CN107057833A - Composite high concentration fresh zanthoxylum oil and preparation method thereof - Google Patents
Composite high concentration fresh zanthoxylum oil and preparation method thereof Download PDFInfo
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- CN107057833A CN107057833A CN201710233396.8A CN201710233396A CN107057833A CN 107057833 A CN107057833 A CN 107057833A CN 201710233396 A CN201710233396 A CN 201710233396A CN 107057833 A CN107057833 A CN 107057833A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
- C11B1/08—Production of fats or fatty oils from raw materials by pressing by hot pressing
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/12—Production of fats or fatty oils from raw materials by melting out
- C11B1/14—Production of fats or fatty oils from raw materials by melting out with hot water or aqueous solutions
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
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Abstract
The invention belongs to production of condiments processing technique field, a kind of composite high concentration fresh zanthoxylum oil and preparation method thereof is disclosed.Zanthoxylum essential oil of the present invention includes the raw material of following parts by weight：60~90 parts of fresh pepper, 5~10 parts of fennel is anistree 5~10 parts, 5~10 parts of ginger, 5~10 parts of shallot, 5~10 parts of garlic, 1~5 part of sesame.Zanthoxylum essential oil preparation method of the present invention is specifically included：The peeling cleaned up is removed into the fresh pepper of wild pepper seed, fennel, anise to be put into stir-frying machine, once does and fries, once adds ethanol solution and continues to stir-fry and obtains the material that stir-fries；Ginger, shallot, garlic, sesame are put into frying pan and fried, punching press crushing is carried out with husky cloth parcel with the material that stir-fries, puts into refinement pot, add volume ratio 1:1 plant blend oil and water is refined at 80~100 DEG C, and centrifugal filtration obtains composite high concentration Zanthoxylum essential oil.The Zanthoxylum essential oil smell that the present invention makes is pleasant, and color is vivid, high with unique compound fragrant, concentration, this preparation method also maximum nutrition for remaining Chinese prickly ash.
Description
Technical field
The present invention relates to production of condiments processing technique field, more particularly to a kind of composite high concentration fresh zanthoxylum oil and its system
Preparation Method.
Background technology
The fruit of Chinese prickly ash, Rutaceae shrub or arbor Chinese pricklyash, is one of Chinese tradition Chinese medicine material and " eight big flavouring ",
With unique enhanced aroma.Chinese prickly ash is pungent, property is hot, returns spleen, stomach, there is fragrant stomach invigorating, warming spleen and stomach for dispelling cold, damp dispelling and pain relieving, desinsection solution
The effect of poison, antipruritic solution raw meat；Primary treatment is vomitted, wind-cold-dampness arthralgia, the disease such as dentalgia.Chinese prickly ash is that Sichuan cuisine and chongqing chafing dish are indispensable
Few main flavouring, with color and luster is dark green, fragrance overflows people, numb taste is pure the characteristics of.It is easily black but fresh pepper is not easy to maintain
Become, go mouldy, spreading the shelf-life under normal temperature only has 3~5 days, stacking the shelf-life is no more than 2 days；Refrigerator cold storage was occurred as soon as less than 7 days
Blacking phenomenon.Therefore, domestic Chinese prickly ash is more is deposited with dry product.But fresh green pepper is after drying, fragrance loss is big, lacks the fresh peculiar perfume (or spice) of green pepper
Gas.Therefore many food production processing enterprises start to make flavouring with Zanthoxylum essential oil substitution Chinese prickly ash in production at present.
Current domestic production Zanthoxylum essential oil is mainly using the side such as oily molten method, solvent extraction, supercritical carbon dioxide extraction method
Method, wherein oily molten method is the conventional method for producing Zanthoxylum essential oil, is used by domestic most Zanthoxylum essential oil factories, its Main be by
Chinese prickly ash is squeezed with hot vegetable oil, active ingredient is dissolved in oil, produces Zanthoxylum essential oil, and it has the disadvantage the bad grasp of oil temperature, oil temperature mistake
Height can cause the fragrance in Chinese prickly ash with numb taste into loss, and oil temperature is too low to cause Chinese prickly ash oil extract not exclusively, cause to waste and produce
Product high expensive.The major defect of solvent extraction is that problem of solvent residual causes product fragrance impure.Supercritical carbon dioxide
Although the Zanthoxylum essential oil quality of extraction production is preferably, the method is time-consuming longer, in order to shorten extraction time, generally in extraction process
Middle use ethanol is made entrainer and extracted, but easily causes dissolvent residual after extraction, and the product of available things of Zanthoxylum bungeanum are have impact on again
Matter.
In summary, the making of current Zanthoxylum essential oil is to prepare at relatively high temperatures, have lost most volatilization
Oil, leverages the pure local flavor of Zanthoxylum essential oil, while some harmful materials can be also produced at high temperature, and simply
The Zanthoxylum essential oil that oil immersion is extracted, local flavor is single, and flavor substance content is relatively low, therefore, develops a kind of composite high concentration fresh zanthoxylum oil
Preparation method is very important.
The content of the invention
The technical problem to be solved in the present invention is to overcome drawbacks described above there is provided a kind of composite high concentration fresh zanthoxylum oil and its system
Preparation Method.
In order to solve the above-mentioned technical problem, the technical scheme is that：
An object of the present invention is to provide a kind of composite high concentration fresh zanthoxylum oil, includes the raw material of following parts by weight：It is fresh
60~90 parts of Chinese prickly ash, 5~10 parts of fennel is anistree 5~10 parts, 5~10 parts of ginger, 5~10 parts of shallot, 5~10 parts of garlic, sesame
1~5 part.
It is preferred that, a kind of composite high concentration fresh zanthoxylum oil includes the raw material of following parts by weight：80~90 parts of fresh pepper, fennel
It is fragrant 8~10 parts, anistree 6~8 parts, 5~8 parts of ginger, 5~6 parts of shallot, 8~10 parts of garlic, 3~5 parts of sesame.
It is preferred that, a kind of composite high concentration fresh zanthoxylum oil includes the raw material of following parts by weight：80 parts of fresh pepper, fennel 8
Part, anistree 6 parts, 6 parts of ginger, 5 parts of shallot, 8 parts of garlic, 4 parts of sesame.
The second object of the present invention is to provide a kind of preparation method of composite high concentration fresh zanthoxylum oil, comprises the following steps：
(1) fresh pepper, fennel, anise are cleaned by weight, wild pepper seed is removed into fresh pepper peeling and obtains fresh pepper
Skin；
(2) fresh pepper skin, fennel, the anise for obtaining step (1) are put into stir-frying machine, and stir-fry 5~10min for the first time,
Compound is obtained, ethanol solution is added and continues to stir-fry for the second time, stir-fry 10~20min of time；
(3) ginger, shallot, garlic, sesame are put into frying pan and fried by weight, fried to smelling fragrance and do not paste and be
Preferably；
(4) material that stir-fries for obtaining step (2), (3) carries out punching press crushing with husky cloth parcel, obtains particle diameter≤100 μm
Mixed-powder slurry；
(5) the mixed-powder slurry obtained in step (4) is put into refinement pot, by volume ratio 1:1 plant reconciles
Oil and water are added in refinement pot, and 2~3h is kept in 80~100 DEG C of temperature, and centrifugation is carried out at first filtering in filter plant
Reason；
(6) oil water mixture obtained after being filtered in step (5) is separated off moisture by rectifying, recycles filtering to set
It is standby to filter 2~3 times, obtain composite high concentration Zanthoxylum essential oil.
It is preferred that, the temperature that the first time described in step (2) stir-fries is 30~50 DEG C, and the temperature stir-fried for the second time is 50
~65 DEG C.
It is preferred that, the weight ratio of ethanol and compound described in step (2) is 1~5:1.
It is preferred that, the concentration of ethanol described in step (2) is 80~95%.
It is preferred that, the plant blend oil described in step (5) includes rapeseed oil 60%, corn oil 15%, peanut oil 10%, Portugal
Grape seed oil 10%, Lavender 5%.
Compared with prior art the beneficial effects of the invention are as follows：
Zanthoxylum essential oil of the present invention is based on Chinese prickly ash, and different spices of arranging in pairs or groups carry out frying using suitable method, produced more
Plus unique composite flavor, local flavor content of material is stable in Zanthoxylum essential oil, and color is vivid, with unique compound fragrant, concentration
It is high.Chinese prickly ash oil product of the present invention has the due flavour of this product and smell, free from extraneous odour, moisture 0.2%, acid value 0.8mg/g, mistake
Oxidation number 0.01mg/kg, insoluble impurities 0.05%.
The technique of the present invention will not destroy the natural characteristic of Chinese prickly ash and vegetable oil using low temperature oil refining, physical filtering method, and
The fully natural green aromatic substance of fresh pepper inherently is just completely organically kept down, and therefore, solves traditional life
In production method numb taste, the fragrance of Chinese prickly ash be easy to run off, it is volatile, be difficult the shortcoming that preserves for a long time, and it is natural to remain Chinese prickly ash
Aromatic substance and numb taste.
Embodiment
The embodiment to the present invention is described further below.Herein it should be noted that for these implementations
The explanation of mode is used to help understand the present invention, but does not constitute limitation of the invention.In addition, invention described below
As long as involved technical characteristic does not constitute conflict and can be just mutually combined each other in each embodiment.
Embodiment 1
A kind of composite high concentration fresh zanthoxylum oil, includes the raw material of following parts by weight：60 parts of fresh pepper, 5 parts of fennel, anise 5
Part, 5 parts of ginger, 5 parts of shallot, 5 parts of garlic, 1 part of sesame；Its preparation method comprises the following steps：
(1) 60 parts by weight fresh peppers, 5 parts by weight fennels, 5 parts by weight anise are cleaned, Chinese prickly ash is removed into fresh pepper peeling
Seed obtains fresh pepper skin；
(2) fresh pepper skin, fennel, the anise for obtaining step (1) are put into stir-frying machine, are stir-fried for the first time at 30 DEG C
10min, obtains compound, and it is that 80% ethanol solution continues to stir-fry for the second time to add concentration, in 65 DEG C of 10min that stir-fry；Wherein second
The weight ratio of alcohol and compound is 5:1；
(3) 5 parts by weight gingers, 5 parts by weight shallots, 5 parts by weight garlics, 1 parts by weight sesame are put into frying pan and fried, stir-fry is arrived
Smell fragrance and do not paste and be advisable；
(4) material that stir-fries for obtaining step (2), (3) carries out punching press crushing with husky cloth parcel, obtains particle diameter≤100 μm
Mixed-powder slurry；
(5) the mixed-powder slurry obtained in step (4) is put into refinement pot, by volume ratio 1:1 plant reconciles
Oil and water are added in refinement pot, and 3h is kept in 80 DEG C of temperature, and centrifugation carries out first filtration treatment in filter plant；
(6) oil water mixture obtained after being filtered in step (5) is separated off moisture by rectifying, recycles filtering to set
It is standby to filter 2~3 times, obtain composite high concentration Zanthoxylum essential oil.
Embodiment 2
A kind of composite high concentration fresh zanthoxylum oil, includes the raw material of following parts by weight：80 parts of fresh pepper, 8 parts of fennel, anise 6
Part, 6 parts of ginger, 5 parts of shallot, 8 parts of garlic, 4 parts of sesame；Its preparation method comprises the following steps：
(1) 80 parts by weight fresh peppers, 8 parts by weight fennels, 6 parts by weight anise are cleaned, Chinese prickly ash is removed into fresh pepper peeling
Seed obtains fresh pepper skin；
(2) fresh pepper skin, fennel, the anise for obtaining step (1) are put into stir-frying machine, are stir-fried for the first time at 40 DEG C
8min, obtains compound, and it is that 90% ethanol solution continues to stir-fry for the second time to add concentration, in 60 DEG C of 15min that stir-fry；Wherein ethanol
Weight ratio with compound is 3:1；
(3) 6 parts by weight gingers, 5 parts by weight shallots, 8 parts by weight garlics, 4 parts by weight sesames are put into frying pan and fried, stir-fry is arrived
Smell fragrance and do not paste and be advisable；
(4) material that stir-fries for obtaining step (2), (3) carries out punching press crushing with husky cloth parcel, obtains particle diameter≤100 μm
Mixed-powder slurry；
(5) the mixed-powder slurry obtained in step (4) is put into refinement pot, by volume ratio 1:1 plant reconciles
Oil and water are added in refinement pot, and 2h is kept in 90 DEG C of temperature, and centrifugation carries out first filtration treatment in filter plant；
(6) oil water mixture obtained after being filtered in step (5) is separated off moisture by rectifying, recycles filtering to set
It is standby to filter 2~3 times, obtain composite high concentration Zanthoxylum essential oil.
Embodiment 3
A kind of composite high concentration fresh zanthoxylum oil, includes the raw material of following parts by weight：90 parts of fresh pepper, 10 parts of fennel is anistree
10 parts, 10 parts of ginger, 10 parts of shallot, 10 parts of garlic, 5 parts of sesame；Its preparation method comprises the following steps：
(1) 90 parts by weight fresh peppers, 10 parts by weight fennels, 10 parts by weight anise are cleaned, flower is removed into fresh pepper peeling
Green pepper seed obtains fresh pepper skin；
(2) fresh pepper skin, fennel, the anise for obtaining step (1) are put into stir-frying machine, are stir-fried for the first time at 50 DEG C
5min, obtains compound, and it is that 95% ethanol solution continues to stir-fry for the second time to add concentration, in 50 DEG C of 20min that stir-fry；Wherein ethanol
Weight ratio with compound is 1:1；
(3) 10 parts by weight gingers, 10 parts by weight shallots, 10 parts by weight garlics, 5 parts by weight sesames are put into frying pan and fried,
Fry to smell fragrance and do not paste and be advisable；
(4) material that stir-fries for obtaining step (2), (3) carries out punching press crushing with husky cloth parcel, obtains particle diameter≤100 μm
Mixed-powder slurry；
(5) the mixed-powder slurry obtained in step (4) is put into refinement pot, by volume ratio 1:1 plant reconciles
Oil and water are added in refinement pot, and 2h is kept in 100 DEG C of temperature, and centrifugation carries out first filtration treatment in filter plant；
(6) oil water mixture obtained after being filtered in step (5) is separated off moisture by rectifying, recycles filtering to set
It is standby to filter 2~3 times, obtain composite high concentration Zanthoxylum essential oil.
It is above present pre-ferred embodiments, is only applicable to help the principle for understanding the embodiment of the present invention；Simultaneously for this
The those skilled in the art in field, according to the present embodiment, will change in embodiment and application, comprehensive
Upper described, this specification content should not be construed as limiting the invention.
Claims (8)
1. a kind of composite high concentration Zanthoxylum essential oil, it is characterised in that：Include the raw material of following parts by weight：60~90 parts of fresh pepper, fennel
It is fragrant 5~10 parts, anistree 5~10 parts, 5~10 parts of ginger, 5~10 parts of shallot, 5~10 parts of garlic, 1~5 part of sesame.
2. composite high concentration fresh zanthoxylum oil according to claim 1, it is characterised in that：Include the raw material of following parts by weight：
80~90 parts of fresh pepper, 8~10 parts of fennel is anistree 6~8 parts, 5~8 parts of ginger, 5~6 parts of shallot, 8~10 parts of garlic, sesame 3
~5 parts.
3. composite high concentration fresh zanthoxylum oil according to claim 1, it is characterised in that：Include the raw material of following parts by weight：
80 parts of fresh pepper, 8 parts of fennel is anistree 6 parts, 6 parts of ginger, 5 parts of shallot, 8 parts of garlic, 4 parts of sesame.
4. a kind of preparation method of the composite high concentration fresh zanthoxylum oil described in claim 1, it is characterised in that：Including following step
Suddenly：
(1) fresh pepper, fennel, anise are cleaned by weight, wild pepper seed is removed into fresh pepper peeling and obtains fresh pepper skin；
(2) fresh pepper skin, fennel, the anise for obtaining step (1) are put into stir-frying machine, and stir-fry 5~10min for the first time, obtains
Compound, adds ethanol solution and continues to stir-fry for the second time, stir-fry 10~20min of time；
(3) ginger, shallot, garlic, sesame are put into frying pan and fried by weight, fried to smelling fragrance and do not paste and be advisable；
(4) material that stir-fries for obtaining step (2), (3) carries out punching press crushing with husky cloth parcel, obtains the mixed of particle diameter≤100 μm
Close powder slurries；
(5) the mixed-powder slurry obtained in step (4) is put into refinement pot, by volume ratio 1:1 plant blend oil and
Water is added in refinement pot, and 2~3h is kept in 80~100 DEG C of temperature, and centrifugation carries out first filtration treatment in filter plant；
(6) oil water mixture obtained after being filtered in step (5) is separated off moisture by rectifying, recycles filter plant mistake
Filter 2~3 times, obtains composite high concentration Zanthoxylum essential oil.
5. the preparation method of composite high concentration fresh zanthoxylum oil according to claim 4, it is characterised in that：Institute in step (2)
The temperature that the first time stated stir-fries is 30~50 DEG C, and the temperature stir-fried for the second time is 50~65 DEG C.
6. the preparation method of composite high concentration fresh zanthoxylum oil according to claim 4, it is characterised in that：Institute in step (2)
The weight ratio for stating ethanol and compound is 1~5:1.
7. the preparation method of composite high concentration fresh zanthoxylum oil according to claim 4, it is characterised in that：Institute in step (2)
The concentration for stating ethanol is 80~95%.
8. the preparation method of composite high concentration fresh zanthoxylum oil according to claim 4, it is characterised in that：Step (5) is described
Plant blend oil include rapeseed oil 60%, corn oil 15%, peanut oil 10%, grape-kernel oil 10%, Lavender 5%.
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Cited By (4)
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| CN109090266A (en) * | 2018-08-29 | 2018-12-28 | 陕西为康食品科技股份有限公司 | A kind of production method of quick-fried wild citron oil |
| CN109679763A (en) * | 2019-02-21 | 2019-04-26 | 湖南大三湘茶油股份有限公司 | Tea seed is rendered palatable oil and preparation method thereof |
| CN109699991A (en) * | 2019-03-19 | 2019-05-03 | 成都珪一食品开发股份有限公司 | Crisp-fried Chinese prickly ash and its production technology and crisp-fried Chinese prickly ash seasoning and its production technology |
| CN112655776A (en) * | 2020-12-10 | 2021-04-16 | 四川饭扫光食品集团股份有限公司 | Preparation method and application of compound zanthoxylum oil |
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| CN109699991A (en) * | 2019-03-19 | 2019-05-03 | 成都珪一食品开发股份有限公司 | Crisp-fried Chinese prickly ash and its production technology and crisp-fried Chinese prickly ash seasoning and its production technology |
| CN112655776A (en) * | 2020-12-10 | 2021-04-16 | 四川饭扫光食品集团股份有限公司 | Preparation method and application of compound zanthoxylum oil |
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