CN108192767A - A kind of hyperconcetration dishwashing liquid and preparation method thereof - Google Patents

A kind of hyperconcetration dishwashing liquid and preparation method thereof Download PDF

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Publication number
CN108192767A
CN108192767A CN201810018899.8A CN201810018899A CN108192767A CN 108192767 A CN108192767 A CN 108192767A CN 201810018899 A CN201810018899 A CN 201810018899A CN 108192767 A CN108192767 A CN 108192767A
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Prior art keywords
parts
hyperconcetration
liquid
minutes
mixing speed
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CN201810018899.8A
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Chinese (zh)
Inventor
熊鸣
熊一鸣
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Guangzhou City Jiaqian Ya Cosmetics Co Ltd
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Guangzhou City Jiaqian Ya Cosmetics Co Ltd
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Priority to CN201810018899.8A priority Critical patent/CN108192767A/en
Publication of CN108192767A publication Critical patent/CN108192767A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/835Mixtures of non-ionic with cationic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/046Salts
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/046Salts
    • C11D3/048Nitrates or nitrites
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2041Dihydric alcohols
    • C11D3/2044Dihydric alcohols linear
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2065Polyhydric alcohols
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/26Organic compounds containing nitrogen
    • C11D3/30Amines; Substituted amines ; Quaternized amines
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/26Organic compounds containing nitrogen
    • C11D3/32Amides; Substituted amides
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/26Organic compounds containing nitrogen
    • C11D3/33Amino carboxylic acids
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/34Organic compounds containing sulfur
    • C11D3/349Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3703Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3707Polyethers, e.g. polyalkyleneoxides
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/12Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Inorganic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

The present invention relates to a kind of hyperconcetration dishwashing liquids, include the raw material of following parts by weight:6.0 12.0 parts of deionized water;15.0 25.0 parts of laureth sodium sulfovinate;0.05 0.15 parts of EDTA disodiums;30 45 parts of surfactant;20 30 parts of dispersant;3.0 5.0 parts of triethanolamine;0.3 0.5 parts of essence;High-quality 25.0 35.0 parts of isomery C13 alkanols polyoxyethylene ether;10.0 15.0 parts of dodecanamide propyl amine oxide;0.2 0.5 parts of citric acid;0.1 0.2 parts of preservative;Wherein, dispersant is glycerine and the mixture of propylene glycol.A kind of hyperconcetration dishwashing liquid of the present invention, the liquid detergent of capsule-type packaging are protected in a manner of wrapping up, can reduce liquid detergent composition and be contacted with bad outside environmental elements, convenience in transport, preservation and use.

Description

A kind of hyperconcetration dishwashing liquid and preparation method thereof
Technical field
The present invention relates to liquid detergent field, especially a kind of hyperconcetration dishwashing liquid and preparation method thereof.
Background technology
Liquid detergent, daily life cleaning supplies.It contains a variety of active ingredients, emulsifier, these ingredients are to various greasy Spot, harmful substance dissolving, emulsification, dispersion suspend, and subsequent clear water rinsing is separated from tableware surface;Its clean mild, bubble Foam is soft and fine, decomposes greasy, fast decontaminating, degerming rapidly, effectively thoroughly cleans, does not remain, distributes simple and elegant fruit flavor, wash rear pure white It is bright such as new.Often it is used to ensure that household sanitation, avoids germina infection.
Liquid detergent active constituent is generally 15% or so currently on the market, and use is bottled, and packing specification is in 500ml-5000ml It differs, this product is very high in transport and energy consumption, and liquid detergent internal component is easily affected by environment, is easily destroyed or waves Hair, holding time are not grown.Capsule-type packaging liquid detergent protected in a manner of wrapping up, can reduce liquid detergent composition with not Good outside environmental elements contact, convenience in transport, preservation and use, therefore a kind of liquid detergent of low activity ingredient is researched and developed, make to wash clean Essence can stabilising packaging in capsule, be of great significance.
Invention content
The technical problem to be solved by the present invention is to:In order to overcome the shortcomings of existing liquid detergent, provide a kind of hyperconcetration and wash Bowl liquid.
The technical solution adopted by the present invention to solve the technical problems is:A kind of hyperconcetration dishwashing liquid, includes following weight The raw material of part:
6.0-12.0 parts of deionized water;
15.0-25.0 parts of laureth sodium sulfovinate;
0.05-0.15 parts of EDTA disodiums;
30-45 parts of surfactant;
20-30 parts of dispersant;
3.0-5.0 parts of triethanolamine;
0.3-0.5 parts of essence;
High-quality 25.0-35.0 parts of isomery C13 alkanol polyoxyethylene ether;
10.0-15.0 parts of dodecanamide propyl amine oxide;
0.2-0.5 parts of citric acid;0.1-0.2 parts of preservative;
Wherein, dispersant is glycerine and the mixture of propylene glycol.
Preferably, the raw material for including following parts by weight of the dispersant:5.0-10.0 parts of glycerine, propylene glycol 15.0- 20.0 parts.
Preferably, the surfactant includes the raw material of following parts by weight:
15-25 parts of alkyl glycosides;
15-20 parts of alkyl benzene sulphonate.
It is further preferred that include the raw material of following parts by weight:
8 parts of deionized water;
0.1 part of EDTA disodiums;
20 parts of laureth sodium sulfovinate;
20 parts of alkyl glycosides;
8 parts of glycerine;
18 parts of propylene glycol;
20 parts of alkyl benzene sulphonate;
3 parts of triethanolamine;
0.5 part of essence;
High-quality 30 parts of isomery C13 alkanols polyoxyethylene ether;
10 parts of dodecanamide propyl amine-oxides;
0.2 part of citric acid;
0.1 part of preservative.
Preferably, the preservative is methylchloroisothiazandnone and methylisothiazolinone and magnesium chloride and magnesium nitrate Mixture.
The present invention also provides a kind of preparation methods of above-mentioned hyperconcetration dishwashing liquid, comprise the steps of:
1)It weighs deionized water and EDTA disodiums is added in agitated kettle, stir to transparency liquid.
2)It weighs laureth sodium sulfovinate, alkyl glycosides, glycerine, propylene glycol respectively to add in agitated kettle, stirring is extremely Uniform liquid.
3)Alkyl benzene sulphonate, triethanolamine, isomery C13 alkanols polyoxyethylene ether, dodecanamide propyl oxidation are weighed respectively Ammonium is added in pot, is stirred to transparency liquid.
4)It weighs citric acid to add in agitated kettle, stirs to transparency liquid and adjust pH value 7.2-8.0.
5)It weighs essence to add in agitated kettle, stir to transparency liquid.
6)It weighs preservative to add in agitated kettle, stir to transparency liquid.
7)It carries out being packaged into capsule-like structure using PVA water soluble films.
Preferably, the step 1)Mixing speed be 20r/min;The step 2)Mixing speed for 20r/min, stir It is 30 minutes to mix the time.
Preferably, the step 3)Mixing speed for 20r/min, mixing time is 15 minutes;The step 4)Stir Speed is mixed as 15r/min, mixing time is 10 minutes.
Preferably, the step 5)Mixing speed for 15r/min, mixing time is 10 minutes;The step 6)Stir Speed is mixed as 15r/min, mixing time is 15 minutes.
The beneficial effects of the invention are as follows:Disperseed using glycerine, propylene glycol as solvent, instead of most of deionized water Dissolving, using glycerine, propylene glycol high dispersive Thief zone the characteristics of can quickly dissolve surface agent, stability is high, at low cost, allows High activity object surfactant is using process to absorb large quantity of moisture performance cleaning efficacy, and biological degradability height, is ideal Dispersed solvent;PVA water soluble films could preserve under addition of the water less than less than 12%, deionized water additive amount in the present invention It, can be with PVA water soluble film long-term co-existence, convenience in transport, preservation and use less than 12%.
Specific embodiment
The present invention is explained further, but embodiment does not do any type of limit to the present invention below in conjunction with specific embodiment It is fixed.
Embodiment 1
Hyperconcetration dishwashing liquid includes the raw material of following parts by weight:8 parts of deionized water;0.1 part of EDTA disodiums;Laureth 20 parts of sodium sulfovinate;20 parts of alkyl glycosides;8 parts of glycerine;18 parts of propylene glycol;20 parts of alkyl benzene sulphonate;Triethanolamine 3 Part;0.5 part of essence;High-quality 30 parts of isomery C13 alkanols polyoxyethylene ether;10 parts of dodecanamide propyl amine-oxides;Citric acid 0.2 part;0.1 part of preservative.The preservative is methylchloroisothiazandnone and methylisothiazolinone and magnesium chloride and nitre The mixture of sour magnesium.
The preparation method of hyperconcetration dishwashing liquid, comprises the steps of:
1)It weighs deionized water and EDTA disodiums is added in agitated kettle, mixing speed 20r/min;It stirs to transparency liquid.
2)It weighs laureth sodium sulfovinate, alkyl glycosides, glycerine, propylene glycol respectively to add in agitated kettle, stirring speed It spends for 20r/min, mixing time is 30 minutes, is stirred until homogeneous liquid.
3)Alkyl benzene sulphonate, triethanolamine, isomery C13 alkanols polyoxyethylene ether, dodecanamide propyl oxidation are weighed respectively Ammonium is added in pot, mixing speed 20r/min, and mixing time is 15 minutes, is stirred to transparency liquid.
4)It weighs citric acid to add in agitated kettle, mixing speed 15r/min, mixing time is 10 minutes, is stirred to saturating Prescribed liquid adjusts pH value 7.2-8.0.
5)It weighs essence to add in agitated kettle, mixing speed 15r/min, mixing time is 10 minutes, is stirred to transparent Liquid.
6)It weighs preservative to add in agitated kettle, mixing speed 15r/min, mixing time is 15 minutes, is stirred to saturating Prescribed liquid.
7)Using the packing method of capsule routine, carried out being packaged into capsule-like structure with PVA water soluble films.
Embodiment 2
Hyperconcetration dishwashing liquid includes the raw material of following parts by weight:6 parts of deionized water;0.05 part of EDTA disodiums;Laureth 15 parts of sodium sulfovinate;25 parts of alkyl glycosides;5 parts of glycerine;20 parts of propylene glycol;15 parts of alkyl benzene sulphonate;5 parts of triethanolamine; 0.3 part of essence;High-quality 35 parts of isomery C13 alkanols polyoxyethylene ether;15 parts of dodecanamide propyl amine-oxides;0.5 part of citric acid; 0.2 part of preservative.The preservative is methylchloroisothiazandnone and methylisothiazolinone and magnesium chloride and magnesium nitrate Mixture.
The preparation method of hyperconcetration dishwashing liquid, comprises the steps of:
1)It weighs deionized water and EDTA disodiums is added in agitated kettle, mixing speed 20r/min;It stirs to transparency liquid.
2)It weighs laureth sodium sulfovinate, alkyl glycosides, glycerine, propylene glycol respectively to add in agitated kettle, stirring speed It spends for 20r/min, mixing time is 30 minutes, is stirred until homogeneous liquid.
3)Alkyl benzene sulphonate, triethanolamine, isomery C13 alkanols polyoxyethylene ether, dodecanamide propyl oxidation are weighed respectively Ammonium is added in pot, mixing speed 20r/min, and mixing time is 15 minutes, is stirred to transparency liquid.
4)It weighs citric acid to add in agitated kettle, mixing speed 15r/min, mixing time is 10 minutes, is stirred to saturating Prescribed liquid adjusts pH value 7.2-8.0.
5)It weighs essence to add in agitated kettle, mixing speed 15r/min, mixing time is 10 minutes, is stirred to transparent Liquid.
6)It weighs preservative to add in agitated kettle, mixing speed 15r/min, mixing time is 15 minutes, is stirred to saturating Prescribed liquid.
7)Using the packing method of capsule routine, carried out being packaged into capsule-like structure with PVA water soluble films.
Embodiment 3
Hyperconcetration dishwashing liquid includes the raw material of following parts by weight:11 parts of deionized water;0.15 part of EDTA disodiums;Laruyl alcohol gathers 25 parts of ether sodium sulfovinate;15 parts of alkyl glycosides;10 parts of glycerine;15 parts of propylene glycol;20 parts of alkyl benzene sulphonate;4 parts of triethanolamine; 0.4 part of essence;High-quality 25 parts of isomery C13 alkanols polyoxyethylene ether;10 parts of dodecanamide propyl amine-oxides;0.3 part of citric acid;It is anti- Rotten 0.1 part of agent.The preservative is mixed for methylchloroisothiazandnone and methylisothiazolinone and magnesium chloride and magnesium nitrate Close object.
The preparation method of hyperconcetration dishwashing liquid, comprises the steps of:
1)It weighs deionized water and EDTA disodiums is added in agitated kettle, mixing speed 20r/min;It stirs to transparency liquid.
2)It weighs laureth sodium sulfovinate, alkyl glycosides, glycerine, propylene glycol respectively to add in agitated kettle, stirring speed It spends for 20r/min, mixing time is 30 minutes, is stirred until homogeneous liquid.
3)Alkyl benzene sulphonate, triethanolamine, isomery C13 alkanols polyoxyethylene ether, dodecanamide propyl oxidation are weighed respectively Ammonium is added in pot, mixing speed 20r/min, and mixing time is 15 minutes, is stirred to transparency liquid.
4)It weighs citric acid to add in agitated kettle, mixing speed 15r/min, mixing time is 10 minutes, is stirred to saturating Prescribed liquid adjusts pH value 7.2-8.0.
5)It weighs essence to add in agitated kettle, mixing speed 15r/min, mixing time is 10 minutes, is stirred to transparent Liquid.
6)It weighs preservative to add in agitated kettle, mixing speed 15r/min, mixing time is 15 minutes, is stirred to saturating Prescribed liquid.
7)Using the packing method of capsule routine, carried out being packaged into capsule-like structure with PVA water soluble films.
Embodiment 4
Hyperconcetration dishwashing liquid includes the raw material of following parts by weight:12 parts of deionized water;0.15 part of EDTA disodiums;Laruyl alcohol gathers 24 parts of ether sodium sulfovinate;15 parts of alkyl glycosides;10 parts of glycerine;15 parts of propylene glycol;20 parts of alkyl benzene sulphonate;4 parts of triethanolamine; 0.4 part of essence;High-quality 23 parts of isomery C13 alkanols polyoxyethylene ether;9 parts of dodecanamide propyl amine-oxides;0.3 part of citric acid;It is anti- Rotten 0.1 part of agent.The preservative is mixed for methylchloroisothiazandnone and methylisothiazolinone and magnesium chloride and magnesium nitrate Close object.
The preparation method of hyperconcetration dishwashing liquid, comprises the steps of:
1)It weighs deionized water and EDTA disodiums is added in agitated kettle, mixing speed 20r/min;It stirs to transparency liquid.
2)It weighs laureth sodium sulfovinate, alkyl glycosides, glycerine, propylene glycol respectively to add in agitated kettle, stirring speed It spends for 20r/min, mixing time is 30 minutes, is stirred until homogeneous liquid.
3)Alkyl benzene sulphonate, triethanolamine, isomery C13 alkanols polyoxyethylene ether, dodecanamide propyl oxidation are weighed respectively Ammonium is added in pot, mixing speed 20r/min, and mixing time is 15 minutes, is stirred to transparency liquid.
4)It weighs citric acid to add in agitated kettle, mixing speed 15r/min, mixing time is 10 minutes, is stirred to saturating Prescribed liquid adjusts pH value 7.2-8.0.
5)It weighs essence to add in agitated kettle, mixing speed 15r/min, mixing time is 10 minutes, is stirred to transparent Liquid.
6)It weighs preservative to add in agitated kettle, mixing speed 15r/min, mixing time is 15 minutes, is stirred to saturating Prescribed liquid.
7)Using the packing method of capsule routine, carried out being packaged into capsule-like structure with PVA water soluble films.
Embodiment 5
The stability experiment after capsule is made in hyperconcetration dishwashing liquid, takes the capsule 20 of the preparation in above-described embodiment 1-4 respectively, Be placed in constant temperature and humidity study on the stability chamber, respectively at 0 month, 3 months, 6 months, 9 months, 12 months, 18 months, 24 Detection of Stability is carried out respectively within a month.As a result such as the following table 1:
It can be seen that embodiment 1-3 is that hyperconcetration dishwashing liquid capsule stability obtained is good according to the experimental configuration of table 1, hyperconcetration Dishwashing liquid can be with PVA water soluble film long-term co-existence, and the deionized water content in embodiment 4 is high, can not be with PVA water soluble films for a long time altogether It deposits, is unsuitable for that capsule is made.
Using above-mentioned desirable embodiment according to the present invention as enlightenment, by above-mentioned description, relevant staff is complete Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention Property range is not limited to the content on specification, it is necessary to determine its technical scope according to right.

Claims (9)

1. a kind of hyperconcetration dishwashing liquid, which is characterized in that include the raw material of following parts by weight:
6.0-12.0 parts of deionized water;
15.0-25.0 parts of laureth sodium sulfovinate;
0.05-0.15 parts of EDTA disodiums;
30-45 parts of surfactant;
20-30 parts of dispersant;
3.0-5.0 parts of triethanolamine;
0.3-0.5 parts of essence;
High-quality 25.0-35.0 parts of isomery C13 alkanol polyoxyethylene ether;
10.0-15.0 parts of dodecanamide propyl amine oxide;
0.2-0.5 parts of citric acid;
0.1-0.2 parts of preservative;
Wherein, dispersant is glycerine and the mixture of propylene glycol.
2. hyperconcetration dishwashing liquid according to claim 1, which is characterized in that the dispersant comprising following parts by weight Raw material:5.0-10.0 parts of glycerine, 15.0-20.0 parts of propylene glycol.
3. hyperconcetration dishwashing liquid according to claim 1, which is characterized in that the surfactant includes following weight The raw material of part:
15-25 parts of alkyl glycosides;
15-20 parts of alkyl benzene sulphonate.
4. according to the hyperconcetration dishwashing liquid described in claim 1-3 any one, which is characterized in that include the original of following parts by weight Material:
8 parts of deionized water;
0.1 part of EDTA disodiums;
20 parts of laureth sodium sulfovinate;
20 parts of alkyl glycosides;
8 parts of glycerine;
18 parts of propylene glycol;
20 parts of alkyl benzene sulphonate;
3 parts of triethanolamine;
0.5 part of essence;
High-quality 30 parts of isomery C13 alkanols polyoxyethylene ether;
10 parts of dodecanamide propyl amine-oxides;
0.2 part of citric acid;
0.1 part of preservative.
5. hyperconcetration dishwashing liquid according to claim 4, which is characterized in that the preservative is methyl chloride isothiazoline Ketone and methylisothiazolinone and magnesium chloride and the mixture of magnesium nitrate.
6. the preparation method of the hyperconcetration dishwashing liquid according to claim 1-3 any one, which is characterized in that comprising following Step:
1)It weighs deionized water and EDTA disodiums is added in agitated kettle, stir to transparency liquid.
2)Laureth sodium sulfovinate, alkyl glycosides, glycerine, propylene glycol are weighed respectively to add in agitated kettle, are stirred until homogeneous Liquid.
3)Alkyl benzene sulphonate, triethanolamine, isomery C13 alkanols polyoxyethylene ether, dodecanamide propyl amine-oxides are weighed respectively to add Enter in pot, stir to transparency liquid.
4)It weighs citric acid to add in agitated kettle, stirs to transparency liquid and adjust pH value 7.2-8.0.
5)It weighs essence to add in agitated kettle, stir to transparency liquid.
6)It weighs preservative to add in agitated kettle, stir to transparency liquid.
7)It carries out being packaged into capsule-like structure using PVA water soluble films.
7. preparation method according to claim 6, which is characterized in that the step 1)Mixing speed be 20r/min;Institute State step 2)Mixing speed for 20r/min, mixing time is 30 minutes.
8. preparation method according to claim 6, which is characterized in that the step 3)Mixing speed for 20r/min, stir It is 15 minutes to mix the time;The step 4)Mixing speed for 15r/min, mixing time is 10 minutes.
9. preparation method according to claim 6, which is characterized in that the step 5)Mixing speed for 15r/min, stir It is 10 minutes to mix the time;The step 6)Mixing speed for 15r/min, mixing time is 15 minutes.
CN201810018899.8A 2018-01-09 2018-01-09 A kind of hyperconcetration dishwashing liquid and preparation method thereof Pending CN108192767A (en)

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CN109112003A (en) * 2018-09-28 2019-01-01 广州市加茜亚化妆品有限公司 A kind of use in dishwasher washs solidifying pearl and preparation method
CN111117804A (en) * 2020-01-16 2020-05-08 长沙而道新能源科技有限公司 Detergent for efficiently removing grease and preparation method thereof
CN111234953A (en) * 2020-03-06 2020-06-05 广州市百爱神生物科技有限公司 Plant extract tableware detergent wrapped by PVA water-soluble film and preparation method thereof
CN111286424A (en) * 2018-12-06 2020-06-16 南风化工集团股份有限公司 Super-concentrated detergent composition
CN115873667A (en) * 2022-11-28 2023-03-31 上饶市春宇科技有限公司 Capsule type super-concentrated detergent and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN109112003A (en) * 2018-09-28 2019-01-01 广州市加茜亚化妆品有限公司 A kind of use in dishwasher washs solidifying pearl and preparation method
CN109112003B (en) * 2018-09-28 2021-08-06 广州市加茜亚化妆品有限公司 Washing gel bead for dish-washing machine and preparation method
CN111286424A (en) * 2018-12-06 2020-06-16 南风化工集团股份有限公司 Super-concentrated detergent composition
CN111117804A (en) * 2020-01-16 2020-05-08 长沙而道新能源科技有限公司 Detergent for efficiently removing grease and preparation method thereof
CN111234953A (en) * 2020-03-06 2020-06-05 广州市百爱神生物科技有限公司 Plant extract tableware detergent wrapped by PVA water-soluble film and preparation method thereof
CN115873667A (en) * 2022-11-28 2023-03-31 上饶市春宇科技有限公司 Capsule type super-concentrated detergent and preparation method thereof

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Application publication date: 20180622