CN108218328A - A kind of environment-friendly type porcelain tendre and preparation method thereof - Google Patents
A kind of environment-friendly type porcelain tendre and preparation method thereof Download PDFInfo
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- CN108218328A CN108218328A CN201711285608.3A CN201711285608A CN108218328A CN 108218328 A CN108218328 A CN 108218328A CN 201711285608 A CN201711285608 A CN 201711285608A CN 108218328 A CN108218328 A CN 108218328A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00017—Aspects relating to the protection of the environment
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/34—Non-shrinking or non-cracking materials
- C04B2111/343—Crack resistant materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/50—Flexible or elastic materials
- C04B2111/506—Bendable material
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
A kind of environment-friendly type porcelain tendre includes the raw material of following parts by weight：9 12 parts of earthenware brick powder, cement 15 20,45 55 parts of quartz sand, 38 parts of SILICA FUME, 8 12 parts of acrylic emulsion, 25 parts of water-reducing agent, 13 parts of sintering aid, 12 parts of dispersant, 18 25 parts of water, with porcelain tendre produced by the present invention, water absorption rate is small, tensile strength is good, High anti bending strength, it is not easy to break and can guarantee porcelain tendre make on the cylinder of a diameter of 20cm 180 ° make around folding, it is flawless.
Description
Technical field
The invention belongs to build and decoration material field, and in particular to a kind of environment-friendly type porcelain tendre and preparation method thereof.
Background technology
Porcelain tendre is a kind of novel energy-saving low-carbon ornament materials, is formulated according to Guangdong Province《Porcelain tendre building decoration engineering skill
Art regulation》It explains：By wanting raw material based on modified cement, formed with special temperature control moulding system molding, baking, cross-linking radiation
It is a kind of there is flexible building decoration plane materiel, porcelain tendre is used as decorative material for wall surface, and with lightweight, flexible, appearance and modeling is more
The features such as sample, good weatherability, is used as floor decorative material, has the characteristics that wear-resisting, anti-skidding, comfortable foot feeling, easy construction is fast
Victory is shortened the construction period than traditional material, saves space, cost-effective and not easily to fall off, is built suitable for exterior wall, interior wall, ground etc.
Build decoration, especially suitable for skyscraper exterior finish engineering, facade decorative engineering, Old City Reconstruction exterior wall plane materiel,
The opposite sex building such as the finish coat and curved wall of external insulation system, arch column it is surface-veneer engineered；
Ceramic Tiles can inevitably generate various waste materials, such as useless mud, waste residue, useless powder, useless brick or useless base in process of production, give up
Mud is due to containing more impurity and colorant, it is difficult to be used in high-grade polished bricks, it is common practice to fill；Useless base is to press
The rotten base that is generated in the production processes such as brick, drying, stamp lacks the unqualified green compact such as flower, due to contain more impurity and
Colorant, it is difficult to be used in high-grade polished bricks, it is common practice to fill；Useless powder is typically to sell cheap；Waste residue is that brick body is being burnt into
The solid waste generated in the manufacturing procedures such as edging chamfering is needed later, since the harmful substance contained is too many, can not be returned
It receives, it is common practice to fill；Useless brick be polished bricks in sintering process, in process and during the examination and test of products
The irretrievable defective work for generating and finding, it is common practice to which degrade processing and landfill, and the waste material of generation is basic to be done
Method is landfill, causes the waste of material, also causes influence on environment to a certain extent.
Invention content
The shortcomings that the purpose of the present invention is overcoming the prior art, it is soft to provide a kind of flexible, High anti bending strength environment-friendly type
Porcelain, another object are to provide a kind of manufacturing method of above-mentioned porcelain tendre.
The present invention adopts the following technical scheme that：
A kind of environment-friendly type porcelain tendre includes the raw material of following parts by weight：9-12 parts of earthenware brick powder, cement 15-20, quartz sand 45-
55 parts, 3-8 parts of SILICA FUME, 8-12 parts of acrylic emulsion, 2-5 parts of water-reducing agent, 1-3 parts of sintering aid, 1-2 parts of dispersant, water 18-
25 parts.
Further, the water-reducing agent for sodium metasilicate, sodium pyrophosphate, calgon, waterglass, sodium tripolyphosphate,
It is one or more in polycarboxylic acids ammonium.
Further, Han Jian Liang≤0.6% of the cement.
Further, the sintering aid is one or more in wollastonite, mullite, black talc and lepidolite.
Further, the dispersant is ammonium polymethacrylate, methylcellulose, ammonium citrate, polyethylene glycol, three second
It is one or more in hydramine.
Further, the earthenware brick powder is generated in process of production by Ceramic Tiles useless powder, useless mud, waste residue, useless base, useless brick
In one or more mixing crush.
A kind of preparation method of environment-friendly type porcelain tendre, includes the following steps：
(1), after raw material required outside water removal and quartz sand is weighed by its parts by weight, the broken powder that is sieved to obtain；
(2), powder obtained and quartz sand are mixed, then adds in water and obtained slurry is mixed；
(3), slurry obtained is poured into mold, vibrations exhaust, dry obtained matrix；
(4), matrix is sent into drying kiln, 90-150min is handled at a temperature of 85-95 DEG C, obtains initial porcelain tendre；
(5), after initial porcelain tendre natural cooling, finished product.
Further, the step (1) includes：It will remove water after weighing with raw material required outside quartz sand by its parts by weight,
It crushed 200-300 mesh and sieves to obtain powder.
By the above-mentioned description of this invention it is found that compared with prior art, the beneficial effects of the invention are as follows：The present invention passes through
The waste material generated in ceramic tile producing process is recycled, as the basic material of porcelain tendre, reduces the waste of resource,
Reduce the pollution to environment；
By adding in dispersant, the time of slurry mixing is reduced, under the premise of ensureing that incorporation time is reduced, fills slurry
Divide and be uniformly mixed, and the dispersant added in does not interfere with the performance of porcelain tendre obtained；
Under the premise of porcelain tendre performance is not influenced, sintering aid is added in, drying temperature of the matrix in drying kiln is reduced, subtracts
The use of few energy, it is cost-effective；
Used porcelain tendre produced by the present invention, water absorption rate is small, tensile strength is good, High anti bending strength, not easy to break and can guarantee
Porcelain tendre is made 180 ° on the cylinder of a diameter of 20cm and is made around folding, flawless.
Specific embodiment
Below by way of specific embodiment, the invention will be further described.
A kind of environment-friendly type porcelain tendre includes the raw material of following parts by weight：9-12 parts of earthenware brick powder, cement 15-20, quartz sand 45-
55 parts, 3-8 parts of SILICA FUME, 8-12 parts of acrylic emulsion, 2-5 parts of water-reducing agent, 1-3 parts of sintering aid, 1-2 parts of dispersant, water 18-
25 parts；
Wherein, Han Jian Liang≤0.6% of cement；
Water-reducing agent is one in sodium metasilicate, sodium pyrophosphate, calgon, waterglass, sodium tripolyphosphate, polycarboxylic acids ammonium
Kind is a variety of；
Sintering aid is one or more in wollastonite, mullite, black talc and lepidolite；
Dispersant is ammonium polymethacrylate, one kind in methylcellulose, ammonium citrate, polyethylene glycol, triethanolamine
It is or a variety of；
One kind or more in useless powder that earthenware brick powder is generated in process of production by Ceramic Tiles, useless mud, waste residue, useless base, useless brick
Kind mixing is broken to be formed；
A kind of preparation method of environment-friendly type porcelain tendre, includes the following steps：
(1), it after raw material required outside water removal and quartz sand is weighed by its parts by weight, crushed 200-300 mesh and sieved
Powder；
(2), powder obtained and quartz sand are mixed, then adds in water and obtained slurry is mixed；
(3), slurry obtained is poured into mold, vibrations exhaust, dry obtained matrix；
(4), matrix is sent into drying kiln, 90-150min is handled at a temperature of 85-95 DEG C, obtains initial porcelain tendre；
(5), after initial porcelain tendre natural cooling, finished product.
Embodiment 1
A kind of environment-friendly type porcelain tendre includes the raw material of following parts by weight：12 parts of earthenware brick powder, cement 15,45 parts of quartz sand, micro- silicon
3 parts of powder, 12 parts of acrylic emulsion, 2 parts of sodium metasilicate, 1.5 parts of polycarboxylic acids ammonium, 1.5 parts of calgon, 1 part of wollastonite, poly- first
1 part of base ammonium acrylate, 1 part of ammonium citrate, 25 parts of water；
Wherein, earthenware brick powder is crushed by useless mud；
Han Jian Liang≤0.6% of cement；
A kind of preparation method of environment-friendly type porcelain tendre, includes the following steps：
(1), after raw material required outside water removal and quartz sand is weighed by its parts by weight, 200 mesh was crushed and sieve to obtain powder；
(2), powder obtained and quartz sand are mixed, then adds in water and obtained slurry is mixed；
(3), slurry obtained is poured into mold, vibrations exhaust, dry obtained matrix；
(4), matrix is sent into drying kiln, handles 90min at a temperature of 95 DEG C, obtain initial porcelain tendre；
(5), after initial porcelain tendre natural cooling, finished product.
Porcelain tendre obtained above obtains following performance parameter through experiment：
Flexural strength 13.9MPa；
Xi Shui Shuai≤1.5%；
Tensile strength：8.6MPa；
Pass through above-mentioned test data：By the way that porcelain tendre water absorption rate produced by the present invention is small, tensile strength is good, anti-folding is strong
Degree is high, not easy to break and can guarantee that porcelain tendre makees 180 ° of works around folding on the cylinder of a diameter of 20cm, flawless.
Embodiment 2
A kind of environment-friendly type porcelain tendre includes the raw material of following parts by weight：9 parts of earthenware brick powder, cement 20,55 parts of quartz sand, micro- silicon
8 parts of powder, 8 parts of acrylic emulsion, 1 part of waterglass, 1 part of sodium pyrophosphate, 2 parts of mullite, 1 part of black talc, methylcellulose 0.2
Part, 0.8 part of triethanolamine, 18 parts of water；
Wherein, earthenware brick powder is crushed and is formed by useless brick and waste residue mixing；
Han Jian Liang≤0.6% of cement；
A kind of preparation method of environment-friendly type porcelain tendre, includes the following steps：
(1), after raw material required outside water removal and quartz sand is weighed by its parts by weight, 300 mesh was crushed and sieve to obtain powder；
(2), powder obtained and quartz sand are mixed, then adds in water and obtained slurry is mixed；
(3), slurry obtained is poured into mold, vibrations exhaust, dry obtained matrix；
(4), matrix is sent into drying kiln, handles 150min at a temperature of 85 DEG C, obtain initial porcelain tendre；
(5), after initial porcelain tendre natural cooling, finished product.
Porcelain tendre obtained above obtains following performance parameter through experiment：
Flexural strength 14.1MPa；
Xi Shui Shuai≤1.5%；
Tensile strength：8.3MPa；
Pass through above-mentioned test data：By the way that porcelain tendre water absorption rate produced by the present invention is small, tensile strength is good, anti-folding is strong
Degree is high, not easy to break and can guarantee that porcelain tendre makees 180 ° of works around folding on the cylinder of a diameter of 20cm, flawless.
Embodiment 3
A kind of environment-friendly type porcelain tendre includes the raw material of following parts by weight：10 parts of earthenware brick powder, cement 18,50 parts of quartz sand, micro- silicon
5 parts of powder, 10 parts of acrylic emulsion, 1 part of sodium tripolyphosphate, 1 part of waterglass, 1 part of sodium pyrophosphate, 1 part of wollastonite, 1 part of lepidolite,
0.7 part of methylcellulose, 0.5 part of polyethylene glycol, 0.3 part of triethanolamine, 18 parts of water；
Wherein, earthenware brick powder is crushed by 1 useless powder；
Han Jian Liang≤0.6% of cement；
A kind of preparation method of environment-friendly type porcelain tendre, includes the following steps：
(1), after raw material required outside water removal and quartz sand is weighed by its parts by weight, 250 mesh was crushed and sieve to obtain powder；
(2), powder obtained and quartz sand are mixed, then adds in water and obtained slurry is mixed；
(3), slurry obtained is poured into mold, vibrations exhaust, dry obtained matrix；
(4), matrix is sent into drying kiln, handles 120min at a temperature of 90 DEG C, obtain initial porcelain tendre；
(5), after initial porcelain tendre natural cooling, finished product.
Porcelain tendre obtained above obtains following performance parameter through experiment：
Flexural strength 14.5MPa；
Xi Shui Shuai≤1.5%；
Tensile strength：8.7MPa；
Pass through above-mentioned test data：By the way that porcelain tendre water absorption rate produced by the present invention is small, tensile strength is good, anti-folding is strong
Degree is high, not easy to break and can guarantee that porcelain tendre makees 180 ° of works around folding on the cylinder of a diameter of 20cm, flawless.
Embodiment 4
A kind of environment-friendly type porcelain tendre includes the raw material of following parts by weight：9 parts of earthenware brick powder, cement 20,50 parts of quartz sand, micro- silicon
8 parts of powder, 8 parts of acrylic emulsion, 1 part of waterglass, 1 part of sodium pyrophosphate, 2 parts of mullite, 1 part of lepidolite, 0.4 part of polycarboxylic acids ammonium,
0.6 part of triethanolamine, 18 parts of water；
Wherein, earthenware brick powder is crushed by useless base；
Han Jian Liang≤0.6% of cement；
A kind of preparation method of environment-friendly type porcelain tendre, includes the following steps：
(1), after raw material required outside water removal and quartz sand is weighed by its parts by weight, 300 mesh was crushed and sieve to obtain powder；
(2), powder obtained and quartz sand are mixed, then adds in water and obtained slurry is mixed；
(3), slurry obtained is poured into mold, vibrations exhaust, dry obtained matrix；
(4), matrix is sent into drying kiln, handles 150min at a temperature of 85 DEG C, obtain initial porcelain tendre；
(5), after initial porcelain tendre natural cooling, finished product.
Porcelain tendre obtained above obtains following performance parameter through experiment：
Flexural strength 14.0MPa；
Xi Shui Shuai≤1.5%；
Tensile strength：8.2MPa；
Pass through above-mentioned test data：By the way that porcelain tendre water absorption rate produced by the present invention is small, tensile strength is good, anti-folding is strong
Degree is high, not easy to break and can guarantee that porcelain tendre makees 180 ° of works around folding on the cylinder of a diameter of 20cm, flawless.
The foregoing is only a preferred embodiment of the present invention, therefore the range that the present invention is implemented cannot be limited with this, i.e.,
According to the equivalent changes and modifications that scope of the present invention patent and description are made, it all should still belong to what patent of the present invention covered
In the range of.
Claims (8)
1. a kind of environment-friendly type porcelain tendre, it is characterised in that：Include the raw material of following parts by weight：9-12 parts of earthenware brick powder, cement 15-20,
45-55 parts of quartz sand, 3-8 parts of SILICA FUME, 8-12 parts of acrylic emulsion, 2-5 parts of water-reducing agent, 1-3 parts of sintering aid, dispersant 1-
2 parts, 18-25 parts of water.
2. a kind of environment-friendly type porcelain tendre according to claim 1, it is characterised in that：The water-reducing agent is sodium metasilicate, burnt phosphorus
It is one or more in sour sodium, calgon, waterglass, sodium tripolyphosphate, polycarboxylic acids ammonium.
3. a kind of environment-friendly type porcelain tendre according to claim 1, it is characterised in that：Han Jian Liang≤0.6% of the cement.
4. a kind of environment-friendly type porcelain tendre according to claim 1, it is characterised in that：The sintering aid is wollastonite, Mo Lai
It is one or more in stone, black talc and lepidolite.
5. a kind of environment-friendly type porcelain tendre according to claim 1, it is characterised in that：The dispersant is polymethylacrylic acid
It is one or more in ammonium, methylcellulose, ammonium citrate, polyethylene glycol, triethanolamine.
6. a kind of environment-friendly type porcelain tendre according to claim 1, it is characterised in that：The earthenware brick powder was being produced by Ceramic Tiles
One or more mixing in the useless powder generated in journey, the mud that gives up, waste residue, useless base, useless brick crush.
7. a kind of preparation method of environment-friendly type porcelain tendre, it is characterised in that：Include the following steps：
(1), after raw material required outside water removal and quartz sand is weighed by its parts by weight, the broken powder that is sieved to obtain；
(2), powder obtained and quartz sand are mixed, then adds in water and obtained slurry is mixed；
(3), slurry obtained is poured into mold, vibrations exhaust, dry obtained matrix；
(4), matrix is sent into drying kiln, 90-150min is handled at a temperature of 85-95 DEG C, obtains initial porcelain tendre；
(5), after initial porcelain tendre natural cooling, finished product.
8. a kind of preparation method of environment-friendly type porcelain tendre according to claim 7, it is characterised in that：The step (1) includes：
It will remove water after weighing with raw material required outside quartz sand by its parts by weight, crushed 200-300 mesh and sieve to obtain powder.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111499326A (en) * | 2020-04-17 | 2020-08-07 | 四川海聚环保科技有限责任公司 | Preparation method of water-based cement elastic emulsion-based flexible veneer substrate |
| CN113416039A (en) * | 2021-07-12 | 2021-09-21 | 湖北垚美软瓷有限公司 | Soft porcelain material with high weather resistance |
| CN117209247A (en) * | 2023-08-04 | 2023-12-12 | 常州市柚米家居用品有限公司 | Lithium-free heat-resistant ceramic and preparation method thereof |
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| CN105731877A (en) * | 2014-12-09 | 2016-07-06 | 辽宁利永盛新材料有限公司 | Formula and preparation method of novel green environment-friendly flexible soft-paste porcelain decorative tile |
| CN106495613A (en) * | 2016-11-03 | 2017-03-15 | 威骏（湖北）高新实业股份有限公司 | A kind of heat preservation decoration integrative tapestry brick and preparation method thereof |
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| WO2009146470A1 (en) * | 2008-06-02 | 2009-12-10 | Mikayel Hamamchyan | The method of manufacturing building brick |
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| CN111499326A (en) * | 2020-04-17 | 2020-08-07 | 四川海聚环保科技有限责任公司 | Preparation method of water-based cement elastic emulsion-based flexible veneer substrate |
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| CN113416039A (en) * | 2021-07-12 | 2021-09-21 | 湖北垚美软瓷有限公司 | Soft porcelain material with high weather resistance |
| CN117209247A (en) * | 2023-08-04 | 2023-12-12 | 常州市柚米家居用品有限公司 | Lithium-free heat-resistant ceramic and preparation method thereof |
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Application publication date: 20180629 |