CN108272707B - Chinese herbal medicine hair conditioner and preparation method thereof - Google Patents
Chinese herbal medicine hair conditioner and preparation method thereof Download PDFInfo
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- CN108272707B CN108272707B CN201810368381.7A CN201810368381A CN108272707B CN 108272707 B CN108272707 B CN 108272707B CN 201810368381 A CN201810368381 A CN 201810368381A CN 108272707 B CN108272707 B CN 108272707B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention belongs to the technical field of daily cosmetics, and particularly relates to a Chinese herbal medicine hair conditioner and a preparation method thereof. The Chinese herbal medicine extract for preparing the Chinese herbal medicine hair conditioner is prepared from the following raw materials in parts by mass: 1-60 parts of ginseng, 1-60 parts of rhizoma polygonati, 1-30 parts of polygonum multiflorum and 1-30 parts of ginger. The invention takes the traditional Chinese medicine theory and the modern Chinese medicine research as guidance to carry out Chinese herbal medicine composing prescription and exert the advantages of the traditional Chinese medicine. The prepared Chinese herbal medicine hair conditioner plays the effects of blackening and growing hair, preventing alopecia and relieving itching, and nourishing hair roots and scalp by depending on pure plants, has the advantages of simple preparation method, low cost, no anaphylactic reaction after use, no toxic or side effect, smoothness and smoothness of hair, capability of meeting the requirements of people on health preservation, easiness in favorite and acceptance of the public, and suitability for daily and long-term use by consumers.
Description
Technical Field
The invention belongs to the technical field of daily cosmetics, and particularly relates to a Chinese herbal medicine hair conditioner and a preparation method thereof.
Background
With the improvement of the living standard of residents, the increasing popularity of hair perming and hair dyeing and the factors of environment, pressure and the like cause the common malnutrition of hair roots and hair of people, and then the hair becomes thinner, dry and even becomes crisp and falls off. Therefore, the hair care products become one of the necessities of modern families, and the plant herbal hair care series products are particularly sought by people.
The traditional Chinese medicine is a traditional medicine in China, the history is long, and at present, the washing and caring product containing the Chinese herbal medicines is declared to have the following problems in the market: the advantages of the Chinese herbal medicine components are not really exerted, or a large amount of chemical reagents or hormones and the like are added, so that the natural effects of the plants are not exerted; or the scientific nature of the formula needs to be studied without adopting the theoretical basis of the traditional Chinese medicine as guidance; or the extraction method has poor specialty, and the system is unstable after the Chinese herbal medicine extract is added, so that the advantages of the Chinese herbal medicine cannot be really exerted; furthermore, as is known, the Chinese herbal medicine extract has a plurality of components, and these complex components directly affect the uniformity of the product and the stability in the placing process, and are easy to cause phenomena such as product discoloration, paste thinning, layering and the like, thereby causing the product to be unqualified.
The hair care products become one of the necessities of modern families, and the plant herbal hair care series products are more popular and accepted by the public and are a future trend. Therefore, an effective hair care product really containing natural and green Chinese herbal medicine effective components needs to be developed, and another way is provided for the Chinese medicinal science development in China.
Disclosure of Invention
In view of the above, the present invention aims to provide a Chinese herbal medicine extract for hair nourishing and caring and a Chinese herbal medicine hair conditioner prepared by using the Chinese herbal medicine extract, which relies on pure plant components to exert the effects of hair blacking and regrowing, hair loss prevention and itching relief, and hair root and scalp nutrition.
In order to achieve the purpose, the technical scheme of the invention is as follows:
the Chinese herbal medicine extract for nourishing and protecting hair is prepared from the following raw materials in parts by mass: 1-60 parts of ginseng, 1-60 parts of rhizoma polygonati, 1-30 parts of polygonum multiflorum and 1-30 parts of ginger.
Preferably, the Chinese herbal medicine extract is prepared from the following raw materials in parts by mass: 5-45 parts of ginseng, 5-50 parts of rhizoma polygonati, 5-25 parts of polygonum multiflorum and 5-25 parts of ginger.
Preferably, the Chinese herbal medicine extract is prepared from the following raw materials in parts by mass: 10-20 parts of ginseng, 15-45 parts of rhizoma polygonati, 10-20 parts of polygonum multiflorum and 10-20 parts of ginger.
Preferably, the Chinese herbal medicine extract is prepared from the following raw materials in parts by mass: 15 parts of ginseng, 45 parts of rhizoma polygonati, 15 parts of polygonum multiflorum and 15 parts of ginger.
The invention takes the traditional Chinese medicine theory and the research of the modern traditional Chinese medicine as guidance, carries out Chinese herbal medicine composing prescription, prepares the pure plant extracts of rhizoma polygonati, ginseng, fleece-flower root and ginger, exerts the advantages of the traditional Chinese medicine, and reasonably mixes the extracts according to the traditional Chinese medicine theory to exert the functions of blackening hair, nourishing hair root and hair.
According to the theory of Chinese traditional medicine: the causes of hair loss, white hair, and hair malnutrition are thought to be mainly in the liver, kidneys, and lung and spleen. The spleen is the acquired root, the food is the source of the generation, the kidney is the innate root, the kidney stores essence, the essence is bloomed in hair, the liver stores blood, the hair is the rest of the blood, the essence and the blood are homologous, and the essence and the blood are integrated, so the spleen, the liver and the kidney are sufficient, the essence and the blood are sufficient, and the hair can be nourished; the liver governs smoothing flow of qi, maintains blood circulation, the lung governs dispersing hair, and combines skin in vivo, and the liver and lung function are normal, so essence and blood can be transported to hair, and the hair is nutritious, glossy, black and bright.
According to the theory of traditional Chinese medicine, ginseng is used as a monarch drug, qi is tonified, spleen and lung are benefited, body fluid is generated, blood is nourished, rhizoma polygonati is used for nourishing yin and moistening lung, qi is tonified, spleen is invigorated, fleece-flower root is used as a ministerial drug for tonifying liver and kidney and benefiting essence and blood, and ginger is used as an assistant drug for detoxifying and growing hair. The whole formula is compatible, and the effects of tonifying qi and yin, benefiting essence and blood, growing hair, blackening hair, preventing alopecia, removing dandruff and relieving itching are achieved.
The medicinal materials for tonifying qi, strengthening spleen and benefiting lung comprise: red ginseng, ginseng leaf, codonopsis pilosula, American ginseng, radix pseudostellariae, astragalus membranaceus, bighead atractylodes rhizome, Chinese yam, hyacinth bean, sea buckthorn, acanthopanax, gynostemma pentaphylla, rhodiola rosea and honey.
The medicinal materials for tonifying liver and kidney and benefiting essence and blood comprise: rehmannia root, Chinese angelica, white paeony root, longan pulp, human placenta, longspur epimedium, eucommia bark, south dodder seed, desertliving cistanche, flatstem milkvetch seed, common macrocarpium fruit and malaytea scurfpea fruit.
Yin-nourishing medicinal materials: radix adenophorae, lily, radix ophiopogonis, asparagus cochinchinensis, dendrobe, radix polygonati officinalis, wolfberry, black sesame, eclipta alba, glossy privet fruit and mulberry.
The medicinal materials for detoxifying and relieving itching comprise: garlic, mint, propolis, fructus cnidii, sulfur, radix sophorae flavescentis, cortex dictamni, rhizoma smilacis glabrae and caulis polygoni multiflori.
The Ginseng radix can be replaced by one or more of Ginseng radix Rubri, folium Ginseng, radix Codonopsis, radix Panacis Quinquefolii, radix Pseudostellariae, radix astragali, Atractylodis rhizoma, rhizoma Dioscoreae, semen lablab album, fructus Hippophae, radix Acanthopanacis Senticosi, herba Gynostemmatis, radix Rhodiolae, and Mel.
The Polygoni Multiflori radix can be replaced by one or more of rehmanniae radix, radix Angelicae sinensis, radix Paeoniae alba, arillus longan, placenta hominis, herba Epimedii, Eucommiae cortex, semen Cuscutae, Cistanchis herba, semen astragali Complanati, Corni fructus, and fructus Psoraleae.
The rhizoma Polygonati can be replaced by one or more of radix Adenophorae, Bulbus Lilii, radix Ophiopogonis, radix asparagi, herba Dendrobii, rhizoma Polygonati Odorati, fructus Lycii, semen Sesami Niger, Ecliptae herba, fructus Ligustri Lucidi, and Mori fructus.
The rhizoma Zingiberis recens can be replaced by one or more of Bulbus Allii, herba Menthae, propolis, fructus Cnidii, Sulfur, radix Sophorae Flavescentis, cortex Dictamni Radicis, rhizoma Smilacis Glabrae, and caulis Polygoni Multiflori.
The invention also aims to provide a preparation method of the Chinese herbal medicine extract, which comprises the following steps:
1) extracting volatile oil from the ginger in parts by mass to obtain a Chinese herbal medicine extract A, and separating ginger decoction dregs and water extraction liquid medicine for later use;
2) taking the ginger decoction dregs separated in the step 1) and the polygonum multiflorum, the polygonatum and the ginseng in parts by mass, adding water for decoction and extraction, collecting an extracting solution, combining the extracting solution and the ginger water extracting liquid medicine separated in the step 1), and concentrating to obtain a Chinese herbal medicine extract B; the Chinese herbal medicine extract A and the Chinese herbal medicine extract B which are prepared from the raw materials in parts by mass are Chinese herbal medicine extracts together.
Further, the method for extracting the volatile oil in the step 1) is one of a co-water distillation method, a supercritical extraction method, a microwave extraction method, a solvent extraction method and a steam distillation method; the extraction method in the step 2) can be replaced by an ethanol extraction method, a solvent extraction method and a percolation method.
The preparation method of the Chinese herbal medicine extract comprises the following steps:
1) taking the ginger in parts by mass, cleaning, adding water, extracting volatile oil by a steam distillation method to obtain a Chinese herbal medicine extract A, and separating ginger decoction dregs and water extraction liquid medicine for later use;
2) taking the ginger dregs separated in the step 1), taking the polygonum multiflorum, the polygonatum sibiricum and the ginseng in parts by mass, combining the ginger dregs, adding water to soak the ginger dregs for 0.5-5 hours, decocting and extracting for 0.5-5 hours, filtering, collecting an extracting solution, adding water to the dregs, decocting and extracting for 0.5-5 hours, filtering, combining the extracting solution obtained in the two times and ginger water extracting liquid medicine, and concentrating until the amount of the crude drug is 0.5-3 times that of the crude drug to obtain a Chinese herbal medicine extract B; the Chinese herbal medicine extract A and the Chinese herbal medicine extract B which are prepared from the raw materials in parts by mass are Chinese herbal medicine extracts together.
The method of the invention furthest reserves the effective components in the Chinese herbal medicine, and the prepared Chinese herbal medicine extract has the effects of blacking hair, nourishing hair and nourishing hair roots, has no toxic or side effect after being used, and is suitable for long-term use by people.
The invention also aims to provide a Chinese herbal medicine hair conditioner which comprises the following components in parts by mass: 1-45 parts of Chinese herbal medicine extract, 0.1-1 part of chelating agent, 3-20 parts of fatting agent, 3-20 parts of conditioner, 1-10 parts of nutritional humectant, 0.01-1 part of preservative, 0.1-1 part of essential oil or essence and 2-95 parts of water.
Preferably, the Chinese herbal medicine hair conditioner comprises the following components in parts by mass: 10-30 parts of Chinese herbal medicine extract, 0.1-0.5 part of chelating agent, 5-15 parts of fat-imparting agent, 5-15 parts of conditioner, 2-8 parts of nutritional humectant, 0.1-0.7 part of preservative, 0.1-0.5 part of essential oil or essence and 20-90 parts of water.
Preferably, the Chinese herbal medicine hair conditioner comprises the following components in parts by mass: 15-20 parts of Chinese herbal medicine extract, 0.1-0.3 part of chelating agent, 5-10 parts of fat-liquoring agent, 5-10 parts of conditioner, 2-5 parts of nutritional humectant, 0.2-0.5 part of preservative, 0.2-0.5 part of essential oil or essence and 40-80 parts of water.
Preferably, the Chinese herbal medicine hair conditioner comprises the following components in parts by mass: 15 parts of Chinese herbal medicine extract, 0.1 part of chelating agent, 6 parts of fat-imparting agent, 6 parts of conditioner, 4 parts of nutrition humectant, 0.3 part of preservative, 0.2 part of essential oil or essence and 80 parts of water.
The Chinese herbal medicine hair conditioner is a hair care product containing natural and green Chinese herbal medicine effective components, and provides another approach for the Chinese medicinal and Chinese medicinal science development.
Further, the chelating agent is disodium ethylene diamine tetraacetate or tetrasodium ethylene diamine tetraacetate; the nutritional moisturizer comprises one or more of glycerol, propylene glycol, sorbitol, mannitol, polyethylene glycol, dextran, and olive oil.
Preferably, the chelating agent is disodium edetate; the nutritional humectant is glycerol.
Further, the fat-liquoring agent comprises one or more of fatty alcohol, vegetable fat, animal fat and artificial synthetic fat-liquoring agent; the fatty alcohol comprises cetyl alcohol, stearyl alcohol, and cetearyl alcohol; the vegetable oil comprises palm oil, jojoba oil and olive oil; the animal oil comprises lanolin and horse oil; the artificial synthetic fat-imparting agent comprises fatty glyceride.
Preferably, the fatting agent is cetearyl alcohol and olive oil.
Further, the conditioning agent comprises one or more of cationic quaternary ammonium salts, semi-synthetic polyquaternary ammonium salts, synthetic polyquaternary ammonium salts and silicone oils; the cationic quaternary ammonium salts comprise alkyl (C12-C22) trimethyl ammonium chloride, guar gum hydroxypropyl trimethyl ammonium chloride, cassia gum hydroxypropyl trimethyl ammonium chloride, diisostearyl amidopropyl hydroxypropyl dimethyl ammonium chloride, and distearyl dimethyl ammonium chloride; the semisynthetic polyquaternary salts comprise polyquaternary salt 10, polyquaternary salt 67 and polyquaternary salt 55; the synthetic polyquaternary salts comprise polyquaternary ammonium salt 47, polyquaternary ammonium salt 28, polyquaternary ammonium salt 68 and polyquaternary ammonium salt 7; the silicone oil comprises polydimethylsiloxane, modified polydimethylsiloxane, polyether polysiloxane copolymer and emulsified silicone oil.
Preferably, the modified polydimethylsiloxanes include amino-terminated polydimethylsiloxanes and hydrogenated polydimethylsiloxanes.
Preferably, the conditioning agent is behenyl trimethyl ammonium chloride, polydimethylsiloxane and amino terminated polydimethylsiloxane.
Further, the Chinese herbal medicine hair conditioner comprises the following components in parts by mass: 1-45 parts of Chinese herbal medicine extract, 3-15 parts of cetearyl alcohol, 1-5 parts of behenyl trimethyl ammonium chloride, 1-10 parts of glycerol, 0.5-5 parts of polydimethylsiloxane, 1.5-10 parts of amino-terminated polydimethylsiloxane, 0.01-1 part of preservative, 0.1-5 parts of olive oil, 0.1-1 part of citric acid, 0.1-0.5 part of disodium ethylenediamine tetraacetic acid, 0.1-1 part of essence or essential oil and 2-95 parts of water.
Preferably, the Chinese herbal medicine hair conditioner consists of the following components in parts by mass: 15 parts of Chinese herbal medicine extract, 6 parts of cetostearyl alcohol, 2 parts of behenyl trimethyl ammonium chloride, 3 parts of glycerol, 1 part of polydimethylsiloxane, 3 parts of amino-terminated polydimethylsiloxane, 0.3 part of preservative, 0.5 part of olive oil, 0.1 part of citric acid, 0.1 part of disodium ethylene diamine tetraacetate, 0.3 part of essence or essential oil and 69 parts of water.
Preferably, the Chinese herbal medicine hair conditioner consists of the following components in parts by mass: 5 parts of Chinese herbal medicine extract, 1 part of cetyl alcohol, 3 parts of stearyl alcohol, 1 part of hexadecyl trimethyl ammonium chloride, 1 part of glycerol, 3 parts of propylene glycol, 1 part of hydrogenated polydimethylsiloxane, 3 parts of emulsified silicone oil, 0.2 part of preservative, 1 part of horse oil, 0.1 part of citric acid, 0.1 part of disodium ethylene diamine tetraacetate, 0.2 part of essence or essential oil and 80 parts of water.
The chelating agent disodium ethylene diamine tetraacetate is adopted to effectively chelate unstable metal ions in the environment, so that the harm of harmful metal ions to hair and scalp is reduced, and the influence of the metal ions on the stability of the product is effectively reduced; meanwhile, cetostearyl alcohol, polydimethylsiloxane and amino-terminated polydimethylsiloxane are used as the oily matrix of the hair conditioner, so that the opened hair flakes in the hair cleaning process are effectively smoothed, and the hair protection effect of the hair flakes on hair is exerted; the conditioner behenyl trimethyl ammonium chloride is adopted to effectively reduce the friction damage between hairs caused by the generation of hair static electricity; the nutritional humectant glycerin and the olive oil are adopted to effectively moisturize and lock water, so that the hair is effectively improved in frigidity and dullness after long-term use, and the hair is moisturized and glossy.
The invention also aims to provide a preparation method of the Chinese herbal medicine hair conditioner, which comprises the following steps:
1) adding the disodium ethylene diamine tetraacetate, the behenyl trimethyl ammonium chloride, the glycerol and the citric acid in parts by mass into water, and stirring to completely dissolve to obtain a water phase;
2) heating the cetearyl alcohol in parts by mass until the cetearyl alcohol is completely melted to obtain an oil phase;
3) emulsifying the water phase in the step 1) and the oil phase in the step under stirring to obtain an emulsifying system;
4) adding ammonia-terminated polydimethylsiloxane, polydimethylsiloxane and olive oil into the emulsifying system obtained in the step 3), stirring, homogenizing and emulsifying under vacuum until the mixture is uniform, cooling, adding Chinese herbal medicine extract, essence or essential oil and preservative, stirring, homogenizing and emulsifying under vacuum to obtain the Chinese herbal medicine hair conditioner.
The preparation method of the Chinese herbal medicine hair conditioner comprises the following steps:
1) adding the disodium ethylene diamine tetraacetate, the behenyl trimethyl ammonium chloride, the glycerol and the citric acid in parts by mass into water under a vacuum environment, stirring to completely dissolve, completely clarifying and transparent a system, and heating to above 70 ℃ to obtain a water phase;
2) heating the cetearyl alcohol in parts by mass to above 70 ℃ until the cetearyl alcohol is completely melted to obtain an oil phase;
3) stirring the water phase in the step 1) and the oil phase in the step for more than 15min in a vacuum environment, and homogenizing and emulsifying for more than 5min to obtain an emulsifying system;
4) cooling the emulsification system obtained in the step 3) to below 65 ℃, adding the amino-terminated polydimethylsiloxane, the polydimethylsiloxane and the olive oil, and stirring for more than 15 min. Homogenizing and emulsifying under vacuum condition for more than 5min at the emulsifying speed of 40-120 Hz, and repeating and intermittently operating; and (3) cooling after emulsification is finished, adding the Chinese herbal medicine extract, essence or essential oil and preservative when the temperature of the system is reduced to be below 55 ℃, stirring and mixing for more than 10min, homogenizing, emulsifying and stirring for more than 5min under a vacuum condition, and emulsifying at the rotating speed of 40-120 Hz until the system is in a uniform and fine state to obtain the hair conditioner.
Through a series of researches, the hair conditioner product is prepared by adopting the raw materials according to a reasonable proportion and controlling stirring homogenization time, parameters and the like to prepare a uniform and stable paste, so that the hair conditioner product is smooth and soft, has no toxic or side effect, and has the effects of blackening hair, nourishing hair and nourishing hair roots and scalp.
The preparation method solves the problem of unstable system after the Chinese herbal medicine extract is added, solves the technical bottleneck restricting the development of the industry, plays the roles of blackening the hair, nourishing the hair root and the scalp of the Chinese herbal medicine, has simple and convenient operation and low cost, and is suitable for industrialized mass production. Meanwhile, the hair conditioner belongs to cream type hair care products, is very thick, and brings a large amount of bubbles into stirring and homogenizing in the production process, and the bubbles are difficult to eliminate, so that the product quality is influenced, and the production cost is increased. The invention adopts specific process technical method and parameters for production in negative pressure environment, effectively avoids bubbles generated in the production process and ensures the product quality.
The Chinese herbal medicine hair conditioner prepared by the invention is uniform and fine in paste, has the effects of smoothing hair, nourishing scalp, relieving itching and removing dandruff, and can effectively nourish hair roots, blacken hair, grow hair, prevent alopecia and stop alopecia after long-term use. At present, hair care products become one of the necessities of modern families, and plant herbal hair care series products are more popular and accepted by the public and are a future trend.
The invention also aims to provide application of the Chinese herbal medicine extract or the Chinese herbal medicine hair conditioner in hair blackening, hair nourishing, hair root nourishing, hair loss prevention and hair loss prevention hair care products.
The invention has the beneficial effects that:
1) the invention adopts the rhizoma polygonati, the ginseng, the polygonum multiflorum and the ginger to play roles in tonifying qi and kidney, moistening lung, promoting the production of body fluid and nourishing blood, relieving exterior syndrome and dispelling cold; the hair blackening and nourishing shampoo has the effects of blackening hair, nourishing hair, and nourishing hair root and scalp by effectively treating scalp sore, carbuncle, scrofula and pruritus. Meanwhile, the theory of the traditional Chinese medicine is adopted, the modern Chinese herbal medicine extraction technology is combined, the pure plant extract is effectively extracted, the advantages of the traditional Chinese medicine are exerted, and the effects of blackening hair, nourishing hair roots and hair are exerted according to the reasonable proportion of the traditional Chinese medicine theory.
2) The invention takes the traditional Chinese medicine theory and the modern Chinese medicine research as guidance to carry out Chinese herbal medicine composing prescription and exert the advantages of the traditional Chinese medicine. The hair-blackening and hair-growing shampoo has the effects of blackening and growing hair, preventing alopecia and relieving itching and nourishing hair roots and scalp, has simple preparation method, low cost, no anaphylactic reaction after use and no toxic or side effect, can make hair smooth and soft, meets the requirements of people on health preservation, is easier to be favored and accepted by the public, and is suitable for daily and long-term use of consumers.
3) The preparation method solves the problem of unstable system after the Chinese herbal medicine extract is added, solves the technical bottleneck restricting the development of the industry, plays the roles of blackening hair, nourishing hair roots and scalp of the Chinese herbal medicine, adopts a specific process technical method and parameters for production in a negative pressure environment, effectively avoids bubbles generated in the production process, and ensures the product quality; the preparation method is simple and convenient to operate, low in cost and suitable for industrial mass production.
Detailed Description
Hereinafter, preferred embodiments of the present invention will be described in detail. The experimental methods of the preferred embodiments, which do not indicate specific conditions, are generally performed according to conventional conditions, and the examples are given for better illustration of the present invention, but the present invention is not limited to the examples. Therefore, those skilled in the art should make insubstantial modifications and adaptations to the embodiments of the present invention in light of the above teachings and remain within the scope of the invention.
Example 1 herbal extracts for hair nourishing and caring
The Chinese herbal medicine extract for nourishing and protecting hair is prepared from the following raw materials in parts by mass: 5 parts of ginseng, 15 parts of rhizoma polygonati, 5 parts of polygonum multiflorum and 5 parts of ginger.
Example 2 herbal extracts for hair nourishing and caring
The Chinese herbal medicine extract for nourishing and protecting hair is prepared from the following raw materials in parts by mass: 45 parts of ginseng, 45 parts of rhizoma polygonati, 20 parts of polygonum multiflorum and 20 parts of ginger.
Example 3 herbal extracts for hair nourishing and caring
The Chinese herbal medicine extract for nourishing and protecting hair is prepared from the following raw materials in parts by mass: 30 parts of ginseng, 10 parts of rhizoma polygonati, 20 parts of polygonum multiflorum and 10 parts of ginger.
Example 4 method for preparing herbal extracts
The method of preparing the herbal extracts of examples 1-3, comprising the steps of:
1) cleaning rhizoma Zingiberis recens, adding 8 times of water, extracting volatile oil by steam distillation to obtain Chinese medicinal extract A, and separating rhizoma Zingiberis recens residue and water extractive solution;
2) taking the ginger dregs separated in the step 1), taking the polygonum multiflorum, the polygonatum sibiricum and the ginseng in parts by mass, cleaning, combining the ginger dregs, soaking the ginger dregs in 10 times of water by mass for 1 hour, decocting and extracting for 2 hours, filtering, collecting an extracting solution, adding water equivalent to 6 times of the medicinal materials into the dregs, decocting and extracting for 1.5 hours, filtering, combining the two extracting solutions and ginger water extracting liquid medicine, and concentrating until the crude drug amount is 2/3 to obtain a Chinese herbal medicine extract B; the Chinese herbal medicine extract A and the Chinese herbal medicine extract B which are prepared from the raw materials in parts by mass are Chinese herbal medicine extracts together.
Example 5 Chinese herbal medicine Hair conditioner and preparation method thereof
The Chinese herbal medicine hair conditioner comprises the following components in parts by mass: 2 parts of Chinese herbal medicine extract, 6 parts of cetostearyl alcohol, 2 parts of behenyl trimethyl ammonium chloride, 3 parts of glycerol, 1 part of polydimethylsiloxane, 3 parts of amino-terminated polydimethylsiloxane, 0.3 part of preservative, 0.5 part of olive oil, 0.1 part of citric acid, 0.1 part of disodium ethylene diamine tetraacetate, 0.3 part of essence or essential oil and 85 parts of water.
The preparation method of the Chinese herbal medicine hair conditioner comprises the following steps:
1) water phase: adding water, disodium ethylene diamine tetraacetate, behenyl trimethyl ammonium chloride, glycerol and citric acid into a vacuum emulsification stirrer, stirring to completely dissolve, completely clarifying and transparent the system, and heating to 75-80 ℃;
2) oil phase: adding cetyl stearyl alcohol into a container, and heating to 75-80 deg.C; to complete melting;
3) adding the oil phase into vacuum emulsifying mixer, mixing with the water phase, stirring for 20min, homogenizing and emulsifying for 25 min. Cooling to 55-65 deg.C, adding ammonia-terminated polydimethylsiloxane, polydimethylsiloxane and olive oil, and stirring for 20 min. When the vacuum degree reaches-0.06 MPa, the homogenizing and emulsifying time is 25min, and the emulsifying rotating speed is 40-50 Hz. And (3) cooling after emulsification is finished, adding the Chinese herbal medicine extract, the daily essence/essential oil and the preservative when the temperature of the system is reduced to be below 55 ℃, stirring and mixing for 20min, homogenizing, emulsifying and stirring for 25min under the condition that the vacuum degree is-0.06 MPa, and emulsifying at the rotating speed of 40-50 Hz until the system is in a uniform and fine state to obtain the hair conditioner.
Example 6 Chinese herbal medicine Hair conditioner and preparation method thereof
The Chinese herbal medicine hair conditioner comprises the following components in parts by mass: 15 parts of Chinese herbal medicine extract, 15 parts of cetearyl alcohol, 3 parts of behenyl trimethyl ammonium chloride, 5 parts of glycerol, 5 parts of polydimethylsiloxane, 5 parts of amino-terminated polydimethylsiloxane, 0.01 part of preservative, 5 parts of olive oil, 0.3 part of citric acid, 0.5 part of disodium ethylene diamine tetraacetate, 1 part of essence or essential oil and 50 parts of water.
The preparation method of the Chinese herbal medicine hair conditioner comprises the following steps:
1) water phase: adding water, disodium ethylene diamine tetraacetate, behenyl trimethyl ammonium chloride, glycerol and citric acid into a vacuum emulsification stirrer, stirring to completely dissolve, completely clarifying and transparent the system, and heating to 70-75 ℃;
2) oil phase: adding cetyl stearyl alcohol into a container, and heating to 70-75 deg.C; to complete melting;
3) adding the oil phase into vacuum emulsifying mixer, mixing with the water phase, stirring for 30min, homogenizing and emulsifying for 20 min. Cooling to 45-55 deg.C, adding ammonia-terminated polydimethylsiloxane, polydimethylsiloxane and olive oil, and stirring for 30 min. The vacuum degree reaches-0.1 MPa, the homogenizing and emulsifying time is 20min, and the emulsifying rotating speed is 50-60 Hz. And (3) cooling after emulsification is finished, adding the Chinese herbal medicine extract, the daily essence/essential oil and the preservative when the temperature of the system is reduced to be below 45 ℃, stirring and mixing for 30min, homogenizing, emulsifying and stirring for 20min under the condition that the vacuum degree is minus 0.1MPa, and emulsifying at the rotating speed of 50-60 Hz until the system is in a uniform and fine state to obtain the hair conditioner.
Example 7 Chinese herbal medicine Hair conditioner and preparation method thereof
The Chinese herbal medicine hair conditioner comprises the following components in parts by mass: 20 parts of Chinese herbal medicine extract, 3 parts of cetostearyl alcohol, 5 parts of behenyl trimethyl ammonium chloride, 5 parts of glycerol, 0.5 part of polydimethylsiloxane, 1.5 parts of amino-terminated polydimethylsiloxane, 1 part of preservative, 0.1 part of olive oil, 0.1 part of citric acid, 0.1 part of disodium ethylene diamine tetraacetate, 0.2 part of essence or essential oil and 75 parts of water.
The preparation method of the Chinese herbal medicine hair conditioner comprises the following steps:
1) water phase: adding water, disodium ethylene diamine tetraacetate, behenyl trimethyl ammonium chloride, glycerol and citric acid into a vacuum emulsification stirrer, stirring to completely dissolve, completely clarifying and transparent the system, and heating to 80-85 ℃;
2) oil phase: adding cetyl stearyl alcohol into a container, and heating to 80-85 deg.C; to complete melting.
3) Adding the oil phase into vacuum emulsifying mixer, mixing with the water phase, stirring for 15min, homogenizing and emulsifying for 5 min. Cooling to 40-50 deg.C, adding ammonia-terminated polydimethylsiloxane, polydimethylsiloxane and olive oil, and stirring for 15 min. When the vacuum degree reaches-0.05 MPa, the homogenizing and emulsifying time is 5min, and the emulsifying rotating speed is 110-120 Hz. And (3) cooling after emulsification is finished, adding the Chinese herbal medicine extract, the daily essence/essential oil and the preservative when the temperature of the system is reduced to be below 40 ℃, stirring and mixing for 15min, homogenizing, emulsifying and stirring for 5min under the condition that the vacuum degree is minus 0.05MPa, and emulsifying at the rotating speed of 110-120 Hz until the system is in a uniform and fine state to obtain the hair conditioner.
Example 8 Chinese herbal Hair conditioner
The Chinese herbal medicine hair conditioner comprises the following components in parts by mass: 35 parts of Chinese herbal medicine extract, 3 parts of cetyl alcohol, 3 parts of stearyl alcohol, 0.5 part of hexadecyl trimethyl ammonium chloride, 0.5 part of distearyl dimethyl ammonium chloride, 1 part of glycerol, 3 parts of propylene glycol, 1 part of hydrogenated polydimethylsiloxane, 1 part of silicone emulsion, 0.3 part of preservative, 0.5 part of jojoba oil, 0.1 part of citric acid, 0.1 part of disodium ethylene diamine tetraacetate, 0.5 part of essence or essential oil and 55 parts of water.
The preparation method of the Chinese herbal medicine hair conditioner comprises the following steps:
1) water phase: adding water, disodium ethylene diamine tetraacetate, hexadecyl trimethyl ammonium chloride, distearyl dimethyl ammonium chloride, glycerol, propylene glycol and citric acid into a vacuum emulsification stirrer, stirring to completely dissolve, completely clarifying and transparent a system, and heating to 85-90 ℃;
2) oil phase: adding cetyl alcohol and stearyl alcohol into a container, and heating to 85-90 deg.C; to complete melting.
3) Adding the oil phase into vacuum emulsifying mixer, mixing with the water phase, stirring for 35min, homogenizing and emulsifying for 15 min. Cooling to 30-40 deg.C, adding hydrogenated polydimethylsiloxane, emulsified silicone oil, and jojoba oil, and stirring for 35 min. The vacuum degree reaches-0.08 MPa, the homogenizing and emulsifying time is 15min, and the emulsifying rotating speed is 70-80 Hz. And (3) cooling after emulsification is finished, adding the Chinese herbal medicine extract, the daily essence/essential oil and the preservative when the temperature of the system is reduced to be below 30 ℃, stirring and mixing for 35min, homogenizing, emulsifying and stirring for 15min under the condition that the vacuum degree is minus 0.08MPa, and emulsifying at the rotating speed of 70-80 Hz until the system is in a uniform and fine state to obtain the hair conditioner.
EXAMPLE 9 preparation of Chinese herbal medicine Hair conditioner
The Chinese herbal medicine hair conditioner comprises the following components in parts by mass: 45 parts of Chinese herbal medicine extract, 1 part of cetyl alcohol, 3 parts of cetostearyl alcohol, 0.5 part of behenyl trimethyl ammonium chloride, 1 part of guar gum hydroxypropyl trimethyl ammonium chloride, 1 part of glycerol, 3 parts of polyethylene glycol, 1 part of hydrogenated polydimethylsiloxane, 2 parts of amino-terminated polydimethylsiloxane, 0.3 part of preservative, 0.5 part of horse oil, 0.1 part of citric acid, 0.1 part of disodium ethylene diamine tetraacetate, 0.5 part of essence or essential oil and 45 parts of water.
The preparation method of the Chinese herbal medicine hair conditioner comprises the following steps:
1) water phase: adding water, disodium ethylene diamine tetraacetate, behenyl trimethyl ammonium chloride, guar gum hydroxypropyl trimethyl ammonium chloride, glycerol, polyethylene glycol and citric acid into a vacuum emulsification stirrer, stirring to completely dissolve, completely clarifying and transparent the system, and heating to 90-95 ℃;
2) oil phase: adding cetyl alcohol and cetearyl alcohol into a container, and heating to 90-95 ℃; to complete melting.
3) Adding the oil phase into vacuum emulsifying mixer, mixing with the water phase, stirring for 40min, homogenizing and emulsifying for 15 min. Cooling to 20-30 deg.C, adding hydrogenated polydimethylsiloxane, ammonia-terminated polydimethylsiloxane, and melted horse oil, and stirring for 40 min. The vacuum degree reaches-0.04 MPa, the homogenizing and emulsifying time is 15min, and the emulsifying rotating speed is 90-100 Hz. And (3) cooling after emulsification is finished, adding the Chinese herbal medicine extract, the daily essence/essential oil and the preservative when the temperature of the system is reduced to be below 20 ℃, stirring and mixing for 40min, homogenizing, emulsifying and stirring for 15min under the condition that the vacuum degree is-0.04 MPa, and emulsifying at the rotating speed of 90-100 Hz until the system is in a uniform and fine state to obtain the hair conditioner.
EXAMPLE 10 Hair conditioner Effect test
1000 specially trained test persons were allowed to use the herbal conditioners obtained in examples 5 to 9 for 3 months. The testers used the samples according to the same method, and scored the hair conditioner effect according to the same scoring standard, so as to obtain the average effect score of the Chinese herbal medicine hair conditioners obtained in examples 5-9, and the results are shown in table 1.
TABLE 1 Hair conditioner Effect test results (percent)
Finally, the above embodiments are only for illustrating the technical solutions of the present invention and not for limiting, although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions may be made to the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention, and all of them should be covered in the claims of the present invention.
Claims (3)
1. The Chinese herbal medicine hair conditioner is characterized by comprising the following components in parts by mass: 15-45 parts of Chinese herbal medicine extract, 3-15 parts of cetearyl alcohol, 1-5 parts of behenyl trimethyl ammonium chloride, 1-10 parts of glycerol, 0.5-5 parts of polydimethylsiloxane, 1.5-10 parts of amino-terminated polydimethylsiloxane, 0.01-1 part of preservative, 0.1-5 parts of olive oil, 0.1-1 part of citric acid, 0.1-1 part of disodium ethylenediamine tetraacetic acid, 0.1-1 part of essence or essential oil and 2-95 parts of water; the Chinese herbal medicine extract is prepared from the following raw materials in parts by mass: 5-45 parts of ginseng, 5-50 parts of rhizoma polygonati, 5-25 parts of polygonum multiflorum and 5-25 parts of ginger; the preparation method of the Chinese herbal medicine extract comprises the following steps: 1) taking the ginger in parts by mass, cleaning, adding water, extracting volatile oil by a steam distillation method to obtain a Chinese herbal medicine extract A, and separating ginger decoction dregs and water extraction liquid medicine for later use; 2) taking the ginger dregs separated in the step 1), taking the polygonum multiflorum, the polygonatum sibiricum and the ginseng in parts by mass, combining the ginger dregs, adding water to soak the ginger dregs for 0.5-5 hours, decocting and extracting for 0.5-5 hours, filtering, collecting an extracting solution, adding water to the dregs, decocting and extracting for 0.5-5 hours, filtering, combining the extracting solution obtained in the two times and ginger water extracting liquid medicine, and concentrating until the amount of the crude drug is 0.5-3 times that of the crude drug to obtain a Chinese herbal medicine extract B; the Chinese herbal medicine extract A and the Chinese herbal medicine extract B which are prepared from the raw materials in parts by mass are Chinese herbal medicine extracts together.
2. The method for preparing the herbal hair conditioner of claim 1, comprising the steps of: 1) adding the disodium ethylene diamine tetraacetate, the behenyl trimethyl ammonium chloride, the glycerol and the citric acid in parts by mass into water under a vacuum environment, stirring to completely dissolve, completely clarifying and transparent a system, and heating to above 70 ℃ to obtain a water phase; 2) heating the cetearyl alcohol in parts by mass to above 70 ℃ until the cetearyl alcohol is completely melted to obtain an oil phase; 3) stirring the water phase in the step 1) and the oil phase in the step for more than 15min in a vacuum environment, and homogenizing and emulsifying for more than 5min to obtain an emulsifying system; 4) cooling the emulsification system obtained in the step 3) to below 65 ℃, adding ammonia-terminated polydimethylsiloxane, polydimethylsiloxane and olive oil, and stirring for more than 15 min;
homogenizing and emulsifying under vacuum condition for more than 5min at the emulsifying speed of 40-120 Hz, and repeating and intermittently operating; and (3) cooling after emulsification is finished, adding the Chinese herbal medicine extract, essence or essential oil and preservative when the temperature of the system is reduced to be below 55 ℃, stirring and mixing for more than 10min, homogenizing, emulsifying and stirring for more than 5min under a vacuum condition, and emulsifying at the rotating speed of 40-120 Hz until the system is in a uniform and fine state to obtain the hair conditioner.
3. The use of the herbal hair conditioner of claim 1 in a hair care product.
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| CN108685820A (en) * | 2018-08-08 | 2018-10-23 | 廖家平 | Hair conditioner |
| CN109972404A (en) * | 2019-04-18 | 2019-07-05 | 太和县欧得利毛发制品有限公司 | A kind of hair unhairing scale immersion treatment technique |
| CN110151655A (en) * | 2019-06-21 | 2019-08-23 | 朱志辉 | It is a kind of to use hair product made of Chinese medical extract and preparation method thereof |
| CN110302120A (en) * | 2019-08-16 | 2019-10-08 | 肇庆市凯捷科技有限公司 | A kind of hair conditioner with moist antiallergy effect |
| CN113197829B (en) * | 2021-04-29 | 2022-11-08 | 代晓丽 | Anti-hair-loss hair-care essence and preparation method thereof |
| CN114246819B (en) * | 2021-12-30 | 2023-09-01 | 浙江宜格企业管理集团有限公司 | Anti-allergy and soothing composition and preparation method thereof |
| CN114712286A (en) * | 2022-04-26 | 2022-07-08 | 彭氏(惠州)实业发展有限公司 | Hair care agent comprising extract of Chinese herbal medicine source as active ingredient |
| CN114848556B (en) * | 2022-06-02 | 2023-11-10 | 安徽师范大学 | Application of gynostemma pentaphylla extract and eucommia ulmoides extract in preparing hair washing and caring product for promoting hair blackening/preventing white hair |
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