CN106418665B - A kind of cassia bark flavor cigarette paper essence and its preparation method and application - Google Patents
A kind of cassia bark flavor cigarette paper essence and its preparation method and application Download PDFInfo
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- CN106418665B CN106418665B CN201610853883.XA CN201610853883A CN106418665B CN 106418665 B CN106418665 B CN 106418665B CN 201610853883 A CN201610853883 A CN 201610853883A CN 106418665 B CN106418665 B CN 106418665B
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 125
- 244000037364 Cinnamomum aromaticum Species 0.000 title claims abstract description 43
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 title claims abstract description 43
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 43
- 235000019634 flavors Nutrition 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 238000000576 coating method Methods 0.000 claims abstract description 30
- 239000011248 coating agent Substances 0.000 claims abstract description 29
- 239000012530 fluid Substances 0.000 claims abstract description 21
- TZMFJUDUGYTVRY-UHFFFAOYSA-N pentane-2,3-dione Chemical class CCC(=O)C(C)=O TZMFJUDUGYTVRY-UHFFFAOYSA-N 0.000 claims abstract description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- KJPRLNWUNMBNBZ-QPJJXVBHSA-N (E)-cinnamaldehyde Chemical compound O=C\C=C\C1=CC=CC=C1 KJPRLNWUNMBNBZ-QPJJXVBHSA-N 0.000 claims abstract description 8
- WBYWAXJHAXSJNI-VOTSOKGWSA-M .beta-Phenylacrylic acid Natural products [O-]C(=O)\C=C\C1=CC=CC=C1 WBYWAXJHAXSJNI-VOTSOKGWSA-M 0.000 claims abstract description 8
- WBYWAXJHAXSJNI-SREVYHEPSA-N Cinnamic acid Chemical compound OC(=O)\C=C/C1=CC=CC=C1 WBYWAXJHAXSJNI-SREVYHEPSA-N 0.000 claims abstract description 8
- AXMVYSVVTMKQSL-UHFFFAOYSA-N UNPD142122 Natural products OC1=CC=C(C=CC=O)C=C1O AXMVYSVVTMKQSL-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229930016911 cinnamic acid Natural products 0.000 claims abstract description 8
- 235000013985 cinnamic acid Nutrition 0.000 claims abstract description 8
- KJPRLNWUNMBNBZ-UHFFFAOYSA-N cinnamic aldehyde Natural products O=CC=CC1=CC=CC=C1 KJPRLNWUNMBNBZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229940117916 cinnamic aldehyde Drugs 0.000 claims abstract description 8
- WBYWAXJHAXSJNI-UHFFFAOYSA-N methyl p-hydroxycinnamate Natural products OC(=O)C=CC1=CC=CC=C1 WBYWAXJHAXSJNI-UHFFFAOYSA-N 0.000 claims abstract description 8
- SDOFMBGMRVAJNF-KVTDHHQDSA-N (2r,3r,4r,5r)-6-aminohexane-1,2,3,4,5-pentol Chemical compound NC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO SDOFMBGMRVAJNF-KVTDHHQDSA-N 0.000 claims abstract description 7
- WJSDHUCWMSHDCR-VMPITWQZSA-N cinnamyl acetate Natural products CC(=O)OC\C=C\C1=CC=CC=C1 WJSDHUCWMSHDCR-VMPITWQZSA-N 0.000 claims abstract description 7
- WTWBUQJHJGUZCY-UHFFFAOYSA-N cuminaldehyde Chemical compound CC(C)C1=CC=C(C=O)C=C1 WTWBUQJHJGUZCY-UHFFFAOYSA-N 0.000 claims abstract description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 28
- 235000019198 oils Nutrition 0.000 claims description 25
- 239000002994 raw material Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 9
- ROWKJAVDOGWPAT-UHFFFAOYSA-N Acetoin Chemical compound CC(O)C(C)=O ROWKJAVDOGWPAT-UHFFFAOYSA-N 0.000 claims description 7
- 241001104043 Syringa Species 0.000 claims description 5
- 235000004338 Syringa vulgaris Nutrition 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 5
- 235000019476 oil-water mixture Nutrition 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 150000001299 aldehydes Chemical class 0.000 claims description 2
- 244000269722 Thea sinensis Species 0.000 claims 1
- 150000002148 esters Chemical class 0.000 claims 1
- 239000004744 fabric Substances 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 11
- 241000208125 Nicotiana Species 0.000 abstract description 8
- 235000002637 Nicotiana tabacum Nutrition 0.000 abstract description 8
- 230000002045 lasting effect Effects 0.000 abstract description 5
- 239000002304 perfume Substances 0.000 abstract description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 abstract description 2
- 238000005096 rolling process Methods 0.000 abstract description 2
- 235000013599 spices Nutrition 0.000 abstract description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 6
- 239000003546 flue gas Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 241001062472 Stokellia anisodon Species 0.000 description 3
- 235000019506 cigar Nutrition 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 125000003118 aryl group Chemical group 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 240000000203 Salix gracilistyla Species 0.000 description 1
- 244000223014 Syzygium aromaticum Species 0.000 description 1
- 235000016639 Syzygium aromaticum Nutrition 0.000 description 1
- -1 Xin Xiang Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012259 ether extract Substances 0.000 description 1
- DQYBDCGIPTYXML-UHFFFAOYSA-N ethoxyethane;hydrate Chemical compound O.CCOCC DQYBDCGIPTYXML-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000008447 perception Effects 0.000 description 1
- 230000000644 propagated effect Effects 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 230000016776 visual perception Effects 0.000 description 1
- 230000003313 weakening effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
- A24C5/00—Making cigarettes; Making tipping materials for, or attaching filters or mouthpieces to, cigars or cigarettes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The present invention provides a kind of cassia bark flavor cigarette paper essence and its preparation method and application.The cassia bark flavor cigarette paper essence is by 20 40 parts of cinnamyl acetate, 5 15 parts of cinnamic acid, 90 100 parts of phenmethylol, 700 800 parts of cinnamic aldehyde, 24 parts of 10% cumal, 13 parts of 10% salicylide, 1% 46 parts of 3 hydroxyl, 2 butanone, the 2 of 1%, 346 parts of pentanediones, 10 30 parts of caryophyllus oil, 95% 50 200 parts of alcohol, which mixes, to be formulated, by it in cigarette paper coating process, it is added to according to the ratio of coating fluid weight 3 6% in coating fluid, is then coated on cigarette paper.Essence fragrance in the present invention is mutually coordinated, and can assign ramuscule cigarette unique style rich in level with tobacco taste；Be added in cigarette paper, can be tobacco rolling belt protrude and it is lasting smell perfume (or spice), and can overcome the disadvantages that the fragrance loss that reducing tar and reducing harm is brought, improve the quality of cigarette.
Description
Technical field
The present invention relates to field of cigarette producing technology, refer specifically to a kind of cassia bark flavor cigarette paper essence and preparation method thereof and
Application in cigarette.
Background technology
At present, occupy-place of the ramuscule cigarette at home in cigarette market is more and more important, and its target consumer population is from women
Consumer groups are further expanded to male consumer groups, and the label of " Ms's cigarette " is weakening, and " thin " is no longer female consumption crowd
The patent of selection, " thin " can also be that the embodiment of fashion, the showing of individual character, the protrusion of style, grade are bragged about, tangible
" thin " is the visual perception that external size thickness gives people, and invisible " thin " is more filled with fashion, individual character, style, product
The perception of the inherent values such as position.Wherein, having the whole society to advocate the low burnt, trend of less harmful makes so, also to have benefited from the tax of tobacco producer
Ramuscule cigarette more novelty, fashion, personality elements features are given, hold the seasonable act of trend of the market in time.
Although external ramuscule tobacco board is propagated its belief on a large scale in the domestic market, in unbreakable general layout is seemed
Blank spot also be present, that is, external ramuscule smoke product is almost blended type cigarette, rarely has suitable Chinese cigarette consumer mouth
The ramuscule cigarette manufacturing enterprise of the fire-cured tobacco type ramuscule smoke product country of taste, has not only filled up this blank and has also observantly captured cigarette city
The new change of field, environmental protection, the importance of health idea are recognized earlier.Thus, ramuscule cigarette is have selected as reducing tar and reducing harm
Breach, go to have catered to consumer to health, environmental protection, the demand saved.Compared with conventional cigarette, ramuscule cigarette generally has flue gas
The features such as soft, fine and smooth, excitant is small, and concentration of smoking, strength are moderate, and pleasant impression is clean, comfortable.
The breakthrough of target consumer population, the differentiation of high-endization development trend, these are all meaning the prominent of ramuscule cigarette market
Broken, strategic location of the following ramuscule cigarette at home in cigarette market will more highlight, and following ramuscule cigarette market potential is difficult to limit the quantity.
Low tar ramuscule smoke product continues to bring out, and has catered to the consumption demand that low evil, safety etc. are pursued by core consumer groups.Exactly
Ramuscule cigarette is unique in itself, be totally different from normal conventional cigarette less harmful innate advantage, disappear just with consumer
Take a lot of trouble reason mutually to agree with, win favor for ramuscule cigarette, chance of winning the market creates condition, lays a good foundation.
With the development of low tar ramuscule cigarette, cigarette products fragrance is filtered and dilutes and obvious deficiency, and therefore, cigarette is auxiliary
Material perfuming is more and more important.Auxiliary material of the cigarette paper as cigarette, there is critical role in production of cigarettes.With domestic different volumes
The embodiment of cigarette perfume type, cigarette paper not only play parcel pipe tobacco, participate in the effect of burning regulation carbon monoxide and tar, more
Cigarette style characteristic can be adjusted by adding flavouring in cigarette paper, it is fragrant that flavor is added in cigarette paper production process
Material, compared to other cigarette materials are made an addition to, addition is greatly reduced, while flavouring can be made to be combined closely, surely with cigarette paper
Fixed uniform, flavor preserves lasting under natural conditions, assigns ramuscule cigarette individual style.
The content of the invention
In order to solve above-mentioned problems of the prior art, the invention provides a kind of cassia bark flavor cigarette paper essence and
Its preparation method and applied in cigarette, the essence can assign a kind of cigar type cigarette style of cassia bark flavor of ramuscule cigarette.
Technical scheme provided by the invention is：A kind of cassia bark flavor cigarette paper essence, it is characterised in that the essence
It is made up of the raw material of following parts by weight：Cinnamyl acetate 20-40 parts, cinnamic acid 5-15 parts, phenmethylol 90-100 parts, cinnamic aldehyde
700-800 parts, mass concentration are 10% cumal 2-4 parts, and mass concentration is 10% salicylide 1-3 parts, and mass concentration is
1% 3- hydroxy-2-butanone 4-6 parts, mass concentration be 1% 2,3 pentanedione 4-6 parts, caryophyllus oil 10-30 parts, volume ratio
95% alcohol 50-200 parts；
Wherein described caryophyllus oil is to be placed in after lilac is crushed in cucurbit, according to solid-liquid ratio 1:5-10 adds water, so
3h-15h is distilled under conditions of being afterwards 100 DEG C in temperature；Stood in the oil water mixture dislocation separatory funnel that gained will be distilled
10h-14h, layering obtain rough caryophyllus oil, and the absolute ether extraction of 1-3 times of its weight is added in rough caryophyllus oil, then
Ether layer is taken, in pressure 0.05MPa, caryophyllus oil that temperature obtains after ether is volatilized under conditions of being 12-18 DEG C.
The preparation method of a kind of cassia bark flavor cigarette paper essence provided by the invention, it is characterised in that comprise the following steps that：
(1) it is placed in after lilac is crushed in cucurbit, according to solid-liquid ratio 1:5-10 adds water, is then 100 in temperature
3h-15h is distilled under conditions of DEG C；10h-14h is stood in the oil water mixture dislocation separatory funnel that gained will be distilled, layering obtains
Rough caryophyllus oil；
(2) the absolute ether extraction of 1-3 times of its weight is added in rough caryophyllus oil, ether layer is then taken, in pressure
0.05MPa, temperature remove the caryophyllus oil that ether obtains under conditions of being 12-18 DEG C；
(3) the following raw material by following parts by weight is weighed：20-40 parts of cinnamyl acetate, 5-15 parts of cinnamic acid, benzene first
90-100 parts of alcohol, 700-800 parts of cinnamic aldehyde, mass concentration are 10% 2-4 parts of cumal, and mass concentration is 10% bigcatkin willow
1-3 parts of aldehyde, mass concentration are 1% 4-6 parts of 3- hydroxy-2-butanones, and mass concentration is 1% 2,3 4-6 parts of pentanediones, is walked
Suddenly the caryophyllus oil 10-30 parts prepared in (1), alcohol 50-200 parts of volume ratio 95%；All raw materials are mixed into preparation
Into cassia bark flavor cigarette paper essence.
A kind of application of cassia bark flavor cigarette paper essence provided by the invention, it is characterised in that：Above-mentioned cassia bark flavor is rolled up
Cigarette paper essence is added in coating fluid in cigarette paper moulding process, and stirs, and its addition is the 3 of coating fluid gross weight
~6%；Then the coating fluid added with cassia bark flavor cigarette paper essence is uniformly coated on cigarette paper by coating machine, and led to
Cross oven for drying and form the cigarette paper with cassia bark flavor.
The further technical scheme of the present invention：When adding cassia bark flavor cigarette paper essence, coating fluid is placed in carry and stirred
In the container for mixing device, stirred with the high speed dispersor that rotating speed is 200 revs/min, be slowly added to cassia bark flavor cigarette paper essence, it is fragrant
Finishing it is complete it is follow-up it is continuous be kept stirring for 1h, essence and coating fluid is sufficiently mixed uniformly.
The present invention preferably technical scheme：The speed of the coating machine coating cigarette paper is 60-80m/min.
Cassia bark fragrance is presented in cigarette paper essence of the present invention, suitable for cigarette producing field, is especially suitable for being added to volume
In cigarette paper, ramuscule cigarette cigar style is assigned.The cigarette paper essence contains multiple fragrance composition, combines blue or green perfume, Xin Xiang, milk
Etc. a variety of odor types, level enriches, and transition is naturally, and can preferably protrude cigar type cigarette main body note.
Shown by sensory evaluation, after adding cigarette paper essence of the present invention, it is fragrant prominent lasting that cigarette is smelt, and has uniqueness
Style, fragrance texture are slightly lifted, and flue gas concentration and moisture feeling also increased, and do not influence fragrance harmony and flue gas is soft
With exquisiteness.
Essence fragrance prepared by the present invention is mutually coordinated, and can assign ramuscule cigarette uniqueness rich in level with tobacco taste
Style；It is added in cigarette paper on a small quantity, can be tobacco rolling belt protrude and it is lasting smell perfume (or spice), and can overcome the disadvantages that reducing tar and reducing harm is brought
Fragrance loss, preferable modification is played to the overall organoleptic attribute of cigarette, be advantageous to improve cigarette quality.
Embodiment
Below in conjunction with embodiment, the invention will be further described.
Caryophyllus oil preparation method in following examples is as follows：It is placed in after lilac is crushed in cucurbit, according to material
Liquor ratio 1:5-10 adds water, distills 3h-15h under conditions of being then 100 DEG C in temperature；The oil water mixture for distilling gained is moved
Put and 10h-14h is stood in separatory funnel, layering obtains rough caryophyllus oil；The nothing of 1-3 times of its weight is added in rough caryophyllus oil
Water ether extracts, and then takes ether layer, and in pressure 0.05MPa, temperature removes the cloves that ether obtains under conditions of being 12-18 DEG C
Oil.
Embodiment 1, a kind of cassia bark flavor cigarette paper essence, its specific preparation method are：
Weigh the raw material of following parts by weight：20 parts of cinnamyl acetate, 5 parts of cinnamic acid, 90 parts of phenmethylol, 800 parts of cinnamic aldehyde, matter
2 parts of the cumal that concentration is 10% is measured, mass concentration is 10% 2 parts of salicylide, and mass concentration is 1% 3- hydroxyl -2- fourths
4 parts of ketone, mass concentration are 1% 4 parts of 2,3 pentanedione, and 10 parts of caryophyllus oil, volumetric concentration is 95% 63 parts of alcohol；Will be above-mentioned
Raw material is mixed evenly, and is configured to cassia bark flavor cigarette paper essence A.
The cassia bark flavor cigarette paper essence A prepared in embodiment 1 is added in coating fluid in cigarette paper moulding process,
And stir, its addition is the 5% of coating fluid gross weight；Then by the coating fluid added with cassia bark flavor cigarette paper essence
It is uniformly coated on by coating machine on cigarette paper, and the cigarette paper with cassia bark flavor is formed by oven for drying, and is rolled up with this
Cigarettes tested, i.e. cigarette A is made in cigarette paper.
Embodiment 2, a kind of cassia bark flavor cigarette paper essence, its specific preparation method are：
Weigh following raw materials in parts by weight：25 parts of cinnamyl acetate, 10 parts of cinnamic acid, 100 parts of phenmethylol, cinnamic aldehyde
750 parts, 3 parts of the cumal of mass concentration 10%, 1.5 parts of the salicylide of mass concentration 10%, the 3- hydroxyls of mass concentration 1%-
5 parts of 2- butanone, the 2 of mass concentration 1%, 35 parts of pentanediones, 30 parts of caryophyllus oil, 80.5 parts of the alcohol of volumetric concentration 95%；Will be upper
State raw material to be mixed evenly, be configured to cassia bark flavor cigarette paper essence B.
The cassia bark flavor cigarette paper essence B prepared in embodiment 2 is added in coating fluid in cigarette paper moulding process,
And stir, its addition is the 5% of coating fluid gross weight；Then by the coating fluid added with cassia bark flavor cigarette paper essence
It is uniformly coated on by coating machine on cigarette paper, and the cigarette paper with cassia bark flavor is formed by oven for drying, and is rolled up with this
Cigarettes tested, i.e. cigarette B is made in cigarette paper.
Embodiment 3, a kind of cassia bark flavor cigarette paper essence, its specific preparation method are：
Weigh following raw materials in parts by weight：30 parts of cinnamyl acetate, 10 parts of cinnamic acid, 95 parts of phenmethylol, cinnamic aldehyde 700
Part, 4 parts of the cumal of mass concentration 10%, 1 part of the salicylide of mass concentration 10%, the 3- hydroxy-2-butanones of mass concentration 1%
6 parts, the 2 of mass concentration 1%, 36 parts of pentanediones, 20 parts of caryophyllus oil, 95% 128 parts of (volume ratio) alcohol；Above-mentioned raw materials are mixed
Stir, be configured to cassia bark flavor cigarette paper essence C.
The cassia bark flavor cigarette paper essence C prepared in embodiment 3 is added in coating fluid in cigarette paper moulding process,
And stir, its addition is the 5% of coating fluid gross weight；Then by the coating fluid added with cassia bark flavor cigarette paper essence
It is uniformly coated on by coating machine on cigarette paper, and the cigarette paper with cassia bark flavor is formed by oven for drying, and is rolled up with this
Cigarettes tested, i.e. cigarette C is made in cigarette paper.
Embodiment 4
Blank control：Cigarette paper do not add essence be made test use cigarette, i.e. cigarette paper D.
By cigarette A, B, C, D of the preparation of embodiment 1,2,3,4, evaluated, commented referring next to State Bureau's standard of smokeing panel test
Suction group is made up of 7 cigarette sensory evaluation experts, using secretly commenting mode to carry out sensory evaluation and give a mark, in cigarette smell it is fragrant and
Aromatic style performance is as shown in table 1, and sensory evaluation grade form is as shown in table 2：
Fragrant and aromatic style is smelt in the cigarette of table 1
The sensory evaluation grade form of table 2
| Test specimen | A | B | C | D |
| Essence (%) | 5 | 5 | 5 | 0 |
| Mean scores | 88.5 | 88 | 87.5 | 82 |
As can be seen that being shown by sensory evaluation from above-mentioned Tables 1 and 2, after adding cigarette paper essence of the present invention,
It is fragrant prominent lasting that cigarette is smelt, and has individual style, and fragrance texture is slightly lifted, and flue gas concentration and moisture feeling also increased,
And do not influence fragrance harmony and the soft exquisiteness of flue gas.
The foregoing is only a specific embodiment of the invention, but protection scope of the present invention is not limited thereto, any
Belong to those skilled in the art the invention discloses technical scope in, the change or replacement that can readily occur in, all should
It is included within the scope of the present invention.
Claims (5)
1. a kind of cassia bark flavor cigarette paper essence, it is characterised in that the essence is made up of the raw material of following parts by weight：Second
Sour cinnamic ester 20-40 parts, cinnamic acid 5-15 parts, phenmethylol 90-100 parts, cinnamic aldehyde 700-800 parts, mass concentration be 10% it is withered
Tender tea leaves aldehyde 2-4 parts, mass concentration be 10% salicylide 1-3 parts, mass concentration be 1% 3- hydroxy-2-butanone 4-6 parts, quality
Concentration be 1% 2,3 pentanedione 4-6 parts, caryophyllus oil 10-30 parts, alcohol 50-200 parts of volume ratio 95%；
Wherein described caryophyllus oil is to be placed in after lilac is crushed in cucurbit, according to solid-liquid ratio 1:5-10 adds water, Ran Hou
Temperature distills 3h-15h under conditions of being 100 DEG C；10h- is stood in the oil water mixture dislocation separatory funnel that gained will be distilled
14h, layering obtain rough caryophyllus oil, and the absolute ether extraction of 1-3 times of its weight is added in rough caryophyllus oil, then take second
Ether layer, in pressure 0.05MPa, caryophyllus oil that temperature obtains after ether is volatilized under conditions of being 12-18 DEG C.
2. the preparation method of the cassia bark flavor cigarette paper essence described in a kind of claim 1, it is characterised in that specific steps are such as
Under：
(1) it is placed in after lilac is crushed in cucurbit, according to solid-liquid ratio 1:5-10 adds water, is then 100 DEG C in temperature
Under the conditions of distill 3h-15h；10h-14h is stood in the oil water mixture dislocation separatory funnel that gained will be distilled, layering obtains rough
Caryophyllus oil；
(2) the absolute ether extraction of 1-3 times of its weight is added in rough caryophyllus oil, ether layer is then taken, in pressure
0.05MPa, temperature remove the caryophyllus oil that ether obtains under conditions of being 12-18 DEG C；
(3) the following raw material by following parts by weight is weighed：20-40 parts of cinnamyl acetate, 5-15 parts of cinnamic acid, phenmethylol
90-100 parts, 700-800 parts of cinnamic aldehyde, mass concentration is 10% 2-4 parts of cumal, and mass concentration is 10% salicylide
1-3 parts, mass concentration be 1% 4-6 parts of 3- hydroxy-2-butanones, mass concentration be 1% 2,3 4-6 parts of pentanediones, step
(1) the caryophyllus oil 10-30 parts prepared in, alcohol 50-200 parts of volume ratio 95%；All raw materials are mixed and are configured to
Cassia bark flavor cigarette paper essence.
A kind of 3. application of the cassia bark flavor cigarette paper essence in claim 1 or 2, it is characterised in that：By above-mentioned cassia bark flavor
Cigarette paper essence is added in coating fluid in cigarette paper moulding process, and stirs, and its addition is coating fluid gross weight
3~6%；Then the coating fluid added with cassia bark flavor cigarette paper essence is uniformly coated on cigarette paper by coating machine,
And the cigarette paper with cassia bark flavor is formed by oven for drying.
A kind of 4. application of cassia bark flavor cigarette paper essence according to claim 3, it is characterised in that：In addition cassia bark wind
During taste cigarette paper essence, coating fluid is placed in the container with agitating device, with the high speed dispersor that rotating speed is 200 revs/min
Stirring, is slowly added to cassia bark flavor cigarette paper essence, essence add it is follow-up it is continuous be kept stirring for 1h, make essence and coating fluid fully mixed
Close uniform.
A kind of 5. application of cassia bark flavor cigarette paper essence according to claim 3, it is characterised in that：The coating machine applies
The speed of cloth cigarette paper is 60-80m/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610853883.XA CN106418665B (en) | 2016-09-27 | 2016-09-27 | A kind of cassia bark flavor cigarette paper essence and its preparation method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610853883.XA CN106418665B (en) | 2016-09-27 | 2016-09-27 | A kind of cassia bark flavor cigarette paper essence and its preparation method and application |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106418665A CN106418665A (en) | 2017-02-22 |
| CN106418665B true CN106418665B (en) | 2018-01-02 |
Family
ID=58170330
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN110819455A (en) * | 2019-11-18 | 2020-02-21 | 四川中烟工业有限责任公司 | Preparation method of halogen-flavor essence for cigar |
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| JP2010252771A (en) * | 2009-04-24 | 2010-11-11 | Kunio Nakajima | Aromatherapeutic fragrance in which general view resembles cigarette |
| CN102942993B (en) * | 2012-11-21 | 2013-12-25 | 红塔烟草(集团)有限责任公司 | Aromatic tobacco enhanced tobacco essence, preparation method and application |
| CN103054166B (en) * | 2013-01-15 | 2015-11-25 | 吕国栋 | A kind of Chinese cinnamon type snuff |
| CN103266014B (en) * | 2013-05-29 | 2014-05-28 | 江苏中烟工业有限责任公司徐州卷烟厂 | Spicy sweet flue-cured tobacco essence and application thereof |
| CN104611136A (en) * | 2014-12-24 | 2015-05-13 | 杨秋慧 | Cigarette essence prepared by utilization of passion fruit and preparing method thereof |
| CN105112161B (en) * | 2015-07-31 | 2018-10-12 | 湖北中烟工业有限责任公司 | A kind of flavoring essence of cigar cigarette paper |
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