CN114886814A - Plant anti-dandruff shampoo and preparation method thereof - Google Patents
Plant anti-dandruff shampoo and preparation method thereof Download PDFInfo
- Publication number
- CN114886814A CN114886814A CN202210598376.1A CN202210598376A CN114886814A CN 114886814 A CN114886814 A CN 114886814A CN 202210598376 A CN202210598376 A CN 202210598376A CN 114886814 A CN114886814 A CN 114886814A
- Authority
- CN
- China
- Prior art keywords
- dandruff
- filtering
- percent
- extract
- ethanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9755—Gymnosperms [Coniferophyta]
- A61K8/9761—Cupressaceae [Cypress family], e.g. juniper or cypress
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention relates to a plant anti-dandruff shampoo and a preparation method thereof, wherein an anti-dandruff agent consisting of plant extracts and a traditional Chinese medicine compound extract are added into a basic formula of the shampoo according to a specific proportion, so that the shampoo has the effects of inhibiting bacterial growth, removing dandruff, relieving itching obviously, preventing broken hairs and hair from falling, relieving the stimulation of a chemical anti-dandruff agent on the scalp, and safely removing dandruff. In addition, the shampoo has the characteristics of rich foam, easy washing, good combing property, flexibility and glossiness after hair washing, and the comprehensive conditioning performance of the shampoo is superior to that of domestic and foreign mainstream anti-dandruff products.
Description
Technical Field
The invention relates to the technical field of daily washing products, in particular to a plant anti-dandruff shampoo and a preparation method thereof.
Background
The shampoo is also called shampoo or shampoo, which is a basic nursing cosmetic applied to the hair and scalp. Shampoo of fatty alcohol sulfate is generally used. The shampoo contains various components, and the combined action of the components can play a role in cleaning scalp and hair. The most effective component of a shampoo is a surfactant, which functions to cleanse the hair and scalp and to generate foam when the shampoo is mixed with water.
Dandruff is mainly caused by dandruff spores. Many anti-dandruff shampoo products are on the market, and special components for removing dandruff are added into the shampoo, and the components are usually chemical agents and have large irritation to the scalp. Many shampoos are added with traditional Chinese medicine extract components, but the anti-dandruff and sterilizing effects are not obvious, and meanwhile, the addition of the traditional Chinese medicine extract can reduce the combing property, flexibility and glossiness of the shampoo, and other chemical preparations are required to be additionally added for supplement.
Disclosure of Invention
The invention aims to provide a plant anti-dandruff shampoo and a preparation method thereof, and the shampoo is prepared by adding a plant anti-dandruff agent and a traditional Chinese medicine compound extract of a specific formula into a shampoo basic formula according to a specific proportion, so that the effects of cleaning scalp, controlling oil, removing dandruff and nourishing hair are achieved.
A plant anti-dandruff shampoo is prepared from the following components in percentage by mass:
10-15% of main surfactant
5-10% of auxiliary surfactant
1-5% of plant anti-dandruff agent
1-5% of traditional Chinese medicine compound
1 to 5 percent of silicone oil
1-2% of nutritional additive
1 to 2 percent of thickening agent
0 to 0.5 percent of chelating agent
0 to 0.5 percent of acid-base regulator
0 to 0.5 percent of preservative
0 to 1 percent of essence
The balance of deionized water;
the plant anti-dandruff agent is prepared from the following components in percentage by mass:
20-40% of coptis extract
30 to 55 percent of scutellaria baicalensis extract
5-25% of centella asiatica extract
10-40% of white willow bark extract;
the traditional Chinese medicine compound comprises the following raw materials in percentage by mass: chinese angelica: white atractylodes rhizome: mulberry leaf: mulberry root bark: ligusticum wallichii: cacumen biotae = (5-10): (1-5): (1-5): (10-15): (10-15): (10-15): (1-5), the preparation method of the traditional Chinese medicine compound comprises the following steps: putting the medicinal materials into a reflux tank according to the mass ratio, adding 75% ethanol which is 4 times of the mass of the medicinal materials, heating and refluxing at 95 ℃, calculating the time from the beginning of ethanol reflux, wherein the extraction time is 2.5 hours, filtering and collecting the extracting solution after the reflux is finished, repeating the operation, and combining the extracting solutions for later use.
Preferably, the main surfactant is selected from one or two of sodium laureth sulfate and ammonium laureth sulfate.
Preferably, the co-surfactant is selected from one or a combination of two of cocamidopropyl betaine, cocamidomethyl MEA.
Preferably, the nutritional additive adopts one or more of PEG-75 lanolin, cetrimide and sodium lactate.
Preferably, the thickener employs one or a combination of both of acrolein/acrylic acid copolymer or sodium chloride.
Preferably, the chelating agent is ethylenediaminetetraacetic acid disodium salt.
Preferably, the pH regulator adopts citric acid or 10% potassium hydroxide solution.
Preferably, the preservative is one or the combination of two of phenoxyethanol and sodium benzoate.
Preferably, the preparation method of the coptis chinensis extract comprises: drying and pulverizing Coptidis rhizoma, adding 30-60% ethanol water solution 8-15 times the volume of Coptidis rhizoma, reflux extracting for 2-4 hr, filtering the extractive solution with filter paper, and evaporating and concentrating to obtain Coptidis rhizoma extract.
Preferably, the preparation method of the scutellaria baicalensis extract comprises the following steps: adding appropriate amount of Scutellariae radix into 10-15 times of water, boiling, decocting for 30-40 min, filtering the extractive solution with filter paper, concentrating to appropriate amount, adjusting pH to 1.0-2.0 with hydrochloric acid, maintaining at 70-90 deg.C, standing, filtering, adding appropriate amount of water into precipitate, stirring, adjusting pH to 7.0 with 20-40% sodium hydroxide solution, adding equal amount of ethanol, stirring for dissolving, filtering, adjusting pH to 1.0-2.0 with hydrochloric acid, maintaining at 50-70 deg.C, standing, filtering, washing precipitate with appropriate amount of water and ethanol of different concentrations to pH to 7.0, volatilizing ethanol, and drying under reduced pressure to obtain Scutellariae radix extract.
Preferably, the preparation method of the centella asiatica extract comprises: adding an appropriate amount of herba Centellae into 8-15 times of water solution, reflux-extracting for 1-3 h, filtering the extractive solution with filter paper, evaporating and concentrating to obtain dry powder, dissolving with distilled water, and extracting with petroleum ether to obtain herba Centellae extract.
Preferably, the preparation method of the white willow bark extract comprises the following steps: drying and crushing a proper amount of white willow bark, adding an ethanol water solution with the concentration of 65-90 percent and the volume of 8-12 times of the white willow bark, performing reflux extraction for 2-5 h, filtering an extracting solution through filter paper, concentrating to a proper amount, adjusting the pH value to 1.0-2.0 by hydrochloric acid, preserving heat at 75-95 ℃, standing, filtering, adding a proper amount of water into a precipitate, uniformly stirring, adjusting the pH value to 7.0 by 15-35% of a sodium hydroxide solution, adding an equivalent amount of ethanol, stirring to dissolve, filtering, adjusting the pH value of a filtrate to 1.0-2.0 by hydrochloric acid, preserving heat at 55-75 ℃, standing, filtering, washing the precipitate to a pH value of 7.0 by sequentially using a proper amount of water and ethanol with different concentrations, volatilizing the ethanol, and drying under reduced pressure to obtain the white willow bark extract.
Preferably, the mass ratio of the raw materials in the traditional Chinese medicine compound is bupleurum: chinese angelica: white atractylodes rhizome: mulberry leaf: mulberry root bark: ligusticum wallichii: cacumen biotae = 2: 1: 1: 3: 3: 3: 1.
as another object of the invention, the invention provides a preparation method of the plant anti-dandruff shampoo, which comprises the following steps:
weighing corresponding raw materials according to mass percent, firstly adding powder in the nutritional additive into an emulsifying pot, adding deionized water, stirring to form a uniform mixture, heating to 75 ℃, adding a main surfactant, an auxiliary surfactant and a chelating agent, starting a homogenizer at a stirring speed of 540-; and adding a thickening agent, homogenizing and stirring for 10-25 min, stopping homogenizing and heating after complete dissolution, cooling to 50 ℃, adding silicone oil, a plant anti-dandruff agent and a Chinese medicine compound, uniformly stirring, adding essence and a preservative when the temperature is reduced to 45 ℃, finally adjusting the pH of the liquid to 6-7 by using an acid-base regulator, adjusting to 5000-8000mPa.s (25 ℃), pumping into a stainless steel container, and standing for half an hour to obtain the plant anti-dandruff liquid.
The invention introduces a plant anti-dandruff agent and a traditional Chinese medicine compound extract into the anti-dandruff shampoo, and the extract is added into a shampoo basic formula according to a specific proportion. The plant anti-dandruff agent is prepared by using natural plants of coptis chinensis, scutellaria baicalensis, centella asiatica and white willow bark as main raw materials, extracting and improving the raw materials to prepare the raw materials with strong antibacterial capacity, and has an inhibiting effect on malassezia furfur. The traditional Chinese medicine compound is extracted from traditional Chinese medicines such as radix bupleuri, Chinese angelica, bighead atractylodes rhizome, mulberry leaves, mulberry root bark, ligusticum wallichii and cacumen biotae, the radix bupleuri has the effect of soothing liver-qi stagnation, the Chinese angelica has the effect of promoting blood circulation to remove blood stasis, the bighead atractylodes rhizome has the effect of tonifying spleen and qi, the mulberry leaves have the effect of dispelling wind and dissipating heat, the mulberry root bark has the effect of sterilizing, the ligusticum wallichii has the effects of dispelling wind and dissipating heat, and tranquilizing and relieving pain, and the cacumen biotae has the effects of dispelling wind and removing dampness. The two groups of functional additives are added, so that the effects of inhibiting bacterial growth, removing dandruff, relieving itching are obvious, the effects of preventing broken hairs and hair loss are achieved, the stimulation of a chemical dandruff remover to the scalp is relieved, and dandruff is safely removed. In addition, the shampoo has the characteristics of rich foam, easy washing, good combing property, flexibility and glossiness after hair washing, and the comprehensive conditioning performance of the shampoo is superior to that of domestic and foreign mainstream anti-dandruff products.
Drawings
FIG. 1 is a photograph of hair quality before use of a shampoo of the invention;
FIG. 2 is a microscopic enlarged view of FIG. 1;
FIG. 3 is a photograph of the hair quality after four weeks of use of the shampoo of the invention;
fig. 4 is a microscopic enlarged view of fig. 3.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the following examples, the plant anti-dandruff agent is prepared from the following components in percentage by mass:
rhizoma Coptidis extract 30%
Scutellariae radix extract 40%
Centella asiatica extract 15%
15% of white willow bark extract.
The preparation method of the coptis extract comprises the following steps: drying and pulverizing Coptidis rhizoma, adding 12 times of ethanol water solution with concentration of 50%, reflux extracting for 3 hr, filtering the extractive solution with filter paper, and evaporating to concentrate to obtain Coptidis rhizoma extract.
The preparation method of Scutellariae radix extract comprises: adding appropriate amount of Scutellariae radix into 12 times of water, boiling, decocting for 40 min, filtering the extractive solution with filter paper, concentrating to appropriate amount, adjusting pH to 1.5 with hydrochloric acid, maintaining at 80 deg.C, standing, filtering, adding appropriate amount of water into the precipitate, stirring, adjusting pH to 7.0 with 30% sodium hydroxide solution, adding equal amount of ethanol, stirring for dissolving, filtering, adjusting pH to 1.5 with hydrochloric acid, maintaining at 60 deg.C, standing, filtering, washing the precipitate with appropriate amount of water and ethanol of different concentrations to pH 7.0, volatilizing ethanol, and drying under reduced pressure to obtain Scutellariae radix extract.
The preparation method of centella asiatica extract comprises: adding appropriate amount of herba Centellae into 12 times volume of water solution, reflux extracting for 2.5 hr, filtering the extractive solution with filter paper, evaporating, concentrating to obtain dry powder, dissolving with distilled water, and extracting with petroleum ether to obtain herba Centellae extract.
The preparation method of white willow bark extract comprises: drying and crushing a proper amount of white willow bark, adding an ethanol water solution with the concentration of 85 percent and the volume of 10 times of the white willow bark, performing reflux extraction for 4 hours, filtering an extracting solution through filter paper, concentrating to a proper amount, adjusting the pH value to 1.5 by hydrochloric acid, preserving heat at 85 ℃, standing, filtering, adding a proper amount of water into a precipitate, uniformly stirring, adjusting the pH value to 7.0 by a 25 percent sodium hydroxide solution, adding an equal amount of ethanol, stirring to dissolve, filtering, adjusting the pH value of a filtrate to 1.5 by hydrochloric acid, preserving heat at 65 ℃, standing, filtering, washing the precipitate to a pH value of 7.0 by a proper amount of water and ethanol with different concentrations in sequence, volatilizing the ethanol, and drying under reduced pressure to obtain the white willow bark extract.
In the following examples, the Chinese medicinal composition is prepared by the following method: radix bupleuri, angelica, bighead atractylodes rhizome, mulberry leaves, mulberry root bark, ligusticum wallichii and cacumen biotae are mixed according to the mass ratio of 2: 1: 1: 3: 3: 3: 1, adding 75% ethanol with the mass 4 times of that of the medicinal materials into a reflux tank, heating and refluxing at 95 ℃, calculating the time from the beginning of ethanol reflux, wherein the extraction time is 2.5 hours, filtering and collecting the extracting solution after the reflux is finished, repeating the operation, and combining the extracting solutions for later use.
Example 1
A plant anti-dandruff shampoo is prepared from the following components in percentage by mass:
sodium laureth sulfate 15%
Coconut oil amide methyl MEA 6%
3 percent of plant anti-dandruff agent
Chinese medicinal composition 3%
2 percent of silicone oil
PEG-75 lanolin 1%
1 percent of sodium chloride
Ethylenediaminetetraacetic acid disodium salt 0.1%
0.1 percent of citric acid
0.1 percent of phenoxyethanol
0.5 percent of essence
68.2 percent of deionized water.
The preparation method comprises the following steps:
weighing corresponding raw materials according to mass percentage, firstly adding powder in the nutritional additive into an emulsifying pot, adding deionized water, stirring to form a uniform mixture, heating to 75 ℃, adding the main surfactant, the auxiliary surfactant and the chelating agent, starting a homogenizer, stirring at a speed of 650r/min, keeping homogenization, heating to 85 ℃, and ensuring complete dissolution; adding thickener, homogenizing and stirring for 20min, stopping homogenizing and heating after completely dissolving, cooling to 50 deg.C, adding silicone oil, plant dandruff removing agent and Chinese medicinal composition, stirring, cooling to 45 deg.C, adding essence and antiseptic, adjusting pH to appropriate value with acid-base regulator, adjusting viscosity to appropriate value, pumping into stainless steel container, and standing for half an hour.
Example 2
A plant anti-dandruff shampoo is prepared from the following components in percentage by mass:
15 percent of lauryl alcohol ether ammonium sulfate
Cocoamidopropyl betaine 6%
4 percent of plant anti-dandruff agent
Chinese medicinal composition 2%
2 percent of silicone oil
Sodium lactate 1%
1 percent of sodium chloride
Ethylenediaminetetraacetic acid disodium salt 0.1%
0.2 percent of citric acid
0.1 percent of phenoxyethanol
0.6 percent of essence
68% of deionized water.
The preparation method is the same as example 1.
Example 3
A plant anti-dandruff shampoo is prepared from the following components in percentage by mass:
sodium laureth sulfate 7%
8 percent of lauryl alcohol ether ammonium sulfate
Cocamide methyl MEA 3%
Cocoamidopropyl betaine 3%
2 percent of plant anti-dandruff agent
Chinese medicinal composition 4%
1.5 percent of silicone oil
1.5 percent of cetroronium chloride
Acrolein/acrylic acid copolymer 0.8%
Ethylenediaminetetraacetic acid disodium salt 0.1%
0.2 percent of citric acid
Sodium benzoate 0.1%
0.6 percent of essence
68.2 percent of deionized water
The preparation method is the same as example 1.
Test examples
Randomly selecting 20 volunteers with different degrees of dandruff, wherein 5 men and 15 women are aged 19-38 years, and the using method comprises the following steps: the volunteers use the shampoo of example 2 to wash hair by themselves, and the shampoo can be used by themselves according to the amount and length of hair, and is used for 1 time every 2 days, with the usage amount of at least one coin. Visits were made before and four weeks after use.
Evaluation of antidandruff effect of the shampoo by volunteers is shown in table 2.
As can be seen from the statistical data, 75% of the volunteers experienced the anti-dandruff effect of the shampoo of the present application. Wherein, more than 80% of volunteers with oily skin feel the anti-dandruff effect; of the skin-neutral volunteers, more than 60% experienced an anti-dandruff effect. FIGS. 1-2 show photographs of the head of a volunteer before applying the shampoo of the present invention, and FIGS. 3-4 show photographs of the head of a volunteer after applying the shampoo of the present invention for four weeks. From the photo image, it can be seen that the anti-dandruff effect is significant.
In the evaluation of the effect of relieving itching, 75% of the volunteers considered that the scalp was not uncomfortable with the shampoo of the present invention, and the original itching of the scalp was improved. 20 volunteers showed no skin discomfort or adverse skin reactions caused by the use of the shampoo of the invention.
The shampoo of the invention is used for detecting the sterilization effect (QB/T27382012 (7.3)), and the shampoo stock solution is used for acting on the designated strains for 20min, and the results are as follows:
as described above, the above embodiments are only illustrative of the preferred embodiments of the present invention, and do not include all the scope of the invention. Various changes and modifications can be made by one skilled in the art without departing from the spirit and scope of the invention, and the scope of the invention is defined by the appended claims.
Claims (8)
1. The plant anti-dandruff shampoo is characterized by being prepared from the following components in percentage by mass:
10-15% of main surfactant
5-10% of auxiliary surfactant
1-5% of plant anti-dandruff agent
1-5% of traditional Chinese medicine compound
1 to 5 percent of silicone oil
1-2% of nutritional additive
1 to 2 percent of thickening agent
0 to 0.5 percent of chelating agent
0 to 0.5 percent of acid-base regulator
0 to 0.5 percent of preservative
0 to 1 percent of essence
The balance of deionized water;
the plant anti-dandruff agent is prepared from the following components in percentage by mass:
20-40% of coptis extract
30 to 55 percent of scutellaria baicalensis extract
5-25% of centella asiatica extract
10-40% of white willow bark extract;
the traditional Chinese medicine compound comprises the following raw materials in percentage by mass: chinese angelica: white atractylodes rhizome: mulberry leaf: mulberry root bark: ligusticum wallichii: cacumen biotae = (5-10): (1-5): (1-5): (10-15): (10-15): (10-15): (1-5), the preparation method of the traditional Chinese medicine compound comprises the following steps: putting the medicinal materials into a reflux tank according to the mass ratio, adding 75% ethanol which is 4 times of the mass of the medicinal materials, heating and refluxing at 95 ℃, calculating the time from the beginning of ethanol reflux, wherein the extraction time is 2.5 hours, filtering and collecting the extracting solution after the reflux is finished, repeating the operation, and combining the extracting solutions for later use.
2. The shampoo according to claim 1, wherein the primary surfactant is selected from one or a combination of two of sodium laureth sulfate and ammonium laureth sulfate; the cosurfactant is selected from one or a combination of two of cocamidopropyl betaine and cocamidomethyl MEA; the nutritional additive adopts one or more of PEG-75 lanolin, cetrimide and sodium lactate; the thickening agent adopts one or the combination of two of acrolein/acrylic acid copolymer or sodium chloride; the chelating agent adopts ethylene diamine tetraacetic acid disodium salt; the acid-base regulator adopts citric acid or 10% potassium hydroxide solution; the preservative is one or the combination of two of phenoxyethanol and sodium benzoate.
3. The plant anti-dandruff shampoo according to claim 1, wherein the preparation method of the coptis extract comprises: drying and pulverizing Coptidis rhizoma, adding 30-60% ethanol water solution 8-15 times the volume of Coptidis rhizoma, reflux extracting for 2-4 hr, filtering the extractive solution with filter paper, and evaporating and concentrating to obtain Coptidis rhizoma extract.
4. The plant anti-dandruff shampoo according to claim 1, wherein the preparation method of the scutellaria baicalensis extract comprises: adding appropriate amount of Scutellariae radix into 10-15 times of water, boiling, decocting for 30-40 min, filtering the extractive solution with filter paper, concentrating to appropriate amount, adjusting pH to 1.0-2.0 with hydrochloric acid, maintaining at 70-90 deg.C, standing, filtering, adding appropriate amount of water into precipitate, stirring, adjusting pH to 7.0 with 20-40% sodium hydroxide solution, adding equal amount of ethanol, stirring for dissolving, filtering, adjusting pH to 1.0-2.0 with hydrochloric acid, maintaining at 50-70 deg.C, standing, filtering, washing precipitate with appropriate amount of water and ethanol of different concentrations to pH to 7.0, volatilizing ethanol, and drying under reduced pressure to obtain Scutellariae radix extract.
5. The plant anti-dandruff shampoo according to claim 1, wherein the preparation method of the centella asiatica extract comprises: adding appropriate amount of herba Centellae into 8-15 times of water solution, reflux extracting for 1-3 hr, filtering the extractive solution with filter paper, evaporating, concentrating to obtain dry powder, dissolving with distilled water, and extracting with petroleum ether to obtain herba Centellae extract.
6. The plant anti-dandruff shampoo according to claim 1, wherein the white willow bark extract is prepared by a method comprising: drying and crushing a proper amount of white willow bark, adding an ethanol water solution with the concentration of 65-90 percent and the volume of 8-12 times of the white willow bark, performing reflux extraction for 2-5 h, filtering an extracting solution through filter paper, concentrating to a proper amount, adjusting the pH value to 1.0-2.0 by hydrochloric acid, preserving heat at 75-95 ℃, standing, filtering, adding a proper amount of water into a precipitate, uniformly stirring, adjusting the pH value to 7.0 by 15-35% of a sodium hydroxide solution, adding an equivalent amount of ethanol, stirring to dissolve, filtering, adjusting the pH value of a filtrate to 1.0-2.0 by hydrochloric acid, preserving heat at 55-75 ℃, standing, filtering, washing the precipitate to a pH value of 7.0 by sequentially using a proper amount of water and ethanol with different concentrations, volatilizing the ethanol, and drying under reduced pressure to obtain the white willow bark extract.
7. The plant anti-dandruff shampoo according to claim 1, wherein the mass ratio of the raw materials in the traditional Chinese medicine compound is bupleurum: chinese angelica: white atractylodes rhizome: mulberry leaf: mulberry root bark: ligusticum wallichii: cacumen biotae = 2: 1: 1: 3: 3: 3: 1.
8. the method for preparing the plant anti-dandruff shampoo of any one of claims 1 to 7, comprising the following steps:
weighing corresponding raw materials according to mass percent, firstly adding powder in the nutritional additive into an emulsifying pot, adding deionized water, stirring to form a uniform mixture, heating to 75 ℃, adding a main surfactant, an auxiliary surfactant and a chelating agent, starting a homogenizer at a stirring speed of 540-; and adding a thickening agent, homogenizing and stirring for 10-25 min, stopping homogenizing and heating after complete dissolution, cooling to 50 ℃, adding silicone oil, a plant anti-dandruff agent and a Chinese medicine compound, uniformly stirring, adding essence and a preservative when the temperature is reduced to 45 ℃, finally adjusting the pH of the liquid to 6-7 by using an acid-base regulator, adjusting to proper value of 5000-plus-material 8000mPa.s (25 ℃), pumping into a stainless steel container, and standing for half an hour to obtain the plant anti-dandruff liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210598376.1A CN114886814A (en) | 2022-05-30 | 2022-05-30 | Plant anti-dandruff shampoo and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210598376.1A CN114886814A (en) | 2022-05-30 | 2022-05-30 | Plant anti-dandruff shampoo and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114886814A true CN114886814A (en) | 2022-08-12 |
Family
ID=82725839
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210598376.1A Pending CN114886814A (en) | 2022-05-30 | 2022-05-30 | Plant anti-dandruff shampoo and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114886814A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116196243A (en) * | 2023-01-17 | 2023-06-02 | 广州宝仪生物科技有限公司 | Vegetable oil-control and dandruff-removing composition and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104434691A (en) * | 2014-12-12 | 2015-03-25 | 安徽新华学院 | Natural anti-dandruff effervescent granule or effervescent tablet and preparation method thereof |
| CN109846967A (en) * | 2019-03-20 | 2019-06-07 | 广东省中药研究所 | A kind of Chinese medicine composition with bacterio static itching-relieving anti-oxidation efficacy |
| CN110074999A (en) * | 2019-05-29 | 2019-08-02 | 两面针（江苏）实业有限公司 | A kind of shampoo and preparation method thereof |
| CN114028292A (en) * | 2021-12-06 | 2022-02-11 | 广州市发歌精细化工有限公司 | Shampoo containing plant composite anti-dandruff agent and preparation method thereof |
-
2022
- 2022-05-30 CN CN202210598376.1A patent/CN114886814A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104434691A (en) * | 2014-12-12 | 2015-03-25 | 安徽新华学院 | Natural anti-dandruff effervescent granule or effervescent tablet and preparation method thereof |
| CN109846967A (en) * | 2019-03-20 | 2019-06-07 | 广东省中药研究所 | A kind of Chinese medicine composition with bacterio static itching-relieving anti-oxidation efficacy |
| CN110074999A (en) * | 2019-05-29 | 2019-08-02 | 两面针（江苏）实业有限公司 | A kind of shampoo and preparation method thereof |
| CN114028292A (en) * | 2021-12-06 | 2022-02-11 | 广州市发歌精细化工有限公司 | Shampoo containing plant composite anti-dandruff agent and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116196243A (en) * | 2023-01-17 | 2023-06-02 | 广州宝仪生物科技有限公司 | Vegetable oil-control and dandruff-removing composition and preparation method thereof |
| CN116196243B (en) * | 2023-01-17 | 2023-09-15 | 广州宝仪生物科技有限公司 | Preparation method of plant oil-control and anti-dandruff composition |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107536749B (en) | Traditional Chinese medicine shampoo and preparation process thereof | |
| CN101904908B (en) | Anti-hair loss traditional Chinese medicine composition, preparation method and application thereof to preparing anti-hair loss products | |
| CN102614102B (en) | Dandruff-removing medicinal composition and preparation method thereof | |
| CN103655383B (en) | Chinese medicinal herb extract and preparation method and application thereof | |
| CN103520036B (en) | Hair-loss-preventing shampoo | |
| CN102038626B (en) | Traditional Chinese medicinal hair-restoring and anti-alopecia shampoo and preparation method thereof | |
| CN101890080B (en) | Hair-loss preventing and hair-restoring medicinal composition and preparation method thereof, shampoo containing medicinal composition and preparation method thereof | |
| CN102274473B (en) | Compound natural plant hair loss preventing liquid and preparation method and application thereof in shampoo liquid | |
| CN103784358A (en) | Shampoo | |
| CN109568556B (en) | Traditional Chinese medicine composition and shampoo for treating alopecia | |
| CN103315933B (en) | Traditional Chinese medicine acne-removing extraction liquid and acne-removing paste | |
| CN101926973B (en) | Chinese medicinal essence capable of penetrating into skin to stop hair loss, remove dandruffs, relieve itching and nourish hair, and preparation method thereof | |
| CN104107375A (en) | Traditional Chinese medicinal composition for nourishing and solidifying hair, as well as preparation method and application of traditional Chinese medicinal composition | |
| CN111557879A (en) | Traditional Chinese medicine herbal anti-dandruff shampoo and preparation method thereof | |
| CN114886814A (en) | Plant anti-dandruff shampoo and preparation method thereof | |
| CN115120547A (en) | Non-irritant hair repairing composition and anti-hair loss shampoo | |
| CN108096174A (en) | A kind of compound plant extract with hair care anti-off effect and preparation method and application | |
| CN108309905A (en) | A kind of black hair anti-dandruff and itching-relieving shampoo and preparation method | |
| CN106726993A (en) | Chinese medicine hair cream and preparation method | |
| CN104147103A (en) | Traditional Chinese medicinal composition for reducing dandruff, sterilizing, relieving itching and promoting hair growth and preparation method thereof | |
| CN115006336A (en) | Plant shampoo capable of preventing hair loss, strengthening hair, removing dandruff and relieving itching and preparation method thereof | |
| CN108210433A (en) | Cardamom skin care compositions and its application with oil-control and/or acne-removing | |
| JPH0217118A (en) | Japanese and chinese drug for hair growth | |
| CN103637956B (en) | Shampoo | |
| CN102210640B (en) | Shampoo and preparing method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |