CN107224416A - A kind of anti-oxidant face mask - Google Patents

A kind of anti-oxidant face mask Download PDF

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Publication number
CN107224416A
CN107224416A CN201710436119.7A CN201710436119A CN107224416A CN 107224416 A CN107224416 A CN 107224416A CN 201710436119 A CN201710436119 A CN 201710436119A CN 107224416 A CN107224416 A CN 107224416A
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Prior art keywords
extract
face mask
ali
quinoa
oxidant face
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CN201710436119.7A
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Chinese (zh)
Inventor
鲁翠容
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Foshan Huili Cosmetics Science And Technology Co Ltd
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Foshan Huili Cosmetics Science And Technology Co Ltd
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Priority to CN201710436119.7A priority Critical patent/CN107224416A/en
Publication of CN107224416A publication Critical patent/CN107224416A/en
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/592—Mixtures of compounds complementing their respective functions

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Engineering & Computer Science (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Biotechnology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to a kind of anti-oxidant face mask, including following mass percent component：NMF：10 25%, fullerene：0.1 3%, quinoa extract：0.1 5%, Ali's sage extract：0.1 5%, thickener：0.1 3%, conditioner：0.1 0.5%.The fullerene that the present invention is used has good antioxygenic property, can effective scavenging capacity oxygen radical, activating skin cells, pre- anti-aging；Quinoa extract is rich in polyphenol and Flavonoid substances, with good in vitro anti-oxidation；Ali's sage extract contains the chemical compositions such as flavones, polysaccharide, soaping agents and terpenes, can improve the immunocompetence of skin, play a part of antioxidant and anti-aging；There is Synergistic in formula between each component, the effects such as with moisturizing, anti-oxidant, anti-aging.

Description

A kind of anti-oxidant face mask
Technical field
The present invention relates to cosmetic field, a kind of anti-oxidant face mask is specifically related to.
Background technology
Free radical (free radical) is also known as free radical, is the atom containing unpaired electron, atomic group, molecule, from Son or its group are referred to as free radical.It is referred to as oxygen radical (oxygen free if the oxygen containing unpaired electron Radical, OFR), more than the 95% of machine interior free yl is accounted for, it is that discharge during people's vivo oxidation a kind of active has Evil material.It robs the electronics of other molecules wantonly in vivo, destroys the structure of cell, DNA, RNA and protein, makes in vivo The dirty function of cell tissue, device is reduced, can not repaired again, declines internal function of immune system, so as to cause various The generation of disease, even death.
Aging course is related to many internal and external factors, and the most common endogenous Some Circulating Factors relevant with aging course are certainly By base.Domestic and international numerous studies have proven to：Geriatric animals and the elderly's serum lipids free radical (MDA) level increase (especially brain, liver cell in) lipofuscin content increases in height, tissue.Organize lipofuscin content how much can be as the objective of aging One of according to, its formation is relevant with lipid free radical.The catabolite of lipid free radical is aldehydes, and it can be with protein, phosphorus matter Reacted with the amino of nucleic acid, crosslink molecule, the result of crosslinking makes protein denaturation, inactivates enzyme.These denaturation things Matter is swallowed by phagocyte, but can not digest completely, is as a result continuously increased intracellular year pigment.Harman is pointed out, in escaping The toxic action that the free radical of sum is gathered, it may be possible to the basic reason of aging.
The A of Chinese patent application CN 104224602 disclose a kind of anti-oxidant face mask, using water lily anthocyanidin as main antioxygen Chemical conversion point, by mask matrix of aloe glue, natural grape seed oil as substrate oil, without using chemical emulsifier or mineral Oil, anti-corrosion composition is the natural antibacterial agent from marine organisms, and acid-base modifier is natural lemon acid.Although the facial mask is containing anti- Oxidizing component, but its oxidation-resistant active ingredient is too single, it is impossible to play good antioxidant effect.
The content of the invention
The present invention according to the deficiencies in the prior art there is provided a kind of anti-oxidant face mask, from fullerene Scavenger of ROS from By base, activating skin cells, pre- anti-aging, coordinate the work that antioxidant and anti-aging is reached with quinoa extract, Ali's sage extract With playing a part of Synergistic.
To achieve the above object, the present invention is adopted the following technical scheme that：
A kind of anti-oxidant face mask of the present invention, including following mass percent component：
NMF：10-25%；
Fullerene：0.01-3%；
Quinoa extract：0.01-5%；
Ali's sage extract：0.01-5%；
Thickener：0.1-3%；
Conditioner：0.1-0.5%；
The quinoa extract is placed in 250ml round-bottomed flasks to take dry quinoa 5.0-10.0g, adds water to flask 1/ At 3-1/2, extracted, filtered 2-3 times using ultrasonic extraction, reflux extraction or cold soaking extraction method, quinoa is contained in gained filtrate Activity substance content is 28-43%；
Ali's sage extract is that Ali red is dried into medicinal material 8.0-12.0g to crush, and crosses 50-100 mesh sieves, plus 8-15 times Measure deionized water to flow back 2-3 times, each 1.5-3h, mixed extract is placed in rotary evaporator and is concentrated into 10-20ml, gained Activity substance content containing Ali red is 26-39% in concentrate.
It is preferred that, in a preferred embodiment of the invention, a kind of described anti-oxidant face mask, including following quality hundred Divide and compare component：
NMF：15-20%；
Fullerene：1-2%；
Quinoa extract：1-4%；
Ali's sage extract：1.5-3.5%；
Thickener：1-2%；
Conditioner：0.2-0.4%.
In a preferred embodiment of the invention, the NMF is glycerine, butanediol, polyethylene glycol, sorbierite, thoroughly At least one of sour sodium of bright matter.
In a preferred embodiment of the invention, the thickener is at least one in carbomer, xanthans, guar gum Kind.
In a preferred embodiment of the invention, the conditioner is allantoin.
Quinoa is a kind of full nutrition adequate proteins " false cereal ", and it is not only containing abundant protein, fat, starch, dimension The conventional nutrients such as raw element and mineral matter, also containing the nutrition of the bioactivity such as polyphenol, flavones, saponin(e, Quercetin, agglutinin into Point.It is reported that the polyphenols in quinoa extract has good in vitro anti-oxidation, wherein, quinoa seed, bud and leaf Content is very high in piece.Therefore, quinoa is a kind of rare antioxidation foodstuff.Flavonoid substances are rich in quinoa, and content is special Not high, 36~73mg/100g has averagely reached 58mg/100g, wherein, most important component is flavonols, average out to 174mg/100g, Quercetin average out to 36mg/100g, Kaempferol average out to 20mg/100g.Rich in many in quinoa seed extract Aldehydes matter, is topmost polyphenoils.
Ali red, also known as bitter white hoof, category Basidiomycetes, Aphyllophorales, Polyporaceae, heterophyta fungi, are larch Pathogen, is mainly distributed on China western part and northeast, and wherein Xinjiang forest zone is widely distributed, is produced and is write the most with Altay forest zone especially Name, easily collection.As conventional Uygur's medicinal material, there are warm stomach eliminating the phlegm, dispelling wind and eliminating dampness, the function of swelling diuretic, and can increase The stress ability of strong muscle power and body.Ali red contains the chemical compositions such as flavones, polysaccharide, soaping agents and terpenes.Ali red is more Sugar can effectively remove O in vitro2 -, have significant immunological enhancement, with certain anti-aging effects.Ali red flavones can Mitigate body lipid peroxidation injury, improve activities of antioxidant enzymes, enhancing intrinsic antioxidative ability, so as to play anti-aging work With.There are some researches show Ali red polysaccharide has certain anti-aging effects, it is it to absolutely prove flavones in Ali red, polysaccharide Anti-aging active ingredient.
In the 1980s, the mankind are found that C60, the new stage recognized carbon is thus opened, stone is being found that in succession After ink, diamond, the third simple substance existed with carbon crystal form is found.C60It is that there is uniqueness containing numerous double bonds The three-dimensional aromatic compound of cagelike structure.The carbon atom that its 60 are located on summit constitutes spherical 32 face body, wherein having 12 Individual face is pentagon, and 20 faces are hexagons.This structure is similar to the football seen in daily life, therefore also referred to as " football alkene ".This special structure makes it have the excellent property such as special superconduction, ferromagnetism, high pressure resistant, resist chemical Matter.Had a extensive future in fields such as superconductor, photoconductive material, cosmetics, nanometer particle material, biomedicines.
It is well known that vitamin C has inoxidizability.But fullerene C60Oxidation resistance be ascorbic 125 times. In addition to antioxidation, fullerene C60Can also effective scavenging capacity oxygen radical, activating skin cells, pre- anti-aging etc. Effect.
Compared with prior art, beneficial effects of the present invention are：, can be effective 1. fullerene has good antioxygenic property Scavenging capacity oxygen radical, activating skin cells, pre- anti-aging；2. quinoa extract is rich in polyphenol and Flavonoid substances, tool There is good in vitro anti-oxidation；3. Ali's sage extract contains the chemical compositions such as flavones, polysaccharide, soaping agents and terpenes, can The immunocompetence of skin is improved, plays a part of antioxidant and anti-aging；4. playing the role of Synergistic between each component in formula, have The effects such as having moisturizing, anti-oxidant, anti-aging.
Embodiment
With reference to specific embodiment, the present invention is described in further detail.
Embodiment 1
Dry quinoa 5.0g is taken, is placed in 250ml round-bottomed flasks, is added water at flask 1/3, using ultrasonic extraction, is returned Flow extraction method or cold soaking extraction method is extracted, crude extract is filtered 2 times；
Embodiment 2
Dry quinoa 7.5g is taken, is placed in 250ml round-bottomed flasks, is added water at flask 1/3, using ultrasonic extraction, is returned Flow extraction method or cold soaking extraction method is extracted, by crude extract filter 23；
Embodiment 3
Dry quinoa 10.0g is taken, is placed in 250ml round-bottomed flasks, is added water at flask 1/2, using ultrasonic extraction, is returned Flow extraction method or cold soaking extraction method is extracted, by crude extract filter 23；
Embodiment 4
Take Ali red to dry medicinal material 8.0g to crush, cross 50 mesh sieves, plus 8 times of amount deionized waters flow back 2 times, each 1.5h is mixed Extract solution is closed, is placed in rotary evaporator and is concentrated into 10ml.
Embodiment 5
Take Ali red to dry medicinal material 10.0g to crush, cross 75 mesh sieves, plus 11 times of amount deionized waters flow back 3 times, each 2.2h, Mixed extract, is placed in rotary evaporator and is concentrated into 15ml.
Embodiment 6
Take Ali red to dry medicinal material 12.0g to crush, cross 100 mesh sieves, plus 15 times of amount deionized waters flow back 3 times, each 3h is mixed Extract solution is closed, is placed in rotary evaporator and is concentrated into 20ml.
Embodiment 7~11
A kind of 5 specific embodiments of anti-oxidant face mask of the present invention are listed in table 1.
Quinoa extract in embodiment 7-8 derives from above-described embodiment 1 and embodiment 4 with Ali's sage extract；Implement Quinoa extract in example 9 derives from above-described embodiment 2 and embodiment 5 with Ali's sage extract；Quinoa in embodiment 10-11 Extract derives from above-described embodiment 3 and embodiment 6 with Ali's sage extract.
Table 1
A kind of 5 specific comparative examples of anti-oxidant face mask of the present invention are listed in table 2.
Table 2
Oxidation resistance is tested
Determination oxidative is carried out to above-described embodiment 7-11.
DPPH free radical 10mg accurately are weighed, is dissolved with absolute ethyl alcohol and constant volume is in 250ml volumetric flasks, then DPPH The mass concentration of free radical reagent is 0.04mg/mL, is kept in dark place standby.Different implementations are determined by following assay method respectively The oxidation resistance of example.
The facial mask of embodiment 7 that the above-mentioned DPPH free radicals reagent solutions of 2mL and 2mL are prepared is added in first test tube Liquid, is sufficiently mixed；The facial mask liquid of embodiment 7 and 2mL deionized waters that 2mL has been configured are added in second test tube；At the 3rd 2mLDPPH free radicals reagent solution and 2mL deionized waters are added in test tube.Determine three after 30min respectively under the conditions of 517nm Solution absorbance in branch test tube.Clearance rate K of the solution to DPPH free radicals in first test tube1It can be calculated with following formula：
K1=[Ac- (Ai-Aj)]/Ac*100%
In above formula：
The absorbance of solution in first test tube of Ai=；
The absorbance of solution in second test tube of Aj=；
The absorbance of solution in the 3rd test tube of Ac=.
The K of said determination1Value is the oxidation resistance of the facial mask liquid of embodiment 7 (i.e. to the removing of DPPH free radicals Rate).Equally determine the oxidation resistance of embodiment 8,9,10,11 respectively as stated above, the different embodiment samples measured The clearance rate of DPPH free radicals is as shown in table 3 below：
Table 3
Sample Embodiment 7 Embodiment 8 Embodiment 9 Embodiment 10 Embodiment 11
Clearance rate (K) 85.65% 74.98% 98.79% 81.87% 92.36%
As can be seen from the above table, embodiment 9 has reached highest to the clearance rate of DPPH free radicals in the present embodiment, freely The clearance rate of base has reached 98.79%.
Evaluation test on probation
Preferably to prove that a kind of anti-oxidant face mask provided by the present invention has an excellent effect, choose embodiment 7,8, 9th, 10,11 and reference examples 1,2,3,4,5 carry out further on probation investigation and evaluation test.Embodiment is as follows：Choose 100 Special volunteer, age distribution is 28-58 Sui.The wherein people of male 40, the people of women 60.Evaluation test is carried out to embodiment, each The sampling phase is one month, and it is facial drying, aging crowd to try out object.Table 4 is test index and result.
Table 4
As a result show：
The number that embodiment 7-11 dry skins, aging crowd are obviously improved as seen from Table 4 will be significantly more than comparative example 1- 5, illustrate a kind of anti-oxidant face mask of the invention containing fullerene, quinoa extract and Ali's sage extract is used for a long time, have significantly Improve facial drying, the effect of aging, the effect for improving significantly and alleviating.And embodiment 9 substantially changes with best Effect that is kind and alleviating, embodiment 9 is optimization formula of the present invention.Comparative example 1 is obviously improved dry skin number for 5 people, hence it is evident that It is 4 people to improve skin aging number, hence it is evident that less than other embodiment and comparative example, show a kind of master of anti-oxidant face mask of the invention It is fullerene, quinoa extract and Ali's sage extract to want functional component.Comparative example 1-4 contrasts the visible present invention with embodiment 9 In anti-oxidant face mask, functional component fullerene, quinoa extract and Ali's sage extract have the effect of Synergistic.In addition by There is not allergy or are related to the phenomenon of skin lesion in examination personnel, i.e., security of the present invention is preferable.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art is in the technical scope of present disclosure, the change or replacement that can be readily occurred in, It should all be included within the scope of the present invention.Therefore, protection scope of the present invention should be with the protection of claims Scope is defined.

Claims (6)

1. a kind of anti-oxidant face mask, including following mass percent component：NMF：10-25%, fullerene：0.01-3%, lamb's-quarters Wheat extract：0.01-5%, Ali's sage extract：0.01-5%, thickener：0.1-3%, conditioner：0.1-0.5%；It is described The preparation process of quinoa extract is placed in 250ml round-bottomed flasks to take dry quinoa 5.0-10.0g, adds water to flask 1/3- At 1/2, extracted using ultrasonic extraction, reflux extraction or cold soaking extraction method, crude extract is filtered 2-3 times；The Ali red The preparation process of extract is that Ali red is dried into medicinal material 8.0-12.0g to crush, and crosses 50-100 mesh sieves, plus 8-15 times is measured deionization Water flows back 2-3 times, and each 1.5-3h, mixed extract is placed in rotary evaporator and is concentrated into 10-20ml.
2. anti-oxidant face mask according to claim 1, including following mass percent component：NMF：15-20%, richness Strangle alkene：1-2%, quinoa extract：1-4%, Ali's sage extract：1.5-3.5%, thickener：1-2%, conditioner：0.2- 0.4%.
3. anti-oxidant face mask according to claim 1 or 2, it is characterised in that the NMF is glycerine, butanediol, gathered At least one of ethylene glycol, sorbierite, Sodium Hyaluronate.
4. anti-oxidant face mask according to claim 1 or 2, it is characterised in that the thickener be carbomer, xanthans, At least one of guar gum.
5. anti-oxidant face mask according to claim 1 or 2, it is characterised in that the conditioner is allantoin.
6. the anti-oxidant face mask according to claim 1-2, it is characterised in that including following mass percent component：Fowler Alkene：1.5%th, butanediol：1%th, glycerine：18.5%th, Sodium Hyaluronate：0.5%th, quinoa extract：2.5%th, Ali red is extracted Thing：2.5%th, guar gum：1.5%th, allantoin：0.2%.
CN201710436119.7A 2017-06-09 2017-06-09 A kind of anti-oxidant face mask Withdrawn CN107224416A (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108324636A (en) * 2018-03-23 2018-07-27 北京明弘科贸有限责任公司 A kind of skin care compositions and with careful pore effect cosmetic, preparation method
CN108379190A (en) * 2018-04-16 2018-08-10 广州雷诺生物科技有限公司 A kind of dried noodle film containing fullerene
CN108578337A (en) * 2018-05-02 2018-09-28 广州雷诺生物科技有限公司 A kind of nourishing pack containing fullerene
CN108938506A (en) * 2018-10-09 2018-12-07 姜广建 Wrinkle lotion and preparation method thereof is gone in a kind of moisturizing
CN109316363A (en) * 2018-12-07 2019-02-12 北京富乐喜科技有限公司 A method of there is the skin conditioner of moisturizing, anti-senescence function using fullerene preparation
CN109350573A (en) * 2018-12-03 2019-02-19 陈雄 A kind of gel
CN109364212A (en) * 2018-11-20 2019-02-22 尤永宽 A kind of toxin-expelling and face nourishing umbilica sticking plaster
CN109966203A (en) * 2019-04-02 2019-07-05 北京旋光普利生物医药科技开发有限公司 A kind of preparation of hydrosol fullerene facial mask
CN111265460A (en) * 2020-03-13 2020-06-12 佛山市奥姿美生物科技有限公司 Skin barrier repair compositions and uses thereof
CN114469818A (en) * 2022-03-17 2022-05-13 广东丸美生物技术股份有限公司 Chenopodium quinoa willd extract, preparation method and application thereof, and extracting agent for extracting chenopodium quinoa willd polyphenol

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108324636A (en) * 2018-03-23 2018-07-27 北京明弘科贸有限责任公司 A kind of skin care compositions and with careful pore effect cosmetic, preparation method
CN108379190A (en) * 2018-04-16 2018-08-10 广州雷诺生物科技有限公司 A kind of dried noodle film containing fullerene
CN108578337A (en) * 2018-05-02 2018-09-28 广州雷诺生物科技有限公司 A kind of nourishing pack containing fullerene
CN108938506A (en) * 2018-10-09 2018-12-07 姜广建 Wrinkle lotion and preparation method thereof is gone in a kind of moisturizing
CN108938506B (en) * 2018-10-09 2021-04-30 姜广建 Moisturizing and wrinkle-removing emulsion and preparation method thereof
CN109364212A (en) * 2018-11-20 2019-02-22 尤永宽 A kind of toxin-expelling and face nourishing umbilica sticking plaster
CN109350573A (en) * 2018-12-03 2019-02-19 陈雄 A kind of gel
CN109316363A (en) * 2018-12-07 2019-02-12 北京富乐喜科技有限公司 A method of there is the skin conditioner of moisturizing, anti-senescence function using fullerene preparation
CN109966203A (en) * 2019-04-02 2019-07-05 北京旋光普利生物医药科技开发有限公司 A kind of preparation of hydrosol fullerene facial mask
CN111265460A (en) * 2020-03-13 2020-06-12 佛山市奥姿美生物科技有限公司 Skin barrier repair compositions and uses thereof
CN114469818A (en) * 2022-03-17 2022-05-13 广东丸美生物技术股份有限公司 Chenopodium quinoa willd extract, preparation method and application thereof, and extracting agent for extracting chenopodium quinoa willd polyphenol
CN114469818B (en) * 2022-03-17 2023-09-15 广东丸美生物技术股份有限公司 Quinoa extract, preparation method and application thereof, and extractant for extracting quinoa polyphenol

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