CN109972404A - A kind of hair unhairing scale immersion treatment technique - Google Patents
A kind of hair unhairing scale immersion treatment technique Download PDFInfo
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- CN109972404A CN109972404A CN201910311848.9A CN201910311848A CN109972404A CN 109972404 A CN109972404 A CN 109972404A CN 201910311848 A CN201910311848 A CN 201910311848A CN 109972404 A CN109972404 A CN 109972404A
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- hair
- immersion treatment
- unhairing
- treatment technique
- deionized water
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- 210000004209 hair Anatomy 0.000 title claims abstract description 126
- 238000000034 method Methods 0.000 title claims abstract description 34
- 238000007654 immersion Methods 0.000 title claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 38
- 239000008367 deionised water Substances 0.000 claims abstract description 29
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 29
- 206010040844 Skin exfoliation Diseases 0.000 claims abstract description 20
- 230000035618 desquamation Effects 0.000 claims abstract description 20
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 15
- 108090000790 Enzymes Proteins 0.000 claims abstract description 13
- 102000004190 Enzymes Human genes 0.000 claims abstract description 13
- 230000007071 enzymatic hydrolysis Effects 0.000 claims abstract description 11
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 claims abstract description 11
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000005977 Ethylene Substances 0.000 claims abstract description 10
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 10
- 238000004140 cleaning Methods 0.000 claims abstract description 7
- 230000002255 enzymatic effect Effects 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims abstract description 7
- 238000007598 dipping method Methods 0.000 claims abstract description 5
- 239000000284 extract Substances 0.000 claims description 14
- 229940088598 enzyme Drugs 0.000 claims description 12
- 240000004638 Dendrobium nobile Species 0.000 claims description 11
- 230000010355 oscillation Effects 0.000 claims description 11
- 108090000317 Chymotrypsin Proteins 0.000 claims description 10
- 241000196324 Embryophyta Species 0.000 claims description 10
- 229960002376 chymotrypsin Drugs 0.000 claims description 10
- 239000004615 ingredient Substances 0.000 claims description 9
- JLIDBLDQVAYHNE-YKALOCIXSA-N (+)-Abscisic acid Chemical compound OC(=O)/C=C(/C)\C=C\[C@@]1(O)C(C)=CC(=O)CC1(C)C JLIDBLDQVAYHNE-YKALOCIXSA-N 0.000 claims description 8
- 102000013392 Carboxylesterase Human genes 0.000 claims description 8
- 108010051152 Carboxylesterase Proteins 0.000 claims description 8
- HNDVDQJCIGZPNO-UHFFFAOYSA-N histidine Natural products OC(=O)C(N)CC1=CN=CN1 HNDVDQJCIGZPNO-UHFFFAOYSA-N 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 5
- 241001523383 Achnatherum Species 0.000 claims description 4
- 241000026010 Dendrobium candidum Species 0.000 claims description 4
- 235000010254 Jasminum officinale Nutrition 0.000 claims description 4
- 240000005385 Jasminum sambac Species 0.000 claims description 4
- 241000218378 Magnolia Species 0.000 claims description 4
- 235000003140 Panax quinquefolius Nutrition 0.000 claims description 4
- 240000001341 Reynoutria japonica Species 0.000 claims description 4
- 235000018167 Reynoutria japonica Nutrition 0.000 claims description 4
- ATBOMIWRCZXYSZ-XZBBILGWSA-N [1-[2,3-dihydroxypropoxy(hydroxy)phosphoryl]oxy-3-hexadecanoyloxypropan-2-yl] (9e,12e)-octadeca-9,12-dienoate Chemical compound CCCCCCCCCCCCCCCC(=O)OCC(COP(O)(=O)OCC(O)CO)OC(=O)CCCCCCC\C=C\C\C=C\CCCCC ATBOMIWRCZXYSZ-XZBBILGWSA-N 0.000 claims description 4
- AWUCVROLDVIAJX-UHFFFAOYSA-N alpha-glycerophosphate Natural products OCC(O)COP(O)(O)=O AWUCVROLDVIAJX-UHFFFAOYSA-N 0.000 claims description 4
- FCRACOPGPMPSHN-UHFFFAOYSA-N desoxyabscisic acid Natural products OC(=O)C=C(C)C=CC1C(C)=CC(=O)CC1(C)C FCRACOPGPMPSHN-UHFFFAOYSA-N 0.000 claims description 4
- 238000004090 dissolution Methods 0.000 claims description 4
- 238000000855 fermentation Methods 0.000 claims description 4
- 230000004151 fermentation Effects 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 4
- 238000011010 flushing procedure Methods 0.000 claims description 4
- 238000005286 illumination Methods 0.000 claims description 4
- 239000001771 mentha piperita Substances 0.000 claims description 4
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 4
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 4
- 238000004321 preservation Methods 0.000 claims description 4
- 150000003333 secondary alcohols Chemical class 0.000 claims description 4
- 229910001220 stainless steel Inorganic materials 0.000 claims description 4
- 239000010935 stainless steel Substances 0.000 claims description 4
- UZKQTCBAMSWPJD-UQCOIBPSSA-N trans-Zeatin Natural products OCC(/C)=C\CNC1=NC=NC2=C1N=CN2 UZKQTCBAMSWPJD-UQCOIBPSSA-N 0.000 claims description 4
- UZKQTCBAMSWPJD-FARCUNLSSA-N trans-zeatin Chemical compound OCC(/C)=C/CNC1=NC=NC2=C1N=CN2 UZKQTCBAMSWPJD-FARCUNLSSA-N 0.000 claims description 4
- 238000010792 warming Methods 0.000 claims description 4
- 229940023877 zeatin Drugs 0.000 claims description 4
- 150000007942 carboxylates Chemical class 0.000 claims description 2
- 238000010992 reflux Methods 0.000 claims description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims 2
- 241001523681 Dendrobium Species 0.000 claims 1
- 240000005373 Panax quinquefolius Species 0.000 claims 1
- 229910021529 ammonia Inorganic materials 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 238000002604 ultrasonography Methods 0.000 claims 1
- 230000010356 wave oscillation Effects 0.000 claims 1
- 230000003648 hair appearance Effects 0.000 abstract description 18
- 235000016709 nutrition Nutrition 0.000 abstract description 3
- 238000003912 environmental pollution Methods 0.000 abstract description 2
- 230000009469 supplementation Effects 0.000 abstract description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 241000208340 Araliaceae Species 0.000 description 3
- 206010061245 Internal injury Diseases 0.000 description 3
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 235000019441 ethanol Nutrition 0.000 description 3
- 235000008434 ginseng Nutrition 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- 230000015556 catabolic process Effects 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical compound Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 description 2
- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical compound ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 description 2
- 238000012804 iterative process Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- DWNBOPVKNPVNQG-LURJTMIESA-N (2s)-4-hydroxy-2-(propylamino)butanoic acid Chemical compound CCCN[C@H](C(O)=O)CCO DWNBOPVKNPVNQG-LURJTMIESA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- -1 amino, hydroxyl Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000001413 cellular effect Effects 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000009881 electrostatic interaction Effects 0.000 description 1
- 230000003699 hair surface Effects 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 230000003752 improving hair Effects 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229920001184 polypeptide Polymers 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/001—Treatment with visible light, infrared or ultraviolet, X-rays
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/13—Ammonium halides or halides of elements of Groups 1 or 11 of the Periodic System
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
- D06M16/003—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic with enzymes or microorganisms
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
- D06M2101/12—Keratin fibres or silk
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of hair unhairing scale immersion treatment techniques, comprising the following steps: (1) hair beam immerses constant temperature in saline solution and impregnates, and acetum is immersed after taking-up and is impregnated；(2) hair beam is irradiated as ultraviolet lamp, and enzymatic vessel constant temperature enzymatic hydrolysis is put into after taking-up, hair beam must be digested after cleaning；(3) desquamation agent is added into deionized water, sealed thermal insulating stands and vibrates after stirring and dissolving, then hangs on vapor tight tank and is passed through ethylene standing；(4) processing hair beam is immersed into plant enzyme solution, is kept the temperature after closed and stands and vibrate；(5) dipping hair beam is washed through roller, desquamation hair beam is made.The method of the present invention has rate height of scaling, damaging to hair quality small, and can carry out nutritional supplementation and hair quality reparation to hair quality after scaling, and improves the flexibility of hair, and environmental pollution is small.
Description
Technical field
The invention belongs to hair processing technique fields, and in particular to a kind of hair unhairing scale immersion treatment technique.
Background technique
Hair is made of hair cuticle, hair cortex and hair medulla three parts from outside to inside, and wherein hair cuticle is commonly called as hair scale piece,
Protective action is arrived in its main correct initiation, and hair is the important raw material of hair products processing industry, can be used for being processed into shoe brush, bed brush
With the adornments such as wig, the re-using to hair was not only realized, but also improve the added value of hair products, boosted economic growth
And employment, China are that the main hair products production in the world, processing and product distributing center, hair products export volume account for world's general export
50% or more of amount.It is processed into hair products using hair, needs to carry out preliminary treatment to hair, wherein just including removing defeathering
For the hair of growth, with good protective action, the glossiness and compliance of hair can be improved in scale, hair scale piece
Etc. performances, but for hair products following process, the hair scale piece of hair surface will cause frictional force between hair and rise, and
And be easy to produce electrostatic interaction, so that the tangling property between hair be made to improve, for subsequent hair products procedure of processing cause compared with
Big difficulty.And traditional method that hair scale piece is removed using hypochlorous acid and oxidizing mode, although improving hair removal
Hair scale piece, still, larger to the damage of the pollution and legal system of environment, usability is restricted；And it is carried out using enzyme method
The hair scale piece on surface is hydrolyzed, pollution is lower, and still, the controlling depth of enzymatic hydrolysis is difficult to hold, and hair scale piece removal rate is horizontal
It is lower, cause the cost of iterative process to waste.
Summary of the invention
The purpose of the present invention: traditional method that hair scale piece is removed using hypochlorous acid and oxidizing mode, although mentioning
High hair removes hair scale piece, and still, larger to the damage of the pollution and legal system of environment, usability is restricted；And make
The hair scale piece on surface is hydrolyzed with enzyme method, pollution is lower, and still, the controlling depth of enzymatic hydrolysis is difficult to hold, and hair scale
Piece removal rate level is lower, and the cost of iterative process is caused to waste.To solve the above problems, the present invention provides a kind of hairs to go
Hair scale piece immersion treatment technique.
The present invention is achieved by the following technical solutions:
A kind of hair unhairing scale immersion treatment technique, comprising the following steps:
(1) it pre-processes: by hair binding bunchy, obtaining hair beam, first hair beam is immersed and carries out perseverance in thermostat water bath saline solution
Temperature impregnates 34-48min, and temperature is 52-60 DEG C；Sealed soak 1-2h in acetum is immersed in clear water flushing again after taking-up, cleans
Pre-treat hair beam is obtained afterwards；
(2) mixed enzymolysis: by pre-treat hair beam as 12-19min is irradiated under ultraviolet lamp, being put into enzymatic vessel after taking-up, then
Deionized water is added into enzymatic vessel and submerges hair beam, is then separately added into histidine aminonialyase, chymotrypsin and carboxylate again
Enzyme is stirred and carries out constant temperature enzymatic hydrolysis, and 37-43 DEG C of temperature, time 4-6h must digest hair beam after cleaning；
(3) desquamation agent is handled: enzymatic hydrolysis hair beam being immersed and is vibrated in its device deionized water, then desquamation is added into deionized water
Agent, it is closed after stirring and dissolving to be warming up to 34-39 DEG C of standing 52-67min, supersonic oscillations 15-22min is then used, after taking-up
It completely hangs in vapor tight tank clearly, ethylene is passed through into vapor tight tank and stands 1-2h, hair beam must be handled；
(4) it impregnates: deionized water is added into the closed bucket of stainless steel, processing hair beam is immersed, plant ferment is then added
Element is stirred dissolution, keeps the temperature and stands after closed, and use supersonic oscillations 21-27min, must impregnate hair beam；
(5) it cleans: dipping hair beam being washed through roller, desquamation hair beam is made.
Saline solution described in step (1), mass concentration 1.3%-2.2%；The acetum, mass concentration are
3.5%-6.3%。
Ultraviolet light described in step (2), intensity of illumination 180-270Lux.
Histidine aminonialyase, chymotrypsin and carboxy-lesterase described in step (2), additional amount are respectively deionized water
1.1%-1.6%, 0.35%-0.58% and 0.72%-1.07% of amount.
Desquamation agent described in step (3), ingredient be phosphatidyl glycerol, zeatin, abscisic acid, secondary alcohol polyoxyethylene ether and
Dendrobium nobile leaf extract, each ingredient additional amount are respectively 1.2%-2.4%, 0.53%-0.71%, 0.37%- of deionized water quality
0.42%, 0.25%-0.78% and 0.18%-0.32%.
The dendrobium nobile leaf extract, using fresh dendrobium candidum leaf as raw material, use mass concentration for 70% alcohol reflux
It extracts, concentration drying is carried out to extracting solution, dendrobium nobile leaf extract is made.
Supersonic oscillations described in step (3), frequency 14-21Khz.
Ethylene described in step (3), additional amount are the 7%-12% of closed tank volume.
Plant enzyme described in step (4) is by orange leaf, Jasmine, magnolia, splendid achnatherum, the fleece-flower root, the West
Ginseng, Drymoglossum subcordatum and dried peppermint leaf are made through crushing, depth fermentation, filtering and concentration powder, and additional amount is deionized water quality
11%-16%.
Heat preservation described in step (4) is stood, and temperature is 40-48 DEG C, time 2-3h.
The present invention have the advantage that compared with prior art in pretreatment using saline solution to hair Shu Jinhang immersion at
Reason, but hair quality part cellular contraction improves hair quality density, and reduces degradation of the subsequent mixed enzyme to hair quality internal structure
Rate plays protective action to a certain extent；And impregnated using acetic acid, surface hair scale piece can be made to soften, be conducive to subsequent
Locate solvent to the osmosis of hair scale piece, improves hair scale piece removal efficiency.Hair quality is irradiated using ultraviolet light, hair quality can be made
Part, which is tightened, increases density, reduces solvent to the infiltration degradation inside hair quality, and can make hair scale piece Aging Damage；Pass through group
Propylhomoserin aminonialyase, chymotrypsin and carboxy-lesterase can to amino, hydroxyl terminal polypeptide and the hydrolysis of lipid in hair scale piece albumen, thus
Make hair scale piece protein structure partial hydrolysis, forms the hair scale chip architecture of loose crushing shape.The present invention passes through actual use discovery,
Hair Shu Jinhang is vibrated by using desquamation agent, and by the further closed processes of ethylene, loose crushing shape hair scale can be made
Piece degrade and fall off, improve the removal rate of hair scale piece, and other adverse effects will not be generated, with intention less than effect
Fruit.Using plant enzyme to hair Shu Jinhang impregnation, absorption of the hair quality to nutritional ingredient is improved, the glossiness of hair quality is improved
And flexibility, and extend the service life of hair quality.
Specific embodiment
Embodiment 1:
A kind of hair unhairing scale immersion treatment technique, comprising the following steps:
(1) it pre-processes: by hair binding bunchy, obtaining hair beam, first hair beam is immersed and carries out perseverance in thermostat water bath saline solution
Temperature impregnates 35min, and temperature is 53 DEG C；Sealed soak 1.5h in acetum is immersed in clear water flushing again after taking-up, obtains in advance after cleaning
Handle hair beam；
(2) mixed enzymolysis: by pre-treat hair beam as 13min is irradiated under ultraviolet lamp, being put into enzymatic vessel after taking-up, then to enzyme
It solves and deionized water submergence hair beam is added in tank, be then separately added into histidine aminonialyase, chymotrypsin and carboxy-lesterase again, stir
It mixes mixing and carries out constant temperature enzymatic hydrolysis, 38 DEG C of temperature, time 4.5h must digest hair beam after cleaning；
(3) desquamation agent is handled: enzymatic hydrolysis hair beam being immersed and is vibrated in its device deionized water, then desquamation is added into deionized water
Agent, it is closed after stirring and dissolving to be warming up to 35 DEG C of standing 53min, supersonic oscillations 16min is then used, clear clean suspension after taking-up
In vapor tight tank, it is passed through ethylene into vapor tight tank and stands 1.5h, hair beam must be handled；
(4) it impregnates: deionized water is added into the closed bucket of stainless steel, processing hair beam is immersed, plant ferment is then added
Element is stirred dissolution, keeps the temperature and stands after closed, and use supersonic oscillations 22min, must impregnate hair beam；
(5) it cleans: dipping hair beam being washed through roller, desquamation hair beam is made.
Saline solution described in step (1), mass concentration 1.4%；The acetum, mass concentration 3.6%.
Ultraviolet light described in step (2), intensity of illumination 183Lux.
Histidine aminonialyase, chymotrypsin and carboxy-lesterase described in step (2), additional amount are respectively deionized water
1.2%, 0.36% and the 0.73% of amount.
Desquamation agent described in step (3), ingredient be phosphatidyl glycerol, zeatin, abscisic acid, secondary alcohol polyoxyethylene ether and
Dendrobium nobile leaf extract, each ingredient additional amount are respectively 1.3%, 0.54%, 0.38%, 0.26% and the 0.19% of deionized water quality.
The dendrobium nobile leaf extract, using fresh dendrobium candidum leaf as raw material, to use mass concentration to return for 70% ethyl alcohol
Stream extracts, and carries out concentration drying to extracting solution, and dendrobium nobile leaf extract is made.
Supersonic oscillations described in step (3), frequency 15Khz.
Ethylene described in step (3), additional amount are the 8% of closed tank volume.
Plant enzyme described in step (4) is by orange leaf, Jasmine, magnolia, splendid achnatherum, the fleece-flower root, the West
Ginseng, Drymoglossum subcordatum and dried peppermint leaf are made through crushing, depth fermentation, filtering and concentration powder, and additional amount is deionized water quality
12%.
Heat preservation described in step (4) is stood, and temperature is 41 DEG C, time 2.5h.
Embodiment 2:
A kind of hair unhairing scale immersion treatment technique, comprising the following steps:
(1) it pre-processes: by hair binding bunchy, obtaining hair beam, first hair beam is immersed and carries out perseverance in thermostat water bath saline solution
Temperature impregnates 47min, and temperature is 58 DEG C；Sealed soak 2h in acetum is immersed in clear water flushing again after taking-up, obtains after cleaning and locates in advance
Manage hair beam；
(2) mixed enzymolysis: by pre-treat hair beam as 18min is irradiated under ultraviolet lamp, being put into enzymatic vessel after taking-up, then to enzyme
It solves and deionized water submergence hair beam is added in tank, be then separately added into histidine aminonialyase, chymotrypsin and carboxy-lesterase again, stir
It mixes mixing and carries out constant temperature enzymatic hydrolysis, 42 DEG C of temperature, time 5.5h must digest hair beam after cleaning；
(3) desquamation agent is handled: enzymatic hydrolysis hair beam being immersed and is vibrated in its device deionized water, then desquamation is added into deionized water
Agent, it is closed after stirring and dissolving to be warming up to 38 DEG C of standing 66min, supersonic oscillations 21min is then used, clear clean suspension after taking-up
In vapor tight tank, it is passed through ethylene into vapor tight tank and stands 2h, hair beam must be handled；
(4) it impregnates: deionized water is added into the closed bucket of stainless steel, processing hair beam is immersed, plant ferment is then added
Element is stirred dissolution, keeps the temperature and stands after closed, and use supersonic oscillations 26min, must impregnate hair beam；
(5) it cleans: dipping hair beam being washed through roller, desquamation hair beam is made.
Saline solution described in step (1), mass concentration 2.1%；The acetum, mass concentration 6.2%.
Ultraviolet light described in step (2), intensity of illumination 260Lux.
Histidine aminonialyase, chymotrypsin and carboxy-lesterase described in step (2), additional amount are respectively deionized water
1.5%, 0.57% and the 1.05% of amount.
Desquamation agent described in step (3), ingredient be phosphatidyl glycerol, zeatin, abscisic acid, secondary alcohol polyoxyethylene ether and
Dendrobium nobile leaf extract, each ingredient additional amount are respectively 2.3%, 0.70%, 0.41%, 0.76% and the 0.31% of deionized water quality.
The dendrobium nobile leaf extract, using fresh dendrobium candidum leaf as raw material, to use mass concentration to return for 70% ethyl alcohol
Stream extracts, and carries out concentration drying to extracting solution, and dendrobium nobile leaf extract is made.
Supersonic oscillations described in step (3), frequency 20Khz.
Ethylene described in step (3), additional amount are the 11.5% of closed tank volume.
Plant enzyme described in step (4) is by orange leaf, Jasmine, magnolia, splendid achnatherum, the fleece-flower root, the West
Ginseng, Drymoglossum subcordatum and dried peppermint leaf are made through crushing, depth fermentation, filtering and concentration powder, and additional amount is deionized water quality
15%.
Heat preservation described in step (4) is stood, and temperature is 47 DEG C, time 3h.
Comparison 1:
Saline solution in step (1) is not used compared with embodiment 1 in this comparison 1, other steps are same as Example 1.
Comparison 2:
Ultraviolet light in step (2) is not used compared with embodiment 2 in this comparison 2, other steps are same as Example 2.
Comparison 3:
Histidine aminonialyase, chymotrypsin and carboxy-lesterase in step (2) is not used compared with embodiment 1 in this comparison 3, other
Step is same as Example 1.
Comparison 4:
Step (3) desquamation agent processing is not used compared with embodiment 2 in this comparison 4, other steps are same as Example 2.
Comparison 5:
Plant enzyme in step (4) is not used compared with embodiment 1 in this comparison 5, other steps are same as Example 1.
Control group: the processing of unhairing scale is carried out to hair using hypochlorite, as reference.
To head of scaling obtained by embodiment 1, embodiment 2, comparison 1, comparison 2, comparison 3, comparison 4, comparison 5 and control group
Hair, counts rate of scaling, hair quality internal injury rate, tensile strength and the flexible appraisal of hair.
Flexible appraisal: flexibility is fine +++ ++, good ++++, it is general +++, poor ++, very poor+.
Experimental data:
Table 1:
| Project | Rate of scaling % | Hair quality internal injury rate % | Tensile strength Mpa | Flexible appraisal |
| Embodiment 1 | 98.7 | 0.54 | 17.3 | ﹢ ﹢ ﹢ ﹢ ﹢ |
| Embodiment 2 | 99.1 | 0.51 | 17.1 | ﹢ ﹢ ﹢ ﹢ ﹢ |
| Comparison 1 | 98.9 | 1.11 | 15.2 | ﹢ ﹢ ﹢ ﹢ |
| Comparison 2 | 97.6 | 0.99 | 14.9 | ﹢ ﹢ ﹢ ﹢ |
| Comparison 3 | 87.1 | 2.07 | 17.1 | ﹢ ﹢ ﹢ |
| Comparison 4 | 84.8 | 2.18 | 16.8 | ﹢ ﹢ ﹢ |
| Comparison 5 | 98.4 | 1.15 | 15.5 | ﹢ ﹢ |
| Control group | 98.3 | 4.8 | 10.7 | ﹢ |
Synthesis result: for the present invention relative to control group processing method, rate of scaling data are suitable, with simple proteins hydrolysis method phase
Than rate of scaling improves 27% or more, and hair quality internal injury rate reduces by 4.29%, and tensile strength improves 6.6Mpa, and flexibility is compared
Control group is by largely improving.The method of the present invention has rate height of scaling, damaging to hair quality small, and can be to hair quality after scaling
Nutritional supplementation and hair quality reparation are carried out, improves the flexibility of hair, and environmental pollution is small.
Claims (10)
1. a kind of hair unhairing scale immersion treatment technique, which comprises the following steps:
(1) it pre-processes: by hair binding bunchy, obtaining hair beam, first hair beam is immersed and carries out perseverance in thermostat water bath saline solution
Temperature impregnates 34-48min, and temperature is 52-60 DEG C；Sealed soak 1-2h in acetum is immersed in clear water flushing again after taking-up, cleans
Pre-treat hair beam is obtained afterwards；
(2) mixed enzymolysis: by pre-treat hair beam as 12-19min is irradiated under ultraviolet lamp, being put into enzymatic vessel after taking-up, then
Deionized water is added into enzymatic vessel and submerges hair beam, is then separately added into histidine aminonialyase, chymotrypsin and carboxylate again
Enzyme is stirred and carries out constant temperature enzymatic hydrolysis, and 37-43 DEG C of temperature, time 4-6h must digest hair beam after cleaning；
(3) desquamation agent is handled: enzymatic hydrolysis hair beam is immersed in oscillator deionized water, then desquamation agent is added into deionized water,
It is closed after stirring and dissolving to be warming up to 34-39 DEG C of standing 52-67min, supersonic oscillations 15-22min is then used, it is dry clearly after taking-up
Only it hangs in vapor tight tank, ethylene is passed through into vapor tight tank and stands 1-2h, hair beam must be handled；
(4) it impregnates: deionized water is added into the closed bucket of stainless steel, processing hair beam is immersed, plant ferment is then added
Element is stirred dissolution, keeps the temperature and stands after closed, and use supersonic oscillations 21-27min, must impregnate hair beam；
(5) it cleans: dipping hair beam being washed through roller, desquamation hair beam is made.
2. hair unhairing scale immersion treatment technique as described in claim 1, which is characterized in that salt described in step (1)
Water, mass concentration 1.3%-2.2%；The acetum, mass concentration 3.5%-6.3%.
3. hair unhairing scale immersion treatment technique as described in claim 1, which is characterized in that ultraviolet described in step (2)
Light, intensity of illumination 180-270Lux.
4. hair unhairing scale immersion treatment technique as described in claim 1, which is characterized in that group ammonia described in step (2)
Acidolysis adnosine deaminase, chymotrypsin and carboxy-lesterase, additional amount are respectively 1.1%-1.6%, 0.35%-0.58% of deionized water quality
And 0.72%-1.07%.
5. hair unhairing scale immersion treatment technique as described in claim 1, which is characterized in that desquamation described in step (3)
Agent, ingredient are phosphatidyl glycerol, zeatin, abscisic acid, secondary alcohol polyoxyethylene ether and dendrobium nobile leaf extract, each ingredient additional amount
Respectively 1.2%-2.4%, 0.53%-0.71%, 0.37%-0.42%, 0.25%-0.78% and 0.18%- of deionized water quality
0.32%。
6. hair unhairing scale immersion treatment technique as claimed in claim 5, which is characterized in that the dendrobium leaf is extracted
Object uses mass concentration to extract for 70% alcohol reflux, carries out concentration baking to extracting solution using fresh dendrobium candidum leaf as raw material
It is dry, dendrobium nobile leaf extract is made.
7. hair unhairing scale immersion treatment technique as described in claim 1, which is characterized in that ultrasound described in step (3)
Wave oscillation, frequency 14-21Khz.
8. hair unhairing scale immersion treatment technique as described in claim 1, which is characterized in that ethylene described in step (3),
Its additional amount is the 7%-12% of closed tank volume.
9. hair unhairing scale immersion treatment technique as described in claim 1, which is characterized in that plant described in step (4)
Ferment, to be crushed, deeply orange leaf, Jasmine, magnolia, splendid achnatherum, the fleece-flower root, American Ginseng, Drymoglossum subcordatum and dried peppermint leaf
It spends fermentation, filtering and concentration powder and is made, additional amount is the 11%-16% of deionized water quality.
10. hair unhairing scale immersion treatment technique as described in claim 1, which is characterized in that heat preservation described in step (4)
It stands, temperature is 40-48 DEG C, time 2-3h.
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