
Product prescription (5%), Sensiva SC50 (0.3%), pentanediol (1%), arginine (0.3%), deionized water (complement to
100%);
The specific preparation process of above-mentioned condensation is:
1) it in deionized water by the dissolving of the card wave 940 of formula ratio, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), it is separately added into butanediol, hyaluronic acid, EDTA-2Na, until being completely dissolved;
3) after step 2) dissolving completely, skin care compositions (the sample prescription of embodiment 4), the ethyl hexyl of formula ratio is added
Base glycerol, pentanediol after to be dissolved, continue stirring and are simultaneously stopped heating;
4) it waits for that the solution of step 3) is cooled to 45 DEG C hereinafter, weigh the arginine of formula ratio, is added to the solution of step 3)
In, to get the condensation after stirring evenly.
Embodiment 9
Skin care compositions is with the application in careful pore effect cosmetic.
The cosmetics are cream, and by weight percentage, which includes:
It is extract formula of the present invention (5%), hyaluronic acid (0.3%) described in hexylene glycol (0.5%), embodiment 5, fragrant fresh
Ketone (0.5%), card wave TR-1 (0.4%), PEG-100 stearates (3%), saualane (5%), cetanol (5%), VE
(3%), butter fruit (3%), 5 viscosity silicone oils (5%), DC1403 (3%), DRY-FLO PURE (3%), 10%NaOH
(0.5%), deionized water (complementing to 100%);
The specific preparation process of above-mentioned cream is:
1) it in deionized water by card wave TR-1 dissolvings, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), be separately added into hexylene glycol, skin care compositions (i.e. the extract formula of embodiment 5),
Hyaluronic acid, fragrant fresh ketone obtain water phase material to being completely dissolved;
3) the PEG-100 stearates of formula ratio, saualane, cetanol, VE, butter fruit are completely dissolved respectively, are obtained oily
Phase materials;
4) oil phase material that step 3) obtains is added in the water phase material of step 2), continue heating stirring to completely it is molten
Solution;
5) after the water phase of step 4) and oil phase dissolving completely, 5 viscosity silicone oils, DC1403, DRY-FLO are separately added into
PURE, until being completely dissolved;
6) after above-mentioned all materials dissolving completely, continue stirring and be cooled to 45 DEG C hereinafter, adding 10%NaOH to get cream
Frost.
Embodiment 10
Skin care compositions is with the application in careful pore effect cosmetic.
The cosmetics are the nutrient solution in patch facial mask, and by weight percentage, which includes:
Butanediol (5%), niacinamide (5%), EDTA-2Na (0.02%), card wave 940 (0.4%), xanthans
(0.3%), the extract formula of the present invention (5%) described in embodiment 6, allantoin (0.1%), Sensiva SC50 (0.2%),
Pentanediol (1%), TEA (0.4%), deionized water (complementing to 100%);
The specific preparation process of above-mentioned patch facial mask nutrient solution is:
1) it in deionized water by the dissolving of card wave 940, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), butanediol, niacinamide, EDTA-2Na, xanthans, stirring and dissolving are separately added into;
3) after the solution of step 2) is completely dissolved, skin care compositions (i.e. the extract formula of embodiment 6), allantois is added
Element, Sensiva SC50, pentanediol after to be dissolved, continue stirring and are simultaneously stopped heating;
4) wait for that solution is cooled to 45 DEG C hereinafter, addition TEA, stirs evenly up to the patch facial mask nutrient solution.
The above samples of latex, condensation sample, cream sample and each 3 parts of patch facial mask nutrient solution sample are prepared respectively, respectively
Under room temperature, low temperature (- 15 DEG C), high temperature (40 DEG C), product stability is investigated, investigates primary, lasting one month, breast weekly
Liquid sample, condensation sample, cream sample and patch facial mask nutrient solution sample do not occur discoloration under low temperature and high-temperature condition, divide
Phenomena such as layer, show that product stability is preferable.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
Any modification, equivalent replacement or improvement etc., should all be included in the protection scope of the present invention made by within refreshing and principle.
Claims (9)
1. a kind of skin care compositions, which is characterized in that including Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae, the Swertia patens,
Bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae weight ratio be (1~5):(1~5):(1~5):(1~3):(1~5).
2. a kind of skin care compositions according to claim 1, which is characterized in that the Swertia patens, bitter white hoof, the stem of noble dendrobium, pool
It rushes down, Radix Glycyrrhizae preferably uses Herba Swertiae bimaculatae extract, laricifomes officinalis, Herba Dendrobii extract, Alisma extract, Radix Glycyrrhizae extraction respectively
Object is made by following steps respectively:
Chinese herbal medicine Swertia patens, bitter white hoof, the stem of noble dendrobium, rhizoma alismatis, Radix Glycyrrhizae are crushed respectively, according to feed liquid weight ratio 1:(30~50) it is added
The ethyl alcohol of 90% or more volumetric concentration after extracting 0.5~4 hour, recycles ethyl alcohol, i.e., obtains each extract of medicinal extract form respectively.
3. a kind of skin care compositions according to claim 2, which is characterized in that the Chinese herbal medicine Swertia patens, bitter white hoof, stone
Dry measure used in former times, rhizoma alismatis, Radix Glycyrrhizae smash it through 60 mesh sieve.
4. a kind of skin care compositions according to claim 2, which is characterized in that the Herba Swertiae bimaculatae extract, bitter white hoof carry
Object, Herba Dendrobii extract, Alisma extract, licorice are taken, is made respectively especially by following steps:
1) it uses grinder that each Chinese herbal medicine is ground into powdery fine crushing respectively, crosses 60 mesh sieve, screened mesh Chinese medicine fine crushing;
2) it is 1 according to the feed liquid weight ratio of Chinese herbal medicine and ethyl alcohol:(30~50) weigh ethanol in proper amount reagent, impregnate each Chinese herbal medicine
0.5~2 hour, electric jacket heating is placed, heating temperature opens cool circulation water and carries out circumfluence distillation 1~3 hour to 78 DEG C,
Obtain alcohol extract;
3) alcohol extract is moved into Rotary Evaporators, vacuumized, 60 DEG C of progress heating recovery ethyl alcohol of water-bath, 30min~60min
Afterwards to get each extract of medicinal extract form.
5. one kind having careful pore effect cosmetic, which is characterized in that contain any one of claim 1-4 institutes in the cosmetics
The skin care compositions stated.
6. according to claim 5 a kind of with careful pore effect cosmetic, which is characterized in that the cosmetics are breast
Liquid, by weight percentage, which includes:
AMPHISOL K of 0.4%-0.8%, the butanediol of 4%-8%, the Sensiva SC50 of 0.04%-0.1%, 1%-
3% pentanediol, the trehalose of 2%-6%, 0.02%-0.08% EDTA-2Na, 0.05%-5% skin care compositions,
The hexylene glycol of 0.4%-0.8%, the EMULIM 22 of CARBOMER-TR, 0.4%-0.8% of 0.4%-0.8%, 4%-8%
The TEA of saualane, the VE acetates of DM10,1%-5% of 1%-5%, the butter fruit of 1%-5%, 0.4%-0.8%, surplus
Deionized water;
The specific preparation process of above-mentioned emulsion is:
1) it in deionized water by the CARBOMER-TR of formula ratio dissolvings, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), be separately added into AMPHISOL K of formula ratio, butanediol, Sensiva SC50, pentanediol,
Trehalose, EDTA-2Na, skin care compositions, hexylene glycol obtain water phase material to being completely dissolved;
3) EMULIM 22, saualane, DM10, VE acetate, butter fruit are completely dissolved respectively, obtain oil phase material;
4) oil phase material that step 3) obtains is poured into the water phase material of step 2), continues heating stirring to being completely dissolved;
5) after the dissolving completely of above-mentioned all materials, continue stirring and be cooled to 45 DEG C hereinafter, adding TEA to get the lotion.
7. according to claim 5 a kind of with careful pore effect cosmetic, which is characterized in that the cosmetics are solidifying
Dew, by weight percentage, which includes:
EDTA-2Na, 0.4%-0.8% of the butanediol of 4%-8%, the hyaluronic acid of 0.1%-0.5%, 0.02%-0.08%
Card wave 940, the skin care compositions of 0.05%-5%, the Sensiva SC50 of 0.1%-0.5%, 1%-5% pentanediol,
The arginine of 0.1%-0.5%, the deionized water of surplus;
The specific preparation process of above-mentioned condensation is:
1) it in deionized water by the dissolving of the card wave 940 of formula ratio, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), it is separately added into butanediol, hyaluronic acid, EDTA-2Na, until being completely dissolved;
3) after step 2) dissolving completely, the skin care compositions, Sensiva SC50, pentanediol of formula ratio is added, after to be dissolved,
Continue stirring and is simultaneously stopped heating;
4) it waits for that the solution of step 3) is cooled to 45 DEG C hereinafter, weigh the arginine of formula ratio, is added in the solution of step 3), stirs
To get the condensation after mixing uniformly.
8. according to claim 5 a kind of with careful pore effect cosmetic, which is characterized in that the cosmetics are cream
Frost, by weight percentage, which includes:
The hexylene glycol of 0.4%-0.8%, the skin care compositions of 0.05%-5%, the hyaluronic acid of 0.1%-0.5%, 0.4%-
The spiny dogfish of 0.8% fragrant fresh ketone, the PEG-100 stearates of card wave TR-1,1%-5% of 0.4%-0.8%, 5%-10%
Alkane, the cetanol of 1%-5%, the butter fruit of VE, 1%-5% of 1%-5%, 5 viscosity silicone oils of 1%-5%, 1%-3%
DRY-FLO PURE of DC1403,1%-5%, the 10%NaOH of 0.4%-0.8%, the deionized water of surplus;
The specific preparation process of above-mentioned cream is:
1) it in deionized water by card wave TR-1 dissolvings, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), hexylene glycol, skin care compositions, hyaluronic acid, fragrant fresh ketone is separately added into being completely dissolved, is obtained
Water phase material;
3) the PEG-100 stearates of formula ratio, saualane, cetanol, VE, butter fruit are completely dissolved respectively, obtain oil phase thing
Material;
4) oil phase material that step 3) obtains is added in the water phase material of step 2), continues heating stirring to being completely dissolved;
5) after the water phase of step 4) and oil phase dissolving completely, it is separately added into 5 viscosity silicone oils, DC1403, DRY-FLO PURE, until
It is completely dissolved;
6) after above-mentioned all materials dissolving completely, continue stirring and be cooled to 45 DEG C hereinafter, adding 10%NaOH to get cream.
9. according to claim 5 a kind of with careful pore effect cosmetic, which is characterized in that the cosmetics are patch
Nutrient solution in piece facial mask, by weight percentage, which includes:
The butanediol of 4%-8%, the niacinamide of 1%-8%, 0.02%-0.08% EDTA-2Na, 0.4%-0.8% card wave
940, the xanthans of 0.1%-0.5%, the skin care compositions of 0.05%-5%, the allantoin of 0.1%-0.3%, 0.1%-
The TEA of 0.5% Sensiva SC50, the pentanediol of 1%-5%, 0.4%-0.8%, the deionized water of surplus;
The specific preparation process of above-mentioned patch facial mask nutrient solution is:
1) it in deionized water by the dissolving of card wave 940, is heated with stirring to and is completely dissolved;
2) into the solution of step 1), butanediol, niacinamide, EDTA-2Na, xanthans, stirring and dissolving are separately added into;
3) after the solution of step 2) is completely dissolved, skin care compositions, allantoin, Sensiva SC50, pentanediol is added, waits for molten
Xie Hou continues stirring and is simultaneously stopped heating;
4) wait for that solution is cooled to 45 DEG C hereinafter, addition TEA, stirs evenly up to the patch facial mask nutrient solution.
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CN109512736A (en) * | 2018-11-19 | 2019-03-26 | 北京明弘科贸有限责任公司 | A kind of skin care compositions and the cosmetics with careful pore effect |
CN109535269A (en) * | 2018-09-26 | 2019-03-29 | 北京明弘科贸有限责任公司 | A kind of preparation process and its application of dendrobium nobile micromolecular polysaccharide extracting solution |
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