CN106118884A - A kind of Flower fragrance aroma essence for cigarette drop pill and application - Google Patents

A kind of Flower fragrance aroma essence for cigarette drop pill and application Download PDF

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Publication number
CN106118884A
CN106118884A CN201610567597.7A CN201610567597A CN106118884A CN 106118884 A CN106118884 A CN 106118884A CN 201610567597 A CN201610567597 A CN 201610567597A CN 106118884 A CN106118884 A CN 106118884A
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China
Prior art keywords
cigarette
drop pill
oil
parts
essence
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Pending
Application number
CN201610567597.7A
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Chinese (zh)
Inventor
赵国豪
王娜
熊国玺
董世良
赵同林
马舒翼
潘婷婷
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Priority to CN201610567597.7A priority Critical patent/CN106118884A/en
Publication of CN106118884A publication Critical patent/CN106118884A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/14Use of materials for tobacco smoke filters of organic materials as additive

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)

Abstract

The present invention provides a kind of Flower fragrance aroma essence for cigarette drop pill and application.Described Flower fragrance aroma essence is to be stirred 13 hours to uniformly by oil of Rhizoma et radix valerianae, Citrus aurantium L. var. amara Engl. quintessence oil, Flos Osmanthi Fragrantis quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil, rose ethereal oil, violet leaf extract, iso-amyl iso-valeriate, mixed with olive oil, then, after standing 24 48 hours, cross 60 80 eye mesh screens elimination sediments and obtain.Being used pill dripping machine to be prepared as cigarette drop pill, then location is applied in cigarette filter tip.When drop pill prepared by essence in the present invention, production stability is preferable, and cigarette drop pill breakage rate is low, and yield rate is 80 85%.When the Medicated cigarette made is smoked panel test, sensation is inhaled fragrance of a flower fragrance in taste and is substantially strengthened, and elegant fragrance is elegant, and pleasant impression is comfortable.

Description

A kind of Flower fragrance aroma essence for cigarette drop pill and application
Technical field
The present invention relates to technical field of cigarette flavors, in particular to a kind of Flower fragrance aroma essence for cigarette drop pill And application.
Background technology
Essence and flavoring agent can play in Medicated cigarette and cover shortcoming, improve tobacco aroma and jealous, the physical property of improvement Nicotiana tabacum L. The unique taste of Medicated cigarette and the effect of style, can be given, and product quality differentiation can be realized, stablize cigarette smoking product Matter, style and quality responses for Medicated cigarette have a major impact.Along with State Bureau's " perfumery engineering " implementation, essence and flavoring agent In Chinese-style cigarette core technology, especially the effect in terms of constructing the unique taste of Medicated cigarette and style will be more and more important.
Cigarette drop pill is the drop pill being applied to cigarette filter tip, and centre is surrounded by essence, and consumer can be by pinching when suction Broken cigarette drop pill discharges essence and flavoring agent, brings special fragrance to experience to cigarette flavor.The Patents of existing cigarette drop pill is such as The dripping pills of cigarette additive lapping of patent No. CN200910273417.4 and the drop pill wrapped up with it and the application of drop pill, specially It it is all the system of cigarette drop pill disclosed in the improved wrapping material of the dripping pills of cigarette additive of profit CN201010573777.9 etc. Preparation Method and lapping, for fewer disclosed in the essence of cigarette drop pill.But essence and the tradition for cigarette drop pill Essence spice for cigarette is different, and the essence and flavoring agent added in cigarette drop pill is not by burning, so, tradition flavouring essence for tobacco Spice directly applies in cigarette drop pill, is difficult to obtain the accreditation of consumer on taste.This is accomplished by supplementing novel taste, pin Essence and flavoring agent to cigarette drop pill.
The fragrance of a flower is a kind of essence note more conventional in Nicotiana tabacum L., with its exquisite elegant style by consumer, especially It it is the welcome of female consumer.There is following two problem in existing Flower fragrance aroma essence in cigarette drop pill: one is fragrance Insufficient strength, it is more difficult to appear, causes Medicated cigarette to be smelt fragrant inconspicuous, it is difficult to reaches consumer and has prominent fragrance to cigarette product and want Ask.Two is that fragrance is the most graceful, it is difficult to reach the requirement that consumer is the most high-end to fragrance.
Summary of the invention
It is an object of the invention to for the problem existing for prior art, it is provided that a kind of floral notes for cigarette drop pill Essence and application.Described essence selects molecular weight perfume material little, high volatility to be modulated so that it is be adapted to cigarette drop pill not Through aptitude to burn;And coordinate with the most fragrant and sweet, delicate fragrance, solve the harmony problem with this perfume (or spice) of Nicotiana tabacum L., be applied to cigarette with dripping Ball can give the fragrance of a flower style of Medicated cigarette characteristic, promote the graceful sense of cigarette flavor, make the fragrance of Medicated cigarette enrich comfortable.
The present invention is achieved through the following technical solutions: described a kind of Flower fragrance aroma essence for cigarette drop pill, its It is characterised by, is to be stirred 1-3 hour by the raw material components mix homogeneously of following portions by weight, mistake after then standing 24-48 hour 60-80 eye mesh screen filters off sediment and obtains;Its raw material components forms by weight particularly as follows: oil of Rhizoma et radix valerianae 0.3~5 parts, Citrus aurantium L. var. amara Engl. Quintessence oil 0.5~10 parts, Flos Osmanthi Fragrantis quintessence oil 0.2~5 parts, Herba Lysimachiae foenum-graeci quintessence oil 1~10 parts, rose ethereal oil 0.2~5 parts, violet leaf Extract 1~15 parts, iso-amyl iso-valeriate 0.1~2 parts, olive oil 52~97 parts.
As preferably, described raw material components consists of by weight: oil of Rhizoma et radix valerianae 0.5 part, Citrus aurantium L. var. amara Engl. quintessence oil 3 parts, Flos Osmanthi Fragrantis Absolute oil 0.2 part, Herba Lysimachiae foenum-graeci quintessence oil 1 part, rose ethereal oil 0.5 part, violet leaf extract 3 parts, iso-amyl iso-valeriate 0.1 part, 91.7 parts of olive oil.
As preferably, the described filtrate essence increasing Medicated cigarette floral notes through obtaining can be dissolved completely in olive oil. Described olive oil is commercially available common edible olive oil.
In such scheme, described Citrus aurantium L. var. amara Engl. quintessence oil can use and directly become at the quintessence oil that can be used as spice bought on the market Product, or steam distillation will be used after fresh Citrus aurantium L. var. amara Engl. wash clean to obtain;Oil of Rhizoma et radix valerianae can use directly to be bought on the market The finished product that can be used as spice, or use Rhizoma et radix valerianae to take root to process through water distillation apparatus;Flos Osmanthi Fragrantis quintessence oil can be direct At the absolute oil finished product that can be used as spice bought on the market, or the quintessence oil that directly employing ethanol extracts from osmanthus concrete; Herba Lysimachiae foenum-graeci quintessence oil and rose ethereal oil are directly at the quintessence oil finished product that can be used as spice bought on the market;Violet leaf extracts Thing can use directly at the extract finished product that can be used as spice bought on the market, or violet leaf is cleaned pulverize after Obtain with the EtOH Sonicate countercurrent extraction of 95% under conditions of 55 ± 2 DEG C;Isoamyl isovalerate is for buying product on the market.
The another kind of technical scheme that the present invention provides: the application of a kind of Flower fragrance aroma essence for cigarette drop pill, it is special Levy and be: the essence of above-mentioned increase Medicated cigarette floral notes is added in the hopper of pill dripping machine, regulate the size of discharging opening, then The firming agent contained in ball device with the drop pill lapping being placed in pill dripping machine rubber cement tank and being placed in is according to the preparation technology of drop pill Making weight is 3~10mg, and crushing strength is 0.3kPa~2.0kPa, a diameter of 2~5mm, and moisture is the cigarette use of 6%~20% Drop pill;During cigarette filter wire-beam forming, the cigarette drop pill of preparation is positioned and is applied in filter rod, and make Medicated cigarette.
Method prepared by the drop pill in the present invention is prior art, specifically refers to the open Chinese patent authorized, its patent Number it is: 200910273417.4, invention entitled: dripping pills of cigarette additive lapping and the drop pill wrapped up with it and drop pill Application;This patent specifically discloses the preparation method of cigarette drop pill and the lapping of cigarette drop pill and firming agent.Its Lapping is by the sodium alginate that viscosity is 0.01~2Pa.s, freezes G & W that force value is 100~250 according to weight ratio 1 ~the ratio mixing of 8:0.5~5:85~100 is placed in the retort with heating interlayer, stir under the conditions of temperature 70 C Make mixture dissolve, and be incubated 1-2 hour, stand after foam floats, be filtrated to get under the conditions of being incubated 70 DEG C.The present invention makes The lapping of standby cigarette drop pill is in addition to using lapping disclosed in above-mentioned patent, it is also possible to use other to meet cigarette with dripping The material of ball lapping condition.
The present invention selects molecular weight perfume material little, high volatility to adapt to it for cigarette drop pill without aptitude to burn; Oil of Rhizoma et radix valerianae is selected to increase its property sent out thoroughly;Citrus aurantium L. var. amara Engl. quintessence oil, Flos Osmanthi Fragrantis quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil, rose ethereal oil etc. are selected to give it The fragrance of a flower and graceful sense;And coordinate with the most fragrant and sweet, delicate fragrance, solve Nicotiana tabacum L. this perfume coordination problem.The floral notes modulated is fragrant Essence gives the fragrance of a flower style of Medicated cigarette characteristic, can effectively increase Medicated cigarette fragrance of a flower fragrance, and elegant fragrance is elegant, and pleasant impression is comfortable, carries Rise the graceful sense of cigarette flavor, make the fragrance of Medicated cigarette enrich comfortable.
Pill dripping machine is used to make cigarette drop pill, at cigarette filter rod wire-beam forming the Medicated cigarette Flower fragrance aroma essence in the present invention During position applying and make Medicated cigarette, its medicated cigarette is with drop pill during dripping, and production stability is preferable, cigarette drop pill breakage rate Low, yield rate is 80-85%.When the Medicated cigarette made is smoked panel test, sensation is inhaled fragrance of a flower fragrance in taste and is substantially strengthened, and elegant fragrance is elegant, Pleasant impression is comfortable.And equipment of the presently claimed invention is relatively easy, cost is relatively low, it is easy to industrialized production, has the strongest reality The property used.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail, but embodiment is not to skill of the present invention The restriction of art scheme.
Embodiment 1, a kind of Flower fragrance aroma essence for cigarette drop pill, concrete preparation method is as follows: weigh oil of Rhizoma et radix valerianae 0.5 Part, Citrus aurantium L. var. amara Engl. quintessence oil 3 parts, Flos Osmanthi Fragrantis quintessence oil 0.2 part, Herba Lysimachiae foenum-graeci quintessence oil 1 part, rose ethereal oil 0.5 part, violet leaf extract 3 Part, iso-amyl iso-valeriate 0.1 part, 91.7 parts of olive oil.After the mixing of described raw material components, stir 2 hours, stand 24 hours, filter Sediment is gone to obtain the essence of described increase Medicated cigarette floral notes.
Use pill dripping machine to be dripped by the essence increasing Medicated cigarette floral notes of preparation in embodiment 1 and make cigarette drop pill, at volume During cigarette filter wire-beam forming, location applies cigarette drop pill, makes Medicated cigarette, evaluates the application effect of flowery odour cigarette drop pill.
Embodiment 2, a kind of Flower fragrance aroma essence for cigarette drop pill, concrete preparation method is as follows: weigh oil of Rhizoma et radix valerianae 3 Part, Citrus aurantium L. var. amara Engl. quintessence oil 6 parts, Flos Osmanthi Fragrantis quintessence oil 0.8 part, Herba Lysimachiae foenum-graeci quintessence oil 1 part, rose ethereal oil 1.5 parts, violet leaf extract 8 Part, iso-amyl iso-valeriate 0.2 part, 89.5 parts of olive oil.After the mixing of described raw material components, stir 2 hours, stand 24 hours, filter Sediment is gone to obtain the essence of described increase Medicated cigarette floral notes.
Use pill dripping machine to be dripped by the essence increasing Medicated cigarette floral notes of preparation in embodiment 2 and make cigarette drop pill, at volume During cigarette filter wire-beam forming, location applies cigarette drop pill, makes Medicated cigarette, evaluates the application effect of flowery odour cigarette drop pill.
Embodiment 3, a kind of Flower fragrance aroma essence for cigarette drop pill, concrete preparation method is as follows: weigh oil of Rhizoma et radix valerianae 2.6 Part, Citrus aurantium L. var. amara Engl. quintessence oil 1.0 parts, Flos Osmanthi Fragrantis quintessence oil 3.0 parts, Herba Lysimachiae foenum-graeci quintessence oil 4 parts, rose ethereal oil 2.5 parts, violet leaf extract 12 parts, iso-amyl iso-valeriate 0.3 part, 74.9 parts of olive oil.After the mixing of described raw material components, stir 2 hours, stand 24 hours, Filter off sediment and obtain the essence of described increase Medicated cigarette floral notes.
Use pill dripping machine to be dripped by the essence increasing Medicated cigarette floral notes of preparation in embodiment 3 and make cigarette drop pill, at volume During cigarette filter wire-beam forming, location applies cigarette drop pill, makes Medicated cigarette, evaluates the application effect of flowery odour cigarette drop pill.
The application of the Flower fragrance aroma essence for cigarette drop pill in the present invention, specifically adds Flower fragrance aroma essence and drips Cigarette drop pill it is prepared as in the hopper of ball machine.In embodiment, the concrete dripping method of cigarette drop pill is as follows:
(1) ready cigarette drop pill lapping is placed in the rubber cement tank of pill dripping machine, keeps 70 DEG C, and regulate The size of gum exudation mouth;
(2) then the Flower fragrance aroma essence prepared in the present invention is added in the hopper of pill dripping machine, regulate discharging opening Size;
(3) in drop pill holder, calcium ion salts solution solidifying agent is put into;
(4) open pill dripping machine, make drop pill lapping, Flower fragrance aroma essence, go out from concentric the most at different rates Jiao Kou and discharging opening ooze;Drop pill lapping first drips to above firming agent and launches, and Flower fragrance aroma essence has dropped in just immediately On the glue surface launched, owing to the effect drop pill lapping of gravity continues to decline in firming agent, make drop pill lapping Sealing completely, Flower fragrance aroma essence is just wrapped in inside drop pill lapping, adds surface tension effects, makes drop pill wrap up Material seals completely, and gained spheroidal ball is cigarette drop pill;
(5) cigarette drop pill constantly declines in firming agent, is progressively solidified into flexible glue scrotiform dripping pills of cigarette additive;Described The weight of drop pill is 3mg, and crushing strength is 0.3kPa~2.0kPa.
Contrast test, selects middle-grade blank tobacco shred, smokes panel test the Medicated cigarette made by the embodiment of the present invention 1~3, Medicated cigarette When smokeing panel test, pinch brokenly the cigarette drop pill of floral notes, carry out application effect appraisal.7 people form group of smokeing panel test, and wherein national level is smoked panel test Shi Yiming, provincial teacher of the smokeing panel test two.Evaluation effect is shown in Table 1
Table 1: three kind of fragrance of a flower cigarette drop pill sensory effects evaluation table
Being shown by smoking result in table 1, cigarette quality has been promoted by the cigarette drop pill essence that the present invention is modulated, and has Increasing Medicated cigarette floral notes, improve elegant fragrance sense, increase flue gas thoroughly sends out property and sweet sense, the comfortable effect such as totally of pleasant impression, can To use as Novel tobacco drop pill essence.
By the physical index of the Flower fragrance aroma essence for cigarette drop pill of above-mentioned process exploitation through detection, the most such as Under:
Title Essence of the present invention
Outward appearance Clarification glassy yellow oily liquids
Fragrance The fragrance of a flower
Relative density (20/20 DEG C) 0.9028
Refraction index (20 DEG C) 1.4531
Lead content (mg/kg) ≤5.0
Arsenic content (mg/kg) ≤1.0
Above-mentioned physical index all meets the index of flavouring essence for tobacco.

Claims (4)

1. the Flower fragrance aroma essence for cigarette drop pill, it is characterised in that be to be mixed by the raw material components of following portions by weight Conjunction stirring after then standing 24-48 hour to raw material components mix homogeneously, is crossed 60-80 eye mesh screen elimination sediment and is obtained for 1-3 hour Arrive;Its raw material components forms by weight particularly as follows: oil of Rhizoma et radix valerianae 0.3~5 parts, Citrus aurantium L. var. amara Engl. quintessence oil 0.5~10 parts, Flos Osmanthi Fragrantis quintessence oil 0.2~5 part, Herba Lysimachiae foenum-graeci quintessence oil 1~10 parts, rose ethereal oil 0.2~5 parts, violet leaf extract 1~15 parts, isovaleric acid are different Pentyl ester 0.1~2 parts, olive oil 52~97 parts.
A kind of Flower fragrance aroma essence for cigarette drop pill the most according to claim 1, it is characterised in that described raw material group Divide and consist of by weight: oil of Rhizoma et radix valerianae 0.5 part, Citrus aurantium L. var. amara Engl. quintessence oil 3 parts, Flos Osmanthi Fragrantis quintessence oil 0.2 part, Herba Lysimachiae foenum-graeci quintessence oil 1 part, Flos Rosae Rugosae Flower essential oil 0.5 part, violet leaf extract 3 parts, iso-amyl iso-valeriate 0.1 part, 91.7 parts of olive oil.
A kind of Flower fragrance aroma essence for cigarette drop pill the most according to claim 1 or claim 2, it is characterised in that: described raw material The filtrate that after component mixing, elimination sediment obtains can be dissolved completely in olive oil.
4. the application of the Flower fragrance aroma essence for cigarette drop pill described in a claim 1 or 2, it is characterised in that: by upper State and increase in the hopper that the essence of Medicated cigarette floral notes adds pill dripping machine, regulate the size of discharging opening, then be placed in drop pill Drop pill lapping in machine rubber cement tank and be placed in the firming agent contained in ball device to make weight according to the preparation technology of drop pill be 3 ~10mg, crushing strength is 0.3kPa~2.0kPa, a diameter of 2~5mm, and moisture is the cigarette drop pill of 6%~20%;At Medicated cigarette In filter tow forming process, the cigarette drop pill of preparation is positioned and is applied in filter rod, and make Medicated cigarette.
CN201610567597.7A 2016-07-19 2016-07-19 A kind of Flower fragrance aroma essence for cigarette drop pill and application Pending CN106118884A (en)

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107474963A (en) * 2017-09-01 2017-12-15 云南巴菰生物科技有限公司 A kind of cordate houttuynia essential oil cigarette is with quick-fried pearl and preparation method thereof
CN108203624A (en) * 2018-03-29 2018-06-26 武汉黄鹤楼香精香料有限公司 Essence containing Dendranthema indicum essential oil, cigarette dripping pill and cigarette dripping pill production method
CN109111990A (en) * 2018-10-09 2019-01-01 湖北中烟工业有限责任公司 Utilize the method and its application of wax in impulse electric field efficient removal olive oil
CN109207260A (en) * 2018-11-14 2019-01-15 湖北中烟工业有限责任公司 A kind of strawberry essence and its application for cigarette with mouth stick
CN109439442A (en) * 2018-12-20 2019-03-08 湖北中烟工业有限责任公司 A kind of apricot flavor essence and its preparation method and application for cigarette dripping pill
CN109439439A (en) * 2018-12-20 2019-03-08 湖北中烟工业有限责任公司 A kind of cloves flavor essence and its preparation method and application for cigarette dripping pill
CN109576058A (en) * 2018-12-20 2019-04-05 湖北中烟工业有限责任公司 A kind of cumin flavor essence and its preparation method and application for cigarette dripping pill
WO2019175550A1 (en) * 2018-03-12 2019-09-19 Unex Designs Ltd Calming composition
CN113842488A (en) * 2021-09-27 2021-12-28 江苏格姆思体育科技研究院有限公司 Plant type air freshener and preparation method thereof

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CN102827693A (en) * 2012-08-16 2012-12-19 湖北中烟工业有限责任公司 Flower fragrance aroma essence for tobacco

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107474963A (en) * 2017-09-01 2017-12-15 云南巴菰生物科技有限公司 A kind of cordate houttuynia essential oil cigarette is with quick-fried pearl and preparation method thereof
WO2019175550A1 (en) * 2018-03-12 2019-09-19 Unex Designs Ltd Calming composition
CN108203624A (en) * 2018-03-29 2018-06-26 武汉黄鹤楼香精香料有限公司 Essence containing Dendranthema indicum essential oil, cigarette dripping pill and cigarette dripping pill production method
CN109111990A (en) * 2018-10-09 2019-01-01 湖北中烟工业有限责任公司 Utilize the method and its application of wax in impulse electric field efficient removal olive oil
CN109207260A (en) * 2018-11-14 2019-01-15 湖北中烟工业有限责任公司 A kind of strawberry essence and its application for cigarette with mouth stick
CN109439442A (en) * 2018-12-20 2019-03-08 湖北中烟工业有限责任公司 A kind of apricot flavor essence and its preparation method and application for cigarette dripping pill
CN109439439A (en) * 2018-12-20 2019-03-08 湖北中烟工业有限责任公司 A kind of cloves flavor essence and its preparation method and application for cigarette dripping pill
CN109576058A (en) * 2018-12-20 2019-04-05 湖北中烟工业有限责任公司 A kind of cumin flavor essence and its preparation method and application for cigarette dripping pill
CN113842488A (en) * 2021-09-27 2021-12-28 江苏格姆思体育科技研究院有限公司 Plant type air freshener and preparation method thereof

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