CN108218314A - A kind of preparation method of high plasticity bone porcelain pug - Google Patents
A kind of preparation method of high plasticity bone porcelain pug Download PDFInfo
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- CN108218314A CN108218314A CN201711487698.4A CN201711487698A CN108218314A CN 108218314 A CN108218314 A CN 108218314A CN 201711487698 A CN201711487698 A CN 201711487698A CN 108218314 A CN108218314 A CN 108218314A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/001—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing unburned clay
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B14/00—Use of inorganic materials as fillers, e.g. pigments, for mortars, concrete or artificial stone; Treatment of inorganic materials specially adapted to enhance their filling properties in mortars, concrete or artificial stone
- C04B14/02—Granular materials, e.g. microballoons
- C04B14/36—Inorganic materials not provided for in groups C04B14/022 and C04B14/04 - C04B14/34
- C04B14/366—Phosphates, e.g. apatite
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B40/00—Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
- C04B40/0028—Aspects relating to the mixing step of the mortar preparation
- C04B40/0039—Premixtures of ingredients
- C04B40/0046—Premixtures of ingredients characterised by their processing, e.g. sequence of mixing the ingredients when preparing the premixtures
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Abstract
The present invention relates to a kind of preparation methods of high plasticity bone porcelain pug, belong to Bone China preparing technical field.It is of the invention fully to realize waste utilization,Collect kitchen garbage gutter oil,By itself and the blending fermentation of overbasic saline-alkali soil,Saponification occurs,And there is hot water dissolving's saponification resultant,And using saponification resultant as self-control anionic surfactant,Then using sugarcane and beet as raw material,First natural syrup is obtained through the re-compacted extraction of cellulase degradation,Again with the multiple fruit containing amino acid and organic acid and dusty yeast blending fermentation,Amino acid is further degraded using microorganism and generates the hydrophile amino and carboxyl of a large amount of free properties,Anionic surfactant will finally be made by oneself,Natural syrup and hydrophile amino rich in free property and the ferment filtrate of carboxyl and the mixing of other china raw materials,Up to high plasticity bone porcelain pug after kneading is aging,High plasticity bone porcelain pug plasticity produced by the present invention is good,Billet yield is high,It has broad application prospects.
Description
Technical field
The present invention relates to a kind of preparation methods of high plasticity bone porcelain pug, belong to Bone China preparing technical field.
Background technology
China is the country of ceramics, and long Ceramics Culture is along with the development of ceramic science technology and art and constantly shining
Send out new vitality.Passed on over the past thousands of years in China in the ancient making ceramics skill got off, with winch throwing molding according to
So it is important a kind of molding mode.At present, the research of ceramic material has expanded polynary approach for ceramic art, but art
Uniqueness requirement, the attribute that traditional-handwork makes are still one of an important factor for determining high-end art pottery value.Collector
It still grows tender of and is molded circle device making for hand throwing, ceramic value value preserving and appreciation play an important role.
Bone China is one of high-grade porcelain kind recognized in the world, and Bone China has that pure white, gentle, transparency is good, glaze paint
The features such as brightness is high represents the highest technical merit of contemporary Production of Ceramics.Bone China is with animal bone ash or other alternative
Product are primary raw material, are equipped with the minerals such as clay, feldspar, quartz and manufactured high-grade daily-use fine.It is high, saturating with whiteness
The advantages that lightness is good, glaze paint is smooth, high mechanical strength, but traditional bone porcelain pug poor plasticity, billet yield are low, big part production
Product are difficult to roll forming.
Therefore, it is good to invent a kind of plasticity, billet yield is high, and the bone porcelain pug of hand throwing is suitble to prepare skill to Bone China
Art field has positive effect.
Invention content
Present invention mainly solves the technical issues of, it is low, big for traditional bone porcelain pug poor plasticity, billet yield at present
The defects of part product is difficult to roll forming provides a kind of preparation method of high plasticity bone porcelain pug.
In order to solve the above-mentioned technical problem, the technical solution adopted in the present invention is：
A kind of preparation method of high plasticity bone porcelain pug, it is characterised in that specifically preparation process is：
（1）The saline-alkali soil in gutter oil and salt-soda soil is collected, is put into fermentation tank, will ferment after gutter oil and saline-alkali soil are mixed
It in tank embedment salt-soda soil, is sealed by fermentation 30~40 days, takes out tunning after fermentation, add after tunning and water are mixed
Heat heating, 20~30min of insulated and stirred is separated by filtration to obtain filtrate after stirring, spare；
（2）By mass ratioes are waited to weigh sugarcane and beet, and be put into 20~30min of crushing in tissue pulverizer jointly, will crush
It is fitted into enzymatic vessel after object and cellulase mixing, heat preservation 6~8h of enzymolysis waits that enzymolysis product is moved into squeezer after digesting
Middle squeezing juice obtains mixing juice；
（3）It weighs Kiwi berry, pineapple and new fresh grape to pour into ball mill successively, is 20 by ball material mass ratio:1 into ball grinder
Zirconium oxide ball milling pearl is added in, 20~30min of ball-milling treatment obtains ball-milled mixtures after ball milling；
（4）It is fitted into fermentation tank after above-mentioned ball-milled mixtures and dusty yeast are mixed, after sealed fermenter, heat-preservation fermentation 8~10
My god, tunning is taken out after fermentation and is separated by filtration, and obtains ferment filtrate；
（5）It counts in parts by weight, weighs 40~45 parts of bovine bone powders, 10~12 parts of quartz sands, 8~10 parts of potassium feldspars, 7~9 parts of sides
Xie Shi, 3~6 parts of bentonites, 3~5 parts of spare filtrates, 5~8 portions of mixing juice and 6~9 parts of above-mentioned ferment filtrates and 60~
70 parts of water are put into 1~2h of kneading in masticator, after kneading, stand aging 3~5 days in the greenhouse to get high plasticity bone
Matter porcelain pug.
Step（1）Described in gutter oil and saline-alkali soil mass ratio be 2:1, the mass ratio of tunning and water is 1:5,
The temperature of heat temperature raising is 70~80 DEG C.
Step（2）Described in crushed material and cellulase mass ratio be 10:1, the temperature for keeping the temperature enzymolysis is 25~35
℃。
Step（3）Described in Kiwi berry, pineapple and new fresh grape mass ratio be 1:1:4.
Step（4）Described in ball-milled mixtures and dusty yeast mass ratio be 50:1, the temperature of heat-preservation fermentation for 35~
40℃。
Step（5）Described in greenhouse in relative air humidity for 70~80%, temperature is 30~40 DEG C.
The beneficial effects of the invention are as follows：
Abundant realization waste utilization of the invention, collects kitchen garbage gutter oil, itself and the blending of overbasic saline-alkali soil is fermented,
Gutter oil and saline-alkali soil is made saponification to occur, and have hot water dissolving's saponification resultant, and with saponification under the action of edaphon
Product, then using sugarcane and beet as raw material, is first pressed again as self-control anionic surfactant through cellulase degradation
System extraction obtains natural syrup, then with the multiple fruit containing amino acid and organic acid and dusty yeast blending fermentation, will using microorganism
Amino acid, which is further degraded, generates the hydrophile amino and carboxyl of a large amount of free properties, finally will self-control anionic surfactant,
Natural syrup and hydrophile amino rich in free property and the ferment filtrate of carboxyl and the mixing of other china raw materials, after kneading is aging
It, can will be in pug containing abundant organic acid in bone porcelain pug produced by the present invention up to high plasticity bone porcelain pug
Alkaline matter neutralize, so as to reduce the electrostatic repulsion between pug particle, the cohesive force between pug is improved, in combination with syrup
Hydrophilic caking property, further improve the internal bond strength between pug, enhance its plasticity, and the bone meal surface band in pug
There is a small amount of positive charge, the self-control anionic surfactant that the present invention adds in can improve the knot between pug by charge attraction
Intensity is closed, in addition surfactant can also play the role of moistened surface between particle, abundant free property in combining with fermentation filtrate
Amino and carboxyl improve the hydration capability of pug, and cause different size of even particulate dispersion in pug, throwing molding
When, size particles match arrangement so that and countless capillaries can be formed on green body, keeps the channel of moisture diffusion evaporation,
Molding green body since water content is low and has good capillary diffusion channel, accelerate, can be in very short time by rate of drying
It is interior to obtain larger intensity, the phenomenon that weak and limp will not occur, greatly improve billet yield, due to blank strength height, decrease and repair
The breakage rate of green body improves bone porcelain pug again under the action of last kneading and aging microorganism in the process
Plasticity has broad application prospects.
Specific embodiment
The saline-alkali soil in gutter oil and salt-soda soil is collected, is 2 in mass ratio by gutter oil and saline-alkali soil:It is put into after 1 mixing
In fermentation tank, fermentation tank is embedded in salt-soda soil, is sealed by fermentation 30~40 days, is taken out tunning after fermentation, will ferment
Product and water are 1 in mass ratio:70~80 DEG C, 20~30min of insulated and stirred are heated to after 5 mixing, mistake after stirring
Isolated filtrate is filtered, it is spare；By waiting mass ratioes to weigh sugarcane and beet, and be put into jointly in tissue pulverizer and crush 20~
Crushed material and cellulase are 10 in mass ratio by 30min:It is fitted into enzymatic vessel after 1 mixing, enzymolysis is kept the temperature at 25~35 DEG C
6~8h is waited to move into enzymolysis product in squeezer after digesting and is squeezed juice, obtains mixing juice；It is 1 in mass ratio:1:4
It weighs Kiwi berry, pineapple and new fresh grape to pour into ball mill successively, is 20 by ball material mass ratio:1 adds in oxygen into ball grinder
Change zirconium ball milling pearl, 20~30min of ball-milling treatment obtains ball-milled mixtures after ball milling；Ball-milled mixtures and dusty yeast are pressed
Mass ratio is 50:It is fitted into fermentation tank after 1 mixing, after sealed fermenter, heat-preservation fermentation 8~10 at being 35~40 DEG C in temperature
My god, tunning is taken out after fermentation and is separated by filtration, and obtains ferment filtrate；It counts in parts by weight, weighs 40~45 portions of ox bones
Powder, 10~12 parts of quartz sands, 8~10 parts of potassium feldspars, 7~9 parts of calcites, 3~6 parts of bentonites, 3~5 parts of spare filtrates, 5
~8 portions of mixing juice and 6~9 parts of above-mentioned ferment filtrates and 60~70 parts of water are put into 1~2h of kneading in masticator, and kneading terminates
Afterwards, it is 70~80% in relative air humidity, temperature is to stand aging 3~5 days in 30~40 DEG C of greenhouse to get high plasticity
Bone porcelain pug.
Example 1
The saline-alkali soil in gutter oil and salt-soda soil is collected, is 2 in mass ratio by gutter oil and saline-alkali soil:Fermentation is put into after 1 mixing
In tank, fermentation tank is embedded in salt-soda soil, is sealed by fermentation 30 days, tunning is taken out after fermentation, by tunning and water
It is 1 in mass ratio:70 DEG C, insulated and stirred 20min are heated to after 5 mixing, is separated by filtration to obtain filtrate after stirring, it is standby
With；By mass ratioes are waited to weigh sugarcane and beet, and be put into jointly in tissue pulverizer and crush 20min, by crushed material and fiber
Plain enzyme is 10 in mass ratio:It is fitted into enzymatic vessel after 1 mixing, the heat preservation enzymolysis 6h at 25 DEG C waits to produce enzymolysis after digesting
Object moves into squeezer and squeezes juice, obtains mixing juice；It is 1 in mass ratio:1:4 weigh Kiwi berry, pineapple and new fresh grape
It pours into ball mill successively, is 20 by ball material mass ratio:1 into ball grinder add in zirconium oxide ball milling pearl, ball-milling treatment 20min,
Ball-milled mixtures are obtained after ball milling；It is 50 in mass ratio by ball-milled mixtures and dusty yeast:Fermentation tank is packed into after 1 mixing
In, after sealed fermenter, heat-preservation fermentation 8 days at being 35 DEG C in temperature takes out tunning and is separated by filtration, obtains after fermentation
Ferment filtrate；It counts in parts by weight, weighs 40 parts of bovine bone powders, 10 parts of quartz sands, 8 parts of potassium feldspars, 7 parts of calcites, 3 parts of swellings
Soil, 3 parts of spare filtrates, 5 portions of mixing juice and 6 parts of above-mentioned ferment filtrates and 60 parts of water are put into kneading 1h in masticator, pinch
It is 70% in relative air humidity after refining, temperature is to stand aging 3 days in 30 DEG C of greenhouse to get high plasticity Bone China
Pug.
Example 2
The saline-alkali soil in gutter oil and salt-soda soil is collected, is 2 in mass ratio by gutter oil and saline-alkali soil:Fermentation is put into after 1 mixing
In tank, fermentation tank is embedded in salt-soda soil, is sealed by fermentation 35 days, tunning is taken out after fermentation, by tunning and water
It is 1 in mass ratio:75 DEG C, insulated and stirred 25min are heated to after 5 mixing, is separated by filtration to obtain filtrate after stirring, it is standby
With；By mass ratioes are waited to weigh sugarcane and beet, and be put into jointly in tissue pulverizer and crush 25min, by crushed material and fiber
Plain enzyme is 10 in mass ratio:It is fitted into enzymatic vessel after 1 mixing, the heat preservation enzymolysis 7h at 30 DEG C waits to produce enzymolysis after digesting
Object moves into squeezer and squeezes juice, obtains mixing juice；It is 1 in mass ratio:1:4 weigh Kiwi berry, pineapple and new fresh grape
It pours into ball mill successively, is 20 by ball material mass ratio:1 into ball grinder add in zirconium oxide ball milling pearl, ball-milling treatment 25min,
Ball-milled mixtures are obtained after ball milling；It is 50 in mass ratio by ball-milled mixtures and dusty yeast:Fermentation tank is packed into after 1 mixing
In, after sealed fermenter, heat-preservation fermentation 9 days at being 38 DEG C in temperature takes out tunning and is separated by filtration, obtains after fermentation
Ferment filtrate；It counts in parts by weight, weighs 43 parts of bovine bone powders, 11 parts of quartz sands, 9 parts of potassium feldspars, 8 parts of calcites, 5 parts of swellings
Soil, 4 parts of spare filtrates, 6 portions of mixing juice and 8 parts of above-mentioned ferment filtrates and 65 parts of water are put into kneading 1h in masticator, pinch
It is 75% in relative air humidity after refining, temperature is to stand aging 4 days in 35 DEG C of greenhouse to get high plasticity Bone China
Pug.
Example 3
The saline-alkali soil in gutter oil and salt-soda soil is collected, is 2 in mass ratio by gutter oil and saline-alkali soil:Fermentation is put into after 1 mixing
In tank, fermentation tank is embedded in salt-soda soil, is sealed by fermentation 40 days, tunning is taken out after fermentation, by tunning and water
It is 1 in mass ratio:80 DEG C, insulated and stirred 30min are heated to after 5 mixing, is separated by filtration to obtain filtrate after stirring, it is standby
With；By mass ratioes are waited to weigh sugarcane and beet, and be put into jointly in tissue pulverizer and crush 30min, by crushed material and fiber
Plain enzyme is 10 in mass ratio:It is fitted into enzymatic vessel after 1 mixing, the heat preservation enzymolysis 8h at 35 DEG C waits to produce enzymolysis after digesting
Object moves into squeezer and squeezes juice, obtains mixing juice；It is 1 in mass ratio:1:4 weigh Kiwi berry, pineapple and new fresh grape
It pours into ball mill successively, is 20 by ball material mass ratio:1 into ball grinder add in zirconium oxide ball milling pearl, ball-milling treatment 30min,
Ball-milled mixtures are obtained after ball milling；It is 50 in mass ratio by ball-milled mixtures and dusty yeast:Fermentation tank is packed into after 1 mixing
In, after sealed fermenter, heat-preservation fermentation 10 days at being 40 DEG C in temperature takes out tunning and is separated by filtration, obtains after fermentation
To ferment filtrate；Count in parts by weight, weigh 45 parts of bovine bone powders, 12 parts of quartz sands, 10 parts of potassium feldspars, 9 parts of calcites, 6 parts it is swollen
Profit soil, 5 parts of spare filtrates, 8 portions of mixing juice and 9 parts of above-mentioned ferment filtrates and 70 parts of water are put into kneading 2h in masticator,
It is 80% in relative air humidity after kneading, temperature is to stand aging 5 days in 40 DEG C of greenhouse to get high plasticity sclerotin
Porcelain pug.
Reference examples
Raw material is wanted based on animal bone ash, is equipped with the conventional bone porcelain pug of clay, feldspar, quartz composition as reference examples
Performance detection, testing result such as table 1 are carried out to the bone porcelain pug in bone porcelain pug produced by the present invention and reference examples
It is shown：
Table 1
| Detection project | Example 1 | Example 2 | Example 3 | Reference examples |
| Billet yield（%） | 96.5 | 96.7 | 97.0 | 77.6 |
| Plasticity index（kg·cm） | 2.76 | 2.78 | 2.80 | 2.21 |
| Plasticity index | 0.511 | 0.519 | 0.521 | 0.407 |
| Plastic index | 17.70 | 17.85 | 17.89 | 11.25 |
| Dry tenacity（MPa） | 2.80 | 2.85 | 2.86 | 2.31 |
High plasticity bone porcelain pug plasticity produced by the present invention is good it can be seen from detection data in upper table, billet yield is high,
It has broad application prospects.
Claims (6)
1. a kind of preparation method of high plasticity bone porcelain pug, it is characterised in that specifically preparation process is：
（1）The saline-alkali soil in gutter oil and salt-soda soil is collected, is put into fermentation tank, will ferment after gutter oil and saline-alkali soil are mixed
It in tank embedment salt-soda soil, is sealed by fermentation 30~40 days, takes out tunning after fermentation, add after tunning and water are mixed
Heat heating, 20~30min of insulated and stirred is separated by filtration to obtain filtrate after stirring, spare；
（2）By mass ratioes are waited to weigh sugarcane and beet, and be put into 20~30min of crushing in tissue pulverizer jointly, will crush
It is fitted into enzymatic vessel after object and cellulase mixing, heat preservation 6~8h of enzymolysis waits that enzymolysis product is moved into squeezer after digesting
Middle squeezing juice obtains mixing juice；
（3）It weighs Kiwi berry, pineapple and new fresh grape to pour into ball mill successively, is 20 by ball material mass ratio:1 into ball grinder
Zirconium oxide ball milling pearl is added in, 20~30min of ball-milling treatment obtains ball-milled mixtures after ball milling；
（4）It is fitted into fermentation tank after above-mentioned ball-milled mixtures and dusty yeast are mixed, after sealed fermenter, heat-preservation fermentation 8~10
My god, tunning is taken out after fermentation and is separated by filtration, and obtains ferment filtrate；
（5）It counts in parts by weight, weighs 40~45 parts of bovine bone powders, 10~12 parts of quartz sands, 8~10 parts of potassium feldspars, 7~9 parts of sides
Xie Shi, 3~6 parts of bentonites, 3~5 parts of spare filtrates, 5~8 portions of mixing juice and 6~9 parts of above-mentioned ferment filtrates and 60~
70 parts of water are put into 1~2h of kneading in masticator, after kneading, stand aging 3~5 days in the greenhouse to get high plasticity bone
Matter porcelain pug.
2. a kind of preparation method of high plasticity bone porcelain pug according to claim 1, it is characterised in that：Step（1）
Described in gutter oil and saline-alkali soil mass ratio be 2:1, the mass ratio of tunning and water is 1:5, the temperature of heat temperature raising
It is 70~80 DEG C.
3. a kind of preparation method of high plasticity bone porcelain pug according to claim 1, it is characterised in that：Step（2）
Described in crushed material and cellulase mass ratio be 10:1, the temperature for keeping the temperature enzymolysis is 25~35 DEG C.
4. a kind of preparation method of high plasticity bone porcelain pug according to claim 1, it is characterised in that：Step（3）
Described in Kiwi berry, pineapple and new fresh grape mass ratio be 1:1:4.
5. a kind of preparation method of high plasticity bone porcelain pug according to claim 1, it is characterised in that：Step（4）
Described in ball-milled mixtures and dusty yeast mass ratio be 50:1, the temperature of heat-preservation fermentation is 35~40 DEG C.
6. a kind of preparation method of high plasticity bone porcelain pug according to claim 1, it is characterised in that：Step（5）
Described in greenhouse in relative air humidity for 70~80%, temperature is 30~40 DEG C.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108936702A (en) * | 2018-09-20 | 2018-12-07 | 吴亚琴 | A kind of preparation method of the edible plasticine of easy moulding |
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| CN108936702A (en) * | 2018-09-20 | 2018-12-07 | 吴亚琴 | A kind of preparation method of the edible plasticine of easy moulding |
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Application publication date: 20180629 |