CN108219993A - A kind of micro-perfume capsule liquid detergent and preparation method thereof - Google Patents
A kind of micro-perfume capsule liquid detergent and preparation method thereof Download PDFInfo
- Publication number
- CN108219993A CN108219993A CN201810018655.XA CN201810018655A CN108219993A CN 108219993 A CN108219993 A CN 108219993A CN 201810018655 A CN201810018655 A CN 201810018655A CN 108219993 A CN108219993 A CN 108219993A
- Authority
- CN
- China
- Prior art keywords
- parts
- essence
- micro
- deionized water
- liquid detergent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
- C11D3/048—Nitrates or nitrites
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/28—Heterocyclic compounds containing nitrogen in the ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
- C11D3/3765—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in liquid compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38618—Protease or amylase in liquid compositions only
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38627—Preparations containing enzymes, e.g. protease or amylase containing lipase
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38645—Preparations containing enzymes, e.g. protease or amylase containing cellulase
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
- C11D3/502—Protected perfumes
- C11D3/505—Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
- C11D1/721—End blocked ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
Abstract
The present invention relates to a kind of micro-perfume capsule liquid detergents：Include the raw material of following parts by weight：60.0 78.0 parts of deionized water；Tetra- sodium of EDTA：0.05 0.2 parts；Laureth sodium sulfovinate：10.0 18.0 parts；Fatty alcohol polyoxyethylene ether 9：1.0 4.0 parts；Cocamide diethanolamine：1.0 3.0 parts；Cocoamidopropyl betaine：1.0 5.0 parts；Alkyl glycosides：5.0 10.0 parts；Microcapsule essence：0.2 1.0 parts；Essence：0.2 1.0 parts；Styrene/acrylic（Ester）Analog copolymer：0.3 1.0 parts；Citric acid：0.1 0.5 parts；Preservative：0.1 0.5 parts；Fungicide：0.1 0.5 parts；Catalyst：0.3 1.0 parts.A kind of micro-perfume capsule liquid detergent of the present invention has the effect of strong detergency and prolonged aroma retaining effect.
Description
Technical field
The present invention relates to liquid detergent field, especially a kind of micro-perfume capsule liquid detergent and preparation method thereof.
Background technology
With the development of economy with the progress of life, demand of the people to life is also higher and higher, and liquid detergent gradually replaces
Washing powder becomes daily necessities indispensable in daily life, and the active ingredient of liquid detergent is mainly non-ionic surfactant
Agent, structure include water-wet side and hydrophobic end, and wherein hydrophobic end is combined with spot, then passes through physical motion（Such as hand rubbing, machine
Movement）Detach spot and fabric.Surfactant reduces the tension of water simultaneously, enables water to reach fabric surface, makes effectively
Ingredient plays a role, and there are fragranceds, fragrance after clothing dries to make us the advantages of happy with environment breath is improved,
Have again and a variety of psychological, medical health care functions physiologically such as sterilize, refresh oneself.Fragrance remaining time one after current liquid detergent use
As at 24 hours or so, and need plus a large amount of essence, could realize 24 hours lastings of aroma retaining effect, thus can be long when
Between lasting liquid detergent, be worth research subject field.
Invention content
The present invention is above-mentioned in order to solve the problems, such as, provides a kind of micro-perfume capsule laundry for being capable of long-time lasting
Liquid.
The technical solution adopted by the present invention to solve the technical problems is：A kind of micro-perfume capsule liquid detergent：Include following weight
Measure the raw material of part：60.0-78.0 parts of deionized water；Tetra- sodium of EDTA：0.05-0.2 parts；Laureth sodium sulfovinate：10.0-
18.0 parts；Fatty alcohol polyoxyethylene ether -9：1.0-4.0 part；Cocamide diethanolamine：1.0-3.0 part；Cocamidopropyl propyl amide sweet tea
Dish alkali：1.0-5.0 part；Alkyl glycosides：5.0-10.0 part；Microcapsule essence：0.2-1.0 parts；Essence：0.2-1.0 parts；Benzene second
Alkene/acrylic acid（Ester）Analog copolymer：0.3-1.0 parts；Citric acid：0.1-0.5 parts；Preservative：0.1-0.5 parts；Fungicide：0.1-
0.5 part；Catalyst：0.3-1.0 parts.
Preferably, the raw material of following parts by weight is included：Include the raw material of following parts by weight：65.0-75.0 parts of deionized water；
Tetra- sodium of EDTA：0.05-0.15 parts；Laureth sodium sulfovinate：12.0-15.0 parts；Fatty alcohol polyoxyethylene ether -9：2.0-
3.0 part；Cocamide diethanolamine：2.0-3.0 part；Cocoamidopropyl betaine：1.0-3.0 part；Alkyl glycosides：5.0-
8.0 part；Microcapsule essence：0.2-0.5 parts；Essence：0.2-0.5 parts；Styrene/acrylic（Ester）Analog copolymer：0.3-0.5
Part；Citric acid：0.1-0.2 parts；Preservative：0.1-0.2 parts of fungicide：0.1-0.2 parts；Catalyst：0.3-0.5 parts.
It is further preferred that include the raw material of following parts by weight：65.0 parts of deionized water；Tetra- sodium of EDTA：0.05 part；Bay
Alcohol polyethers sodium sulfovinate：12.0 parts；Fatty alcohol polyoxyethylene ether -9：2.0 part；Cocamide diethanolamine：3.0 part；Cocounut oil acyl
Amine propyl betaine：3.0 part；Alkyl glycosides：8.0 part；Microcapsule essence：0.5 part；Essence：0.5 part；Styrene/acrylic
（Ester）Analog copolymer：0.5 part；Citric acid：0.2 part；Preservative：0.2 part；Fungicide：0.2 part；Catalyst：0.5 part.
It is further preferred that include the raw material of following parts by weight：Include the raw material of following parts by weight：Deionized water 75.0
Part；Tetra- sodium of EDTA：0.15 part；Laureth sodium sulfovinate：15.0 parts；Fatty alcohol polyoxyethylene ether -9：3.0 part；Cocounut oil acyl
Amine diethanol amine：3.0 part；Cocoamidopropyl betaine：1.0 part；Alkyl glycosides：5.0 part；Microcapsule essence：0.2 part；It is fragrant
Essence：0.2 part；Styrene/acrylic（Ester）Analog copolymer：0.3 part；Citric acid：0.1 part；Preservative：0.1 part；Fungicide：0.1
Part；Catalyst：0.3 part.
Preferably, the preservative is methylchloroisothiazandnone part, methyl-isothiazol ketone and magnesium chloride and magnesium nitrate
Mixture；The fungicide is DMDM hydantoins；The catalyst is protease, lipase and cellulase form
Complex enzyme.
The present invention also provides a kind of preparation methods of above-mentioned micro-perfume capsule liquid detergent, comprise the following steps：1）Weigh from
Sub- water and tetra- sodium of EDTA are added in agitated kettle, are stirred to transparency liquid；
2）Laureth sodium sulfovinate is weighed respectively, alkyl glycosides, fatty alcohol polyoxyethylene ether -9, is added in agitated kettle, is stirred
It mixes to transparency liquid；
3）It weighs in cocamide diethanolamine, Cocoamidopropyl betaine addition pot, is stirred to transparency liquid respectively；
4）Microcapsule essence and deionized water are weighed by 1:It is uniformly dispersed and is added in agitated kettle after 5 dilution proportion and filtering, stirred
It mixes to translucent liquid；
5）Weigh styrene/acrylic（Ester）Analog copolymer is added in after being diluted with deionized water in agitated kettle, is stirred to white breast
Liquid；
6）Weigh after citric acid is diluted with deionized water add in pot in stirring pH value adjust to 6.0-8.0；
7）Weigh respectively essence, methylchloroisothiazandnone part, methyl-isothiazol ketone and magnesium chloride and magnesium nitrate mixture,
DMDMD hydantoins is added in agitated kettle, is stirred to milky emulsion；
8）It weighs complex enzyme to add in agitated kettle, stir to milky emulsion.
9）The lotion of above-mentioned preparation is packed using PVA water soluble films, is packaged into granular texture.
Preferably, the step 1）Mixing speed be 20r/min；The step 2）Mixing speed for 20r/min, stir
It is 30 minutes to mix the time.
Preferably, the step 3）Mixing speed for 20r/min, mixing time is 15 minutes；The step 4）Stir
Speed is mixed as 15r/min, mixing time is 15 minutes.
Preferably, the step 5）Mixing speed for 15r/min, mixing time is 15 minutes；The step 6）Stir
Speed is mixed as 15r/min.
Preferably, the step 7）Mixing speed for 15r/min, mixing time is 15 minutes；The step 8）Stir
Speed is mixed as 15r/min, mixing time is 15 minutes.
The beneficial effects of the invention are as follows：Micro-perfume capsule liquid detergent has the effect of strong detergency, employs coconut oleoyl amine third
The complex enzyme of base glycine betaine, fatty alcohol polyoxyethylene ether -9 and protease, lipase and cellulase composition is compound；With it is long when
Between aroma retaining effect, be sufficiently mixed with microcapsule essence, allow during use and adsorb on the fabric, clothing dry after with temperature
Degree, the time, action variation release fragrance.
Specific embodiment
The present invention is explained further, but embodiment does not do any type of limit to the present invention below in conjunction with specific embodiment
It is fixed.
Embodiment 1
Micro-perfume capsule liquid detergent includes the raw material of following parts by weight：75.0 parts of deionized water；Tetra- sodium of EDTA：0.15 part；Bay
Alcohol polyethers sodium sulfovinate：15.0 parts；Fatty alcohol polyoxyethylene ether -9：3.0 part；Cocamide diethanolamine：3.0 part；Cocounut oil acyl
Amine propyl betaine：1.0 part；Alkyl glycosides：5.0 part；Microcapsule essence：0.2 part；Essence：0.2 part；Styrene/acrylic
（Ester）Analog copolymer：0.3 part；Citric acid：0.1 part；Preservative：0.1 part；Fungicide：0.1 part；Catalyst：0.3 part.
The preservative is methylchloroisothiazandnone part, the mixing of methyl-isothiazol ketone and magnesium chloride and magnesium nitrate
Object；The fungicide is DMDM hydantoins；The catalyst is the compound of protease, lipase and cellulase composition
Enzyme.
Preparation method, 1）It weighs deionized water and tetra- sodium of EDTA is added in agitated kettle, stir to transparency liquid；Stirring speed
It spends for 20r/min.
2）Laureth sodium sulfovinate is weighed respectively, alkyl glycosides, fatty alcohol polyoxyethylene ether -9, adds in agitated kettle
In, it stirs to transparency liquid；Mixing speed is 20r/min, and mixing time is 30 minutes；
3）It weighs in cocamide diethanolamine, Cocoamidopropyl betaine addition pot, is stirred to transparency liquid respectively；Stirring
Speed is 20r/min, and mixing time is 15 minutes；
4）Microcapsule essence and deionized water are weighed by 1:It is uniformly dispersed and is added in agitated kettle after 5 dilution proportion and filtering, stirred
It mixes to translucent liquid；Mixing speed is 15r/min, and mixing time is 15 minutes.
5）Weigh styrene/acrylic（Ester）Analog copolymer is added in after being diluted with deionized water in agitated kettle, is stirred to white
Color lotion；Mixing speed is 15r/min, and mixing time is 15 minutes；
6）Weigh after citric acid is diluted with deionized water add in pot in stirring pH value adjust to 6.0-8.0；The step 6）Stir
Speed is mixed as 15r/min；
7）Weigh respectively essence, methylchloroisothiazandnone part, methyl-isothiazol ketone and magnesium chloride and magnesium nitrate mixture,
DMDMD hydantoins is added in agitated kettle, is stirred to milky emulsion；Mixing speed is 15r/min, and mixing time is 15 points
Clock；Mixing speed is 15r/min, and mixing time is 15 minutes
8）It weighs complex enzyme to add in agitated kettle, stir to milky emulsion.
9）The lotion of above-mentioned preparation is packed using PVA water soluble films, is packaged into granular texture.
Embodiment 2
Micro-perfume capsule liquid detergent includes the raw material of following parts by weight：65.0 parts of deionized water；Tetra- sodium of EDTA：0.1 part；Bay
Alcohol polyethers sodium sulfovinate：15.0 parts；Fatty alcohol polyoxyethylene ether -9：3.0 part；Cocamide diethanolamine：2.0 part；Cocounut oil acyl
Amine propyl betaine：3.0 part；Alkyl glycosides：8.0 part；Microcapsule essence：0.5 part；Essence：0.5 part；Styrene/acrylic
（Ester）Analog copolymer：0.5 part；Citric acid：0.2 part；Preservative：0.2 part；Fungicide：0.15 part；Catalyst：0.5 part.
The preservative is methylchloroisothiazandnone part, the mixing of methyl-isothiazol ketone and magnesium chloride and magnesium nitrate
Object；The fungicide is DMDM hydantoins；The catalyst is the compound of protease, lipase and cellulase composition
Enzyme.
Preparation method, 1）It weighs deionized water and tetra- sodium of EDTA is added in agitated kettle, stir to transparency liquid；Stirring speed
It spends for 20r/min.
2）Laureth sodium sulfovinate is weighed respectively, alkyl glycosides, fatty alcohol polyoxyethylene ether -9, adds in agitated kettle
In, it stirs to transparency liquid；Mixing speed is 20r/min, and mixing time is 30 minutes；
3）It weighs in cocamide diethanolamine, Cocoamidopropyl betaine addition pot, is stirred to transparency liquid respectively；Stirring
Speed is 20r/min, and mixing time is 15 minutes；
4）Microcapsule essence and deionized water are weighed by 1:It is uniformly dispersed and is added in agitated kettle after 5 dilution proportion and filtering, stirred
It mixes to translucent liquid；Mixing speed is 15r/min, and mixing time is 15 minutes.
5）Weigh styrene/acrylic（Ester）Analog copolymer is added in after being diluted with deionized water in agitated kettle, is stirred to white
Color lotion；Mixing speed is 15r/min, and mixing time is 15 minutes；
6）Weigh after citric acid is diluted with deionized water add in pot in stirring pH value adjust to 6.0-8.0；The step 6）Stir
Speed is mixed as 15r/min；
7）Weigh respectively essence, methylchloroisothiazandnone part, methyl-isothiazol ketone and magnesium chloride and magnesium nitrate mixture,
DMDMD hydantoins is added in agitated kettle, is stirred to milky emulsion；Mixing speed is 15r/min, and mixing time is 15 points
Clock；Mixing speed is 15r/min, and mixing time is 15 minutes
8）It weighs complex enzyme to add in agitated kettle, stir to milky emulsion.
9）The lotion of above-mentioned preparation is packed using PVA water soluble films, is packaged into granular texture.
Embodiment 3
Micro-perfume capsule liquid detergent includes the raw material of following parts by weight：70.0 parts of deionized water；Tetra- sodium of EDTA：0.15 part；Bay
Alcohol polyethers sodium sulfovinate：13.0 parts；Fatty alcohol polyoxyethylene ether -9：2.5 part；Cocamide diethanolamine：2.5 part；Cocounut oil acyl
Amine propyl betaine：1.5 part；Alkyl glycosides：6.0 part；Microcapsule essence：0.3 part；Essence：0.3 part；Styrene/acrylic
（Ester）Analog copolymer：0.4 part；Citric acid：0.2 part；Preservative：0.15 part；Fungicide：0.15 part；Catalyst：0.4 part.
The preservative is methylchloroisothiazandnone part, the mixing of methyl-isothiazol ketone and magnesium chloride and magnesium nitrate
Object；The fungicide is DMDM hydantoins；The catalyst is the compound of protease, lipase and cellulase composition
Enzyme.
Preparation method, 1）It weighs deionized water and tetra- sodium of EDTA is added in agitated kettle, stir to transparency liquid；Stirring speed
It spends for 20r/min.
2）Laureth sodium sulfovinate is weighed respectively, alkyl glycosides, fatty alcohol polyoxyethylene ether -9, adds in agitated kettle
In, it stirs to transparency liquid；Mixing speed is 20r/min, and mixing time is 30 minutes；
3）It weighs in cocamide diethanolamine, Cocoamidopropyl betaine addition pot, is stirred to transparency liquid respectively；Stirring
Speed is 20r/min, and mixing time is 15 minutes；
4）Microcapsule essence and deionized water are weighed by 1:It is uniformly dispersed and is added in agitated kettle after 5 dilution proportion and filtering, stirred
It mixes to translucent liquid；Mixing speed is 15r/min, and mixing time is 15 minutes.
5）Weigh styrene/acrylic（Ester）Analog copolymer is added in after being diluted with deionized water in agitated kettle, is stirred to white
Color lotion；Mixing speed is 15r/min, and mixing time is 15 minutes；
6）Weigh after citric acid is diluted with deionized water add in pot in stirring pH value adjust to 6.0-8.0；The step 6）Stir
Speed is mixed as 15r/min；
7）Weigh respectively essence, methylchloroisothiazandnone part, methyl-isothiazol ketone and magnesium chloride and magnesium nitrate mixture,
DMDMD hydantoins is added in agitated kettle, is stirred to milky emulsion；Mixing speed is 15r/min, and mixing time is 15 points
Clock；Mixing speed is 15r/min, and mixing time is 15 minutes
8）It weighs complex enzyme to add in agitated kettle, stir to milky emulsion.
9）The lotion of above-mentioned preparation is packed using PVA water soluble films, is packaged into granular texture.
Embodiment 4
The stability experiment after capsule is made in micro-perfume capsule liquid detergent, takes the capsule 20 of the preparation in above-described embodiment 1-3 respectively
Grain and ordinary liquid laundry detergent and capsule particle shape made of PVA water soluble films, are placed in constant temperature and humidity study on the stability chamber, point
Detection of Stability is not carried out respectively in 0 month, 3 months, 6 months, 9 months, 12 months, 18 months, 24 months.As a result it is as follows
Table 1：
It can be seen that embodiment 1-3 is that micro-perfume capsule liquid detergent stability obtained is good according to the experimental configuration of table 1, hyperconcetration is washed
Bowl liquid energy reaches and PVA water soluble film long-term co-existence；Using ordinary liquid laundry detergent and capsule particle made of PVA water soluble films in comparative example
Shape, it is difficult to be coexisted for a long time with PVA water soluble films.
Embodiment 5
The cleaning experiment of micro-perfume capsule liquid detergent, take respectively preparation in above-described embodiment 1-3 micro-perfume capsule liquid detergent and
Common control's liquid detergent, as a result such as the following table 2：
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example | |
| Decontamination ratio,（Carbon black soiled cotton）, P | 1.13 | 1.22 | 1.28 | 0.85 |
| Decontamination ratio,（Albumen soiled cotton）, P | 1.33 | 1.51 | 1.41 | 0.93 |
| Decontamination ratio,（Sebum soiled cotton）, P | 1.21 | 1.29 | 1.19 | 0.89 |
There is good cleaning performance by the micro-perfume capsule liquid detergent in 2 present invention of table and common liquid detergent comparison.
Embodiment 6
Fragrance experiment after the cleaning of micro-perfume capsule liquid detergent, takes the micro-perfume capsule of the preparation in above-described embodiment 1-3 to wash respectively
Clothing liquid and common control's example liquid detergent use the micro-perfume capsule liquid detergent of preparation in embodiment 1-3 and general in this experiment
Logical comparative example liquid detergent respectively cleans clothing, after cleaning is dried, in the environment of gravity-flow ventilation after 24 hours by
100 ordinary peoples are judged, as a result such as the following table 3：
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example | |
| Fragrant（%） | 46 | 57 | 32 | 9 |
| Light fragrance（%） | 33 | 29 | 51 | 18 |
| It is tasteless（%） | 21 | 14 | 17 | 73 |
The micro-perfume capsule liquid detergent in the present invention is compared with common liquid detergent as shown in Table 3, has good aroma retaining effect.
Using above-mentioned desirable embodiment according to the present invention as enlightenment, by above-mentioned description, relevant staff is complete
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property range is not limited to the content on specification, it is necessary to determine its technical scope according to right.
Claims (10)
1. a kind of micro-perfume capsule liquid detergent, it is characterised in that：Include the raw material of following parts by weight：
60.0-78.0 parts of deionized water；
Tetra- sodium of EDTA：0.05-0.2 parts；
Laureth sodium sulfovinate：10.0-18.0 parts；
Fatty alcohol polyoxyethylene ether -9：1.0-4.0 part；
Cocamide diethanolamine：1.0-3.0 part；
Cocoamidopropyl betaine：1.0-5.0 part；
Alkyl glycosides：5.0-10.0 part；
Microcapsule essence：0.2-1.0 parts；
Essence：0.2-1.0 parts；
Styrene/acrylic（Ester）Analog copolymer：0.3-1.0 parts；
Citric acid：0.1-0.5 parts；
Preservative：0.1-0.5 parts；
Fungicide：0.1-0.5 parts；
Catalyst：0.3-1.0 parts.
2. a kind of micro-perfume capsule liquid detergent according to claim 1, it is characterised in that：Include the raw material of following parts by weight：
Include the raw material of following parts by weight：
65.0-75.0 parts of deionized water；
Tetra- sodium of EDTA：0.05-0.15 parts；
Laureth sodium sulfovinate：12.0-15.0 parts；
Fatty alcohol polyoxyethylene ether -9：2.0-3.0 part；
Cocamide diethanolamine：2.0-3.0 part；
Cocoamidopropyl betaine：1.0-3.0 part；
Alkyl glycosides：5.0-8.0 part；
Microcapsule essence：0.2-0.5 parts；
Essence：0.2-0.5 parts；
Styrene/acrylic（Ester）Analog copolymer：0.3-0.5 parts；
Citric acid：0.1-0.2 parts；
Preservative：0.1-0.2 parts；
Fungicide：0.1-0.2 parts；
Catalyst：0.3-0.5 parts.
3. a kind of micro-perfume capsule liquid detergent according to claim 1, it is characterised in that：Include the raw material of following parts by weight：
65.0 parts of deionized water；
Tetra- sodium of EDTA：0.05 part；
Laureth sodium sulfovinate：12.0 parts；
Fatty alcohol polyoxyethylene ether -9：2.0 part；
Cocamide diethanolamine：3.0 part；
Cocoamidopropyl betaine：3.0 part；
Alkyl glycosides：8.0 part；
Microcapsule essence：0.5 part；
Essence：0.5 part；
Styrene/acrylic（Ester）Analog copolymer：0.5 part；
Citric acid：0.2 part；
Preservative：0.2 part；
Fungicide：0.2 part；
Catalyst：0.5 part.
4. a kind of micro-perfume capsule liquid detergent according to claim 1, it is characterised in that：Include the raw material of following parts by weight：
Include the raw material of following parts by weight：
75.0 parts of deionized water；
Tetra- sodium of EDTA：0.15 part；
Laureth sodium sulfovinate：15.0 parts；
Fatty alcohol polyoxyethylene ether -9：3.0 part；
Cocamide diethanolamine：3.0 part；
Cocoamidopropyl betaine：1.0 part；
Alkyl glycosides：5.0 part；
Microcapsule essence：0.2 part；
Essence：0.2 part；
Styrene/acrylic（Ester）Analog copolymer：0.3 part；
Citric acid：0.1 part；
Preservative：0.1 part；
Fungicide：0.1 part；
Catalyst：0.3 part.
5. a kind of micro-perfume capsule liquid detergent according to any one of claims 1-4, it is characterised in that：The preservative
For methylchloroisothiazandnone part, methyl-isothiazol ketone and magnesium chloride and the mixture of magnesium nitrate；The fungicide is DMDM
Hydantoins；The complex enzyme that the catalyst is protease, lipase and cellulase form.
6. the preparation method of micro-perfume capsule liquid detergent according to any one of claims 1-4, it is characterised in that：Comprising such as
Lower step：1）It weighs deionized water and tetra- sodium of EDTA is added in agitated kettle, stir to transparency liquid；
2）Laureth sodium sulfovinate is weighed respectively, alkyl glycosides, fatty alcohol polyoxyethylene ether -9, is added in agitated kettle, is stirred
It mixes to transparency liquid；
3）It weighs in cocamide diethanolamine, Cocoamidopropyl betaine addition pot, is stirred to transparency liquid respectively；
4）Microcapsule essence and deionized water are weighed by 1:It is uniformly dispersed and is added in agitated kettle after 5 dilution proportion and filtering, stirred
It mixes to translucent liquid；
5）Weigh styrene/acrylic（Ester）Analog copolymer is added in after being diluted with deionized water in agitated kettle, is stirred to white breast
Liquid；
6）Weigh after citric acid is diluted with deionized water add in pot in stirring pH value adjust to 6.0-8.0；
7）Weigh respectively essence, methylchloroisothiazandnone part, methyl-isothiazol ketone and magnesium chloride and magnesium nitrate mixture,
DMDMD hydantoins is added in agitated kettle, is stirred to milky emulsion；
8）It weighs complex enzyme to add in agitated kettle, stir to milky emulsion.
9）The lotion of above-mentioned preparation is packed using PVA water soluble films, is packaged into granular texture.
7. preparation method according to claim 6, it is characterised in that：The step 1）Mixing speed be 20r/min；Institute
State step 2）Mixing speed for 20r/min, mixing time is 30 minutes.
8. preparation method according to claim 6, which is characterized in that the step 3）Mixing speed for 20r/min, stir
It is 15 minutes to mix the time；The step 4）Mixing speed for 15r/min, mixing time is 15 minutes.
9. preparation method according to claim 6, which is characterized in that the step 5）Mixing speed for 15r/min, stir
It is 15 minutes to mix the time；The step 6）Mixing speed be 15r/min.
10. preparation method according to claim 6, which is characterized in that the step 7）Mixing speed for 15r/min,
Mixing time is 15 minutes；The step 8）Mixing speed for 15r/min, mixing time is 15 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810018655.XA CN108219993A (en) | 2018-01-09 | 2018-01-09 | A kind of micro-perfume capsule liquid detergent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810018655.XA CN108219993A (en) | 2018-01-09 | 2018-01-09 | A kind of micro-perfume capsule liquid detergent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108219993A true CN108219993A (en) | 2018-06-29 |
Family
ID=62640566
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810018655.XA Pending CN108219993A (en) | 2018-01-09 | 2018-01-09 | A kind of micro-perfume capsule liquid detergent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108219993A (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108913383A (en) * | 2018-08-04 | 2018-11-30 | 中山市妙洁精细化工有限公司 | A kind of floor cleaner and preparation method thereof |
| CN109112003A (en) * | 2018-09-28 | 2019-01-01 | 广州市加茜亚化妆品有限公司 | A kind of use in dishwasher washs solidifying pearl and preparation method |
| CN109439465A (en) * | 2018-11-19 | 2019-03-08 | 苏州绿叶日用品有限公司 | Fastness natural detergent composition and its preparation method and application |
| CN109679779A (en) * | 2018-12-14 | 2019-04-26 | 广州市骅香生物科技有限公司 | A kind of micro-sachet liquid detergent and preparation method thereof |
| CN109705994A (en) * | 2018-12-25 | 2019-05-03 | 广东爱车小屋实业发展股份有限公司 | Decontamination fumet and preparation method thereof |
| CN109810796A (en) * | 2019-01-24 | 2019-05-28 | 北京日光旭升精细化工技术研究所 | A kind of color protection exempts from brush liquid detergent and preparation method thereof |
| CN110465250A (en) * | 2019-08-09 | 2019-11-19 | 广州市蔻妍化妆品有限公司 | A kind of microcapsules compound wall materials, microcapsule essence and its preparation method and application |
| CN111234954A (en) * | 2020-03-06 | 2020-06-05 | 广州市百爱神生物科技有限公司 | Plant extract-containing microcapsule fragrance-retaining mother-infant detergent and preparation method thereof |
| CN111870544A (en) * | 2020-08-11 | 2020-11-03 | 青岛美今生物科技有限公司 | Formula and preparation method of sustained-release fragrance-lasting shampoo |
| CN112592774A (en) * | 2020-12-21 | 2021-04-02 | 上海东大化学有限公司 | Washing gel bead for wool fabric washing and preparation method thereof |
| CN112877150A (en) * | 2021-02-09 | 2021-06-01 | 浙江施维康生物医学材料有限公司 | Antibacterial and deodorant laundry detergent and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104818168A (en) * | 2015-04-28 | 2015-08-05 | 威莱(广州)日用品有限公司 | Laundry soap solution and preparation method thereof |
| CN105779159A (en) * | 2016-04-09 | 2016-07-20 | 福建省金鹿日化股份有限公司 | Softening clothes washing condensate ball and preparation method thereof |
| CN106833952A (en) * | 2017-01-03 | 2017-06-13 | 广州科玛生物科技股份有限公司 | A kind of infant liquid laundry detergent and preparation method thereof |
| CN107057876A (en) * | 2017-04-14 | 2017-08-18 | 广州市加茜亚化妆品有限公司 | A kind of solidifying pearl of antibacterial laundry and preparation method thereof |
-
2018
- 2018-01-09 CN CN201810018655.XA patent/CN108219993A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104818168A (en) * | 2015-04-28 | 2015-08-05 | 威莱(广州)日用品有限公司 | Laundry soap solution and preparation method thereof |
| CN105779159A (en) * | 2016-04-09 | 2016-07-20 | 福建省金鹿日化股份有限公司 | Softening clothes washing condensate ball and preparation method thereof |
| CN106833952A (en) * | 2017-01-03 | 2017-06-13 | 广州科玛生物科技股份有限公司 | A kind of infant liquid laundry detergent and preparation method thereof |
| CN107057876A (en) * | 2017-04-14 | 2017-08-18 | 广州市加茜亚化妆品有限公司 | A kind of solidifying pearl of antibacterial laundry and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 张流波，杨华明主编: "《医学消毒学最新进展》", 31 December 2015 * |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108913383A (en) * | 2018-08-04 | 2018-11-30 | 中山市妙洁精细化工有限公司 | A kind of floor cleaner and preparation method thereof |
| CN109112003B (en) * | 2018-09-28 | 2021-08-06 | 广州市加茜亚化妆品有限公司 | Washing gel bead for dish-washing machine and preparation method |
| CN109112003A (en) * | 2018-09-28 | 2019-01-01 | 广州市加茜亚化妆品有限公司 | A kind of use in dishwasher washs solidifying pearl and preparation method |
| CN109439465A (en) * | 2018-11-19 | 2019-03-08 | 苏州绿叶日用品有限公司 | Fastness natural detergent composition and its preparation method and application |
| CN109679779A (en) * | 2018-12-14 | 2019-04-26 | 广州市骅香生物科技有限公司 | A kind of micro-sachet liquid detergent and preparation method thereof |
| CN109705994A (en) * | 2018-12-25 | 2019-05-03 | 广东爱车小屋实业发展股份有限公司 | Decontamination fumet and preparation method thereof |
| CN109810796A (en) * | 2019-01-24 | 2019-05-28 | 北京日光旭升精细化工技术研究所 | A kind of color protection exempts from brush liquid detergent and preparation method thereof |
| CN110465250A (en) * | 2019-08-09 | 2019-11-19 | 广州市蔻妍化妆品有限公司 | A kind of microcapsules compound wall materials, microcapsule essence and its preparation method and application |
| CN111234954A (en) * | 2020-03-06 | 2020-06-05 | 广州市百爱神生物科技有限公司 | Plant extract-containing microcapsule fragrance-retaining mother-infant detergent and preparation method thereof |
| CN111870544A (en) * | 2020-08-11 | 2020-11-03 | 青岛美今生物科技有限公司 | Formula and preparation method of sustained-release fragrance-lasting shampoo |
| CN112592774A (en) * | 2020-12-21 | 2021-04-02 | 上海东大化学有限公司 | Washing gel bead for wool fabric washing and preparation method thereof |
| CN112592774B (en) * | 2020-12-21 | 2022-05-27 | 上海东大化学有限公司 | Washing gel bead for wool fabric washing and preparation method thereof |
| CN112877150A (en) * | 2021-02-09 | 2021-06-01 | 浙江施维康生物医学材料有限公司 | Antibacterial and deodorant laundry detergent and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108219993A (en) | A kind of micro-perfume capsule liquid detergent and preparation method thereof | |
| CN101851564B (en) | Laundry detergent used for washing underwear | |
| CN109536296B (en) | Antibacterial biological detergent for infants and preparation method thereof | |
| CN108841463A (en) | detergent composition | |
| CN108893212A (en) | A kind of solidifying pearl and preparation method thereof of doing washing | |
| CN102533479A (en) | Formulation and manufacturing method of Sapindus handmade soap | |
| CN105950312B (en) | A kind of garden stuff pesticide residue cleaning agent and preparation method thereof | |
| CN107418779A (en) | A kind of method of detergent composition and enhancing detergent emulsion dispersion greasy dirt ability | |
| CN106544173A (en) | Solidifying pearl of a kind of softening laundry and preparation method and application | |
| CN108300606A (en) | Liquid detergent | |
| CN111471543A (en) | Close-fitting clothes washing gel bead and preparation method thereof | |
| CN110184133A (en) | A kind of liquid detergent that can allow clothing long-acting bacteriostatic | |
| CN108192767A (en) | A kind of hyperconcetration dishwashing liquid and preparation method thereof | |
| CN106929247A (en) | A kind of lasting type laundry sheet and preparation method thereof | |
| CN107574032A (en) | A kind of liquid detergent and preparation method | |
| CN111876272A (en) | Laundry detergent | |
| CN108884417A (en) | Stable liquid detergent compositions comprising self-structure surfactant system | |
| CN104232372A (en) | Potent oxgall cleansing soap | |
| CN109609302A (en) | It is a kind of for clothing macula lutea, the cleaning solution of pigment and preparation method | |
| CN108865505A (en) | A kind of Tea Saponin dish washing liquid and preparation method thereof | |
| CN109602667B (en) | Antibacterial hand sanitizer and preparation method thereof | |
| CN107287059B (en) | Baby's children's clothes object bio-enzyme cleaning agent | |
| CN103710973A (en) | Non-woven fabrics special finishing agent used for paper diapers | |
| CN108410593A (en) | A kind of multiple-effect type liquid detergent and preparation method thereof | |
| CN113430068B (en) | Lasting fragrance washing gel bead and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180629 |