CN108192776A - A kind of astral oil rattan craft transparent soap and preparation method thereof - Google Patents
A kind of astral oil rattan craft transparent soap and preparation method thereof Download PDFInfo
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- CN108192776A CN108192776A CN201711462508.3A CN201711462508A CN108192776A CN 108192776 A CN108192776 A CN 108192776A CN 201711462508 A CN201711462508 A CN 201711462508A CN 108192776 A CN108192776 A CN 108192776A
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- oil
- astral
- rattan
- craft
- transparent soap
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of astral oil rattan craft transparent soaps, include the raw material of following weight percent：The sweet amino proline 1 5% of natural oil 20 40%, alkali 20 25%, glycerine 5 20%, carboxybetaine 1 3%, methyl, honey 1 3%, astral oil rattan oil 0.5 3%, astral oil rattan leaf composite fermentation liquid 0.5 3%, essential oil 0.01 0.5%, surplus are water, the astral oil rattan craft transparent soap moistening effect is good, while skin is moderately cleaned, skin damage can be repaired, skin is made to keep moistening smooth flexible；The invention also discloses a kind of preparation methods of astral oil rattan craft transparent soap, and the preparation method is simple and practical, the astral oil rattan craft transparent soap good product quality produced.
Description
Technical field
The present invention relates to transparent soap preparing technical fields, and in particular to a kind of astral oil rattan craft transparent soap and its preparation side
Method.
Background technology
In recent years, being gradually increased with people's living standard, pure natural, nonirritant transparent soap is increasingly by city
The welcome of field, transparent soap is using vegetable oil and alkali as raw material, is obtained through cold process soap, it can be effectively maintained in vegetable oil largely
Nutriment, effective cleaning, moisturizing can be played the role of.
Containing abundant unrighted acid and tocopherol in astral oil rattan oil, there is excellent affinity and infiltration to skin
Power is easily absorbed by the skin, to supplement the lipid nutrient needed for skin.Repair dry skin and due to contact surface activating agent and
The skin fat sour water of damage is put down, and is maintained and is enhanced Skin Cell film and the normal configuration and function of interstitial；It simultaneously can also be
Skin surface forms ventilative water-retaining film, weakens the moisture loss of deep skin, and skin is made to keep moistening smooth flexible, has pole
High cosmetic values.In the prior art, it yet there are no the report applied in manual transparent soap in relation to astral oil rattan oil.
Invention content
The purpose of the present invention is to provide a kind of good astral oil rattan craft transparent soap of moistening effect, in moderately cleaning skin
Meanwhile skin damage can be repaired, skin is made to keep moistening smooth flexible.
To achieve the above object, the technical solution adopted by the present invention is：A kind of astral oil rattan craft transparent soap, feature exist
In including the raw material of following weight percent：
Preferably, above-mentioned astral oil rattan craft transparent soap, wherein the natural oil is selected from coconut oil, castor oil, flax
At least one of seed oil, olive oil, camellia oil, green tea seed oil, hemp-seed oil.
Preferably, above-mentioned astral oil rattan craft transparent soap, wherein the purity of the alkali is not less than 98%.
Another object of the present invention is to provide a kind of method simplicity, the system of the astral oil rattan craft transparent soap of good product quality
Preparation Method.
To achieve the above object, the technical solution adopted by the present invention is：Include the following steps：
(1) astral oil rattan oil is produced：
A. astral oil rattan fruit is taken, is shelled and dry to moisture content 2% hereinafter, obtaining the first crude oil using physical squeezing method；Surpassed with CO2
The critical treatment by extraction astral oil rattan fruitcake dregs of rice obtain the second crude oil；Merge the first crude oil and the second crude oil, obtain astral oil rattan crude oil；
B. by astral oil rattan heating crude oil to 45-50 DEG C, with citric acid degumming；
C. it is 90 DEG C to continue to be heated to oil temperature, adds in boiling water and is washed；It is cooled to room temperature, carries out water-oil separating；
D. winterization is carried out to astral oil rattan oil, then carries out initial filter with slipstream membrane separation technique, then with NF membrane to primary filtrate into
Row secondary filter is to get astral oil rattan oil；
(2) astral oil rattan leaf composite fermentation liquid is produced：
A. astral oil rattan leaf is cleaned, dried in the shade, crushed, extracted with flooding, obtain crude extract；
B. the alkaline earth of 20-30wt% is added in into crude extract, stirs evenly, centrifuge slagging-off, then with micro-filtrate membrane filtration, must be clarified
Liquid；
C. the mixed fermentation strain of 0.002-0.005vt% is accessed into clarified solution, adds in honey and the astral oil rattan oil of 20wt%,
It is uniformly mixed, is placed in China fir tank constant temperature static fermentation 2-6 months；
D. tunning is taken out, is filtered with slipstream membrane separation technique, collects filtrate；
E. high-temperature sterilization is carried out to filtrate at 100 DEG C, is subsequently cooled to composite fermentation liquid of the room temperature to get astral oil rattan leaf；
(3) transparent soap is prepared：
A. natural oil and astral oil rattan oil are stirred and heated to 60 DEG C by formula, divide 2-5 addition alkali, stir 10-30 minutes
Saponification is completed, obtains soap base；
B. glycerine, carboxybetaine and methyl sweet amino proline are added in when soap base is cooled to 35 DEG C, is stirred to glue；
C. continue to stir, the composite fermentation liquid of astral oil rattan leaf is added in when temperature is down to room temperature, treats that bubble completely disappears and pours into
Mold；
D. it is put at 2-10 DEG C and freezes 24 hours, up to Transparent handmade soap after taking-up.
Preferably, the preparation method of above-mentioned astral oil rattan craft transparent soap, wherein the mixed fermentation strain is including as follows
The raw material of percent by volume：The Bulgarian Lactobacillus bacterium solution of 1.5-2.0%, the red saccharomycete bacterium solution of 1.5-2.0%,
The long shoot trichoderma bacterium solution of 0.01-0.05%, the pure mellow wine essence of 30-35%, the Mucor bacterium solution of 0.1-1%, surplus is pure water.
Preferably, the preparation method of above-mentioned astral oil rattan craft transparent soap, wherein the Bulgarian Lactobacillus is dense
It spends for 400,000,000/ml, a concentration of 200,000,000/ml, a concentration of 0.2 hundred million/ml of the long shoot trichoderma bacterium solution of the red saccharomycete bacterium solution,
A concentration of 0.5 hundred million/ml of Mucor of the Mucor bacterium solution.
Preferably, the preparation method of above-mentioned astral oil rattan craft transparent soap, wherein the slipstream film is flat film, pipe
One kind in formula film, rolled film, hollow fiber form film, the aperture of the slipstream film is 100-300um.
Preferably, the preparation method of above-mentioned astral oil rattan craft transparent soap, wherein being extracted in the step (2) with flooding
During astral oil rattan leaf, the dosage of water is 1-5 times of astral oil rattan leaf volume.
Preferably, the preparation method of above-mentioned astral oil rattan craft transparent soap, wherein constant temperature static fermentation in the step (2)
Temperature be 40-50 DEG C.
The astral oil rattan oil added in the present invention, can remove free radical, eliminate skin lines, and moisturizing water lock effect is good,
Keeping skin, moistening is smooth flexible, and skincare effect is notable；In addition, the astral oil rattan leaf added in the present invention is through hair
After ferment, unrighted acid is decomposed into micromolecule polypeptide, and permeability is more preferable, and transparent soap is made to have stronger moist, reparation and relax
Slow function.
For the present invention by selecting suitable component and its proportioning and preparation method being suitably modified, method is simple,
Produce high-quality astral oil rattan craft transparent soap.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
In technical solution be clearly and completely described, it is clear that described embodiment be only part of the embodiment of the present invention,
Instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making creative labor
All other embodiments obtained under the premise of dynamic, shall fall within the protection scope of the present invention.
Embodiment 1
A kind of astral oil rattan craft transparent soap includes the raw material of following weight percent：
Wherein natural oil is selected from coconut oil, castor oil, linseed oil, olive oil, camellia oil, green tea seed oil, hempseed
At least one of oil.Wherein the purity of alkali is not less than 98%.
The preparation method of astral oil rattan craft transparent soap is as follows in the present invention：
(1) astral oil rattan oil is produced：
A. astral oil rattan fruit is taken, is shelled and dry to moisture content 2% hereinafter, obtaining the first crude oil using physical squeezing method；Surpassed with CO2
The critical treatment by extraction astral oil rattan fruitcake dregs of rice obtain the second crude oil；Merge the first crude oil and the second crude oil, obtain astral oil rattan crude oil；
B. by astral oil rattan heating crude oil to 45-50 DEG C, with citric acid degumming；
C. it is 90 DEG C to continue to be heated to oil temperature, adds in boiling water and is washed；It is cooled to room temperature, carries out water-oil separating；
D. winterization is carried out to astral oil rattan oil, then carries out initial filter with slipstream membrane separation technique, then with NF membrane to primary filtrate into
Row secondary filter is to get astral oil rattan oil；Slipstream film is one in flat film, tubular membrane, rolled film, hollow fiber form film
Kind, the aperture of the slipstream film is 100-300um.
(2) astral oil rattan leaf composite fermentation liquid is produced：
A. astral oil rattan leaf is cleaned, dried in the shade, crushed, extracted with flooding, obtain crude extract；The dosage of water is astral oil rattan cormus
Long-pending 1-5 times；
B. the alkaline earth of 20-30wt% is added in into crude extract, stirs evenly, centrifuge slagging-off, then with micro-filtrate membrane filtration, must be clarified
Liquid；
C. the mixed fermentation strain of 0.002-0.005vt% is accessed into clarified solution, adds in honey and the astral oil rattan oil of 20wt%,
It is uniformly mixed, is placed in China fir tank constant temperature static fermentation 2-6 months, the temperature of constant temperature static fermentation is 40-50 DEG C；
D. tunning is taken out, is filtered with slipstream membrane separation technique, collects filtrate；
E. high-temperature sterilization is carried out to filtrate at 100 DEG C, is subsequently cooled to composite fermentation liquid of the room temperature to get astral oil rattan leaf；
(3) transparent soap is prepared：
A. natural oil and astral oil rattan oil are stirred and heated to 60 DEG C by formula, divide 2-5 addition alkali, stir 10-30 minutes
Saponification is completed, obtains soap base；
B. glycerine, carboxybetaine and methyl sweet amino proline are added in when soap base is cooled to 35 DEG C, is stirred to glue；
C. continue to stir, the composite fermentation liquid of astral oil rattan leaf is added in when temperature is down to room temperature, treats that bubble completely disappears and pours into
Mold；
D. it is put at 2-10 DEG C and freezes 24 hours, up to Transparent handmade soap after taking-up.
Wherein mixed fermentation strain includes the raw material of following percent by volume：The Bulgarian Lactobacillus of 1.5-2.0%
Bacterium solution, the red saccharomycete bacterium solution of 1.5-2.0%, the long shoot trichoderma bacterium solution of 0.01-0.05%, the pure mellow wine essence of 30-35%, 0.1-
1% Mucor bacterium solution, surplus are pure water.Wherein a concentration of 400,000,000/ml of Bulgarian Lactobacillus, the red saccharomycete bacterium
A concentration of 200,000,000/ml of liquid, a concentration of 0.2 hundred million/ml of the long shoot trichoderma bacterium solution, a concentration of Mucor 0.5 of the Mucor bacterium solution
Hundred million/ml.
Embodiment 2
A kind of astral oil rattan craft transparent soap includes the raw material of following weight percent：
Wherein natural oil is selected from coconut oil, castor oil, linseed oil, olive oil, camellia oil, green tea seed oil, hempseed
At least one of oil.Wherein the purity of alkali is not less than 98%.
The preparation method of astral oil rattan craft transparent soap is as follows in the present invention：With embodiment 1.
Embodiment 3
A kind of astral oil rattan craft transparent soap includes the raw material of following weight percent：
Wherein natural oil is selected from coconut oil, castor oil, linseed oil, olive oil, camellia oil, green tea seed oil, hempseed
At least one of oil.Wherein the purity of alkali is not less than 98%.
The preparation method of astral oil rattan craft transparent soap is as follows in the present invention：With embodiment 1.
The effect of embodiment 1-3, is evaluated, efficacy assessments method is as follows：The star described in embodiment 1-3 is prepared respectively
Oily rattan craft transparent soap is respectively issued to 100 testers and compares use, when tester uses sample in the same manner
It is cleaned, each sample respectively uses 2 weeks.Tester according to oneself feel score.Standards of grading take ten point system, and 1
Point worst, 10 points best, and the better score more high effect the better, and various astral oil rattan craft transparent soap using effect evaluation results are as follows
Table A.
Table A astral oil rattan craft transparent soap using effect is evaluated
It can be seen that astral oil rattan oil, the astral oil rattan leaf composite fermentation liquid that different proportion is used in the present invention by embodiment 1-3,
It is apparent different that it, which reaches using effect,.
Several embodiments of the present invention are described in detail above, but the content is only the preferable implementation of the present invention
Example, it is impossible to be construed as limiting the practical range of the present invention.All all the changes and improvements made according to the present patent application range
Deng, should all still belong to the present invention patent covering scope within.
Claims (9)
1. a kind of astral oil rattan craft transparent soap, which is characterized in that include the raw material of following weight percent：
2. astral oil rattan craft transparent soap as described in claim 1, which is characterized in that the natural oil is coconut oil, castor-oil plant
At least one of oil, linseed oil, olive oil, camellia oil, green tea seed oil, hemp-seed oil.
3. astral oil rattan craft transparent soap as described in claim 1, which is characterized in that the purity of the alkali is not less than 98%.
4. the preparation method of the astral oil rattan craft transparent soap as described in any one of claim 1-3, which is characterized in that including such as
Lower step：
(1) astral oil rattan oil is produced：
A. astral oil rattan fruit is taken, is shelled and dry to moisture content 2% hereinafter, obtaining the first crude oil using physical squeezing method；Surpassed with CO2
The critical treatment by extraction astral oil rattan fruitcake dregs of rice obtain the second crude oil；Merge the first crude oil and the second crude oil, obtain astral oil rattan crude oil；
B. by astral oil rattan heating crude oil to 45-50 DEG C, with citric acid degumming；
C. it is 90 DEG C to continue to be heated to oil temperature, adds in boiling water and is washed；It is cooled to room temperature, carries out water-oil separating；
D. winterization is carried out to astral oil rattan oil, then carries out initial filter with slipstream membrane separation technique, then with NF membrane to primary filtrate into
Row secondary filter is to get astral oil rattan oil；
(2) astral oil rattan leaf composite fermentation liquid is produced：
A. astral oil rattan leaf is cleaned, dried in the shade, crushed, extracted with flooding, obtain crude extract；
B. the alkaline earth of 20-30wt% is added in into crude extract, stirs evenly, centrifuge slagging-off, then with micro-filtrate membrane filtration, must be clarified
Liquid；
C. the mixed fermentation strain of 0.002-0.005vt% is accessed into clarified solution, adds in honey and the astral oil rattan oil of 20wt%,
It is uniformly mixed, is placed in China fir tank constant temperature static fermentation 2-6 months；
D. tunning is taken out, is filtered with slipstream membrane separation technique, collects filtrate；
E. high-temperature sterilization is carried out to filtrate at 100 DEG C, is subsequently cooled to composite fermentation liquid of the room temperature to get astral oil rattan leaf；
(3) transparent soap is prepared：
A. natural oil and astral oil rattan oil are stirred and heated to 60 DEG C by formula, divide 2-5 addition alkali, stir 10-30 minutes
Saponification is completed, obtains soap base；
B. glycerine, carboxybetaine and methyl sweet amino proline are added in when soap base is cooled to 35 DEG C, is stirred to glue；
C. continue to stir, the composite fermentation liquid of astral oil rattan leaf is added in when temperature is down to room temperature, treats that bubble completely disappears and pours into
Mold；D. it is put at 2-10 DEG C and freezes 24 hours, up to Transparent handmade soap after taking-up.
5. the preparation method of astral oil rattan craft transparent soap as claimed in claim 4, which is characterized in that the mixed fermentation strain
Include the raw material of following percent by volume：The Bulgarian Lactobacillus bacterium solution of 1.5-2.0%, the red yeast of 1.5-2.0%
Bacterium bacterium solution, the long shoot trichoderma bacterium solution of 0.01-0.05%, the pure mellow wine essence of 30-35%, the Mucor bacterium solution of 0.1-1%, surplus is pure
Water.
6. the preparation method of astral oil rattan craft transparent soap as claimed in claim 5, which is characterized in that Bulgaria's lactic acid
A concentration of 400,000,000/ml of bacillus, a concentration of 200,000,000/ml of the red saccharomycete bacterium solution, the long shoot trichoderma bacterium solution it is a concentration of
0.2 hundred million/ml, a concentration of 0.5 hundred million/ml of Mucor of the Mucor bacterium solution.
7. the preparation method of astral oil rattan craft transparent soap as claimed in claim 4, which is characterized in that the slipstream film is flat
One kind in plate membrane, tubular membrane, rolled film, hollow fiber form film, the aperture of the slipstream film is 100-300um.
8. the preparation method of astral oil rattan craft transparent soap as claimed in claim 4, which is characterized in that used in the step (2)
When flooding extracts astral oil rattan leaf, the dosage of water is 1-5 times of astral oil rattan leaf volume.
9. the preparation method of astral oil rattan craft transparent soap as claimed in claim 4, which is characterized in that permanent in the step (2)
The temperature of warm static fermentation is 40-50 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711462508.3A CN108192776A (en) | 2017-12-28 | 2017-12-28 | A kind of astral oil rattan craft transparent soap and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711462508.3A CN108192776A (en) | 2017-12-28 | 2017-12-28 | A kind of astral oil rattan craft transparent soap and preparation method thereof |
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| CN108192776A true CN108192776A (en) | 2018-06-22 |
Family
ID=62585647
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Citations (6)
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| CN106967542A (en) * | 2017-04-29 | 2017-07-21 | 普洱美藤电子商务有限公司 | A kind of U.S. manual cold process soap of rattan fruit and preparation method thereof |
| CN107603796A (en) * | 2017-10-27 | 2018-01-19 | 李创华 | A kind of astral oil rattan craft transparent soap and preparation method thereof |
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2017
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| CN102199500A (en) * | 2011-04-22 | 2011-09-28 | 江西金乔园林有限公司 | Formula of Chinese soapberry fruit handmade soap and method for preparing Chinese soapberry fruit handmade soap |
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| FR3035118A1 (en) * | 2015-04-16 | 2016-10-21 | Fabrice Balland | PROCESS FOR PRODUCING DERMATOLOGICAL SOAP DERMATOLOGICAL SOAP |
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| CN107603796A (en) * | 2017-10-27 | 2018-01-19 | 李创华 | A kind of astral oil rattan craft transparent soap and preparation method thereof |
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