CN108203624A - Essence containing Dendranthema indicum essential oil, cigarette dripping pill and cigarette dripping pill production method - Google Patents
Essence containing Dendranthema indicum essential oil, cigarette dripping pill and cigarette dripping pill production method Download PDFInfo
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- CN108203624A CN108203624A CN201810269647.2A CN201810269647A CN108203624A CN 108203624 A CN108203624 A CN 108203624A CN 201810269647 A CN201810269647 A CN 201810269647A CN 108203624 A CN108203624 A CN 108203624A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/281—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed
- A24B15/283—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed by encapsulation of the chemical substances
- A24B15/284—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed by encapsulation of the chemical substances the additive being bound to a host by chemical, electrical or like forces, e.g. use of precursors, inclusion complexes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Toxicology (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of essence containing Dendranthema indicum essential oil, cigarette dripping pill and cigarette dripping pill production methods, belong to technical field of cigarettes.The essence containing Dendranthema indicum essential oil of the present invention is made by the raw material of following parts by weight：0.8 1.5 parts of Dendranthema indicum essential oil, 1.2 2.0 parts of linalool, 0.2 0.8 parts of geraniol, 1.2 1.8 parts of benzyl alcohol, third 0.2 0.6 parts of nonalactone, 1.5 2.5 parts of bergamio, 0.5 0.8 parts of B position violet ketone, 89.5 95.5 parts of solvent, and using its essence as cigarette dripping pill, the cigarette dripping pill of the essence containing Dendranthema indicum essential oil is made.Essence prepared by the present invention can be dissolved each other with cigarette with dripping pill manufacturing process solvent for use, cover the bad breath that cigarette pill wall material and solvent bank come completely, and distinctive Scent of Chrysanthemum is comfortable naturally, with cigarette perfume coordination, the soft exquisiteness of flue gas, fragrance texture has promotion；Cigarette made from the production method of the present invention is good with dripping pill stability, and notch is small, improves the ratio of briquetting of dripping pill, and preparation method it is easy, it is of low cost, available for large-scale industrial production.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to a kind of essence containing Dendranthema indicum essential oil contains this essence
Cigarette dripping pill and this cigarette dripping pill production method.
Background technology
As consumer is to the growing interest of own health, to the style and features of cigarette, mouthfeel, sucks comfort and propose
Higher requirement according to the requirement of market and Cigarette design, is developed with preferable flavouring humectation effect and novel visual effect
New cigarette product, will be with fairly obvious economic benefit and social effect.Cigarette with the essence added in dripping pill product because
Cigarette burning is not involved in, therefore can ensure natural true to nature, the reinforcing cigarette brand style and features of fragrance, is dropped in flavouring humectation, harm reduction
In coke have incomparable technical advantage, while cigarette dripping pill product because its have the characteristics that visually, audible, can feel, give
A kind of fresh, peculiar sensory experience of consumer is filled with new personalized element for cigarette brand, and by cigarette consumption person
Favor.
Although currently on the market there are the cigarette product of the addition cigarette dripping pill of different flavor, due to cigarette dripping pill perfume
Smart fragrance causes and tobacco this perfume (or spice) is uncoordinated, pill wall material pinches brokenly that the chemical breath that discharges in the process is heavier to be led without Specialty Design
The suction comfort of cause decline and cigarette with dripping pill essence to dripping pill caused by the dissolving of cigarette pill wall material damaged, ratio of briquetting
Low problem has seriously affected the industrialized production of cigarette dripping pill and the sensory experience of consumer.
Invention content
In view of this, the object of the present invention is to provide a kind of essence containing Dendranthema indicum essential oil, use it as cigarette drop
The essence of ball, is made the cigarette dripping pill of the essence containing Dendranthema indicum essential oil, which can cover wall material when dripping pill is pinched brokenly and release
The adverse chemical breath put, and the Dendranthema indicum Scent of Chrysanthemum coordinated with tobacco this perfume phase can be assigned, enrich cigarette personalization product
Class.
To achieve these goals, the technical solution adopted by the present invention is to provide a kind of perfume (or spice) containing Dendranthema indicum essential oil
Essence is made by the raw material of following parts by weight：0.8-1.5 parts of Dendranthema indicum essential oil, 1.2-2.0 parts of linalool, geraniol 0.2-
0.8 part, 1.2-1.8 parts of benzyl alcohol, third 0.2-0.6 parts of nonalactone, 1.5-2.5 parts of bergamio, B position violet ketone
0.5-0.8 parts, 89.5-95.5 parts of solvent.
Preferably, the solvent is one or more in edible blend oil and Glycerin, mixed triester with caprylic acid capric acid.
Preferably, it is made by the raw material of following parts by weight：1.0 parts of Dendranthema indicum essential oil, 1.6 parts of linalool are fragrant
0.5 part of leaf-alcohol, 1.4 parts of benzyl alcohol, third 0.3 part of nonalactone, 2.0 parts of bergamio, 0.6 part of B position violet ketone are eaten
46.3 parts of ready-mixed oil, 46.3 parts of Glycerin, mixed triester with caprylic acid capric acid.
Preferably, the Dendranthema indicum essential oil is to be made by Dendranthema indicum using the way of distillation.
Preferably, the essence containing Dendranthema indicum essential oil is made according to the following steps：The raw material is mixed equal
Even, the essence containing Dendranthema indicum essential oil is made in agitated, standing.
Preferably, the speed of agitator is 150-250r/min, mixing time 2-3h, time of repose 1-2h.
The present invention also provides a kind of cigarette dripping pill, which contains the above-mentioned essence containing Dendranthema indicum essential oil.
The present invention also provides a kind of production method of above-mentioned cigarette dripping pill, the production method includes the following steps：
（1）The essence containing Dendranthema indicum essential oil is mixed with edible blend oil and Glycerin, mixed triester with caprylic acid capric acid, agitated, standing
Lay-by material is made in sieving packing afterwards；
（2）It collects the filtrate of the lay-by material and carries out ultrasonic defoaming treatment, treat that fogless and floccule occurs, that is, complete essence
Process for preparation；
（3）Cigarette dripping pill is made according to the preparation process of dripping pill in prepared essence, dripping pill lapping and curing agent.
Preferably, the step（1）In the essence containing Dendranthema indicum essential oil account for edible blend oil and pungent capric acid is sweet
The 2-8% of grease total weight, stirring frequency 8-12Hz, mixing time 0.3-0.8h, time of repose 1-3h.
Preferably, the step（2）Filtering use ceramic membrane of the aperture for 100nm, filter pressure 0.1MPa,
Filtration temperature is 30-35 DEG C, and ultrasonic foam time is 3-10min.
The present invention provides a kind of essence containing Dendranthema indicum essential oil, use it as the essence of cigarette dripping pill, are made and contain
There is the cigarette dripping pill of the essence of Dendranthema indicum essential oil.Essence containing Dendranthema indicum essential oil prepared by the present invention can be dripped with cigarette
Ball manufacturing process solvent for use dissolves each other, can cover completely cigarette pill wall material and solvent bank come bad breath, distinctive chrysanthemum
Fragrance of a flower gas is comfortable naturally, coordinating with cigarette perfume, the soft exquisiteness of flue gas, fragrance texture has promotion；Make the raw material of essence and dripping pill
Wall material is insoluble, ensure that the stable quality of cigarette dripping pill；Cigarette is good with dripping pill stability made from production method using the present invention,
Notch is small, improves the ratio of briquetting of cigarette dripping pill, and preparation method it is easy, it is of low cost, available for large-scale industrial production.
Specific embodiment
The following is specific embodiments of the present invention, and technical scheme of the present invention is further described, but the present invention is simultaneously
It is not limited to these embodiments.The embodiment of the present invention uses weight proportion.
Embodiment one
By 0.8 part of Dendranthema indicum essential oil, 1.2 parts of linalool, 0.2 part of geraniol, 1.2 parts of benzyl alcohol, the third of 0.2
Nonalactone, 1.5 bergamio, 0.5 part of B position violet ketone, 40 parts of edible blend oil and 49.5 parts of pungent capric acid are sweet
Grease mixes, and puts into the reaction kettle with agitating device, stirs 2h with the rotating speed of 150r/min, 1h is stood after stirring, i.e.,
The essence containing Dendranthema indicum essential oil is made.
Then contain Dendranthema indicum essential oil according to obtained by 2% addition of edible blend oil and Glycerin, mixed triester with caprylic acid capric acid total weight
Chrysanthemum essence, be put into agitating device, 0.3h stirred under 8HZ stirring frequencies, 1h is stood after stirring, after 80 mesh screens
Lay-by material is made in packing；Lay-by material is carried out under 30 DEG C of temperature, 0.1MPa pressure using the ceramic membrane in 100nm apertures
Filtering collects filtrate and carries out 3min ultrasound defoaming treatments, treats that fogless and floccule occurs, that is, completes the process for preparation of essence；
Cigarette dripping pill is made according to the preparation process of dripping pill in prepared essence, dripping pill lapping and curing agent.
Embodiment two
By 1.5 parts of Dendranthema indicum essential oil, 2.0 parts of linalool, 0.8 part of geraniol, 1.8 parts of benzyl alcohol, the third of 0.6
Nonalactone, 2.5 bergamio, 0.8 part of B position violet ketone, 50.5 parts of edible blend oil and 45 parts of pungent capric acid are sweet
Grease mixes, and puts into the reaction kettle with agitating device, stirs 3h with the rotating speed of 250r/min, 2h is stood after stirring, i.e.,
The essence containing Dendranthema indicum essential oil is made.
Then contain Dendranthema indicum essential oil according to obtained by 8% addition of edible blend oil and Glycerin, mixed triester with caprylic acid capric acid total weight
Chrysanthemum essence, be put into agitating device, 0.8h stirred under 12HZ stirring frequencies, 3h is stood after stirring, passes through 80 mesh screens
After dispense, be made lay-by material；Using the ceramic membrane in 100nm apertures under 35 DEG C of temperature, 0.1MPa pressure to lay-by material into
Row filtering collects filtrate and carries out 10min ultrasound defoaming treatments, treats that fogless and floccule occurs, that is, completes the preparation of essence
Journey；Cigarette dripping pill is made according to the preparation process of dripping pill in prepared essence, dripping pill lapping and curing agent.
Embodiment three
By 1.0 parts of Dendranthema indicum essential oil, 1.6 parts of linalool, 0.5 part of geraniol, 1.4 parts of benzyl alcohol, the third of 0.3
Nonalactone, 2.0 bergamio, 0.6 part of B position violet ketone, 46.3 parts of edible blend oil and 46.3 parts of pungent capric acid
Glyceride mixes, and puts into the reaction kettle with agitating device, stirs 2.5h with the rotating speed of 200r/min, is stood after stirring
1.5h obtains the essence containing Dendranthema indicum essential oil.
Then contain Dendranthema indicum essential oil according to obtained by 5% addition of edible blend oil and Glycerin, mixed triester with caprylic acid capric acid total weight
Chrysanthemum essence, be put into agitating device, 0.5h stirred under 10HZ stirring frequencies, 2h is stood after stirring, passes through 80 mesh screens
After dispense, be made lay-by material；Using the ceramic membrane in 100nm apertures under 32 DEG C of temperature, 0.1MPa pressure to lay-by material into
Row filtering collects filtrate and carries out 5min ultrasound defoaming treatments, treats that fogless and floccule occurs, that is, completes the preparation of essence
Journey；Cigarette dripping pill is made according to the preparation process of dripping pill in prepared essence, dripping pill lapping and curing agent.
Evaluation method
In the filter tow forming process of cigarette, the cigarette of the essence containing Dendranthema indicum essential oil that will be prepared in embodiment 1-3
It is positioned and is applied in filter rod respectively with dripping pill, cigarette is made, evaluated with reference to State Bureau's standard of smokeing panel test, in aspiration procedure
Pinch brokenly cigarette dripping pill.Group of smokeing panel test is made of 7 cigarette sensory evaluation experts, and wherein national level is smoked panel test Shi Yiming, provincial to smoke panel test
Teacher two, using mode is secretly commented to carry out sensory evaluation and is given a mark.Integrated sensory's quality evaluation result is as shown in table 1, sensory evaluation
Grade form is as shown in table 2.
1 integrated sensory's quality evaluation result of table
2 sensory evaluation grade form of table
As can be seen from Table 1 and Table 2, a kind of essence containing Dendranthema indicum essential oil of the invention can be wrapped up with cigarette dripping pill
Solvent dissolve each other, can cover completely cigarette pill wall material and solvent bank come bad breath, and can assign and tobacco this perfume phase
The Scent of Chrysanthemum of coordination, the soft exquisiteness of flue gas, fragrance texture have promotion.
Since the numberical range of each technological parameter involved in the present invention can not possibly all embody in the above-described embodiments,
But as long as those skilled in the art's envisioned any numerical value fallen into the above-mentioned numberical range completely can implement this
Invention also includes the arbitrary combination of occurrence in the range of several numerical value certainly.Herein, for length the considerations of, be omitted to
Go out the embodiment of occurrence in certain one or more numberical range, this disclosure for being not to be construed as technical scheme of the present invention is not filled
Point.
Applicant states that the present invention illustrates the detailed process equipment of the present invention and technological process by above-described embodiment,
But the invention is not limited in above-mentioned detailed process equipment and technological processes, that is, it is above-mentioned detailed not mean that the present invention has to rely on
Process equipment and technological process could be implemented.Person of ordinary skill in the field it will be clearly understood that any improvement in the present invention,
Addition, concrete mode selection of equivalence replacement and auxiliary element to each raw material of product of the present invention etc., fall the protection in the present invention
In the range of.
Claims (10)
1. a kind of essence containing Dendranthema indicum essential oil, it is characterised in that：It is made by the raw material of following parts by weight：
0.8-1.5 parts of Dendranthema indicum essential oil
1.2-2.0 parts of linalool
0.2-0.8 parts of geraniol
1.2-1.8 parts of benzyl alcohol
Third 0.2-0.6 parts of nonalactone
1.5-2.5 parts of bergamio
0.5-0.8 parts of B position violet ketone
89.5-95.5 parts of solvent.
2. the essence as described in claim 1 containing Dendranthema indicum essential oil, it is characterised in that：The solvent is edible blend oil
With it is one or more in Glycerin, mixed triester with caprylic acid capric acid.
3. the essence as claimed in claim 2 containing Dendranthema indicum essential oil, it is characterised in that：By the raw material of following parts by weight
It is made：
1.0 parts of Dendranthema indicum essential oil
1.6 parts of linalool
0.5 part of geraniol
1.4 parts of benzyl alcohol
Third 0.3 part of nonalactone
2.0 parts of bergamio
0.6 part of B position violet ketone
46.3 parts of edible blend oil
46.3 parts of Glycerin, mixed triester with caprylic acid capric acid.
4. the essence as described in claim 1 containing Dendranthema indicum essential oil, it is characterised in that：The Dendranthema indicum essential oil be by
Dendranthema indicum is made using steam distillation.
5. the essence as described in claim 1 containing Dendranthema indicum essential oil, it is characterised in that：It is described to contain Dendranthema indicum essential oil
Essence be made according to the following steps：The raw material is uniformly mixed, the perfume (or spice) containing Dendranthema indicum essential oil is made in agitated, standing
Essence.
6. the essence as claimed in claim 5 containing Dendranthema indicum essential oil, it is characterised in that：The speed of agitator is 150-
250r/min, mixing time 2-3h, time of repose 1-2h.
7. a kind of cigarette dripping pill, it is characterised in that：Contain Dendranthema indicum essential oil containing as claimed in any one of claims 1 to 6
Essence.
8. the production method of cigarette dripping pill as claimed in claim 7, it is characterised in that：The production method includes following step
Suddenly：
（1）The essence containing Dendranthema indicum essential oil is mixed with edible blend oil and Glycerin, mixed triester with caprylic acid capric acid, agitated, standing
Lay-by material is made in sieving packing afterwards；
（2）It collects the filtrate of the lay-by material and carries out ultrasonic defoaming treatment, treat that fogless and floccule occurs, that is, complete essence
Process for preparation；
（3）Cigarette dripping pill is made according to the preparation process of dripping pill in prepared essence, dripping pill lapping and curing agent.
9. application of the essence in cigarette dripping pill as claimed in claim 8 containing Dendranthema indicum essential oil, it is characterised in that：Institute
State step（1）In the essence containing Dendranthema indicum essential oil account for edible blend oil and the 2-8% of Glycerin, mixed triester with caprylic acid capric acid total weight, stir
Frequency is 8-12Hz, mixing time 0.3-0.8h, time of repose 1-3h.
10. application of the essence in cigarette dripping pill as claimed in claim 8 containing Dendranthema indicum essential oil, it is characterised in that：
The step（2）Filtering use ceramic membrane of the aperture for 100nm, filter pressure 0.1MPa, filtration temperature is 30-35 DEG C,
Ultrasonic foam time is 3-10min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810269647.2A CN108203624A (en) | 2018-03-29 | 2018-03-29 | Essence containing Dendranthema indicum essential oil, cigarette dripping pill and cigarette dripping pill production method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810269647.2A CN108203624A (en) | 2018-03-29 | 2018-03-29 | Essence containing Dendranthema indicum essential oil, cigarette dripping pill and cigarette dripping pill production method |
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| CN108203624A true CN108203624A (en) | 2018-06-26 |
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| CN109379664A (en) * | 2018-09-29 | 2019-02-22 | 钟贵富 | Fragrance ball preparation method and the magnetic suspension sound box device for using the fragrance ball |
| CN109439442A (en) * | 2018-12-20 | 2019-03-08 | 湖北中烟工业有限责任公司 | A kind of apricot flavor essence and its preparation method and application for cigarette dripping pill |
| CN113088389A (en) * | 2021-04-08 | 2021-07-09 | 武汉黄鹤楼香精香料有限公司 | Water-soluble dropping pill prepared from porous material and preparation method thereof |
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